Law No. 1741 ratifying the European Agreement Concerning the International Carriage of Dangerous Goods by Road (ADR, Geneva, 1957)

EG)HMEPII THI KYBEPNHrEDI THI EMHNIKHI 4HMOKPATIAI· 11 8 H NA 21 4EKEMBPIOY 1887 TEYXOI nPQTO I. NOMO:I vn· APl8. 1741 Kvewo'Y/ Evewna'ix1fr; Iv,uq;wvla~ yia l'YJ L11eDn) OMiif Me1mpoga ErwetV()VVOJV Eµnogevµa1wv (ADH.) nov vnoyerupl'Jxe 0111 I'evev1J trJv 3017 Iemeµ6elot• .19:j7. 0 nPOE6PO~ THl: EMHNIKHl: 6HMOKPATIAl: 'Ap,9.po 'lt'pW't'O 1. Kup<tlVet~t Y.Cxt exet tr,v t~I> 7t'OU opi~et to czp,9.po 28 mx.p. 1 't'O:> 1:,uvtczyµ.:x't'O<;; 'll (,µ.e t't} qipov-.(a:x 't'<,)"/ Hv(J)µ.,s'I<,)'/ E8-vwv) Eup(J)'lt:X°iY,.'IJ, ~iuµ.f<,)'/t:X, 'ltO·t> :>1toyp&qi.,,y,,e .n'T1 Peveur. "''ll'i 30'1J• 1:1 .. 'lt'nµ.6ptr,t> 1957' «yt:x 't''IJ ate,9.v'IJ 031-x.~ Met:xqiopcx E1t1v.1v'~uv<,>v E).J.1topeuµ.<zt(J)V (ADR) » Y.:XI 1tou :X'ltf::teAeit:xt :xito 't'OU<;; -r6µ.oui;; I ( :t:up.qi<,)v(:x, IIp<,)roy,,o).).o iitoypa:qi'IJ<;; v.a:1 II :x­ pczp't''lpix A), II ( II po0',9.'IJY.e<; II a:p:x,ptwa:toi;; A') X:Xt III ( II a:pczp't''t!\J.1% B'). 2. To y,,evµ.e'VO t't)<;; 1:t¥f(J)'Vl:X<;; 'lt0t> (X'l:Xqiepna:1 O'tTj'V 'ltP~'IJl­ rouµ.evT/ 7':Xp(tj'p:Xqio ae 7tp<,)'t'QtU7t'0 Cl't'IJ'I <XTIAIY.'IJ j'AWCl'C1'1% Y.iXI at µ.e't'czqi,p:XCl''lf Cl''t'IJ'I tAA'lj'l'l'I,.~ exec <a><; e/;.{ii;: APl8MOE Cl>YAAOY 225 E<DHMEPl:r TH:r KYBEPNH:rEO:r (TEYXO:r nPOTO) ECONOMIC COMMISSION FOR EUROPE INLAND TRANSPORT COMMITTEE European Agreement concerning th~ international carriage of dangerous goods by road (ADR) and· protocol of signature done at Geneva on 30 September 195 7 VOLUME 1 (Agreement, Protocol of signature and Annex A) FOREWORD The text below comprises, in addition to the Agreement itself and the Prot~ol of signature, the annexes in the form in which they entered into force on 29 July 1968 as well as the amendments there to up to 1 October 1978. EUROPEAN AGREEMENT CONCERNING THE INTERNATIONAL CARRIAGE OF DANGEROUS GOODS BY ROAD (ADR) THE CONTRACTING PARTIES, DESIRING to increase the safety of international tran­ sport by road, HA VE AGREED as follows: Article 1. For the purpose of this Agreement, . (a) the term «vehicle• shall mean motor vehicles, arli?­ ulated vehicles, trailers and semi-trailers, as defined m article 4 of the Convention on Road Traffic of 19 Septem­ ber 1949, other than 'venicies belonging to or under the orders of the armed forces of a Contracting Party; (b) the term «dangerous goods• shall mean those substances and articles the international carriage by road of which is prohibited by, or authorized ·only on certain conditions by, Annexes A and B; (c) the term «international transport• shall mean any transport operation performed on the territory of at least two Contracting Parties by vehicles defined in (a) above. Article 2. l. Subject to the provisions of article 4, pargraph 3, dangerous goods barred from carriage by Annex A shall not be accepted for international transport. 2. International transport of other dangerous ggods shall be authorized subject to compliance with: (a) the conditions laid down in Annex A for the goods in question, in particular as regards their packaging and labelling, and (b) the conditions laid down in Annex B, in particular as regards. the construction, equipment ani:I operation of the vehicle carrying the goods in question, subject to the provisions of article 4, paragraph 2. Article 3. The Annexes to this Agreement shall form an integral part thereof. • Article 4. 1. Each Contracting Party shall retain the right to reg­ ulate or prohibit, for reasons other than safety during carriage, the entry of dangerous goods into its territory. • 2. Vehicles in service on the territory of a Contracting Party at the time of entry into force of this Agreement of brought into service on such territory within two months after its entry into force. shall be allowed, for a period of three years from such entry into force, to perfrorm the international transport of dangerous goods even if their construction and equipment do not entirely conform to the requirements laid down in Annex B for the transport operation in question. Under special clauses of Annex B, however, this period may be reduced. 3. The Contracting parties shall retain the right. to ar­ range, by special bilateral or multilateral agreements, that certain of the dangerous goods which under this Agree­ ment are barred from from all international transport may, subject to certain conditions, be accepted for interna­ tional transport on their territories, or that dangerous go­ ods ~hich under this Agreement are acceptable for inter­ national transport only on specifiec!. conditions may be accepted for international transport on their territories under conditions less stringent than those laid down in the Annexes to this Agreement. The special bilateral or multilateral agreements referred to in this paragraph shall be communicated to the Secretary - General of ihe United Nations, who shall communicate them to the Contracting Parties which are not signatories to the said agreements. Articles 5. The transport operations to which this Agreement ap­ plies shall remain subject to national or international reg­ ulations applic;able in general to road traffic, international road. transport and international trade. Article 6. 1. Countries members of th Economic Commission for Europe and countries admitted to the Commission in a consultative capacity under paragraph 8 of the Commis­ sion's terms of reference may become Contracting Parties to this Agreement (a) by signing it; (b) by ratifying it after signing it subject to ratification; (c) ·by acceding to it. 2. Such countries as may participate in certain activities of the Economic Commission for Europe in accordance with paragraph 11 of the Commision's terms of reference may become Contracting Parties lo this Agreement by acceding to it after its entry into force. 3. The Agreement shall be Qpen for signature until 15 December 195 7. Thereafter, it shall be open for acces­ sIOn. 4. Ratification or accession shall de effected by the deposi­ ting of an instrument with the Secretary - General of the United Nations. Article 7. 1., This Agreement shall enter into force one month after the date on which the number of countries.mentioned in article 6, paragraph 1, which have signed it without reservation of ratification or have deposited their instr­ umenfs of ratification or accession has reached a total of five. However, the Annexes thereto shall not apply until six months after the entry into force of the Agreement it­ self. 2. For any country ratifying or acceding to this Agree­ ment after five of the countries referred to in article 6, paragraph 1, have signed it without reservation of ratifica­ tion or have deposited their instruments of ratification or accession, this Agreement shall enter into force one month after the said country has deposited its instrument of ratifi­ cation or accession and the Annexes thereto shall apply for the said country either on the same date, if they are already in force by that date, or, if they are not in force by that date, on the date on which they apply under the provisions of paragraph 1 of this article. E<I>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2f65 Article 8. 1. Any Contracting ,Party may denounce this Agr eement by so notifying the Secretary - General of the United Na­ tions. 2. Denunciation shall. take effect twelve months after the date of receipt by the Secretary - General of the notification of denunciation. • • Article 9. 1. This Agreement· shall cease to have effect if, after its entry into force, the number of Contracting Parties is less than five during twelve consecutive months. 2. In the event of the conclusion .of a worldwide agree­ ment for the regulation of the transport of dangerous goods, any provision of this Agreement which is contrary to any provision of the said, worldwide agreement shall, from the date on which the latter enters into force, automa­ tically cease to apply to relations between the Parties to this Agreement which becom~ parties to the worldwide agreement, and shall automatically be replaced by the relevant provision of the said worldwide agreement. Article 10. 1. Any country may, at the time of signing this Agree­ ment without reservation of ratification or -of depositing its instrument of ratification or accession or at any time thereafter, declare by' notification addressed to the Secre­ aty - General of the United Nations that this Agreement shall extend to all or any of the territories for the internatio­ nal relations of which it is responsible. The Agreement and the annexes thereto shall extend to the territory or territories named in the notification one month after it is received by the Secreraty - General. 2. Any country wich has made a declaration under paragraph 1 of this article extenditig this Agreement to ary territory for whose international relations it is respon­ sible may denounce the Agreement separately in respect of the said territory in accordance with the provisions of. article 8. Article 1 i. 1. any dispute between two or more Contracting Paties concerning the interpretation or application of this Agree­ ment shall so far as possible be settled by negotiation between them. 2. Any dispute which is not settled by negotiation shall be submitted to arbitration if any one of the Contracting Parties in dispute so requests and shall be referred accor­ dingly to one or more arbitrators selected by agreement between the Parties in dispute. If whithin three months from the date of the request for arbitration the Parties in dispute are unable to agree on the selection of an arbitrator or arbitrators, any of those Parties may request the Secre­ tary - General of the United Nations to nominate a single arbitrator to whom the dispute shall be referred for deci­ sion. 3. The decision of the arbitrator or arbitrators appointed under paragraph 2 of this article shall be binding on the Contracting Parties in dispute. Article 12. Each Contracting Party may, at the time of signing, ratifying, or acceding to, this Agreement, declare that it does not consider itself bound by article 11. Other Co­ ntracting Parties shall not be bound by article 11 in respect of any Contracting Party which has entered such a reserva­ tion. 2. Any Contracting Party having entered a reservation as provided for in paragraph 1 of this article may at any time withdraw such reservation by notifying the Secretary General of the United Nations. Artie!<;. 13. 1. After this Agreement has been in force for three years, any Contracting Party may. by notification to the Secretary - General of the United Nations, request that a conference be convened for the purpose of reviewing 1he text of the Agreement. The Secretary - General shall.notify. all Contracting Parties of the request and a review confe­ rence shall be convened by the Secretary - General if, whithin a period of four nonths following the date of notifi­ cation by the Secretary - General, not less than one-fourth of the Contracting Parties notify him of their concurre nce with the request. 2. If a conference is convened in accordance with parag­ raph 1 of this article, the Secretary - General sh~ll notify all the Contracting Parties and invite them to submit whi­ thin a period of three monts such proposals as they may wish the Conference to consider. The Secretary - General shall circulate to all Contracting Parties the provisional agenda for the conference, together with the texts of such proposals at least three months before the date on which the conference is to meet. 3. The Secretary - General shall invite to any conference convened in accordance with this article all countries refer­ red to in article 6, paragraph 1, and countries which have become Contrncting Parties under ~rticle 6, paragraph 2. Article 14. 1. Independently of the revision p1:ocedure provided for in article 13, any Contracting Party may propose on or more amendments to the Annexes to this Agreement. To that end it shall transmit the text thereof to the Secretary General of the United Nations. Tl-ie Secretary - General may also propose amendments to the Annexes lo this Agreement for the purpose of ensuring ,!==oncordance bet­ ween those Annexes and other international agreements concerning the carriage of dangerous goods. 2. The Secretar- General shall lransmitt any proposal made under paragraph 1 of this article to all Contracting Parties and inform thereof the. other countries referred to in article 6, pa~agraph 1. 3. Any proposed amendment to the Annexes shall be deemed to be accepted unless, within three months from the date on which the Secretary - General circulates it, at least one-third of the Contracting Parties, or five of them if one-third exceeds that figure, have given the Secretary General written notification of their objection • o the proposed amendment. If the amendment is deemea to be accepted, it shall enter into force for all the Contracting Parties, either on the expiry of a further period of three months or, in cases where similar amendments have been or are likely to be made to the other international agree­ mens referred to in· paragraph 1 of this article, on the expiry of a period the duration of which shall be determi­ ned by the Secretary - General in such a way as to allow, wherever possible, the simultaneous entry into force of the amendment and those that have been or are likely to be made to such other agreements; suchperiod shall not, however, be of less than one month's duration. : 4. Tne Secretary - General shall, as soon as possible, notify all Contracting Parties and all the countries referred to in article 6, paragraph 1, of any objection which may be received from the Contracting Parties to a proposed amendment. • 5. If the proposed amendment to the Annexes is not deemed to be accepted, but if at least one Contracting Party other than the Contracting Party which proposed the amendment has given the Secretary - General written notification of its agreement to the proposal, a meeting of all the Contracting Parties and all the cou:-itries referred 2001 (contd) 2002 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) to in article 6, paragraph 1, shall be convened by the Secretary - General within three months aftPr the expiry of the period of three months within which, under parag­ raph 3 of this article, notification must be given of objection to the amendment. The Secretary - General may also invite to such meetir,g represer.tati<·:-s of: (a) intergovernmental organizations which are concer­ ned with transport matters; (b) international non-governmental organizations whose activities are direclty related to the transport of dangerous goods in the territories of the Contracting Parties. 6. Any amendment adopted by more than half the total number of Contracting Parties at a meeting convened in accordance with paragraph 5 of this article shall enter into force for all Contracting Parties in accordance with the procedure agreed at such meeting by the majority of the Contracting Parties attending it. Article 15. In addition to the notifications provided for in articles P and 14, the Secretary- General of the United Nations shall notify the countries referred to in article 6, paragraph 1, and the countries which have become Contracting Par­ ties under article 6, paragraph 2, of (a) signatures, ratifications and accessions in accor· . dance with article 6; (b) the dates on which this Agreement and the Annexes thereto enter into force in accordance with article 7; (c) denunciations in accordance with article 8; (d) the termination of the Agreement in accordance with article 9; fy,· (e) notifications and denunciations received in accor dance with article 10; (f) declarations and notifications received in accordance with article 12, paragraphs 1 and 2; (g) the acceptance and date of entry into force of amen­ dments in accordance with article 14, paragraphs 3 and 6. Article 16. 1. The Protocol of Signature of this Agreement shall have the same force, effect and duration as the Agreement itself, of which it shall be considered to be an integral part. 2. No reservation to this Agreement, other than those entered in the Protocol of Signature and those made in accordance with article 12, shall be permit.It'd. Article 17. After 15 December 195 7, the ong,na.l of this Agree­ ment s hall be def)<'➔~d wrtl, the Secretary . General of the United Nallons, who ,hall transmit Cfrt1f1ed true copies thereof to each of the countries referred to in article 6. paragraph I . . IN ~ITNESS WHEREOF the undersigned, being duly authorized thereto, have signed this Agreement. . DONE a t Geneva, this thirtieth day of September one thousand nme hundred and fifty - seven, in a ~ingle copy, in the English and French languages for the text of the Agreement proper, and in the French language for the Annexes, each text being equally authentic for the Agree­ ment proper. The Secretary· General of the [nited :'-iations is reques­ ted to prepare an authoritative translation of the Annexes in the English language and attach it to the certified true copies referred to in article 17. PROTOCOL OF SIGNATURE TO THE EUROPEAN AGREEMENT ON THE INTER­ NATIONAL CARRIAGE OF DANGEROUS GOODS BY ROAD (ADR) On proceeding to sign the European Agreement cm the International Carriage ,of Dangerous Goods by Road (ADR) the undersigned, duly authorized, CONSIDERING that the conditions governing the car­ riage of dangerous goods by sea to or from the United Kingdom differ basically from those set forth in Annex A to ADR and that it is impossible to modify them so as to conform to the latter in the near future; HA YING REGARD to the undertaking given by th~ United Kingdom to submit as an amendment to the said Annex A a special appendix containing special provisions for road - sea carriage of dangerous goods between the Continent and the United Kingdom; HA VE AGREED that, until the entry into force of such special appendix, dangerous goods carried under ADR to or from the United Kingdom shall comply with th e provi­ sions of Annex A to ADR and also with the United Kin­ gdom conditions for the carriage of dangerous goods by sea; TAKE NOTE OF a declaration by the representative of France to the effect that the Government of the French Republic reserves the right, notwithstanding the provisions of article 4. paragtaph 2, to refuse to a)low vehicles in service on I.he territory of another Contracting Party, wha­ tever the date or, which they were put into service, to be used for the carriage of dangerous goods on French terri­ tory unless such vehicles comply either with the conditions laid down for such carriage in Annex B or with the condi­ tions laid down for the carriage of the goods in question in the French regulations governing the carriage of dange­ rous goods by road; RECOMMEND that, before submission in accordance with article 14, paragraph 1, or article 13, paragraph 2, proposed amendments to this Agreement or its Annexes shall as far as possible first be discussed at meetings of experts of the Contracting Parties and, if necessary, of . the other countries mentioned in article 6, paragraph 1, of the Agreement and of the international organizations mentioned in article 14, paragraph 5, of the Agreement. EUROPEAN AGREEMENT CONCERNING THE INTERNATIONAL CARRIAGE OF DANGEROUS GOODS BY ROAD (ADR) ANNEX A PROVISIONS CONCERNING DANGEROUS SUBSTANCES AND ARTICLES Contents Part I. DEFINITIONS AND GENERAL PROVISIONS Marginals Definitions .............................. 2000 and 2001 General provisions ........................ 2002 - 2003 Part ll. LIST OF SUBSTANCES AND SPECIAL PR'OVISIONS Class la Class lb Class le. Class 2 Class 3 FOR THE VARIOUS CLASSES Explosive substances and artic les ................ 2100 et seq. Articles filled with explosive substances ............ 2130 » lgniters, fireworks and similar go ods , ................ 2170 • Gases: compressed, liquefied or dis solved under pressure ... 2200 • lnlhrnmabie liquids ..... 2300 . • E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPOTO) 21B7 Class 4.1 Class 4.2 Class 4.3 Class 5.1 Class 5.2 Class 6.1 Class 6.2 . Class 7 Class 8 Inflammable solids ...... 2400 » Substances liable to spontaneous combustion ........... 2430 • Substances which give off inflam­ mable gases on contact with wa ter .................. 2470 • Oxidizing substances .... 2500 • Organic peroxides ...... 2550 • Toxic substances ....... 2600 • Repugnant substances and substan­ ces liable to cause infection 2650 • Radioactive substances .. 2700 • Corrosive substances .... 2800 • Part UL APPENDICES TO ANNEX .A Marginals Appendix A.l • Appendix A.2 Appendix A.3 Appendix A.4 Appendix A.5 Appendix A.6 Appendix A.7 Appendix A.8 Appendix A.9 Stability and safety conditions rela­ ting to explosive substances, inflam­ mable solids and organic peroxides; Rules for teslS ....... 3100 et seq. Provisions relating to the nature of aluminium - alloy receptacles for certain gases of Class 2; provisions relating to the materials and construction of receptacles, interided for the carriage of deeply - refrige­ rated liquefied gases of Class 2; and provisions relating to tests on aerosol dispensers and non - refil­ lable .containers for gases under pressure of Class 2, 10° and 11°······························3200 • Testsrelating lo inflammable liquids of Classes 3 and 6.1 .... 3300 • Reserved .............. 3400 • Provisions relating lo tests on the metal drums referred to in margi­ nals 2303 (6) and 2813 (1), (c) .................. 3500 • Regulations relating lo radioactive substances of Class 7 ... 3600 • Reserved ............. 3 700 • Reserved ............. 3800 • Provisions relating to danger labels; Explanation of symbols, and model labels ................ 3900 • Part I DEFINITIONS AND GENERAL PROVISIONS 1) For the purposes of this Annex: the term «competent authority• means the authority de­ signated as such in each country ·and in each specific case by the Government; • the term «fragile package• means a package containing a fragile receptacle (i.e. a receptacle made of glass, porce­ lain, stoneware or similar materials) which is not enclosed in a packaging with complete sides protecting it effectively against shock [see also marginal 2001 (5)1; the term «gas• means a gas or vapour; the term «dangerous substances», when used alon.e, me ans the substances and articles designated as being substances and articles of AOR: the term·«carriage in bulk» means the carriage of a solid substance without packaging; the term «RID» means the International Regulations 1-1999 2000 concerning the Carriage of Dangerous Goods by Rail [An­ nex 1 to the International Convention concerning the C ... r­ riage of Goods by Rail (CIM)J. (2) For the purposes of this Annex, tanks (see defini­ tions in Annex B) are not placed on the same footing as receptacles, the term •receptacle» being used in a restric­ tive sense. Provisions concerning receptacles are appli­ cable to fixed tanks, batteries of receptacles, demountable tanks and tank - containers only if this is expressly stipula­ ted. (3) The term «full load» means any load originating from one senaer for which the use of a vehicle or of a large container is exclusively reserved and all operations for the loading and-unloading of which are carrie~ out in conformity with the instructions of the sender or of the con­ signee. (1) Unless expressly stated otherwise, the sign •%• in this Annex represenlS: (a) in· the case of mixtures of solids or of liquids, and also in the case of solutions and of solids wetted by a liquid: a percentage by weight based on the total weight of the mixture, the solution or the wetted solid; (b) in the case of gaseous mixtures: a percentage by volume based on the total volume of the gaseous mixture. Definitions and general provisions (2) All weights mentioned for packages in this Annex are, unless otherwise specified, gross weights. The weight .of containers or tanks used for the carriage of goods is not included in the gross weight. . (3) Pressures of all kinds relating to receptacles (such as test pressure, internal pressure, safety - valve opening pressure) are always indicated in kg/cm2 gauge pressure (pressure in excess of atmospheric pressure); however, the vapour pressure of substances is always expressed in kg/cm2 absolute pressure. ..- '· • • (4) Where this Annex specifies a degree of filling for receptacles or tanks, that degree of filling is always refer­ red to a temperature of the· substances of 15 ° C unless some other temperature is indicated. • (5) Fragile receptacles secured, either singly or in groups, by cushioning materials in a strong receptacle are not regarded as fragile receptacles on condition that the strong receptacle is leakproof and so designed that· in the event of breakage or leakage of the fragile receptacles their contents cannot escape from the strong receptacle and that the mechanical sirength of the latter is not impai red by corrosion during carriage. • GENERAL PROVISIONS ( 1) This Annex specifies the dangerous goods to be excluded from international carriage by road and the dan-. gerous goods to be accepted for such carriage under cer­ tain conditions. It groups the dangerous goods in restrictive and non - restrictive Classes. Of the dangerous. goods covered by the headings of the restrictive Classes (Classes . la, lb, le, 2, 4.2, 4.3, 5.2, 6.2 and 7), those which are listed in the clauses concerning these Classes (marginals 2101, 2131, 2171, 2201, 2431, 2471, 2551, 2651 and 2701) are to be accepted for carriage only under the conditions specified in these clauses, and others are to be excluded from carriage. Some of the dangerous goods covered by the headings of the . non - restrictive Classes (Classes 3, 4.1, 5.1., 6.1, and 8) are, by notes inserted in the clauses concerning the various Classes, excluded from carriage; of the other goods covered the various Classes, excluded from carriage; of the other goods cove­ red by the headings of the non - restrictive Classes, tho~ which are mentioned or defined in the clauses concerning these Classes (marginals 2301, 2401; 2501, 2601 and 2801) are to be accepted for carriage only under the conditions specified in these clauses, and those which are not mentionedior defined therein are not deemed to be dangeroui, goods for the purposes of this Agreement and are to be accepted for carriage without any special condi­ tions. 216"8 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Definitions and general provisions (2) The Classes of this Annex are as follows: Class la Explosive • substan ces and articles Restrictive Clas lb Articles filled with explosive substan Class le Class2 Class 3 Class 4.1. Class4.2. Class 4.3 ces lgniters, fireworks and similar goods Gases: compressed, liquefied or dissol­ ved under pressure » Inflammable liquids Non-restrictive Inflammable solids Non-restrictive Substances liable to spontaneous combu stion Substances which give off inflammable gases on with water contact Restrictive Restrictive Class 5.1 Oxidizing substan Class 5.2 Class 6.1. Class 6.2 Class 7 Class 8 ces Non-restrictive . Organic peroxides Restrictive Toxic substances Non-restrictive Repugnant substan ces and substances liable to cause infec tion Restrictive Radioactive substances Restrictive Corrosive substan ces Non-restrictive (3) Any carriage of goods governed by this Annex shall be the subject of a transport document. The sender shall communicate in writing. 1.0 the carrier the particulars to be included in the transport document as laid down for each class in part II of this Annex in sections 2.8. The document may be that already required by other regula­ tions in force. Any goods the carriage of which is so governed shall be described in the transport document in conformity with the indications in section B of the special provisions for each Class. The particulars t? be enter~d in the transport document shall be drafted m an official language of the forwarding country, and also, if that l an­ guage is not English, or French, or German, m English, French or German, unless international road transport tariffs, if any, or agreements concluded between the coun­ tries concerned in the transport operation, provide other­ wise. The transport document shall be accompanied, if appropriate, by instructions to be implemented in the event of an accident (see Annex B, marginal 10185). The tran­ sport document shall accompany the dangerous substan­ ces carried. ( 4) If by reason of the size of the load a consignme?t cannot be loaded in its entirety on a single transport umt, at least as many separate documents, or copies of the single document, shall be made out as transport units loaded. Furthermore, in all cases, separate transport doc­ uments shall be made out for consignments or parts of consignments which may not be loaded together on the same vehicle by reason of the prohibitions set forth in Annex B. (5) Outer packagings additional to those specified in this Annex may be used providing that they do not contra­ vene the spirit of the provisions of this Annex relating to outer packagings.-lf such additional packagings areused, the·prescribed marking and labels shall be applied to them. (6) If the mixed packing of several dangerous substan­ ces with one another or with other goods is allowed by the provisions of section· A. of the provis!ons appli~a?le to the various Classes, the inner packagmgs contammg different dangerous substances shall be carefully and ef­ fective separated from one another in the collective packa­ gings if dangerous reactions, such as the production of dan11;erous heat, combustion, the formation of mixtures 2002 sensitive to friction or shock, and the release of inflam­ mable or toxic gases, are liable to occur as a result of damage to or destruction of the inner packagings, In partic­ ular, if fragile receptacles are used, and especially if the ' said receptacles contain liquids, the danger of the forma­ tion of dangerous mixtures shall be avoided and to this end all appropriate measures shall be taken, such as the use of suitable cushioning materials in sufficie~ quantity, securing of the receptacles in a second strong packaging, and subdivision of the. collective. packaging into several compartments. (7) If mixed packing is used, the provisions of this Annex concerning the particulars in the transport doc­ ument shall apply in respect of each of the different kinds of dangerous substance contained in the collective pac­ kage, and the collective package shall bear all the inscrip­ tions and all the danger labels prescribed in this Annex for the dangerous substances the collective package co­ ntains. (8) If solutions of substances listed in this Annex are not expressly mentioned in the list of the Class lo which the dissolved substances belong, they shall nevertheless be considered as substances of ADR if their concentration is such that they retain the danger inherent in the substan­ ces themselves; their packaging shall in such: event con­ form to the requirements of section A of the special provi­ sions applicable to the Class to which the said substances belong, it being understood thar packagings which would . be unsuitable for the carriage ofliquids may not be· used. (9) Mixtures of substancesof ADR with other substances shall be considered as substances of ADR if they· retain the danger inherent in the substance which is a suostance of ADR. ( 10) The sender, either in the· transport document or in a separate declaration, shall certify that the substance presented may be carried by road in conformity with the provisions of ADR, that its condition, treatment and, as appropriate its packaging and labelling comply with the provisions of ADR. Furthermore, if several dangerous goods are packed together in a collective package or in a single container, the sender is required to declare that this mixed packing is not prohibited. (11) A substance whose specific radioactivity does· not exceed 0.002 microcurie per gramme and which is cove­ red by a collective heading of any Class shall be excluded from carriage if, in addition, it is covered by the heading of a restrictive Class in which it is not listed. (12) A substance whose specific radioactivity does not exceed 0.002 microcurie per gramme and which is not listed by name in a Class, but is covered by two or more collective headings of different Classes, shall be subject to the conditions of carriage laid down: (a) in the restrictive Class, if one of the Classes concer­ ned is a restrictive Class; (b) in the Cl~s corresponding to the predominant dan­ ger exhibited by the substance during carriage, if none of the Classes concerned is a restrictive Class. ( 1) This Annex contains for each Class other than Class 7: (a) a list of the dangerous substances constituting the Class, and, where applicable, in the form of a marginal having a number ending with the letter •a•, the exemptions allowed from the provisions of ADR for some of those substances if they comply with certain conditions; (b) provisions sub-divided as follows: A. Packages: 1. General conditions of packing; 2. Packing of a single substance or of articles of the same kind; 3. Mixed packing; 4. Marking and danger labels on packages. B. Particulars in the transport document. C. E111pty packagings. D. (where appropriate) Other provisions. (2) Provisions concerning: consignment in bulk, in containers and in tanks; method of despatch and restrictions on forwarding; 2003 E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPOTO) prohibitions on mixed loading; and .transport equipment are to be found in Annex B and its appendices, which also contain all other pertinent provi­ sions applying specifically to carriage by roade. (3) The appendices to this Annex contain: Appendix ·A.I: Stability and safety conditions relating to explosive substances, inflammable solids and organic peroxides, together with rules for tests; Appendix A.2: Provisions relating to the nature of al­ uminium-all receptacles for certain gases of Class 2; provi­ sions relating to the materials and construction of receptac­ les, intended for the carriage or deeply-refrigerated lique-· fled gases of Class 2; and -provisions relaiing to tests on aerosol dispensers and non-refillable containers .for gases under pressure of. Class 2, 10° and 11 °; Appendix A.3: Tests relating to inflammable liquids of Classes 3 and 6.1.; Appendix A.5: Provisions relating to tests on the metal drums referred to in marginals 2303(6) and 2813(l)(c); Apvendix • A.6: Regulations relating to radioactive substances of Class 7; Appendix A. 9: Provisions relating to danger labels, and explanation of the symbols. • Appendixes A.4, A.7, and A.8., are reserved. (4) For Class 7, the details concerning conditions of packing, mixed packing, labelling ·and marking of packa: ges as well as provisions governing storage, desP,atch and carriage, including in bulk in containers and in tanks, are specified in the schedules of Annex A listed in marginal 2 7 02. Some of the detailed and technical provisions affec­ ting this Class are elaborated in Appendix A.6 which also include the complete table .of radionuclides and method of testing packagings intended for substances of Class 7. Where the provisions relating to carriage as a «full load• are applied the competent authorities may require the • vehicle or large container used for the transport operation concerned to be loaded at only one point and unloaded at only one point. • (1) If the vehicle carrying out a transport operation · subject to the provisions of ADR is conveyed over a section of the journey other than by road haulage, then any natio­ nal or international regulations on the said section, govern the carriage of dangerous goods by the mode transport used for c onveying the road vehicle shall alone be appli­ cable to the said section of the journey. (2) In cases where a transport operation subject tci·the provision of ADR is likewise subject over the whole or a part of its road journey to the provisions of an international convention which regulates the carriage of dangerous go­ ods by a mode of transport other than road carriage by virtue of clauses extending the applicability of the said convention to certain i:notor-vehicle services, then the pro­ visions of that international convention shall apply, over the journey in question concurrently with those of ADR which are not incompatible therewith; the other clauses . of ADR shall not apply o v,i;r thw journey in question. For the p urpose of carrying out the trials necessary with a view to amending the provisions of this Annex in order to adapt them to technological and industrial deve­ lopments, the competent authorities of the Contracting Parties may agree directly among themselves to authorize certain transport operations in their terri tories by tempo­ rary derogation from the provisions of this Annex .• The authority which has taken the initiative with.respect ·to the temporary derogation so granted shall notify the competent service of the United Nations Secretari~t of the derogation, which service shall bring it to the attention of the Contrac ting Parties. • 2011 • Part II LIST OF SUBSTANCES AND SPECIAL PROVISIONS FOR THE VARIOUS CLASSES CLASS 1~ EXPLOSIVE SUBSTANCES AND ARTIC "' •• . • • LES . • hole: Substances and articles which cannot explode on 2004 2005 2006 2007 2009 2010 2099 contact with a flame and which are not more sensitive to shock or friction than dinitrobenzene are not subject to the provisions of Class la 1. List of substances and articles ( 1) Among the substance and articles covered by the heading of Class la, only those listed in marginal 2101 are to be accepted for ·carriage, and then only subject to the provisions of this Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. (2) In the explosives which are to be accepted for car riage, nitroglycerine may be replaced wholly or in part by: (a) nitroglycol, or • (b) dinitrodiethyleneglycol, or (c) nitrated sugar (nitrated saccharose), or (d) a mixture of the above substances. 1 ° Highly nitrated nitrocellulose (such as guricotton), i.e. with a nitrogen content of more than 12.6 per cent, well stabilized and containing in addition: When the nitrocellulose is not compressed, not less • then 25 per cent water or alcohol (methyl, ethyl, normal propyl or isopropyl, butyl, or amyl alcohol or mixtures thereof), including denatured alcohol; or mixtures of water and alcohol; when the nitrocellulose is compressed, not less than 15 per cent water, or not less than 12 per cent paraffin wax or other similar substances. See also Appendix Al, marginal 3101. Note: 1. Nitrocellulose with a nitrogen content not ex- • ceeding 12.6 per cent is a substance of Class 4.1 if it complies with the specifications set out in marginal 2401, (a), (b) or (c). • 2. Nitrocellulose in the. form of nitroc@ulo~e-film was free from gelatine, in reels, sheets or strips, is a substance of Class 4.2 (see marginal 2431, 4°). 2° Cordite paste, non-gelatinized («powder cake»), for use in the making of smokeless powders and containing not more than 70 per cent anhyding substance and not less than 30 per cent water; the anhydrous substance liquid explosives. 3° Gelatinized nitrocellulose powders and gelatihized nitrocellulose powders containing nitroglycerine (nitrogly­ cerine powders): (a) non-porous and non-dusty; (b) porous or dusty. 4° Plasticized nitrocellulose containing not less than 12 per cent but less than 18 per cent plasticizing substances (such as butyl phthalate whose nitrocellulose has a nitrogen content not exceeding 12.6 per cent, also in the form of chips. Note: Plasticized nitrocellulose containing not less than 18 per cent butyl phthalate or a plasticizer at least equal in effect is a substance of Class 4.1 [see marginal 2401 7° (b) and (c)]. See also Appendix A.l, marginal 3102, 1. 5° Non-gelatinized nitrocellulose powders. See also Ap­ pendix A.I., marginal 3102. 6° Trinitrotoluene (tolite), also when compressed or cast, trinitrotoluene mixed with aluminium, mixtures ter­ med liquid trinitrotoluene, and trinitroanisole. See· also Appendix A.l, marginal 3103. 7° (a) Hexyl (hexanitrodiphenylamine) and picric acid; (b) pentolites (mixtures of pentaerythritol tetranitrate and trinitrotoluene) and hexolites (mixtures of trimethy­ lene -trinitramine and trinitrotoluene) if their trinitrotol­ uene content is such that their sensitiveness to shock does not exceed that of tetryl; (c) phlegmatized penthrite (pentaerythritol tetranitrate) and phlegmatized hexogen (trimethylene-trinitramine), both phlegmatized by incorporation of wax, paraffin wax or other similarly effective sudstances in such quantity 2100 2101 2170 /:..: · ----~E<l>~H:!!M~E!;.!P~II~TH~I~KY.uB~E:.!:P~N~H~IEBQ~I;, J' (l.!.T~Ev~x~o~I:....!n..!!P~Q!!...!T~O:L...) -------- ., that the sensitiveness of these substances to shock does not exceed that of totryl. For (a), (b) and (c), see also Appendix A.l, marginal 3103. Note: Substances of 7° (b) and phlegmatized hexogen of 7° (c) may also contain aluminium. Explosive organic nitro-compounds: (a) soluble in water, e.g. trinitroresorcinol: . (b) insoluble in water, e.g. tetryl (trinitrophenylmethyl nitraminc) (c) tetryl gaines without metal coveri ng. For (a) and (b), see also Appendix A. l, marginal 3103. Note: Except for liquid trinitrotoluene (6°), explosive organic, nitrocompounds in the liquid state are not to be accepted for carriage. (a) Moist penthrite (pentaerythritol tetranitrate) and· moist hexogen (trimethylene- trinitramine) wetted throu­ ghout with not less than 20 per cent water in the case of the former and not less than 15 per cent in the case of the latter; (b) moist pentolites (mixtures of penthrite and trinitro­ toluene) and moist hexolites (mixtures of hexogen and trinitrotoluene) whose sensitiveness to shock in the dry state exceeds that of tetryl and which are wetted throughout with not less than 15 per cent water; (c) moist mixtures of penthritc or of hexogen with wax, paraffin wax or substances similer to wax or paraffin wax, whose sensitiveness to schock in the dry state exceeds that of tetryl and which are wetted throughout with not less than 15 per cent water: (d) compressed penthrite gaines without metal covering. For (a), (b) and (c), see also Appendix A.l, marginal 3103. (a) Benzoyl peroxide: 1. in the dry state or with less than 10 per cent water; 2. with less than 30 per cent phlegmatizer. Note: 1. Benzoyl perox(de with not less than 10 per cent water or with not less than 30 per cent phlegmatizer is a substance of Class 5.2 [see marginal 2551, 8° (a) and (b)]. 2. Benzoyl peroxide with not less than 70 per cent dry and inert solids is not subject to the provisions of ADR. (b) Cyclohexanone per~xides [1-hydroxy -J'hydrope­ roxy - dicyclohexyl peroxide and bis - (1-hydroxycyclohe­ xyl) peroxide and mixtures of these two 1. in the dry state or with Jess than 5 per cent water: 2. with Jess than 30 per cent phlegmatizer. • Note: 1. Cyclohexanone peroxides and their mixtures with not less than 5 per cent water or with not less than 30 per cent phlegmatizer are substances of Class 5.2 [see marginal 2551 9° (a) and (b)]. 2. Cyclohexanone peroxides and their mixtures with not less than 70 per cent dry and inert solids are not subject to the provisions of ADR. (c) Parachlorobenzoyl peroxide: 1. in the dry state or with Jess than 10 per cent water; 2. with Jess than 30 per cent phlegmatizer. Note: 1. Parachlorobenzoyl peroxide with not less than 10 per cent water or with not Jess than 30 P:er cent phlegmatizer is a substance of Class 5.2 [see marginal 2551 17° (a) and (b)]. 2. Parachlorobenzoyl peroxide with not less than 70 per cent dry and inert solids is not subject to the provisions of ADR. 11 ° (a) Black pow~er (with a basis of potassium nitrate) in corned or meal form; (b) slow mining powders similar to black powder (com­ p·osed of sodium nitrate, sulphur and wood charcoal, coal or lignite, or composed of potassium nitrate with or without sodium nitrate, sulphur, coal or lignite). (c) cartridges of compressed black powder or powder similar to compressed blac k powder. Note: The density of the compressed mass must not be less than 1.5.g per 15°. Class la For(a) and (b), see also Appendix A.l, marginal 3104. 12° (a) Nitrate explosives, in powder form, not covered by 11° or 14° (a) or (c) and consisting essentially of ammonium nitrate or of a mixture of ammonium nitrate and alkali or alkaline-earth nitrates or of a mixture of ammonium nitrate and sodium chloride, or of a mixture of alkali or alkaline-earth nitrates and ammonium chloride, or of a mixture of ammonium nitrate with alkali or alkaline­ earth nitrates and of sodium chloride, or of a mixture of ammonium nitrate with alkali or alkaline-earth nitrates and ammonium chloride. They may contain, in addition, combustible substances (such as wood flour, or other vege­ table flour or hydrocarbons), sensitizers (for example, fine aluminium powder), aromatic nitro-compounds, nitrogly­ cerine or nitroglycol or a mixture of the two, and inert stabilizing or colouring substances (see also Appendix A. l, marginal 3105). (b) Explosives not containing inorganic nitrates, in pow­ der form, consisting essentially of a mixture of inert substances (such as alkali chlorides) with nitroglycerine or nitroglycol or a mixture of the two. They may contain, in addition, aromatic nitro-compounds and substances with a phlegmatizing, stabilizing or gelatinizing, or colouring effect. See also Appendix A.I, marginal 3105. 13° Chlorate and perchlorate explosives, i.e. mixtures of chlorates or perchlorates of alkali or alkaline-earth metals with compounds rich in carbon. See also Appendix A.I, marginal 3106. 14° (a) Dynamites with an inert absorbent, and explosi­ ves similar to dynamite with· ari inert absorbent; (b) Blasting gelatine consisting of gun-cotton and not more than 93 per cent nitroglycerine, and gelatinized dynamites with a nitroglycerine content not exceeding 85 per cent; (c) Gelatinous nitrate explosives, consisting essentially of ammonium nitrate or of a mixture of ammonium nitrate with nitrates of alkali or alkaline-earth metals containing not more than 40 per cent gelatinized nitroglycerine or gelatinized nitroglycol or a mixture of the two. They may · contain, in addition, nitro-compounds or combustible substances (such as wood flour or another vegetable flour or hydrocarbons) and, in addition, other inert or colouring • substances. For (a), (b) and (c), see also Appendix A.I, marginal. 3107. 15° Empty packagings, uncleaned, which have contai­ ned dangerous substances of Class la. Class la A. Packages 2. Provisions 1. General conditions of packing (1) Packagings shall be so closed and leak-proof as to prevent any loss of the contents. The use of metal bands or wirec to consure closure is forbidden unless this proced­ ure is specifically authorized in the special provisions rela­ ting to the packing of the substances or article in question. (2) The materials of which the packagings and their. closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there­ with. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent ~y loosening during carriage and to meet the normal require­ ments of carriage. Solid substances shall be firmly secured in their packagings, and inner packagings shall be firmly secured in outer packagings. Unless otherwise specified in the section entitled «Packing of a singl substance or of articles of the same kind», inner packagings may be enclo­ sed in outer packagings, either singly or in groups. (4) Bottles and other glass receptacles must be free from faults liable to impair their strenght; in particular, internal stresses must have been suitably relieved. The 1thickness of the walls must not be ,less than 2 mm. (5) Cushioning materials shall be suited to the natur~ ;of the contents; in particular, they must be absorbent 1f 2101 2102 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2171 the contents are liquid or might exude liquid. 2. Packing of a single substance or of articles of the same kind (1) Substances of 1 ° and 2° shall be packed: (a) in wooden receptacles or in drums made of imperme­ able fibreboard: these receptacles and drums shall in addi­ tion be fitted with a lining impermeable to the liquids the contain; their closure must be leak-proof or (b) in impermeable bags (e.g. made of rubber or of a suitable plastics material not readily inflammable) placed in a wooden case or (c) in iron drums coated inside with zinc or lead or ( d) in receptacles made of tin-plate, zinc sheet or alumi­ nium sheet, which shall be secured by cushioning materials in wooden cases. (2) Metal receptacles shall be fitted with closures or safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2; the presence of these closures or safety devices must not impair the strength of the receptacles nor impair its closure. (3) Nitrocellulose of 1 °, if wetted exclusively with water, may be packed in fibreboard drums; the fibreboard must have undergone a special treatment to render it completely impermeable; the closures of the drums must be water­ vapour proof. (4) A package containing ·substances of 1 ° must not weigh more than 120 kg or, if it can be rolled, more than 300 kg; however, where fibreboard drums are used, a packages must not weigh more than 75 kg. A packages containing substances of 2° must not weigh more than 7 5 kg. (1) Substances of 3° (a) and 4° shall be packed: (a) if they are to be carried as a full load: 1. in drums made of impermeable fibreboard; or 2. in packagings made of wood or of metal other than black sheet-iron; (b) if they are n'ot to be carried as a full load 1. in boxes made of fibreboard, tin-plate, zinc sheet or aluminium sheet, or of a suitable plastics material not readily inflammable, or in bags made of closely-woven textile or of stout paper of at least two plies or of stout paper lined with aluminium foil or with a suitable plastics material. These packaging shall be placed in wooden ca­ ses; or 2. without preliminary packing in boxes or bags: a. in drums made of impermeable fibreboard or in wooden casks; or b. in wooden packagings lined with zinc sheet or alumi nium sheet or c. in receptacles made of metal other than black sheet 1ron. (2) If the powder is in tubes, sticks, threads, bands or sheets it may also be enclosed, without preliminary pac­ king in boxes or bags, in wooden cases. (3) Metal receptacles ·shall be fitted with closures or safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2; the presence of these closures or safety devices must not impair the strength of the receptacle not impair its closure. • (4) The closure of wooden cases may be ensured by means of band or wires made of a suitable metal fastened tightly round them. If the band or wires are made of iron they shall be covered with a material not liable to produce sparks when subjected to impact or friction. (5) A package must not weigh more than 120 kg; however, where fibreboard drums are used, a package must not weigh more than 75 kg. (1) Substances of 3° (b) and 5° shall be packed: (a) if they are to be carried as a full load: 1. in drums made of impermeable fibreboard; or 2. in packagings made of wood or of metal other than black sheet-iron. (b) 'if they are not to be carried as a full load: 1. in boxes made of fibreboard, tin-plate or aluminium sheet. A box must not contain more than 1 kg of powder and must be wrapped in paper. These packagings shall 2103 2104 2104 2105 be placed ih wooden packagings or 2. in bags made of closely-woven textile or of stout paper of at least two plies or of stout paper lined with aluminium foil or with a suitabl~ plastics material. These bags shall be placed in fibreboard drums or in wooden casks or in other wooden packaging's lined with zinc sheet or aluminium sheet, or in receptacles made of zinc sheet or aluminium sheet. Receptacles made of zinc sheet or aluminium sheet shall be completely lined with wood or fibreboard. . . ., . (2) Metal receptacles shall be fitted with clos~~s or safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2; the presence of these closures or safety devices must not impair the strength of the receptacle nor impair its clmmre. (3) The closure of wooden cases may be ensured by means of band or wires made of a suitable metal fastened tightly round them. If the bands or wires are made of iron they shall be covered with a material not liable to produce sparks when subjected to impact or friction. (4)A package under (1) (a) must not weigh more than 100 kg; however, where fibreboard drums are used,'· a package must not weigh more than 75 kg. A package under (1) (b) must not weigh more than 75 kg. It must not contain more than 30 kgr of nitrocellulose powder. (1) Substances of 6° shall be packed in wooden recep­ tacles. Drums made of impermeable fibreboard are like­ wise to be accepted for solid trinitrotoluene and for trinitro­ anisole; and iron receptacles for mixtures termed liquid tri­ nitrotoluene. (2) Metal receptacles shall be fitted with closures or safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2; the presence of these closures or safety devices must not impair the strength of the receptacle nor impair its closure. (3) A package must not weigh mo~ th<\11• 120 kg or, if it can be rolled, more than 300 kgt however, where fibreboard drums are used, a package must not weigh more than 7 5 kg. • 21056z (1) Substances of 7° shall be packed: 2107 (a)Substances of 7° (a): in wooden receptacles or in drums made of impermeable fibreboard, Lead and mate rials containing lead (alloys or compounds) must not be used in the packaging of hexyl (hexanitrodiphenylamine) and picric acid. Picric acid may also be packed, not more than 500 g per receptacle, in receptacles made of glass, porcelain, stoneware or similar materials or of a suitable plastics material, secured in a wooden case by cushioning material ( e.g. corrugated fibreboard). The receptacles shall be clo­ sed by means of a stopper, made of cork or rubber or a suitable plastics material, which shall be held in position by an additional· device (such as a cap, crown, seal or binding) capable of preventing any loosening of the closure system during carriage; (b) Substances of 7° (b) and (c): not more than 30 kg per bag, in cloth bags which do not allow the contents to filter through, or in bags made of stout paper or a suitable plastics material, which shall be placed in leak-proof.woo­ den receptacles or in drums made of hardened fibreboard capable of being so closed as to be leak-proof and whose bottoms and lids shall be made of plywood. The lids of cases shall be secured by means of screws and those of drums by means of a collar. (2) A package containing substance; of 7° (a) must not weigh more than 120 kg if it is a wooden receptacle; where fibreboard drums are used, a package must not weigh more than 7 5 kg. Packages containing picric acid packed in fragile receptacles or in receptacles made of a plastics material must not weigh more than 15 kg. A package containing substances of 7° (b) or (c) must not weigh more than 75 kg; cases which, with th~ir contents, weigh more than 30 kg shall be fitted with means of han­ dling. (1) Substances and articles of 8° shall be packed: 21081 (a) substances of 8° (a): in receptacles made of steel not liable to rust, or of any other suitable material (which 2172 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) in particular excludes lead and its alloys). Nitro­ compounds shall be uniformly \Vetted with sufficient water to ensure that they contain not less than 25 per cent water throughout the journey, at every point in the substance. Metal receptacles shall be fitted with closures or safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2! the presence of these closures or safety devices must not impair the strength of the receptacle nor impair its closure. Receptacles, except those made of steel not liable to rust shall be secured by cushioning materials in wooden packagings; (b) substances of 8° (b): not more than 15 kg per bag, in bags made of cloth or of a suitable plastics material, placed in wooden packagings; (c) substances of 8° (a) and (b) may also be packed, not more than 500 g per receptacle, in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, secured by cushioning material (e.g. corrugated fibreboard) in a wooden case. A package must not contain more than 5 kg of nitro-compounds. The receptacles shall be closed by means of a stopper, made of cork or rubber or a suitable plastics material, which shall be held in position by an additional device (such as a cap, seal or binding) capable of preventing any loosening of the closure system during carriage; (d) articles of 8° (c): separately in stout paper and placed, not more than 100 per box, in sheet-metal boxes. Not more than 100 of these boxes shall be packed in a wooden packing case; • • (2) A package under paragraph (1) (a) or (b) must not weigh more than 75 kg; it must not contain more than 25 kg of substances of 8° (a) or more than 50 kg of substances of 8° (b). A package under paragraph (1) (c) not weigh more than 15 kg, or a package under paragraph (1) (d) more than 40 kg. (1) Substances and articles of 9° shall be packed: (a) substances of 9° (a) to (c): 1. not more than 10 kg per bag, in bags made of cloth or of a suitable plastics material, placed in an impermeable fibreboard box or in a box made of tin-plate or aluminium sheet or zinc sheet; or 2. not more than 10 kg per receptacle, in receptacles made of fibreboard of adequate strenght, impregnated with paraffin wax or rendered impermeable by some other means. Boxes made of tin-plate or aluminium sheet or zinc sheet and boxes or receptacles of other kinds shall be placed in a w.ooden case lined with corrugated fibreboard; •metal boxes so placed shall be separated from one another by means of a corrugated-fibreboard wrapping. A case may not contain more than four boxes or receptacles of other kinds. The lids of cases shall be secured by means of screws. b) penthrite (9° (a)] may also be packed either: 1. not more than 5 kg per receptacle, in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, closed by means of a stopper made of cork or rubber or a suitable plastics material; each receptacle shall be placed in a metal recep­ tacle hermetically closed by welding or soldering and cush­ ioned with resilient materiaie so as to wedge the inner receptacle securely without leaving any empty space. Not more than 4 metal receptacles shall be packed in a wooden case lined with corrugated fibreboard and shall be separa­ ted from one another by several thicknesses of corrugated fibreboard or of another material capable of performing the same function; or 2. not more than 500 g dry weight per receptacle, in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, closed • by means of a stopper made of cork or rubber or a suitable plastics material. These receptacles shall be placed in a wooden case. They shall be separated from one another by means of a corrugated fibreboard wrapping and from the sides of the case by a space of not less than 3 cm filled with cushioning materials; (c) hexogen (9° (a)] may also be packed as provided 2109 2109 under (b) 1. above for penthrite; ( d) articles of 9° ( d): first separately in stout paper and placed, not more than 3 kg per case, in fibreboard cases in which they shall be fixed in position by cushioning materials; tliese cases, not more than 10 per wooden case, shall be so secured by cushioning materials in a wooden case closed by means of screws that there is a space of not less than 3 cm filled with cushioning materials at all points between the fibreboard cases and the packing case. (2) A package under (1) (a) or (1) (b) 1. must not weigh more than 75 kg; a package under 1 (c) must not weigh more than 10 kg; a package under (1) (b) 2. or (1) (d) must not weigh more than 35 kg. Packages which, with their contents, weigh more than 30 kg shall be fitted with means of handling. (1) Substances of 10° shall be packed, not more than 500 g per bag, in firmly-tied bags made of a suitable pliant material; each bag shall be placed in a box made of metal, fibreboard or paperboard; these boxes, not more than 30 per packing case, shall be secured by cushioning materials in a wooden packing case with complete sides not less than 12 mm thick. (2) A package must not weigh more than 25 kg. ( 1) Substances and articles of 11 ° shall be packed: (a) substances of 11 ° (a) and (b): 1. not more than 2.5 kg per bag, in bags placed in boxes made of fibreboard, tin-plate or aluminium. The boxes shall be secured by cushioning materials in wooden packagings; or 2. in bags made of closely-woven fabric, placed in wooden casks or cases; (b) articles of 11 ° (c): rolled in stout paper; each roll must not weigh more than 300 g. The rolls shall be placed in a wooden case lined with stout paper. (2) The lids of the wooden cases shall be secured by means of screws; if the screws are made of iron they shall be coated with a material not liable to produce sparks when subjected to shock or friction. • (3) A package must not weigh more than 75 kg if it is carried as part of a full load, and not more than 35 kg if . it is carried as part of a full load and not more than 35 kg if it is not carried as part of a full load. (1) Substances of 12° shall be cartridged in wrappings made of a suitable plastic material or of paper. The cartrid­ ges may be dipped in paraffin wax, ceresine or resin, or be wrapped in a suitable plastics material, so as to be protected from damp. Explosives containing more than 6 p~f cent liquid nitric esters shall be cartridged in paper coated with paraffin wax or ceresine or in an impermeable plastics material such as polyethylene. The cartridges shall be placed in wooden packagings. (2) Cartridges not coated with paraffin wax or ceresine, or cartridges in permeable wrappings, shall be made up into packets weighing not more than 2.5 kg each. Packets so made up, whose wrapping must consist at least of stout paper, shall be dipped in paraffin wax, ceresin or resin or wrapped in a suitable plastics material so as to be protected from damp. The packets shall be placed in wooden packagings. (3) The closure of wooden packagings may be ensured by means of metal bands or wires fastened tightly round them. (4) A package must not weigh more than 75 kg. It must not contain more than 50 kg of explosives. (5) Instead of the wooden packagings prescribed in paragraph (1) and paragraph (2), it is also permissible to use suitable cases, made of solid fibreboard or corrugated fibreboard, .which are of sufficient mechanical strength and whose lid flaps and bottom flaps must be closed by means of adhesive strips of sufficient strength. The design of cases made of solid fibreboard or corrugated fibreboard must be approved by the competent authority of the coun­ try of departure. Such a package must not weigh more than 30 kg; it must not contain more than 25 kg of explosi ves. . (1) Substances of 13° shall be cartridged in paper wrap­ pings. Cartridges not coated with paraffin wax ·or ceresine 2110 2111 2112 2112 2113 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2173 shall first be rolled in paper that has been rendered imper­ meable. They shall be made up by means of a .paper wrapping into packets weighing not more than 2.5 kg each, which shall be secured by cushioning materials in wooden packagings whose closure may be ensured by means of metal bands or wires fastened tightyl round them. (2) A package must not weigh more than 35 kg. (1) Substances of 14° shall be p~cked: (a) substances of 14° (a): cartridged in wrappings made of paper that has b een rendered impermeable. The cartrid­ ges shall be made up into packets by means of a paper wrapping or, if without a paper wrapping, secured by cushioning materials in fibreboard cases. The packets or fibreboard cases shall be secured by inert cushioning ma­ terials in wooden packagings whose closure may be ens­ ured by means of metal bands or wires fastened' tightly round them; (b) substances of 14° (b): cartridged in wrappings made of paper that has been rendered impermeable. The cartrid­ ges shall be placed in a fibreboard box. The fibreboard boxes, wrapped in paper that has been rendered imperme­ able, shall be secured, leaving no empty spaces, in wooden packaging whose closure may be ensured by means of metal bands or wires fastened tightly round them; (c) substances of 14° (c): 1. ?artridged in wrappings made of suitable plastics matenal or of paper. The cartridges may be dipped in paraffin wax, ceresine or resin or be wrapped in a suitable plastics m at~rial, so as to be protected from damp. Explosi­ ves contammg more than 6 per cent liquid nitric esters shall be cartridged in paper coated with paraffin wax or ceresine or in an impermeable plastics material such as polyethylene. The cartridges shall be placed in wooden packagings; 2. cartridges not coated with paraffin wax or ceresine, or cartridges in permeable wrappings, shall be made up into packets weight more than 2.5 kg each. Packets so made up, whose wrapping may consist at least of stout paper, shall be dipped in paraffin ceresine or resin or be wrapped in a suitable plastics material so as to be protected from damp. The packets shall be placed in wooden packa­ gings; 3. the closure of wooden packagings may be ensured by means of metal bands or wires fastened tightly round them; 4. instead of the wooden packagings prescribed under l. and 2. it is also permissible to use suitable cases, made of solid fibreboard or corrugated fibreboard, which are of sufficient mechanical strength and whose lid flaps and bottom flaps nmst be closed by means of adhesive strips of sufficient strength. The design of cases made of solid fibreboard or corrugated fibreboard must be approved by the competent authority of the country departure. (2) A package containing substances of 14° (a) or (b) must weigh ·more. than 35 kg. A package containing substances of 14° (c) must not weigh more than 75 kgr; it must not contain more than 50 kg of explosives; in the case of a packing conforming to paragraph 1 ( c) 4. package must not weigh more than 30 kg nor contain more than 25 kg of explosives. 3. Mixed packing Substances listed under an item number of marginal 2101 may be included in the same package either with substances grouped • under the same or another item number of that marginal, or with substances or any of other Classes, or with other goods. Note: Packages as referred to in marginal 2108 (1) (c) may contain organic nitro-compounds having different compositions and names. 4. Marking and danger labels on packages (see Appendix A.9) Packages containing picric acid (7° (a)] shall be marked with name of the substance in clearly legible and indelible red characters marking shall be in an official language of the country of departure and also, if that language is not English, or French. or German in English, French or Ger­ ;;·,·;!1. unless interrn1t••mal ro?cl •ransport tariffs, if any 2114 2114 2115 2116 agreements concluded between the countries concerned in the transport operation, provide otherwise. ( 1) Packages containing substances and articles of Class 2117 la shall bear a label conforming to model No. 1. (2) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9. If the fragile receptacles contain liquids, the packa ges sliall in addition, except in the case of sealed ampoules, bear labels conforming to model No. 8; these labeis shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. 2118 B. Particulars in the transport document The description of the goods in the transport document 2119 must conform to one of the names underlined in marginal 2101. Where the name of the substance is not indicated in the case of 8° (a) and (b), the trade name must be used. The description of the goods must be underlined in red and followed by particulars of the Class; the item number (together with the letter, if any), and the initials "ADR" • or "RID" [e.g. la 3° (a) ADR]. • . (2) The following must be certified in the transport doc~ment: "The nature of the goods, anq the packaging, are m conformity with the provisions of ADR". (3) For consig nments which, under marginal 11 400 of Annex B, are to be accepted for carriage as a full load only, the transport document shall also show the weight o'. each package and the number and nature of the packa gmgs. 2120 2125 C. Empty packagings (1) Packagings of 15° must be securely dos~d and be 2126 leak-proof in the same degree 'as though they were full. (2) The description in the transport document must be: "Empty packaging, la, 15°, ADR (or RID)':. This descrip tion must be underlined in red. • 2127 2129 CLASS lb. ARTICLES FILLED WITH EXPLOSIVE SUBSTANCES 1. List of articles (1) Among the articles covered by the heading of Class 2130 1 b, only those listed in marginal 2131 are to be accepted . for carriage, and then only subject to the provisions of this Annex and of Annex B. These articles to be accepted for carriage under certain conditions are to be considered as articles of ADR. .(2) If the articles listed under 7°, 10° or 11 ° of marginal 2131 are composed of, or filled with, explosive substances listed in marginal 2101 those substances must satisfy the stability and safety conditions laid down concerning them in Appendix A. l. 1 ° Fuses, not primed: 2131 (a) rapid combustion fu:,es (fuses consisting of a thick tube with a core of black powder, or with a core of threads impregnated with black powder, or with a core of nitrated. cotton threads); (b) detonating fuses in the form of small-section m·etal tubes with thin walls and a core filled with an explosive substance; see also Appendix A. l, marginal 3108; (c) flexible detonating fuses wrapped in textile or a plastics material, of small section and with a core filled with an explqsive substance; see also Appendix A. l, mar ginal 3109; • (d) instantaneous detonating fuses (small-section woven fuses with a core filled with an explosive substance more dangerous than penthrite ). For other fuses, see Class le, 3° (marginal 2171). 2° Non-detonating primers (primers which do not prod uce a disruptive effect either with the aid of detonators or by other means): (a) percussion caps; (b) 1. primed cases of central-percussion cartridges, not filled with propellent powder, for firearms of all calib res: • • 2174 ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) ·2. primed cases of rim-fire cartridges, not filled with propellent powder, for Flobert weapons and firearms of similar calibres; (c) quick-matches, screw-primers and other similar pri­ mers containing a small charge (black powder or other explosives), set in action by friction, percussion or electri­ city; (d) fuses without any device, e.g. detonator, producing a dispruptive effect and without a transmission charge. 3° Railway for sig~als 4° Small-arms cartridges [with the exception of those containing a bursting charge (see under 11 ?)]: (a) sporting cartridges; (b) Flobert cartridges; ( c) tracer cartridges; ( d) incendiary cartridges; (e) other central-percussion cartridges. Note: Apart from sporting cartridges with lead pellets, only cartridges whose calibre does not exceed 13.2 mm are to be considered as articles of 4°. 5° Detonating fuses: . • (a) detonators with or without a delayed-action device: delayed-action connecting pieces for detonating fuses; (b) electric detonators fitted with fuses with or without a delayed-action device; (c) detonators connected firmly to a black-powder fuse; (d) detonators with gaines (detonators combined with a transmission charge composed of a compressed explosive); see also 1\ppendix A.I, marginal 3110; (e) fuses with detonators (fused detonators) with or without a transmission charge; (f) detonators with percussion cap ("bouchons all­ umeurs") with or without a delayed-a,ction device, with or without a mechanical device for firing, and without a tran­ smission charge. 6° Sounding caps (detonators, with or without primers, contained in sheet-metal tubes). 7° Articles with a propellent charge, other than those listed under 8°; articles with a bursting charge; articles with a propellent and a bursting charge, provided that they contain only explosive substances of Class la all without a device producing a disruptive effect (e.g. detona­ tor). The charge in these articles may comprise a tracer substance (see also under 8° and 11 °). Note: Non-detonating primers (2°)· are allowed in these articles. 8° Articles filled with tracer substances or substances intended for signalling, with or without a propellent charge, with or without an ejection charge, and without a bursting charge, in which the propellent or tracer substance is compressed in such a way that the articles cannot explode when ignited. 9° Smoke-producing devices containing chlorates or carrying an explosive charge or an explosive ignition charge. For smoke-producing substan,ces for agricultural and forestry purposes, see Class le marginal 2171 27°. 10° Boring devices containing a charge of dynamite or of an explosive similar to dynamite, without fuses and without any device producing a disruptive effect (e.g. deto­ nator), hollow-charge devices for industrial purposes, co­ ntaining not more than 1 kg of explosive secured within the casing, and without a detonator. 11 ° Articles with a bursting charge, articles with a pro­ pellent and a bursting charge, all fitted with a device producing a disruptive effect (e.g. detonator), the whole well secured. The weight of each article must not exceed 25 kg. 2. Provisions A. Packages. 1. General conditions of packing (1) Packagings shall be so closed and leak-proof as to prevent any loss of the contents. The use of metal bands or wires fastened round the packages to ensure their clos­ ure is allowed; their use is compulsory with cases having 2132 hinged lids if the lids are not fitted with an effective device to obviate any loosening of the closure. (2) The materials of which the packagings and their closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there­ with. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require• ments of carriage. Articles shall be firmly secured in their packagings, and inner packagings shall be firmly secured in outer packagings. Unless otherwise specified in the section entitled "Packing of articles of the same kind", inner packagings may be enclosed in outer packagings, either ~ingly or in groups. (4) 'cushioning materials shall be suited to the nature of the contents. 2. Packing of articles of the same kind Articles of 1 ° shall be packed as follows: (a) articles of 1 °(a) and (b): in wooden packagings or in drums made of impermeable fibreboard. A package drums must not weigh more than 120 kg; however, a fidre­ board dru must not weiwi more than 75 kg; (b) articles of 1 °(c): rolled in lengths of up to 250 m on reels made of wood or fibreboard. The reels shall be placed in wooden cases in such a manner that they cannot come into contact either with one another or with the sides of the cases. A case must not contain more than 1,000 m of fuse; • (c) articles of 1 °(d): rolled in lengths of up to 125 m on reels made of wood or fibreboard which shall be packed in a wooden case, closed by means of screws and with sides not less than 18 mm thick, in such a manner that the reels cannot come into contact either with one another or with the sides of the case. A case must not contain more than 1,000 m of instantaneous detonating fuse. ( 1) Articles of 2° shall be packed as follows: (a) articles of 2°(a): caps with an uncovered explosive charge, not more than 500 per box or small case, and caps "'.ith a covered explosive charge, not more than 5,000 per box or small case, in sheet-metal boxes, fibreboard boxes or small wooden cases. These packagings shall be placed in a packing case made of wood or sheet-metal; (b) articles of 2°(b) 1: primed cases of central-percussion cartridges, not filled with propellent powder, for firearms of all calibres, for cases made of wood or fibreboard or in textile bags; (c) articles of2°(b)2: primed cases of rim-fire cartridges, not filled with propellent powder, for Flobert weapons and firearms of similar calibres, not more than 5,000 per box, in boxes made of sheet-metal or fibreboard which shall be placed in a packing case made of wood or sheet-metal; however, these primed cases for rim-fire cartridges may also be packed, not more than 25,000 per bag, in a bag which must be secured by means of corrugated fibreboard in a packing case made of wood or iron; (d) articles of 2°(c) and (d): in boxes made of figreboard, wood or sheet-metal which shall be placed in packagings made of wood or metal. (2) A package containing articles of 2°(a), (c) or (d) must not weigh more than 100 kg. (1) Articles of 3° shall be packed in cases made of boards .not less than 18 mm thick, tongued and grooved . and assembled by means of wood screws. Fog signals shall be secured in cases by cushioning materials in such a manner that they cannot come into contact either with one another or with the sides of the case. (2) A package must not weight more than 50 kg. ( 1) Articles of 4 °(a), (b) and ( e) shall be placed tightly in firmly-closing boxes made of sheet-metal, wood or fibre7 board; these boxes shall be housed, leaving no empty spaces, in packing cases made of metal, wood, hardboard, solid fibreboard or corrugated fibreboard; the fibreboard must have been rendered impermeable by impregnation and be of sufficient mechanical strength. Fibreboard cases shall be closed by means of adhesive strips of sufficient strength. The production model of cases 2133 2134 2135 2136 E<l>HMEPIE THE KYBEPNHEEQE (TEYXOr nPQTO) 2175 made of solid fibreboard or corrugated fibreboard must be approved by the competent authority of the country of departure. (2) Articles of 4°(c) and (d) shall be placed, not more than 400 per box, in boxes made of sheet-metal, wood or fibreboard; these boxes shall be packed securely in packing cases made of metal or wood. (~) A package must not weigh more than 100 kg; howe­ ver, where hardboard or fibreboard cases are used, a package containing articles of 4(a), (b) or (e) must not weigh more than 40 kg. (1) Articles of 5° shall be packed as follows: (a) articles of 5°(a): not more than 100 per receptacle in the case of detonators and not more than 50 per recep­ tacle m the case of connecting pieces, in receptacles, made of sheet-metal or impermeable fibreboard, in which they shall be well protected against ignition and secured by cushioning materials. Sheet-metal receptacles shajl be li­ ned with a resilient material. The lids shall he secured all round by adhesive strips. Receptacles·shall, not more than 5 per packet or box in the case of detonators and not more than 10 per packet or box in the case of connecting pieces, be enclosed in a packet or placed in a fibreboard box. The packets or boxes shall he packed in- a wooden case closed by means of screws and with sides not less than 18 mm thick, or in a sheet-metal packaging, the case or packaging being secured by cushioning materials i a packing case with sides not less than 18 mm thick in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points between the wooden case or sheet-metal packaging and the packing case; . (b) articles of 5°(b): not more than 100 per packet,"in packets with alternate detonators lying towards opposite ends of the packet. Not more than 10 of these packets shall be tied together to form a collective packet. Not more than 5 of these collective packets shall be secured by cushioning materials in a wooden packing case with side not less than 18 mm thick, or in a sheet-metal packaging, in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points between the collective packets and the packing case or sheet-metal packaging; (c) articles of 5°(c): fuses fitted with detonators, rolled into coils! not more than 10 coils shall be made into a roll which shall be wrapped in paper. Not more than 10 rolls shall he secured by cushioning materials in a small wooden case closed by means of screws and with sides not less than 12 mm thick. Not more than 10 small cases s~all ~e secured by cushioning materials in a packing case with sides not less than 18 mm thick in such a manner that there is a span of not less than 3 cm filled with • cushioning materials at all points between the small cases and the packing case; (d) articles of 5°(d): 1. not more than 100 detonators per case, in wooden cases with sides not less than 18 mm thick, in such a manner that the detonators are spaced not less than 1 cm from one another and from the sides of the case. The said sides shall be mortised and the !:>ottom and lid shall be secured by screws. If the case and the bottom and lid shall be secured by screws. If the case is lined with zinc sheet or aluminium sheet, a side thickness of 16 mm is sufficient. The case shall be secured by cushioning mate­ rials in a packing case with sides not less than 18 mm thick in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points • between it and the packing case; or 2. not more than 5 detonators per box, in sheet-metal boxes; the detonators being placed there in slatted wooden frames or in holed pieces of wood. The lid shall be secured all round by adhesive strips. Not more than 20 sheet-metal boxes shall be placed in a packing case with sides not less than 18 mm thick; (e) articles of 5°(e): not more than 50 per case, in wo oden cases with sides not less than 18 mm thick. The articles shall be secured within the cases by a wooden structure in such a manner that they are spaced not less than 1 cm from one another and from the sides of the 2137 case. The sides of the case shall be mortised and the bottom and lid shall be secured by screws. Not more than 6 cases shall be secured by cushioning materials in a packing case with sides not less than 18 mm thick in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points between the cases and the packing case. The space may he reduced to not less than 1 cm if it is filled with porous wood-fibre slabs. If the articles are,individually packed and firmly secured in hermetically-closing boxes made of sheet-metal or a plastics material, they may be placed in a wooden packing case with sides not less than 18.mm thick. The articles must be separated from one another and firmly secured by fibreboard or by wood-fibre slabs; (I) articles of 5°(1): 1. not more than 50 per case, in wooden or metal cases; in these cases each detona ting part of the "bouchon allumeur" shall be so accommodated in a slotted wooden support that the distance between adjacent detonators and between the detonators of the outermost "bouchons all­ umeurs" and the side of the case is not less than 2 cm; closing the lid of the case shall ensure complete immobility of the whole; not more than 3 cases shall he placed, leaving no empty spaces, in a wooden packing case with sides not less than 18 mm thick; or 2. in boxes made of wood or metal; in these boxes each "bouchon allumeur" shall he so supported by a frame that the distance between two "bouchoh allumeurs" and between a "houchon allumeur" and the side of the box is not less than 2 cm and that the immobility of the whole is ensured; these boxes shall be placed in a packing case with sides not less than 18 cm thick in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points between the boxes and between the boxes and the packing case; a package must not contain more than 150 "bouchons allumeurs". (2) The lid of the packing case smaH ~~ closed by means of screws or of hinges and folding bars. (3) Each package containing articles of 5° shall be provided with a closure protected either by lead or other seals (stamp or mark) applied to two screw-heads at the ends of the major axis of the lid or the folding bars, or by a strip, bearing the trade mark, gummed on to the lid and on two opposite sides of the case. (4) A package must not weigh more than 75 kg; packa­ ges weigh more than 30 kg shall be fitted with means of handling. (1) Articles of 6° shall be rolled separately ·in paper and placed in corrugated fibreboard wrappings. They shall be packed, not more than 25 per box, in boxes made of fibreboard or sheet-metal. The lids shall be secured all round by adhesive strips. Not more than 20 boxes shall be placed in a wooden packing case. (2) A package must not weigh more than 50 kg. Packa • ges weigh more than 30 kg shall be fitted with means of handling. ( 1) Articles of 7° shall be packed in wooden cases closed by means of screws or of hinges• and folding and with sides not less than 16 mm thick, or in receptacles made of metal or a suitable plastics material of adequate stren­ gth. The lids and bottoms of the wooden cases may also be made of highly-compressed paperboard equalling the sides in strength. Articles weighing more than 20 kg may also be despatched in crates or without packing. (2) A package must not weigh more than 100 kg if it contains articles each of which weighs not more than 1 kg. Cases which, with the contents, weigh more than 30 kg shall be fitted with means of handling. ( 1) Articles of 8° shall be packed in wooden cases, in drums made of fibreboard which has been rendered imper­ meable, or in receptacles made of metal or of a suitable plastics material of adequate strength. The ignition head shall be protected in such a manner as to prevent any scattering of the charge from the article. (2) A package must not weigh more than 100 kg; howe­ ver, when fibreboard drums are used a package shall not 2138 2139 2140 2176 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) weigh more than 75 kg. Cases which, with their contents, weigh more than 30 kg shall be fitted with means of han­ dling. Articles of 9° shall be enclosed in wooden packagings. A package must not weigh more than 75 kg; packages weighing more than 30 kg shall be fitted with means of handling. Articles of 10 ° shall de packed in wooden cases. Packages weighing more than 30 kg shall be fitted with means of handling. Articles of 11 ° shall be packed as follows: (a) articles less than 13.2 mm in diameter: not more than 25 per box, packed tightly in firmly - closing fibreboard boxes or in receptacles made of a sutitable plastics material of adequate strength; these boxes or receptacles shall be placed, leaving no empty spaces, in a wooden case, with sides not less than 18 mm thick, which may be lined with tin - plate, zinc or aluminium sheet, or a suitable plastics or simiral material of adequate strength. A package must not weigh more than 60 kg. Packages weighing more than 30 kg shall be fitted with means of handling. (b) articles from 13.2. mm to 57 mm in diameter: 1. separately in a tube made of fibreboard or of a suitable plastics material, strong, close - fitting and closing firmly at both ends; or in a tube made of fibreboard or of a suitable plastics material, strong, cl :se - fitting, closed at one end and open at the other; or in a tube made of fibreboard or of a suitable plastics material, open at both ends but with an inner projection or other suitable internal device to prevent the article from moving. Packed in this manner, not more than: 300 articles not less than 13.2. mm and not more than 21 mm in diameter; or 60 articles more than 21 mm but not more than 3 7 mm in diameter; or 25 articles more than 37 mm but not more than 57 mm in diameter shall be placed in layers in a wooden case with sides ·not less than 18 mm thick, the wooden case being lined with tin - plate, zinc sheet, or aluminium sheet: In the case of articles packed in tubes open at both ends or at one end, the packing case shall be· lined on the side or sides adjacent to the open ends of the tubes either with a felt pad not less than 7 mm· thick or with a sheet of the same thickness of double - faced corrugated fibreboard or similar material. • ' • A package must not weigh more than 100 kg. Packages weighing more than 30 kg shall be fited with means of han­ dling; 2. articles 20 mm in diameter may also be packed, not more than 10 per box, in strong, closely - fitting fibrebo­ ard boxes coated with paraffin wax and equipped with a honey - combed bottom insert and with partitions made of fibreboard coated with paraffi n wax. The boxes shall be closed by a gummed flap. Not more than 30 boxes shall be tightly packed in a wooden case being with sides not less than 18 mm thick, the wooden case being lined with zinc sheet, tin - plate or aluminium sheet. A package must not weigh more than 100 kg. Packages weighing more than 30 kg shall be fited with means of han­ dling; 3. articles not more than 30 mm in diameter may, in a number not exceeding that indicated under 1., also be put on to strips and packed in a stong steel receptacle. This receptacle may be cylindrical. These articles put on to strips shall be surrou~ded by a suitable device so as to constitute a compact unit and as to prevent individual articles from becoming detached. One or more units shall be so fixed in the receptacle that they cannot be displaced. The ends of articles put on to strips shall rest on shock absorbing non - metallic supports. The lid of the receptacle must be so closed as to be 2141 2143 leak - proof and be so secured by a locking device capable of being sealed that the articles cannot fall out. A pagkage must not weigh more than 100 kg. Packages weighing more than 30 kg shall be fitted with means of handling. Receptacles capable of being rolled shall have their lids fitted with a strong handle enabling them to be carried; 4. articles not less than 30 mm and not more than 5 7 • mm in diameter may also be packed separately in a strong, closely - fitting, hermetically - closed cylindrixal box made of fibreboard, fibre or a sutitable plastics material. Not more than 40 of these boxes shall be placed in layers in a wooden case with sides not less than 18 mm thick. A package must not weigh more than 100 kg. Packages weighing more than 30 kg shall be fitted with means of handling. (c) Other articles of 11 °:inconformity with the provisions of marginal 2139 (1. A package must not weigh more than 100 Kg. Packages weighing more than 30 kg shall be fitted with means of handling. . Note: In the case of articles containing both propellent and bursting charges, the diameter referred to is that of the cylindrical portion containing the bustring charge. 3. Mixed packing. (1 )Articles listed under an item number of marginal 2131 may not be •included in the same package either with articles of a different kind but of the same item number, or with articles of another item number of than marginal, or with substances or articles belonging to other Classes, or with other goods. (2) The following may, however, be included in the same pagkage: {a) articles of 1 ° with one another. When articles of 1 °(a) and (b) are included in the same package, they shall be packed in conformity with marginal 2133 (a). When articles of 1 °(c) are included in the same package with articles of 1 °(a) or (b) or both, those of 1 °(c) shall be made up into packages in conformity with the provisions applicable to them and the outer packaging shall be that prescribed for articles of 1 °(a) or (b). A package must not weigh more than 120 kg; (b) articles of 2°(a) with those of 2°(b), provided that both are contained in inner packagings consisting of boxes placed in wooden cases. A package must not weigh more than 100 Kg; (c) articles of 4owith one another, taking into account the provisions for inner packaging, in a wooden outer packa­ ging. A package must not weigh more than 100 kg; (d) articles of 7° with those of 5°(a) (d), (e) and (f), on condition that the packaging of these latter prevents the transmission of a possible detonation to the articles of 7 °. In one package the number og articles of 5°(a), (d), (e), and (f) must be the same as that of the articles of 7°. A package must riot weigh more than 100 kg. 4. Marking and danger labels on packages (see Appen­ dix A.9) Packaging containing articles of Class ib shall bear a label conforming to model No 1. However, packages, containing articles of 1 °(d), 5° and 6° shall bear two labels conforming to model No. 1. B. Particulars in the transport document (1) The description of the goods in the transport document must conform to one of the names underlined in marginal 2131; it must be underlined in red and followed by partic­ ulars of the Class, the item number together with the letter, if any), and the initials «ADR» or «RID» (e.g. lb 2°(a) ADR. (2) The following must be certified in the transport doc­ ument: «The nature of the goods, and the packaging, are in confor­ mity with the provisions of ADR. C. Empty packaging No provisions. 2144 2145 2146 2147 2148-' 2162 2163 2164 2169 E<DHMEPII THI -KYBEPNHIEQI (TEYXOI nPQTO) 2177 CLASS le IGNITERS, FIREWORKS AND SIMILAR GOODS 1. List of goods ( 1) Among the substances and articles covered by the heading of Class le, only those listed in marginal 2171 are lo be accepted for carriage, and then only subject to the provisions of this Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. (2) Articles to be accepted must fulfil the following condi­ tions: (a) The explosive charge shall be constituted, arranged and distributed in such a manner that neither friction, shaking, shock nor ignition of the packed articles can lead to an exlposion of the whole contents of the package; (b) white or yellow phosphorus may not be used except in articles of 2° and 20°; ( c) the detonating compound of fireworks (21 °- 24°), flash powders (26°), and the smoke - producing compounds of pesticides (27°), must not contain chlorates; ( d) the explosive charge must satisfy the stability conditions of Appendix A.I., Marginal 3111. 4. Ignilens: 1 ° .(a) Safety matches (with a potassium chlorate and sulphur base); • (b) Matches with a base of potassium chlorate and of phosphorus sesquisulphide, also friction igniters. 2 °. Strips of amorces for safety lamps and strips of paraffin - waxed amorces for safety lamps. 1,000 amor­ ces must not contain more than 7 .5- explosive. For strips of caps, see under 15° 3 °. Slow - combustion fuses (fuses consisting of a thin impermeable tube with a narrow - section core of black powder). For other fuses, see Class 1 b, 1 °(Marginal 2131 ). 4 °. Pyroxlin thread (nitrated cotton thread). See also Appendix A.1, marginal 3101. 5°. Tubular igniters («lances d' allumage» (tubes, made of paper or fibreboard, containing a small quantity of a fuse composition of oxygenated substances and organic substances and, possibly, of nitrated aromatic compounds) and thermite caps with pellet igniter. 6 °. Safety igniters for fuses (paper cartridges containing a primer by thread intended to cause friction or tearing, or similar devices). 7t(a) Electic primers without detonator; (b) pellets for electric primers. 8°.Electric igniters (e.g. igniters intended for igniting photograph magnesium powders). The charge of each must not exceed 30 mg nor contain more than 10 per cent fulminate of mercury. Note: Appliances of the electric bulb type producing a sudden light and containing an ignition charge similar to that of electric igniter are not subject lo the provisions of ADR. B. Pyrotechnic articles and toys: caps and (strips) of caps; detonating articles: 9°. Indoor pyrotechnic articles (e. g. Boscocylinders, confetti bombs cotillon fruits). Articles with a nitrated cotton (collodion - cotton) base must not contain more than 1 g per article. 10° .Fulminating bonbons, flower crackers, strips of nitra­ ted paper (collodion paper). 11 ° .(a) Fulminating peas, fulminating grenades and other similar pyrotechriic toys containing fulminate of silver; (b) fulminating matches; (c) accessories with fulminate of silver. Ad (a) (b) and (c): 1,000 articles must not contain more than 2.5 g fulminate of silver. 12°. Detonating -pebbles, each carrying on the outside a charge of no more than 3 g o f an explosive other than fulminate. 13 °. Pyrotechnic matches (e.g. Bengal matches, golden rain matr:hes cascade - of - flowers matches). 2171 14 °. Miracle candles without ignition heads. 15 °. Caps for children's toys, strips (strings) of caps and rings of caps. 1.000 caps must not contain more than 7 .5. g of an explosive free from fulminate. For strips of caps for safety lamps, see under 2° .. 16°. Explosive c~rks with a~ expiosive charge having a phosphorus and chlorate base or with a charge of fulminate or a similar compound compressed into cardboard cartrid­ ges. 1,000 corks must not contain more than 60g chlorate . explosive nor more than 1 0g of fulminate of a compound with a fulminate bace. 1 7 °. Round petards with an explosive ci}arge having a phosrhorus and clorate base. 1,000 petards must not contain more than 45g explosive. 18 °. Cardboard caps (toy ammunition) with an explosive charge having a phosphorus and chlorate bace or with a charge of fuhnin.ate ~r a similar compound. 1,000 caps must not contain more than 25 g explosi~e. 19°. Cardboard caps exploding under foot, with a protec­ ted charge having a phosphorus and chlorate base. 1,000 caps must not contain more than 30 g explosive. 20°. (a) Detomating sheets; (b) Martinikas (so called Spanish fireworks). Both comprise a mixture of white (yellow) and red phosphorus with potassium chlorate and not less than 50 per cent inert substances not taking part in the decomposi­ tion of the mixture of phosphorus and chlorate. A sheet must not weigh more tan 2.5. g and a martinika not more than 0.1 g. C. Fireworks 21°. Anti - hail rockets not fitted with a detonator, bombs and firepots. The charge, including the propellent charge, must not weigh more than 14 kg per article, the bomb or firepol not more than 18 kg in all. 22 °. lncediary bombs, rockets, Roman candles, fou­ ntains, wheels and similar fireworks, with a charge not weighing more than 1,200 g per article. . .. , v 23 °. Cannon shots each containing not more than 600 g granulated black powder or 220 g of an explosive not more dangerous than aluminium powder with potassium perchlorate, rifle shots (crackers) each containing not more than 20 g granulated black powder, all provided with fuses with covered ends; and similar articles for producing a loud detonation. For railway fog - signals, see Class lb, 3o(Marginal 2131). 24 °. Small fireworks ( e.g. jumping - crackers, serpents, golden rain, silver rain, if they contain not more than 1,000 g granulated black powder per 144 articles; volca­ noes and hand comets, if they contain not more than 30 g each of granulated black powder). . 25 °. Bengal fires without ignition heads (e.g .. Bengal torches, lights, flames). 26 °. Magnesium flash - powders, not more than 5 g per bag or tube, in paper bags or in small glass tubes. D. Pesticides (substances and articles): 27°. Smoke producing substances for agricultural and forestry purposes and smoke - producing cartridges for use as pesticides. For smoke - producing devices containing chlorales or carrying an explosive charge or an explosive ignition charge, see Class lb (Marginal 2131). 2. Provisions A. Packages 1. General conditions of packing ( 1) Packings shall be so closed and leak - proof as to prevent any loss of the contents. (2) Packagings, including their closures, must be sufficient rigid and strong in all their parts lo prevent any loosening during carriage and to meet the normal requiremets of carriage. Articles shall be firmly secured in outer packa­ gings. Unless otherwise specified in the section entitled «Packing of a single substance or of articles of the same kind», inner packagings may be enclosed in outer packa­ gings, either singly or in groups. 2172 2178 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) (3) Cushioning materials shall be suited to the nature of the cont~nts. 2. Packing of a single substance or of articles of the same kind (1) Articles of I 0 (A) shall be packed in boxes or in books. These boxes or books shall be wrapped in stout paper- to form a collective packet all the folds of which shall b~ glued. The books may also be placed in boxes made of thin fibreboard or of a material not readily inflam­ mable (e.g. cellulose acetate). The fibreboard boxes or the collective packets shall be placed in a strong case made of wood, metal, compressed - wood hardboard, strong solid fibreboard or double - faced corrugated fibre­ board. All joints of metal cases shall be secured by soft solde­ ring or double - seaming. Fibreboard cases shall be closed by means of joined flaps. The edges of the outer flaps, and all joints, must be either flu ed or firmly closed by some other suitable means. If the fibreboard boxes or collective packets are packed in fibreboard cases, the weight of a package may not ex­ ceed 20 kg. (2) Articles of 1 ° (b) shall be so packed in boxes as to prevent any movement. Not more than 12 of these boxes shall be enclosed in a packet all the folds of which shall be glued. Not more than 12 of these packets shall be wrapped in stout paper to form a collective packet all the folds of which shall be glued. The collective packets shall be placed in a strong case made of wood, metal, compressed - wood hard­ board, strong solid fibreboard or double ·- faced corru­ gated fibreboard. All joints of metal cases shall be secured by soft solde ring or double - seaming. J Fibreboard cases shall be closed by mean·s of joined flaps. The edges of tl ie, outer flaps, and all joints, must be either glued or firmly closed by some other suitable means. If the collective packets are packed in fibreboard cases, the weight of package must not exceed 20 Kg. (1) Articles of 2° shall be packed in boxes made of sheet - metal or fibreboard. Not more than 30 sheet metal or 144 fibreboard boxes shall be enclosed in a packets which must not contain more than 90 g exlosive. These packets shall be placed in a packing case, with well-jointed sides not less than 18 mm thick, lined with stout paper or with thin zinc or aluminium sheet or with a sheet of a plastics material not readily inflammable. A side thickness of 11 mm is sufficient for a package weigh­ ing not more than 35 kg if the case is encircled with an iron band. (2) A package must not weigh more than I 00 kg. (1) Articles of 3° shall be packed in wooden cases lined with stout paper or thin zi.nc or aluminium sheet, or in drums of impermeable fibreboard. Small consignments weighing not more than 20 kg, wrapped in corrugated fibreboard, may also be made up into packets in stout two ply packing paper securely tied with string. • (2) Where fibreboard drums are used, a package must not weigh more than 7 5 kg. • (1) Pyroxylin thread (4°) shall be rolled, in lengths not exceeding 30 m per strip, on fibreboard strips. Each roll shall be wrapped in paper. Not more than 10 of these rolls shall be wrapped in packing paper to form packets which shall be secured by cushioning materials in small wooden cases. The cases shall be placed in a wooden packing case. (2) A package must not contain more than 6,000 m of pyroxylin thread. (!)Articles of 5° shall be packed, not more than 25 per box, in boxes made of tin-plate or fibreboard; however, thermite caps may be packed, not more than 100 per box, in fibreboard boxes. Not more than 40 of these boxes shall be secured br cushioning materials in a wooden case 2173 2174 2175 2176 2177 in such a manner that they cannot come into contact either with one another or with the sides of the case. . (2) A package must not weigh more than 100 kg. (1) Articles of 6° - 8° s; hall be pached. (a) articles of 6°: in wooden cases; (b)articles of 7° (a): in wooden cases 9r in woo.den casks or in drums made of impermeable fibreaboard; (c) articles of 7° (b): not more than· l,000 per box, secured by sawdust cushioning in fibreboard boxes divided into not less than three compartmets each containing ap­ proximately the same number of articles and separated by by interposed fibreboard sheets. The lids of boxes shall be secured by gummerd strips applied all roud. Not more than I 00 of these fibreboard boxes shall be placed in a perforated sheet - iron receptacle. This receptacle shall be secured by cushioning materials in a wooden packing case closed by means of screws and with sides not less than 18 mm thick, in such a manner that there is a space of not less than 3 cm filled with cushioning materials at all points between the sheet - iron receptacle and the packing case; (d) articles of 8°: in fibreboard boxes. The boxes shall be made up into a packet containing not more than 1,000 electric igniters. The packet shall be placed in a wooden packing case. (2) In the case of fibreboard drums, a package contai­ ning articles of 7° (a) must not weigh more than 75 kg. A package containing articles of 7° (b) must not weigh more than 50 kg; if it weighs more than 30 kg it shall be fitted with means of handling. (1) Articles of 9° - 26° shall be enclosed (in~er packa­ ging): (a) articles of9° and 10°: in paper packagings or in boxes; (b) articles of 11 ° (a): not more than 500 per fibredoard box or per small wooden case, secured by sawdust cushio­ ning: 1. in fibreboard boxes which shall be wrapped in paper; or 2. in small wooden cases; (c) articles of 11 • (b): not more than 10 per book,in books; not more than 100 books together shall be packed in a fibreboard box; or wrapped in stout paper; (e) articles of 12~: not more than 25 per box, in fibrebo­ ard boxes; (f) articles of 13°: in boxes wrapped in paper to form packets each containing not more than 12 boxes; (g) articles of 14°: in boxes or i~ bags made of paper or of a suitable plastics material. These packagings shall be wrapped in paper to form packets each containing not more than 144 of these articles; (h) articles of 15°: in fibreboard boxes each containing: not more than I 00 caps each charged with not m~re than 5 mg explosive; or not more tan 50 caps each charged with not more than 7.5. mg explosive. Not more than 12 of these boxes shall be made up in paper into a roll and not more than 12 of these rolls shall be wrapped in packing paper to form a packet. Strips (strings) of 50 caps, each cap being charged with not more than 5 mg explosive, may be packed in the following manner 5 strips (strings) per box, in fibreboard boxes wrapped 6 together in paper equivalent in strength to Kraftspaper of a minimum weigth of 40 mg/m2; 12 small packets so made up shall be wrapped together in paper of the same quality to form a large packet; • (i) articles of 16°: secured by cushioning materials, not more than 50 per box, in fibreboard boxes. The corks shall be glued to the bottom of the boxes or fixed in position there by some equivalent method. Each box shall be wrapped in paper and not more than 10 of these boxes shall be wrapped in packing paper to form a package; (k) articles of 17°: not more than 5 per box, in fibrebo­ ard boxes. Not more than 200 boxes, arranged in rolls, shall be placed together in a collective fibreboard box; (l) articles of I 8°: secured by cushioning materials, not 2178 2179 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2179 more than 10 per box, in fibreboard boxes. Not more . than 100 boxes, arranged·in rolls, shall be wrapped in paper to form a packet; (m) articles of 19°: secured by cushioning materials, not more than 15 per box, in fibreboard boxes. Not more than 144 boxes, arranged in rolls, shall be packed in a ' second fibreboard box; (n) articles of 200 (a) secured by cushibning materials, not more than 144 per case, in fibreboard cases; ' (o) articles of 20° (b): not more than 75 per box, in fibreboard boxes not more than 72 boxes shall be wrapped in fibreboard to form a packet; (p) articles of 21 °: in fibreboard boxes or in stout paper. If the ignition point of the articles is not covered by a protective cap each article must first be wrapped separa­ tely in paper. The propellent charge of bombs weighing more than 5 kg shall be protected by a paper case covering the lower part of bomb; • (q) articles of 22°: in fibreboard boxes or in stout paper. However large fireworks need not have an inner packaging if their igniting point is covered by a protective cap; (r) articles of 23 °: secured by cushioning materials in boxes made wood or fibreboard. The ignition heads shall be protected by a protective cap; Class le in the case of llrlicles of 17°, to 50 outer fibreboard bo xes; in the case of.articles of 18°, to 25 packets; in the case of articles of 20• (a), to 50 fibre-board cases; in the case of articles of 200(b ), to 50 packets, each of 72 fibreboard 'boxes; and • • in the case of articles of 21°, to a number of articles such that the weight of their total charge does not exceed 56 kg; (c) p~ckaging containing magnesium • flash-powders (26°), either in conformity with (b) above, or in wooden packing cases each weighing not more than 5 kg, or, in the case of packagings in. the form of paper bags, in strong fibreboard cases each weighing not more than 5 kg. (3) Wooden cases containing articles °with an explosive charge with a p~osphorus and chlorate base must be clo­ sed by means of screws. (4) A package containing articles of 9°, 11 °, 12°, 15° 22• or 24° - 26° must not weigh more than 100 kg; it must not weigh more than 50 kg if it contains articles of 23° or more than 35 kg if the sides of the case are only 11 mm thick and the case is encircled. with an iron band. 2180 (s) articles of 24°: in fibreboard boxes ·or in stout paper; 2179 (l) Substances of articles of 27° shall be packed in wooden cases lined with packing.paper, oiled paper or corrugated fibreboard. No lining is necessary if tliese substances and articles are wrapped in paper or fibrebo­ ard. (t) articles of 25°: in fibreboard boxes or in stout paper. However, large fireworks need not have an inner packa ging if their ignition point is covered by a protective cap; (u) articles of 26°: in fibreboard boxes. A box ·must not contain more than 3 glass tubes. (2) The inner packagings mentioned under (1) shall be placed: (a) packagings containing articles of 100, 13° and"l4°, in wooden packing cases; (b) packagings containing substances or articles !)f 9°, 11 °, 12° and 15° - 26°, in wooden packing cases with well­ jointed sides not less than 18 mm thick, lined with stout paper or thin zinc or aluminium sheet. A side thickness of 11 • mm is sufficient for a package weighing not more than 35 kg if the case is encircled with an iron band. The contents of a packing case are to be limited as fol­ lows: Special conditions: Class le (2) A package must not weigh more than 100 kg. (3) Smoke-producing cartridges for use as pesticides may, if wrapped in paper or fibreboard, likewise be pac­ ked: (a) in corrugated-fibreboard boxes or in strong fibreboard cases; such a package must not weigh more than 20 kg; or (b) in ordinary-fibreboard cases; such a package must not weigh more than 5 kg. Mixed packing . (1) Substances and articles grouped under:.ili~ same item number may be included in the same package. The inner packagings shall conform to· what is laid down for Class le 2180 2181 Maximunt quantity . Description • Special ~ Special ltepi No. of substance per per provisions receptacle package l• Matches 5 kg 5 kg Must not be packed together with substances of Classes 3 4 1 and 4 2. 2° arid 3° Strips of amorces Mixed packing not and slow-combustion allowd fuses 40 Pyroxylin thread 1.500 m of pyroxylin thread ~· - 8· All articles: Mixed packing not ollnu,...l 9° - 20° All articles Mixed packing allowed only with small wares or non py rotechnic toys, from which they must be kept separate. The collective case must meet the requirements laid bown for those articles contained therien in respect of which mariginal 21 79 (2) and· (3) imposes the most . - stringent conditions . - 21° - 25° All articles Mixed packing allowed only with one another. The col~ • lective case must meet the requirements laid down for those articles contained therein in respect of which mar ginal 2179 (2) and (3) imposes the most stringent con ditions; 26° and 27° All articles and Mixed packing not substances allowed ' ·' ~-·· 2180 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) each dangerous substance, and the outer packaging shall be that laid down for the dangerous substances of the item number in question. In this connexion a fibreboard case ·containing articles of 20° (a) shall be deemed equivalent to· a packet containing articles of 20° (b). • (2) If smaller quantities are not prescribed in the section entitled «Packing of a single substance or of articles of the same kind dangerous substances of this Class, in qua­ ntities not exceeding 6 kg for all of the dangerous substan­ ces listed under the same item number or the same letter, may be enclosed in the same package either with dange­ rous substances of another item number or of another letter· of the same class or with dangerous substances belonging to other Classes (if mixed packing is likewise permitted in the case of such substances), or with other goods, subject to the following special conditions. The inner packagings must satisfy the general and spe­ cial conditions of packing. In addition, the general provi­ sions con~ained in marginals 2001(5) and 2002(?) and (7) must be observed. A package must not weigh more than 100 kg, or more than 50 kg if it contains articles of 23°. Class le 4. Marking and danger labels on packages (see Appen: dix A.9) . ( 1) Packages containing articles of Class 1 c, 16° or 21 ° to 23°, shall bear a label conforming to model No.I.. (2) Packages containing fragile receptacles not visible from tht! outside shall bear a label conforming to model No. 9. B. Particulars in the transport document (1) The description of the goods in the transport doc­ ument must conform to one of the names underlined in marginal 2171; it must be underlined in red and follwed by particulars of the Cla,ss, th,!i item number (together with the letter, if any), and the initials «ADR», or «RID» re.g. le, 1 °(a) «ADR»] The wotding «Fireworus of ADR, le, item number ...... », with particulars of the item numbers under with the substances or articles to be carried are listed, is also allowed in the transport document. (2) In the case of substances or articles of 2°, 4°, 5°, 8°, 9°, 11 °, 12° and 15° - 27°, the following must be certified in the transport document: «The nature of the goods, and the packaging, are in conformity with the provi­ sions of ADR». C. Empty packagings No provisions. CLASS 2. . . GASES: COMPRESSED, LIQUEFIED OR DISSOLVED UNDER PRESSURE 1. List of substances (1) Among the substances and articles covered by the heading of Class 2, only those listed in marginal 2201 are to be accepted for carriage, and then only subject to the requirements of this Annex and to the provisions of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. (2) Substances havitrg a critical temperature lower than 50°C or, at 50°C, a vapour pressure greater than 3 kg/cm2 are deemed to be substances of Class 2. (3) The substances and articles of Class 2 are ~lassified as follows, A: Compressed gases having a critical temperature be­ low -10°C; 2182 2183 2184 2185 2189 2190 2191 2199 2200 B: Liquefied gases having a critical temperature of 10 ° C or above: (a) Liquefied gases having a critical temperature of 70°C or above: (a) Liquefied gases having a critical temperature of 70°C or above; (b) Liquefied gases having a critical temperature of l0°C or above, put below 70°C; C: Deeply-refrigerated liquefied gases; D: Gases dissolved under pressure; E: Aerosol dispensers and non-refillable containers of gas under pressure; F: Gases subject to special requirements; and G: Empty receptacles and empty tanks. The substances and articles of Class 2 are subdivided according to their chemical properties, as follows: (1'1) non-inflammable; (a t) non-inflammable, toxic; (b) inflammable; (b t) inflammable, toxic; (c) chemically unstable; ( c • t) chemically unstable, toxic. Unl·ess otherwise specified, chemically unstable substances shall be considered to be inflammable. Class 2 The names of corrosive gases and of articles containing 2200 such gases shall be followed by the word «corrosive» in brackets. (4) Substances of Class 2 which are listed. among the • chemically unstable gases are to be accepted for carriage only if the necessary steps have been taken to prevent their dangerous decomposition, dismutation or polymeri­ zation during carriage. To this end, care should in particular be taken to ensure that receptacles and tanks do not contain any substances liable to promote these rea.ctions. A. Compressed gases [see ah,o marginal 2201a under 2201 (a). For gases of 1 ° and (b) and 2° (a) in aerosol dispensers or in non-refillable containers for gases under pressure, see under 10° and 11 °]: Gases having a critical temperature below -I0°C are considered to be compressed gases for the purposes of ADR. 1 ° Pure gases and technically-pure gases (a) Non-inflammable Argon; helium; krypton; neon; nitrogen; oxygen; tetraf­ luoromethane (R 14). (a t) Non-inflammable, toxic Boron trifluoride; fluorine (coriosive); silicon tetrafluo ride (corrosive). (b) Inflammable Deuterium; hydrogen; methane. (b t) Inflammable, toxic. Carbon monoxide . (c t) Chemically unstable, toxic Nitric oxide (nitrogen monixide) NO (non-inflam- • mable). 2o Mixtures of gases (a) Non-inflammable Mixtures of two or more of the following gases: rare gases (containing not more than 10 per cent xenon by volume), nitrogen oxygen, carbon dioxide (not more than 30 per cent by volume); non-inflammable mixtures of two or more of the following gases hydrogen, methane, nitro­ gen, rare gases (containing not more thatf 10 per cent xenon by volume), not more than 30 per cent carbon dioxide by volume; nitrogen containing not more than 6 per cent ethylene by volume; air. (b) Inflammable Mixtures of not less than 90 per cent methane by volume with hydrocarbons of 3° (b) and 5° (b); inflam­ mable mixtures of two of the following gases: hydrogen, EQ>HMEPlr THr KYBEPNHrEdt (TEYXOr nPQTO) 2181 methane, nitrogen, rare gases (containing not more than 10 per cent xenon by volume), not more than 30 per cent carbon dioxide by volume; natural gas. • (b t) Inflammable, toxic Town gas; mixtures of hydrogen with not more than 10 per cent hydrogen selenide or phosphine or silane or germane by volume or with not more th an 15 per cent arsine by volume; mixtures of nitrogen or rare gases (co­ ntaining not more than 10 per cent xenon by volume) with not more than 10 per cent hydrogen selenide or phosphine or silane or germane by volume·or with not more than 15 per cent arsine by volume; water gas; synthesis gas (e.g. from the Fischer-Tropsch process); mixtures of carbon monoxide with hydrogi;n or with methane. (c t) Chemically unstable, toxic Mixtures of hydrogen with not more than 10 per cent diborane by volume; mixtures of nitrogen or rare· gases ( containing not more than 10 per cent· xenon by volume) with not more than 10 per cent diborane by volume. Liquefied gases [see also marginal 2201a under (b) and (e). For gases of 5° to 6° in aerosol dispensers or in non-refillable containers for gases under pressure, see under 10° and 11 °): Gases having a critical temperature of -l0°C or above are considered to be liquefied gases for the purposes of ADR .. ·(a) Liquefied gases having a critical temperature of 70°C or above: Pure gases and technically-pure gases (a) Non-inflammable Bromochlorodifluoromethane (R 12 81); chlorodifluo­ romethane (R 22); chloropentafluoroethane (R 115 ); l-chloro-2,2,2-trifluoroethane (R 133a) dichlorodifluoro­ methane (R 12); dichlorofluoromethane (R 21); 1,2 dichloro-1, 1,2,2-tetrafluoroethane .(R 114 ); octofluoro­ cyclobutane (RC 318). (a t) Non-inflammable, toxic .Ammonia: boron chloride (corrosive); chlorine (corro­ sive); chlorine trifluoride (corrosive); hexafluoropropylene (R 216); hydrogen bromide (corrosive); methyl bromide; nitrosyl chloride (corrosive); nitrogen dioxide No~ (nitro~ gen peroxide, nitrogen tetroxide N20J (corrosiveJ; phos­ gene (corrosive); sulphur dioxide; sulphuryl fluoride; tungsten hexafluoride. (b) Inflammable Butane; 1-butylene (I-butene); l-chloro-1, 1-difluoro­ ethane (R 142b); cis-2-butylene (cis-2-butene); cyclopro­ pane; 1,1-difluoroethane (R 152a); isobutane, isobuty­ lene; methylsilane; propane; propylene; trans-2-butylene (trans-2-butene ); 1, 1 1-trifluoroethane. Class 2 (b t) Inflammable, toxic Arsine; dichlorosilane; dimethylamine; dimethyl ether; dimethylsilane; ethylamine; ethyl chloride; hydrogen sele­ nide; hydrogen sulphide; methylamine; methyl chloride; •·methyl mercaptan trimethylamine; trimethylsilane. (c) Chemically unstable 1,3-butadiene; vinyl chloride. (c t) Chemically unstable, toxic Cyanogen; cyanogen chloride (non-inflammable) (cor­ rosive); ethylene oxide; methyl vinyl ether; trifluorochloro­ ethylene (R 1113); vinyl bromide. Note: in the case of halogenated hydrocardons, the use of names customary in the trade, such as the following, is also permitted: Algofrene, Arcton Edifren, Flugene, Forane, Freon, Fresane, Frigen, Isceon, Kaltron, followed by the substance identification number without the letter R. 4° Mixtures of gases (a) Non-inflammable Mixtures of substances listd under 3° (a) with or without hexafluoropropylene of 3° (a t), which as: .mixture F 1 have a vapour pressure at 70°C not excee­ ding 13 Kg/cm2 and a density at 50°C not lower than that of dichlorofluoromethane (1.3). mixture F 2 have a v~pour pressure at 70°C not excee­ ding 19 Kg/cm2 and a density at 50°C not lower than that of dichlorofluoromethane. mixture F 3 have a vapour pressure at 70°C not excee­ ding 30 Kg/cm2 and a density at 50°C not lower than that of dichlorofluoromethane (1.09). Note: 1. Trichloroflu~romethane (R 11), trichlorotrif­ luoroethane (Rll3 and chlorotrifluoroethane (Rl33 are not liquefied gases within the meaning of ADR and thus are not subject. to the requirements of ADR. They may however enter into the composition of mixtures Fl to F3. 2. See Note under 3°. The azeotropic mixture of dichlorodifluoromethane (R 12) and 1,1-difluoroethane (R 152a), known as R500; The azeotropic mixture of chloropentafluoroethane (R 115) and chlorodifluoromethane (R 22), known as R 502; The mixture of 19 to 21 per cent by weight dichlorodif­ luoromethane (R 12) and 79 to 81 per cent by weight bromochlorodifluoromethane (R 12 81). Class 2 (at) Non-inflammable, toxic 2201 Mixtures of methyl bromide and chloropicrin having a vapour pressure above 3 kg/cm2 at 50°C. (b) Inflammable Mixture of hydrocarbons listed under 3° (b) and of ethane and ethylene of 5° (b), which as: mixture A have a vapour pressure at·70°C not excee­ ding 11 kg/cm2 and a density at 50°C not lower than 0.525; mixture AO have a vapour pressure at 70°C not excee­ ding 16 kg/ cm2 and a density at 50 ° C not lower than 0.495; • mixture A 1 have a vapour pressure at 70°C not excee­ ding 21 kg/cm2 and a density at ·5D .. °C,tnot lower than 0.485; mixture B have a vapour pressure at 70°C not excee­ ding 26 kg/c:m2 and a density at 50°C not lower than 0.450; mixture C have a vapour pressure at 70°C not excee­ ding 31 kg/ cm2 and a density at 50 ° C not lower than 0.440. Note: In the case of the foregoing mixtures the use of . the following names customary in the trade is permitted for describing these substances: Name given under 4°(b) Mixture A, mixture A 0 Mixture C Name customary· in the trade butane propane Mixtures of hydrocarbons of 3° (b) and 5° (b) containing methane. (b t) Inflammable, toxic Mixtures of two or more of the following gases: methyl­ silane, dimethylsilane, trimethylsilane; methyl chloride and methylene chloride in mixtures having a vapour press­ ure above 3 kg/cm2 at 50°C; mixtures of methyl chloride and chloropicrin and mixtures of methyl bromide and • ethylene bromide having in either case a vapour pressure above 3 kg/cm2 at 50°C. (c) Chemically unstable Mixtures of methylacetylene and propadiene with the hydrocarbons of 3° (b), which as: mixture P 1 contain not more than 63 per cent methyla­ cetylene and propadiene by volume and not more than 24 per cent propane and propylene by volume, the perce­ ntage of C4-saturated hydrocarbons being not less than 14 per cent by volume; and as mixture P2· contain not E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO). more than 48 per cent methylacetylene and propadiene by volume and not more than 50 per cent propane and propylene by v9lume, the percentage fo C 4 saturated hyd­ rocarbons being not less than 5 per cent by volume4• (c t) Chemically unstable, toxic Ethylene oxide containing not more than 10 per cent carbon dioxide weight; ethylene oxide containing not more than 50 per cent methylene formate by weight, with nitro­ gen up lo a total pressure not exceeded 10 kg/cm2 at 50°C ethylene oxide with nitrogenupto a total preesure of 1 0kg/ cm2 at 50 ° C dichlorodifluoromethane containing 12 per.cent ethylene oxide by deight. (b) Liquefied gases having a critical temperature of l0°C or above, below 70°C: 5° Pure gases and technically-pure gases (a) Non-inflammable Bromotrifluoromethane (R 13 B l); carbon dioxide;­ chlorotrifluoromethane (R 13); hexafluoroethane (R 116); nitrous oxide N 2 0; sulphur hexafluoride; trifluorome­ thane (R 23) xenon. With regard to carbon dioxide, see also marginal 2201a under (c). Note: 1. Nitrous oxide is to be accepted for carriage only if it is less than 99 per cent pure. .2. See Note under' 3°. • (a t) Non-inflammable, toxic Hydrogen chloride (corrosive). (b) Inflammable Ethane; ethylene; silane. (b t) Inflammable, toxic Germane; phosphine. (c) Chemically unstable· 1, 1-difluoroethylene; vinyl fluoride. (c t) Chemically unstable, toxic Diborane. 6° Mixtures of gases (a) Non-inflammable Class 2 Carbon dioxide containing not less than 1 per cent and not more than 10 per cent nitrogen, oxygen, air or rare gases by weight; the azeotropic mixture of chlorotrifluo­ rome thane (R 13) and trifluoromethane (R 23) known as R 503. Note: Carbon dioxide containing less than 1 per cent nitrogen, oxygen, air-or rare gases by weight is a substance of 5°(a). (c) Chemically unstable Carbon dioxide containing not more than 35 per cent ethylene oxide by weight. (c t) Chemically unstable, toxic Ethylene oxide containing more than 10 per cent but not more than 50 per cent carbon dioxide by weight. C. Deeply - refrigerated liquefied gases 7 o Pure gases and technically - pure gases (a) Non-inflammable Argon; carbon dioxide; helium; krypton; neon; nitro­ gen; nitrous oxide N 2 0; oxygen; xenon. (b) Inflammable Ethane; ethylene; hydrogen; methane. 8° Mixtures of gases (a) Non-inflammable Air; mixtures of substances of 7°(a) (b) Inflammable Mixtures of substances of 7°(b); natural gas. D. Gases dissolved under pressure 9o Pure gases and technically - pure gases (a t) Non-inflammable, toxic Ammonia dissolved in water with more than 35 per cent but not more than 40 per cent ammonia by weight; ammonia dissolved in water with more than 40 per cent but not more than 50 per cent ammonia by weight. Note: Ammonia solution with an ammonia content not exceeding 35 per cent by weight is not subject to the requirements of ADR. Class 2 (c) Chemically unestable . 2201 Acetylene dissolved in a solvent (e.g. acetone) absorbed by porous substances. E. Aerosol dispensers and non-refillable containers of gas under pressure (see also marginal 2201a under (d)]: Note: 1. Aerosol dispensers are receptacles which can be used only once are equipped with a release valve or dis­ persal device, and contain, under pressure, a gas or mixt­ ure of gases listed in marginal 2208 (2) or contain an active substance (insecticide, cosmetic, etc.) together with . such a gas or mixture of gases as a propellant. 2. Non-refillable containers of gas under pressure are receptacles which can be used only once and contain a gas or a mixture of gases listed in marginal 2208 (2) and (3) (e.g. butane for camp-cookers, refrigerant gases; etc), but are not equipped with a release valve. 3. The term •inflammable substances» means: (i) gases (propellant in aerosol dispensers; contents of non-refillable containers of gas under pressure) whose mixtures with air can be ignited and have a lower and an upper inflammability limit! (ii) liquids (active substances in aerosol dispensers) of Class 3. 4. The term •chemically unstable» is applied to contents which the absence of special precautions undergo dange­ rous decomposition or self-polymerization at a temperat­ ure of not more than 70°C. 1 0o Aerosol dispensers (a) Non-inflammable With non-inflammable contents. (a t) Non-inflammable, toxic With non-inflammable to"xic contents. (b) Inflammable 2201 1. With not more. than 45 per cent of inflammable contents by weight 2. With more than 45 per cent of inflammable contents by weight (b t) Inflammable, toxic 1. With toxic contents and not more than 45 per cent of inflammable contents by weight. 2. With toxic contents and more than 45 per cent of inflammale contents by weight. Class 2 (c) Chemically unstable 2201 With chemically-unstable contents. (c t) Chemically unstable, toxic With chemically - unstable toxic contents. 11 • Non-refillable containers of gas under pressure (a) Non-inflammable With non-inflammable contents. (a t) Non-inflammable, toxic With non-inflammable toxic contents. (b) Inflammable With inflammable contents. (b t) Inflammable, toxic With inflammable toxic contents. (c) Chemically unstable With chemically-unstable contents. (c t) Chemically unstable, toxic With chemically-unstable toxic contents. F. Gases subject to special requirements 12° Various mixtures of gases Mixtures containing gases listed under· other item numbers of this Class, and mixtures of one or more gases listed under other item numbers of this Class with one· or more varpours of substances not excluded from carriage under ADR, on condition that during carriage: 1. the mixture remains entirely gaseous; and 2. all possibility of a dangerous reaction is excluded. ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2183 13° Test gases . Gases and mixtures of gases not listed under other item numbers of this Class and used only in laboratory tests, on condition that during carriage: (a) the gas or mixture of gases remains entirely,gaseous; and • • (b) all possibility of a dangerous reaction is excluded. G. Empty receptacles and empty tanks 2201 14° Empty receptacles and empty tanks, uncleaned, which have contained tetrafluoromenthane of 1 °(a), substances of 1 °, (a t) - (c t); 2°, (b) - (c t); 3° - 6°; carbon dioxide and nitrous oxide of 7°(a); or substances of 7°(b), 8°(b), 9°, 12° or 13°. • Note: 1. Receptacles and tanks which after being emptied of substances listed under 14 ° still contain small residual amounts are regarded as empty receptacles or empty tanks, uncleaned. 2. Empty receptacles or empty tanks, uncleaned, which have contained gases of 1 °(a) other than tetrafluorome­ thane (R 14), ~r gases 2°(a), 7°(a) other than carbon dioxide and nitrouw oxide, or 8°(a) are not subject lo the requirements of ADR. Gases and articles handed over for carriage in conformity 2201a whith the following provisions are not subject to the requi rements or provisions relating to this Class set out else where· in this Annex or in Annex B: (a) compressed gases which are neither inflammable not toxic nor corrosives and whose pressure in the recep­ tacle, referred to a temperature of 15 ° C, does not exceed 2 kg/cm2 ; the same'rule applies to mixtures of gases co­ ntaining not more than 2 per cent inflammable compo­ nents; (b) liquefied gases contained, in quansities not excee­ ding 60 1, or in quantities of less than 5 1 with not more than 25g hydrogen, in freering appliances (refrigerators, ice machines, etc.) and necessary for their operation; (c) carbon dioxide [5°(a)] in metal capsules (sodors, sparklets) if the carbon dioxide in the gaseous state does not contain more than 0.5 per cent air and the capsules co­ ntain not more thari 25g carbon dioxide and not more than 0.75 g per cm3 of capacity; ( d) articles of 10 ° and 11 ° of a capacity not exceeding 50 cm3• A package of such articles shall not weigh more than 10 kg; (e) liquefied petroleum gases contained in motor­ vehicle tanks firmly secured to the vehicles; the fuel cock between tank and engine must de closed and the electrical contact open. 2. Provisions A. Packages 1. General conditions of packing (1) The materials of which the receptacles and their 2202 closures are made must not be liable lo attack by the co ntents or form harmful or dangerous compounds therwith. Note: Care must be taken not to allow any moisture lo enter receptacles when they are being filled, and to dry receptacles completely after hydraulic pressure tests (see marginal 2216 carried out with water or with aqueous sol utions. (2) Packagings, including their closures, shall be suffi­ ciently rigid and strong in all their parts l~ prevent any loosening during carriage and to meet the n'ormal require­ ments of carriage. When outer packagings are prescribed, the receptacles shall be firmly secured therein. Unless otherwise specified in the section entitled •Packing of a single substance or of articles of the same kind», inner packagings may be enclosed in outer packagings, either singly or in groups. . (3) Metal receptacles intended for the carriage of gases of 1 ° to 6° and 9° shall contain only the gas for which they have been tested and whose name is inscribed on the receptacle [see marginal 2218 (a)]. Derogations are allowed 1. for metal receptacles tested for one of the substances of 3°(a) or 4°(a) or for bromotrifluomethane, chlorotrifluo­ romethane or trifluoromethane of 5° (a). These receptacles may also be filled with some other substance of the afore~ said items on condition that the minimum test pressure prescribed for that substance does not exceed the test pressure of the • receptacle and that the • name of the substance and its permissible maximum filling weight are inscribed on the receptacle; 2. for metal receptacles tested for hydrocarbons of3°(b) or 4°(b). These receptacles may also be filled with some other hydrocarbon on condition that the minimum test pressure prescribed for that substance does not· exceed the test pressure of the receptacle and that the name of the substance and its permissible maximum filling weight are inscribed on the receptacle. For 1 and 2, see also marginals 2215, 2218 (l)(a) and 2220, (1) to (3). ( 4) A change in the use to which a receptacle is assigned is allowed in principle if it does not conflict with national regulations; it requires however the approval of the com­ petent authority and replacement of the former markings by markings relating lo the new use. 2. Packing of a single substance or of articles of the same kind . Note: Carbon dioxide and nitrous oxide [7°(a)] and mixt­ ures of these two gases [8°(a)] may not be carried other­ wise than in specially-equipped tanks (see.Annex B, mar­ ginal 21400). a. Nature o(receptacles (1) Receptacles intended for the carriage of gases of 2203 1 ° to 6°, 9°, 12° and 13° shall be so closed and leak-proof as to prevent any escape of the gases. • (2) These receptacles shall be made of carbon steel or of alloy steel (special steels). The following may however be used: (a) copper receptacles for: 1. compressed gases ·of 1 °, (a), (b) and (b t), and 2o, (a) and (b), whose filling pressure referred lo a temperature of 15 ° C does not exceed 20 kg/ cm2 ; and 2. liquefied gases of 3°(a); sulphur dioxide of 3o(a t); dimethyl-ether, ethyl chloride and methyl chloride of 3°(b) vinyl chloride of 3°(c); vinyl bromide of 3°(a t); mixtures • F 1, F 2 and F 3 of 4°(a); and ethylene oxide containing not m ore than 10 per cent carbon dioxide by weight of 4 ° 0~ .• (b) aluminium - .alloy receptacles (see Appendix A.2) for: • 1. compressed gases of 1 °, (a), (b) and (b t); nitric oxide (nitrogen monoxide) NO of 1 °(c t); and compressed gases of 2 ° (a), (b) and (b t); 2. liquefied gass of 3° (a); sulphur dioxide of 3°(a t); liquefied gases of 3°(b) other than methylsilane; dimethyl ether, hydrogen selenide, and methyl mercaptan of 3°(b t); ethylene oxide of 3°(c t); liquefied gases of 4°, (a) and • (b) ethylene oxide containing not more than 10 per cent carbon dioxide by weight,. of 4°( c t); and liquefied gases of 5°, (a) and (b), and 6° (a) and (c). Sulphur dioxide of 3°(a t) and substances of 3°(a) and 4°(a) shall be dry; and 3. dissolved acetylen of 9°(c). All gases which are to be ~arried in aluminium-alloy recepta<;les must be free from alkaline impurities. (1) Receptacles for dissolved acetylene [9°(c)] shall be 2204 entirelly filled with a porous material, uniformly distrib uted, of a type approved by the competent authtority and which • (a) does not attack the receptacles on form harmful or . dangerous compounds either with acetylene· or with the solvent; (b) does not sh~ke down, even after prolonged us.e or through jolting temperatures up to 60~ C; (c) is capable of preventing the spread of decomposition of the acetyleni; in the mass. (2) The solvent must not attack the receptacles. (1) The following liquefied gases may, in addition, be 2184 ECJ>HMEPl2: THr KYBEPNH2:EQ2: (TEYXOr nPQTO) carried- in thick-walled glass tubes on condition that the quantity of substance each tube and the degree of filling of the tubes do not exceed the indicated below: Names of gases Quantity of substance Carbon dioxide, nitrous oxide N20[ 5°(a)], 3g ethane, ethylene [5°(b)) Ammonia, chlorine, methyl bromide (3°(a t)), 20 g cyclopropane (3 °(b)), ethyl chloride [3°(b t)] Phosgene, sulphur dioxide 100 g [3°(a t) Degree filling of tube one falt of capacity two-thirds of capacity three-quarters of capacity (2) The glass tubes shall be flame-sealed and secured separately by infusorial - earth cushioning in closed sheet metal capsules which shall be placed in a wooden case or in some other outer packaging of sufficient strength (see also marginal 2222). (3) For sulphur dioxide of 3°(a t) stout glass siphons containing not more than 1.5 kg of substance and filled to not more than 88 per cent of their capacity are also allowed. The siphons shall be secured by infusorial earth, sawdust or powdered carbonate of lime, or b)I a mixture of the two latter, in strong wooden cases or in some other outer packaging of sufficient strenght. A package shall not weigh more than 100 kg. If it weighs more than 30 kg it shall be fitted with, means of handling. (1) Gases of 3°(a); 3°(b) other than methylsilane; 3o(b ?!06 t) other than arsine, dichlorosilane, dimethylsilane, hydro­ gen selenide and trimethylsilane; 3°(c); 3°(c t) other than cyanogen chloride; and mixtures of 4°(a) and 4°(b), may also, on condition that the weight of liquid per litre of capacity does not exceed either the maximum weight of contents indicated in marginal 2220 or 150 g per tube, be contained in thick-walled glass tubes, or in thick-walled metal tubes made of a metal allowed by marginal 2203 (2). The tubes shall be free from faults liable to impair their strength; in particular, internal stresses in glass tubes shall have been suitably relieved and the thickness of the tube walls shall not be less than 2 mm. The leakproofness of the closure system shall be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preve­ nting any loosening of the closure system during carriage. The tubes shall be secured by cushioning material in small boxes made of wood or fibreboard, the number of tubes per box being such that the weight of the liquid contained in a box does not exceed 600 g. These small boxes shall be placed in wooden cases or in some other outer packa­ ging of sufficient strenght; if the liquid contents of a case weigh more than 5 kg the case shall be lined with soft­ soldered sheet-metal. (2) A package shall not weigh more than 75 kg. (1) Gases of 7°(a) other than carbon dioxide and nitrous oxide, and of 8°(a) other than mixtures containing carbon dioxide and nitrous oxide, shall be enclosed in closed, double - walled metal receptacles which are so insulated that they cannot become coated with dew or hoar-frost and which are fitted with safety valves. (2) Gases of 7°(a) other than carbon dioxide and nitrous oxide, and of 8°(a) other than mixtures containing carbon dioxide and nitrous oxide, may also be enclosed in recep­ tacles which are not hermetically closed and which are: (a) double - walled vacuum-jacketed glass receptacles 2207 surrounded by an absorbent insulating material; these receptacles shall be protected by iron-wire baskets and placed in metal cases; or (b) metal receptacles protected against heat transmis­ sion in such a way that they cannot become coated with dew or hoar-frost; the capacity of these receptacles shall not exceed 100 litres. (3) The metal cases referred to in subparagraph (2)(a) and the receptacles referred to in subparagraph (2)(b) above shall be fitted with means of handling. The openings of the receptacles referred to in subparagraphs (2)(a) anp (b) shall be fitted with devices allowing gases to escape, preventing any splashing out of the liquid, and so fixed that they cannot fall aut. In the case of oxygen of 7°(a) and mixtures containing oxygen of 8°(a), the devices refer­ red to above and the absorbent insulating material surrou­ nding the receptacles referred to in subparagraph (2)(a) shall be made of incombustible materials. (1) Aerosol dispensers (10°) and non-refillable contai­ ners for gas under pressure (11 °) shall satisfy the following requirements: (a) aerosol dispensers containing only a gas or a mixture of gases, and non-refillable containers for gas under press­ ure, shall be made of metal. This requirement shall not apply to non-refillable containers for gas under pressure with a maximum capacity of 100 ml for butane. Other aerosol dispensers shall be made of metal, a plastics mate­ rial glass. Receptacles made of metl'!I and having an ou­ tside diameter of less than 40 mm shall have a concave bottom; (b) receptacles made of materials liable to shatter, such as glass or certain plastics materials, shall be enclosed in a device ( close - wire netting, flexible cover made of a plastics material, etc.) and affording protection against fragments and their dispersal. Receptacles whose capacity does not exceed 150 cm3 and whose internal pressure 20°C is below 1.5 kg/cm2 are exempted from this requi­ rement; (c) the capacity of receptacles made of metal shall not exceed 1,000 cm3 and that of receptacles made of a plastics material or of glass shall not exceed 500 cm3; ( d) each model of receptacle shall, before being put into service, say a hydraulic pressure test carried out in conformity with Appendix marginal 3291. The iriternal pressure to be applied (test pressure shall be 1.5 times the internal pressure at 50°C, with a minimum of 10 kg/cm2; (e) the release valves of aerosol dispensers, and their· dispersal devises shall ensure that the dispensers -are so closed as to be leak-proof shall be protected against acci­ dental opening. Valves and dispersal devices which close only by the action of the internal pressure are to be accep­ ted. (2) The following gases shall be accepted as propel­ lants, or as constituents of propellants, or as filler gases, for aerosol dispenser gases of 1 °(a) and (b); 2°(a) and (b); 3o, (a) and (b) other than methylsilane; ethyl chloride and dimethyl ether of 3°(b t); 1,3-butadiene of 3°(c); trifluoro- • chloroethylene of 3°(c t); gases of 4°, (a) and (b); gases of 5°, (a) and (b) other than silane; gases of 5°(c) and 6°(a) and (c). (3) All the gases listed under (2) and, in addition, the following gases shall be accepted as filling gases for non­ refillable containers for gas under pressure; methyl bro­ mide of 3 °(at); dimethylamine, ethylamine, methylamine, methyl mercaptan and trimethylamine of 3°(b t); ethylene oxide, methyl vinyl ether and vinyl bromide of 3°(c t); ethylene oxide containing not more than I O per cent car­ bon dioxide by weight, of 4°(c t). ( 1) The internal pressure at 50 ° C of aerosol dispensers and of non-refillale containers of gas under pressure shall exceed neither two-thirds of the test pressure of the recep­ tacle nor 12 kg/cm2; (2) Aerosol dispensers and non refillable containers of gas under pressure shall be so filled that at 50 ° C the liquid phase does not exceed 95 per cent of their capacity. The capacity of aerosol dispensers is the available volume in a closed dispenser fitted with the valve support, the valve and the dip tube. • 2208 2209 ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) 2185 (3) All aerosol dispensers and non-refillable containers for gas under pressure shall satisfy a tightness (leakproof­ ness) tests in conformity with Appanedix A.2, marginal 3292. (1) Aerosol dispensers and non-refillable containers of gas under pressure shall be placed in wooden cases or strong fibreboard or metal boxes; aerosol dispensers made of glass or a plastics material and liable to shatter shall be separated from one another by interposed sheets of fibreboard or of another suitable material. (2) A package shall. not weigh more than 50 kg if fibreboard boxes are used or more than 75 kg if other packagings are used.· (3) Where carriage is by fyll load, eash load comprising only aerosol· dispensers made of metal, the disJ>ensers may de grouped together and secured on tra1s with the . aid of an appropriate plastics material by means of a shrin­ kage and heat-sealing process, on condition that the groups of dispensers are then stacked and suitably sec ured on pallets. • b. Conditions governing metal receptacles (These conditions are not applicable to the metal tubes referred to in marginal 2206, to the receptacles referred to in marginal 2207 (2)(b), or to the aerosol dispensers or non-refillable metal containers for gas under pressure referred to in marginal 2208). 1. Construction and fittings (see also marginal 2238). (1) At the test pressure, the stress in the metal at the most severely stressed point of the receptacle (marginals 2215, 2219 and 2220) shall not exceed three-quarters of the guaranteed minimum yield stress (Re). By «yield stress» is meant the stress at which a permanent elongation of 2%o (i.e. 0.2 per cent) or, for austenitic steels, 1 per cent of the gauge lenght on the test-piece, has been prod­ uced. Note: In the case of sheet-metal the axis of the tensile test-piece shall be at right angles to the direction of rolling. The permanent elongation at fracture (1 = 5 d) shall be measured on a test-piece of circular cross - section in which the gauge length 1 is equal to five times, the diame­ ter d; if test-pieces of rectangular cross-section are used, the gau~length shall be calculated by the formula 1 = 5,65 • VY where F indicates the initial cross-sectional area ot th~ test-piec;, . (2) (a) Steel receptacles whose test pressure exceeds 60 kg/ cm2 shall de of seamless construction or welded. For welded receptacles, steels, (carbon or alloy) of fully satis~ factory weldability shall be used. • (b) Receptacles whose test • pressure does not exceed 60 kg/cm2 shall either conform to the provisions of subpa­ ragraph (a) adove, or beriveted or hard-soldered on condi­ tion that the manufacturer guarantees the workmanship of the riveting and hard-soldering and that the competent au­ thorities of the country of origin have given their approval. (3) Aluminium - alloy receptacles shall be seamless or welded. (4) Welded receptacles are to be accepted only on condition that manufacturer guarantees the workmanship of the welding and that the competent authorities of the country of origin have given their approval. (1) A distinction is made between the following types of receptacles. (a) cylinders of a capacity not exceeding 150 litres; (b) receptacles of a capacity of not less than 100 litres (with the exception of cylinders in conformity with subpa­ ragraph (a)] and not more than, 1,000 litres (e.g. cylindri­ cal receptacles equipped with rolling hoops, and receptac­ les on skids); (c) tanks (see Annex B); . (d) assemblies, known as •frames», of cylinders in confor­ mity with subparagraph (l)(a), the cylinders being inter­ connected by a manifold and held firmly together by a metal fitting; ,. (2) (a) If under the regulations.of the country of depart­ ure the cylinders referred to in subparagraph (l)(a) are required to be fitted with device to prevent rolling, this 2210 2211 2212 device shall not be integral with the valve cap (marginal 2213 (2). • (b) Receptacles in conformity with subparagraph (l)(b) which are capable of being rolled shall be equipped with rolling hoops or b'e otherwise protected against damage due to rolling (e.g. by corrosion - resistant metal sprayed on to the receptacle' s outer surface). Receptacles in conformity with subparagraphs ( 1 )(b) and (l)(c) which are not capable of being rolled shall be fitted with devices (skids, rings straps) ensuring that they can be safely handled by mechanical means and so ar ranged as not to impair the strenght of, nor cause undue 2212 stresses :n, the wall of the receptacle. (c) Frames of cylinders in conformity with subparag­ raph (l)(d) shall be fitted with devices ensuring that they can be handled safely. The manifold and the master cock shall be situated within the frame and be so mounted as to be protected against any damage. (3) (a) With the ~xceptions· of gases of 7° and 8°, gases of Class 2 may be carried in cylinders in conformity with subparagraph (l)(a). Note: For possible limitations on the capacity of cylinders for certain gases, see marginal 2219. (b) With the exception of fluorine and silicon tetrafluo­ ride [1 °(a t)]; nitric oxide (NO) [lo(c t)]; mixtures of hydrogen with not more than 10 per cent hydrogen sele­ nide or phosphine or silane or germane by volume or with not more than 15 per cent arsine by volume; mixtures of nitrogen or rare gases ( containing not more than. 'l O ·per cent xenon by volume) with not more than 10 per cent • • hydrogen selenide or phosphine or silane or germane by volume or with not more than 15 per cent arsine by volume [2°(b t)]; mixtures of hydrogen with not more than • 10 per cent diborane by volume; mixtures of nitrogen or rare gases (containing not more than 10 per cent xenon. by volume) with not more than 10 per cent diborane by. volume [2°(c t)]; boron chloride, chlorine trifluoride, nitro- . syl chloride, sulphuryl fluoride and tungsten hexafluoride [3°(a t)]; methylsilane [3°(b)] arsine, dichlorosilane, dime­ thylsilane, hydrogen selenide and trimethylsilane [3°(b t)]; cyanogen chloride, cyanogen and ethylene oxide [3°(c t)]; mixtures of methylsilanes [4°(b t)]; substances of 4°(c) and 4o(c t) other than dichlorodifluoromethane containing 12 per cent ethylene oxide by weight; nitrous oxide [5°(a)]; • silane [5°(b)]; and substances of 5°(b t), 5°(c t), 7°, 8°, 12° and 13°, gases of Class 2 may be carried in receptac­ les in conformity with subparagraph (1) (b). (c) With the exception of silicon tetrafluoride [l 0(a t)]; nitric oxide [l 0 (c t)]; mixtures of hydrogen with not more thant 10 per cent hydrogen selenide or phosphine or silane or germane by. volume or with not more than 15 per cent arsine by volume; mixtures of nitrogen or rare gases (containing not more than 10 per cent xenon by volume) with not more than 10 per cent hydrogen selenide or phosphine or silane or germane by volume or with not more than 15 per cent arsine by volume [2°(b t)]; mixtures • of hydrogen with not more than 10 per cent diborane by volume; mixtures of nitrogen or rare gases (containing not more thl!,n 10 per cent xenon by volume) with not more than 10 per cent diborane by volume [2°(c t)]; boron chloride, chlorine trifluoride, nitrosyl chloride, sulphuryl fluoride and tungsten nexafluoride [3°(a t)); methylsilane [3°(b)]; arsine, dichlorosilane, dimethylsilane, hydrogen selenide and trimethylsilane [3°(b t)); cyanogen chloride, cyanogen and ethylene oxide [3°(c t)]; mixtures of methyl­ silanes [4°(b t)]; substances of 4°(c) and 4°(c t) other than dichlorodifluoromethane containing 12 per cent ethylene oxide by weight; nitrous oxide [S0 (a)]; silane [5°(b); and substances of 5°(b t), 5°(c t), 7°, 8°, 12° and .13°, gases of Class 2 may be carried in frames of cylinders in confor­ mity with subparagraph (l)(d). The individual cylinders in a frame of cylinders shall contain only one and the same compressed gas, liquefied gas or gas dissolved under 2212 pressure. Each cylinder in a frame of cylinders for fluorine [l 0 (a t)] or dissolved acetylene [9°(c)] shall however be fitted with a cock. The cylinders in a frame of cylinders 2186 E<J>HMEPII THI'. KYBEPNHIEQI (TEYXOI nPOTO) of acl'lylene shall all contain the same porous material (marginal 2201). (1) Openings for filling an d emptying receptacles shall be fitted with flap valves or needle-valves. Valves of other types may however be allowed if they present equivalent guarantees of safety and have been approved in the coun­ try of origin. Nevertheless, whatever the type of valve adopted, its system of attachment shall be strong and such that satisfactory condition can be verified easily before each filling. Apart from a manhole, which if provided shall he closed hy an effective closure, and from the necessary orifice for the removal of deposits, receptacles and tanks in confor­ mity with marginal 2212 (l)(b) and (c) shall not be equip­ ped with more than two openings, for filling and discharge respectively. Nevertheless, receptacles of a capacity of not than 100 1 intended for the carriage of dissolved acety­ lene [9°(c)rmay have more than two openings for filling and discharge. Similarly, receptacles and tanks in conformity with mar­ ginal 2212 (b) and (c), intended for the carriage of substances of 3°(b) and 4"(b) be provided with other ope­ nings 'intended in particular for verifying thelevel of the liquid and the gauge pressure. (2) Valves (cocks) shall be effectively protected by caps or fixed flanges. Caps shall possess vent-holes of sufficient cross-sectional area to evacuate gas·es if leakage occurs at the valves. The caps or glanges shall adequately protect the valve if the cylinder falls and during the carriage and stacking. Valves placed inside the 'neck of the receptacle and protected by a screw-threaded plug, and receptacles carried packed by protective cases, shall not require a cap. Likewise, no protective case will be required for valves (cocks) on frames of cylinders. , (3) Receptacles containing fluorine [l 0(a t)]; chlorine trifluoride [3°(a t)]; or cyanogen chloride [3°(c t)] shall, , whether they are C!!rried packed in protective cases, be fitted with steel caps. These caps shall have no openings and shall, throughout carriage, be equipped with a gasket ensuring gas-tightness and made of a material not liable to attack by the contents of the receptacle. · (1) In the case of receptacles containing boron trifluo­ ride or fluorine [l 0 (a t(]; chlorine trifluoride or liquefied ammonia [3°(a)]; ammonia dissolved in water [9°(a t)]; nitrosyl chloride [3°(a t)]; dimethylamine, ethylamine, me­ thylamine or trimethylamine [3°(b t)]; or made of copper or of any other metal liable to be attacked by these g~es are not to be accepted. (2) The use of substances containing grease or oil for ensuring leakproofnes of joints (seams) or for maintaining the closure device and receptacles used for oxygen [lo(a)]; fluorine (lo(a t)]; mixtures with oxygen [2 °(a)]; nitrogen dioxide, chlorine trifluorid [3 °(at)]; nitrous oxide [5 °(a)]; nitrogen dioxide, chlorine trifluoride [3 °(at)]; nitrus oxide (5°(a)]; or mixtures of 12° containing more than 10 per cent oxygen by volume is proh ibited. (3) The following requirements shall apply to the construction receptacles referred to.in marginal 2207 (1): (a) The materials and construction of the receptacles shall be in conformity with the requirements of Appendix A.2, B, marginals 3250 to 3254. All the mechanical and technological characteristics of the material used shall be established for each receptacle at the first test; with regard to the impact strength and the bending coefficient, see Appendix A.2, marginals 3265 to 3285. (b) Receptacles shall be fitted with a safety valve which shall be capable of opening at the working pressure shown on the receptacle. The valves shall be so constructed as to work perfectly even at their lowest working temperature. Their reliability of functioning at that temperature shall be established and checked by testing each valve or a sample of valves of the same type of construction. (c) The vents and safety valves ·of receptacles shall be so designed as to prevent the liquid from splashing out. (d) The ~losing devices shall be so arranged that they 2213 2214 cannot be opened by unqualified persons. (e) Receptacles whose filling is measured by volume shall be provided with a level indicator. (I) The receptacles shall be thermally insulated. The thermal insulation shall be protected against impact by means of continuous metal sheathing. If the space between the receptacle and the metal sheathing is airless (vacuum insulation), the protective sheathing shall be designed IQ withstand without deformation an external pressure of at least 1 kg/cm2 • If the sheathing is so closed as to be gas-tight (e.g. in the case of vacuum insulation), device shall be provided to prevent any dangerous pressure from developing in the insulating layer in the event of inadeq­ uate gas - tightness of the receptacle or its fittings. The divice shall prevent moisture from penetrating into the ins­ ulation. (4) In the case of receptacles containing mixtures of 4° (c) or dissolved acetylene [9° (c)], metal parts of closing dedces in contact with the contents shall not contain more than 70 per cent copper. Receptacles for dissolved acety­ lene [9° (c)]JTJay also have stop-valves taking yoke connec­ tors. (5) Receptacles containing oxygen of 1° (a) or 7° (a) and fitted in fish-tanks are likewise to be accepted if they are provided with appliances enabling the oxygen to escape gradually. 2. Official test Qf receptacles (for aluminium - alloy receptacles see also Appendix A.2) (1) Metal receptacles shall be subjected to initial and~ periodic tests under the supervision of an expert approved by the competent authority. The nature of these test is specified in marginals 2216 and 2217. (2) In order to ensure compliance with the requirements of marginals 2204 and 2221 (2), tests of receptacles intended to contain dissolved acetylene [9° (c)] shall incl­ ude, in addition, examination of the nature of the porous material and of the quantity of solvent. (l) The. initial test of new or unused receptacles shall comprise: A. On an adequate sample of receptacles: (a) 1 testing of the material of construction in respect at least of yield stress, tensile strength, and permanent elon­ gation at fracture; the values yielded by these tests shall comply with national regulations; (b) measurement of wall thickness at the thinnest point, and calculation of the stress; (c) checking the homogeneity of the material for each manufacturing batch, and inspection of the external and internal condition of the receptacles; B. For all receptacles: (d) a hydraulic pressure test in conformity with the provisions of marginals 2219 to 2221; (e) an ispection of the markings on the receptacles (see marginal) C. In addition, for receptacle: intended for the carriage of dissolved acetylene [9° (c)]: (I) an inspectiori as required by national regulations. (2) Receptacles shall withstand the test pressure without undergoing permanent deformation or exhibiting cracks. (3) At the periodic inspections the following shall be re­ peated: the· hydraylic pressure test; check of the external and internal condition of the receptacle ( e.g. by weighing, inter­ nal inspection, checks of wall thickness); verification of the equipment and markings and, if necessary verification of the characteristics of the material by suitable tests. Periodic inspections shall be carried out: (a) every 2 years in the case of receptacles intended for the carriage of gases of 1 ° (a t) and 1 ° (c t); town gas of 2° (b t); gases of 3° (a t) other than ammonia, hexafluo­ ropropylene and methyl; cyanogen chloride of 3° (c t); and substances of 5° (a t); (b) every 5 years in the case of receptacles intended for the car of other compressed and liquefied gases (subject to the provision of subparagraph (c) below) and 2215 2216 EO>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) 2187 of receptacles for the carriage of ammonia dissolved under pressure (9° (a t)]; (c) every 10 years in the case of receptacles intended for the carriage of gases of 1 ° (a) other than oxygen; of mixtures of nitrogen rare gases, of 2° (a); of gases of 3° ( a and 3 ° (b) other than 1, 1-difluorethane, 1-chloro- l, 1,­ difluorthane, methylsilane 1,1,1-trifluorethane, and of mixtures of gases of 4° (a) and if the receptacles have a capacity of not more than 150 litres the country of origin does not prescribe a shorter interval. (d) in the case of receptacles intended for the carriage of dissolved acetylene (9° (c)], marginal 2217 (1) shall apply, and in that of receptacles conforming to marginal 2207 (1), marginal 2217 (2) shall apply. (l)The external condition (corrosion, deformation) of, 2217 and the condition (loosening, settlement) of the porous material in, receptacles intended for the carriage of dissol-. ved acetylene (9° (c)] shall be examined every 5 yeats/ Sampling shall be performed by cutting up, if considered • necessary, a suitable number of receptacles and inspecting them internally for corrosion and for any changes that may have occurred in the constituent materials and in the porous material. (2) Receptacles conforming to marginal 2207 (1) shall be subjected every 5 years to external inspection and to a tightness (leakproofness) test. The tightness (leakproof­ ness) test shall be carried out with the gas contained in the receptacle or with an inert gas at a pressure of 2 kg/ cm2 • Checking shall be performed by means of a press­ ure gauge or by vacuum measurement. The thermal insula­ tion shall not be removed. The pressure shall not decline during the 8-hour test period. Changes resulting from the nature of the test gas of from variations in temperature . shall be taken into account. 3. Marks on receptacles (1) Metal receptacles shall bear the following particulars 2218 in clearly legible and durable characters: (a) one of the names of the gas or of the mixture of gases in full, as given in marginal 2201, 1 ° to 9°; the name or mark of the maker or owner; and the number of the receptade [see also marginal 2202 (3)]. In the case of halogenated hydrocarbons of 1 ° (a), 3° (a), 3° (a t),. 3° (b), 3° (c t), 4" (a), 5° (a) and 6° (a) the use of the letter R.followed by the substance identification number is also permitted; • (b) in the case of receptacles intended for liquefied ·gases, the tare of the receptacle including such fittings and accessories aas valves, cocks, metal plugs, etc., but excluding the protective cap; (c) in the case of receptacles intended for compressed gases, the tare of the receptacle proper; (d) the test pressure (see marginals 2219 to 2221) and the date (month, year) of the last test undergone (see marginals 2216 and 221 7); (e) the stamp of the expert who carried out the tests and inspections; and in addition: (I) in the case of compressed gases of'mixtures of compressed gases [l 0 , 2°, 12° and 13°]: the maximum filling pressure at 15° C allowed for the receptacle in question (see marginal 2219); (g) in the case of boron fluoride (1 ° (a t)], liquefied gases [3° to 6°] and ammonia dissolved in water (9° (a t)]: the maximum filling allowed, and the capacity. In the cases of deeply-refrigerated gases of ~0 and 8°: the capa0 city; (h) in lhe case of acetylene dissolved in a solvent (9° (c)): the ·permitted filling pressure [see marginal 2221 (2)], and the weight of the empty receptacle including the weight of the fittings and accessories, of the porous mate­ rial, and of the solvent; (1) in the case of mixtures of gases of 12° and test gases of 13°, the words «mixtures of gases» of •lest gases», as the case may be, shall be engraved on the receptacle as a general indication of the content. An exacfdescription of the contents shall be shown in a durable form throughout . carriage; (k) in the case of metal receptacles which, under margi­ nal 2202 (3), are accepted for the carriage of a number . of different gases (multi-purpose receptacles), an exact description of the contents shall be shown in a durable form during carriage. (2) The marks shall be engraved either on a reinforced part of the receptacle, or on a ring, or on a data plate, immovably affixed to the receptacle. In addition, the name of the substance may be indicated on the receptacle by an adherent and clearly - visible inscription applied by pai­ nting or by any other, equivalent, process. (c) Test pressure, degree of filling, and limitation of capacity, of receptacles·(see also marginals 2238, 211· • 180 and 212 180 • ( 1) ln the case of receptacles intended for the carriage 2 219 of compressed gases of 1 °, 2° and 12°, the internal press ure (test pressure to bi applied in the hydraylic pressure test shall bi at least one and one-half times the filling pressure at 15 ° C indicated on the receptacle, but shall not be less than 10 kg/cm2 • (2) In the case of receptacles used for the carriage of substances 1 ° (a) other than tetrafluoromethane; of deute- 1 rium and hydrogen of 1 ° (b) or of gases of 2° {a), the ' filling pressure shall not exceed 300 kg/cm2 referred to 1 a temperature of 15° C. In the case of tanks, the filling 1 pressure shall not exceed 250 kg/cm2 referred to a tempe-' rature of 15° C. • • In the case of receptacles and tanks intended for the carriage of other gases fo 1 ° and 2 ° the filling pressure shall not exceed 200 kg/cm2 referred to a temperature of 15° c. (3) In thr case receptacles intended for the carriage of fluorine (1 °(at)] the internal pressure (test presure) to be applied in the hydraulic pressure test shall be 200kg/cm2 and the filling pressure shall not exceed 28 kg/cm2 at-a temperatures of 15°C; in addition, on receptacl~ may co ntain more than 5 kg fluorine. • ··;. ,. ,,: . . In the case of receptacles for the carriagt"of b<Jron trif­ luoride (1 °(at)] the hydrsulic to be applied in.-the test (test) pressure shall be either 300 kg/cm?, in which· case the. maximum weight of the contents per liure of capacity shall not exceed o.86 kg, or 225 kg/cm2, in which case the ma­ ximum weight of the condents per litre of capacity shall not exceed 0. 715 kg. ( 4) n the case of receptacles in ended for the carriage of nitric oxide No (1 °(c t)], the capacity shall be limited to 50 l; the hydraulic pressure to be applied in the test (test pressure) shall be 200 kg/cm2 ; and the filling pressure shall not exceed 50 kg/cm2 at a temperature of l5°C. • (5) In the case f receptacles indended for, the carriage of mixtures of hydrogen with not more than 10 per cend hyd­ rogen selenide or phosphine or silane or germane by volume or witn not more than 15 per cent arsine by volume; of mixtures of nitrogen or rare gase s (containing not more than 10 per cent xenon by volume) with not more than 10 per cent hydrogen i,elenide or phosphine or silane or germane by volune or with not more than 15 per cent ar­ sine by volume (2 °(b t)]; of mixtures of hydrogen ~ith not more than 10 per cent diborane by·volume; or of mixtures of nitrogen or rare gases (containing not more than 10 per cent xenon by volume) with not more than 10 per cent di­ borane by volune [2 ° (c t)], the capacity shall be limited to 50 l; t~e hydraulic pressure to be applied in the test (test pressure) shall be not less than 200 kg/cm2; and the filling pressure shall not exceed 50 kg/cm2 at a temperature of 15°C. (6) Receptacles in conformity with marginal 2207 (1) shall not, at the filling temperature and at a pressure of 1 kg/ cm 2, be filled beyond 98 per cent of their capacity. Where oxygen of 7° (a) is carried, steps shall be taken to prevent any spillage of the liquid phase. (7) Where dissolved acetylene [9° (c)] is carried in receptacles in conformity with marginal 2212 ( 1) (b ), the capacity of the receptacles shall not exceed 150 I. (8) The capacity of receptacles intended for the carriage of mixtures of gases of 12° shall not exceed 50 I. The pressure of the mixture shall not exceed 150 kg/cm2 at 2188 E<DHMEPlr THr KYBEPNHrEor (TEYXOr nPOTO) a temperature of 15° C. (9) The capacity of receptacles intended for the carriage of test gases of 13° shall not exceed 50 I. The filling pressure at a temperature of 15° C shall not exceed 7 per cent of the test pressure of the receptacle. (10) In the case of tungsten hexafluoride [3° (a t)] the capacity of the receptacles shall be limited to 60 I. The capacity of receptacles for silicon tetrafluoride [l 0 (a t)]; boron chloride, nitrosyl chloride and sulphuryl fluo­ ride [3° (a t)]; methylsilane [3° (b)l; arsine, dichlorosilane, dimethylsilane, hydrogen selenide and trimethylsilane [3 ° (b t)]; cyanogen chlodride and cyanogen [3° (c t)]; mixtures of methylsilanes [4o (b t)]; substances of 4° (c t) other than dichlorodifluoromethane containing 12 per cent ethy­ lene oxide by weight; silane [5° {b)]; and substances of So (b t) and (c t), shall be limited to 50. Description of substance Bromochlorodifluoromethane (R 12 B 1) Chlorodifluoromethane (R 22) Chloropentafluoroethane (R 115) l-chloro-2,2,2-trifluoroethane (R 133a) Dichlorodifluoromethane (R 12) Dichlorofluoromethane (R 21) 1,2-Dichloro-1,1,2,2-tetrafluoroethane (R 114) Octofluorocyclobutane (RC 318) Ammonia Boron chlorid€: Chlorine .. .. Chlorine trifluoride Hexafluoropropylene (R 216) Hydrogen bromide Methyl bromide Nitrogen dioxide Nitrosyl chloride Phosgene Sulphur dioxide Sulphuryl fluoride T\fngsten hexafluoride • Butane .. .. , .. I-Butene l-Chloro-1,1-difluoroethane (R 142b) Cis-2-butene Cyclopropane 1,1-Difluoroethane (R 152a) lsobutane lsobutene Methylsilane Propane Propylene Trans-2-butene 1, 1, 1-T rifluoroethane Arsine Dichlorosilane Dimethylamine I;:>imethyl ether Dimethylsilane I;:tliylamine Ethyl chloride Hydrogen seleriide Hydrogen sulphide Methylamine Methyl chloride (11) In the case of receptacles intended for chlorine trifluoride [3° (a t)] the capacity shall be limited to 40 I. After filling, a receptacle containing chlorine trifluoride [3° (a t)] shall, before being handed over for carriage, be held back for not less than seven days in order to verify that it is leak-proof. (1) In the case of receptacles intended for the carriage of liquefied gases of 3° to 6°, a nd of receptacles intended for the carriage of gases di~solved under pressure of 9°, the hydraulic pressure to be applied in the test (test press­ ure) shall be not less than 10 kg/cm2. (2) In the case of liquefied gases of 3° and 4° the following values shall be complied with for the hydraulic pressure to be applied to the receptacles in the test (test pressure) and for the maximum degree of filling allowed:• !ltSee the end of the table in paragraph (2). 2220 Minimum Maximum weight Item Test of contents per number pressure litre of capacity kg/cm2 l<g 3°(a) 10 1.61 3 °(a) 29 1.03 3 °(a) 25 - 1.06 3 °(a) 10 1.18 3 °(a) 18 1.15 3 °(a) 10 1.23 3 ° (a) . 10 1.30 3°(af 11 1.34 3 °(at) 33 0.53 3 °(at) 10 1.19 3 °(at) • 22 1.25 3 °(at) 30 1.40 3 °(at) 22 1.11 3 °(at) 60 1.20 3 °(at) 10 1.51 3 °(at) 10 1.30 3 °(at) 13 1.10 3 °(at) 20 1.23 3 ° (at) 14 1.23 3 °(at) 50 1.10 3 °(at) 10 2.70 3°(b) 10 0.51 3°(b) 10 0.53 3 ° (b) 3 °(b) 10 0.55 3 °(b) 20 0.53 3 °(b) 18 0.79 3 °(b) 10 0.49 · 3°(b) 10 0.52 3°(b) 225 0.39 3 °(b) 25 0.42 3 °(b) 30 0.43 3 °(b) 10 0.54 3 °(b) 35 0.75 3 °(bt) 42 1.10 3 °(bt) 10 0.90 3 °(bt) 10 0.59 3 °(bt) 18 0.58 3 °(bt) 225 0.39 3 °(bt) 10 0.61 3 °(bt) 10 0.80 3 °(bt) 31 1.60 3 °(bt) 55 0.67 3 °(bt) 13 0.58 3 °(bt) 17 0.81 ECl>HMEPlr THr KYBEPNHIEQr (TEYXOr nPQTO) 2189 Methyl mercaptan Trimethylamine Trirhethylsilane 1,3-Butadiene Vinyl chloride Cyanogen Cyanogen chloride Ethylene oxide Methyl vinyl ether Trifluorochloroethylene (R 1113) Vinyl bromide Mixture Fl Mixture F2 I Mixture F3 Mixture of gases R 500 · Mixture of gases R 502 Mixture of 19 to 21 per cent by weight dichlorodifluoromethane (R 12) and 79 to 81 per cent by weight bromochlorodifluorome thane (R 12 BI) Mixtures of methyl bromide and chloropicrin Mixture A (trade name: butane) Mixture A O (trade name: butane) Mixture A 1 Mixture B Mixture C (trade name: propane) Mixtures of hydrocarbons containing methane Mixtures of methylsilanes Mixtures of methyl chloride and methylene chloride Mixtures of methyl bromide and ethylene bromide Mixtures of methylacetylene / propadiene and hydrocarbons Mixture P 1 Mixture P 2 Ethylene oxide containing not more than 10 per cent carbon dio xide by weight Ethylene oxide containing not more th~n 50 per cent methyl for mate by weight with nitrogen up to a maximum total pressure of 10 kg/cm2 at 50°C Ethylene oxide with nitrogen up to a total pressure of 10 kg/cm2 at 50c Dichlorodifluoromethane containing 12 per cent ethylene oxide h' weight * 1. The test pressures prescribed are at lest equal to the vapour pressures "of the liquids at 70°C, reduced by 1 kg/cm2, the minimum test pressure required being ho­ wever 10 kg/cm2. 2. In view of the high degree of toxicity of phosgene (carbonyl chloride) [3° (at)] and of cyanogen chloride [3°(ct)], the minimum test pressure for these gases has been fixed at 20 kg/cm2• (3) In the case of receptacles intended to contain lique­ fied gases of 5° and 6° the degree of filling shall be such that the internal pressure at 65° C does not exceed the test pressure of the receptacles. The following values shall be complied with [see also paragraph (4)]: 3 °(bt) 3 °(bt) 3 °(bt4 3 °(c) 3 °(c) 3°(ct) 3 °(ct) 3 °(ct) 3 °(ct) 3 °(ct) 3 °(ct) 4°(a) 4°(a) 4°(a) 4°(a) 4°(a4 4°(a) 3 ° (at) 4°(b) 4°(b) 4°(b) 4°(b) 4°(b) 4°(b) 4 ° (bl) 4 ° (bt) 4 ° (bt) 4°(c) 4° (c) 4° (et) 4 ° (et) 4 ° (et) 4°(ct) 10 10 225 i'o 12 100 20 10 10 19 10 12 18 29 22 31 12 10 fo 15 20 25 30 225 300 225 19 10 30 24 28 25 15 18 0.78 0.56 0.39 0.55 0.81 0.70 1.03 0.78 0.67 1.13 1.37 1.23 1.15 1.03 1.01 1.05 1.50 1.51 0.50 0.47 0.46 0.43' 0.42 0.187 0.244 0.39 0.81 1.51 0.49 0.47 0.73 0.80 0.78 1.09 3. The maximum values prescribed for the degree of filling in kg/litre have been determined as follows: ma­ ximum weight of contents per litre of capacity=0.95 times the density of the liquid at 50°C; in addition, the vapour phase must not disappear below 60°C. 2190 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Minimum • Maximum weight Item Test of contents per Description of substance number pressure litre of capacity kg/cm2 kg Bromotrifluoromethane (R 13 B 1) 5°(a) 42 1.13 120 1.44 250 1.60 Carbon dioxide 5°(a) 190 0.66 250 0.75 Chlorotrilluoromethane (R 13) 5°(a) 100 0.83 120 0.90 190 1.04 250 1.10 Hexafluoroethane (R 116) 5°(a) 200 1.10 Nitrous oxide N20 5°(a) 180 0.68 225 0.74 250 0.75 Sulphur hexafluoride 5°(a) 70 1.04 Trifluoromethane (R 23) 5o(a) 190 0.87 250 0.95 Xenon 5°(a) 130 1.24 Hydrogen chloride 5°(at) 100 0.30 .. 120 0.56 150 0.67 200 0.74 Ethane 5°(b) 95 0.25 120 0.29 300 0.39 Ethylene 5 °(b) 225 0.34 300 0.37 Silane 5°(b) 225 0.32 250 0.41 Germane o(bt) 250 1.02 Phosphine 5 ° (bt) 225 0.30 250 0.51 1.1.-Difluoroethylene 5°(c) 250 0.77 Vinyl fluoride 5 °(c) 250 0.64 Class 2 Minimum Maximum weight Description of substance Item test of contents per number pressure litre of capacity kg/cm2 kg Diborane 5 °(ct) 250 Constituents 0.072 Carbon dioxide containing 6°(a) 190 (weight per cent) 1 0.64 1-10 per cent nitrogen, oxy- 190 1-10 0.48 gen, air or r11-re gases by weight 250 1 0.73 250 1-10 0.59 Mixture of gases R 503 6°,(a) 31 0.11 42 0.20 ... 100 0.66 Carbon dioxide containing 60 (c) 190 0.66 not more than 35 per cent 250 0.75 ethylene oxide by weight Ethylene oxide containing 6°(ct) 190 0.66 more than 10 per cent hut 250 0.75 not more than 50 per cent carbon dioxide by weight 60 (et) E<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2191 (4) For substances of 5° other than hydrogen chloride [5° (at)]; germane and phosphine [5° (bt)]; and diborane [5° (ct)J, and for substances of 6°, the use of receptacles tested at a lower pressure than that indicated in paragraph (3) for the substance in question is allowed, but the qua­ ntity of substance per receptacle shall not exceed that which at 65°C would produce inside the receptacle a press­ ure equal to the test pressure. In such a case the permis Description of substance Ammonia dissolved under pressure in water with more than 35 per cent but not more than 40 per cent ammonia by weight with more than 40 per cent but not more than 50 per cent ammonia by weight Dissolved acetylene (2) In the case of dissolved acetylene [9o (c)], once equilibrium has been achieved at 15 ° C the cylinder filling pressure shall not exceed the value prescribed by · the competent authority for the porous mass, which value Special conditions: Item No or letter Description of substance . Gases packed in accordance with marginal 2205 sible, maximum load shall be prescri bed by the expert ~pproved by the competent authority. (1) In the case of gases dissolved under pressure, of 9°, the following values shall be complied with for the hydraulic pressure to be applied to the receptacles in the test (test pressure), and for the maximum degree of filling allowed: 2221 Class 2 Item number 9o (at) 9°(at) 9° (c) Minimum Maximum weight test • of contents per pr~ssure litre of capacity kg/cm2 kg 10 0.80 ( 12 0.77 60 see under (2) shall be engraved on the cylinder. The quantity of solvent and the quantity of acetylene shall likewise correspond to the figures specified in the approval. Class 2 Maximum quantity Special requirements per per receptacle package Chlorine [3° (at)] shall not be packed I All gases listed in this marginal in the quantities pres- 6 kg together with sulphur dioxide [3° (at)] cribed in marginal (a) Non-inflammable gases 2205 Shall not be packed together with substances of Classes la, ld, le, 3, (at) Non-inflammable toxic gases 4.2, 5.2 or 7 ' (b) Inflammable gases Shall not be packed together with substances of Classes la, ld, le, 3, t 4.1, 5.2 7 or 8 Gases packed in accordance with marginal 2206 All gases- listed in the marginal except am monia and cyclopropane (a) Non-inflammable gases Shall not be packed together with (at) Non- inflammable toxic gases 150 g 6 kg substances of Classes la, lb, le, 3, 4.2, 5.2 or 7 (b) Inflammable gases (bt) Inflammable toxic gases Shall not be packed together with (c) Chemically unstable gases (et) Chemically unstable toxic gases substances of Classes la, Id, le, 3, 4.1, 4.2, 4.3, 5.1, 5.2 or 7 6 kg· 3 ° (at) Ammonia 20 g 6 kl!; 3 °(b) Cyclopropane 2192 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 3. Mixed packing (1) Substances of this Class other than substances of 7° and 8° may be enclosed in the same package with one another if they are contained: (a) in metal pressure - receptacles of a volume not exceeding 10 litres; (b) in thick - walled glass tubes or glass syphons in accordance with marginals 2205 and 2206, on condition that these fragile receptacles are secured in accordance with the provisions of marginal 2001 (5). The cushioning materials shall be suited to the properties of the contents. Inner packagings shall be placed in an outer packaging in which they shall be effectively kept apart from one ano­ ther. (2) Articles of 10° and 11 ° may be enclosed in the same package with one another under the conditions pres­ cribed in marginal 2210. (3) In addition, substances packed in accordance with marginals 2205 and 2206 may be enclosed in the same package with one another subject to the following special conditions. (4) A package which meets the requirements of (1) and (2) shall not weigh more than 100 kg, or more than 75 kg if it contains fragile receptacles. Class 2 4. Markings and labels on packages (see Appendix A. 9) (1) Every package containing receptacles holding gases of 1 ° to 9°, 12° or 13° or non-refilla~le containers of gas under pressure of 11 ° shall be marked legibly and indelibly with an indication of its contents, with the addition «Class 2». This marking shall be iri an official language of the country of departure, and also, if that language is not English, French of German, in English, French or German, unless any agreements concluded between the countries concerned in the transport operation provide otherwise. This provision need not be complied with if the receptac­ les and their markings are clearly visible. (2) Packages containing aerosol dispensers of 10° shall be mrked with the word «AEROSOL» in clearly legible and indelible characters. (3) Where a consignment constitutes a full load, the markings referred to in paragraph ( 1) are not mandatory. (1) Packages which contain receptacles made of i:nate­ rials liable to shatter, such as glass or certain plastics materials, shall bear a label conforming to model No. 9. (2) Every package containing gases of 7° (a) or 8° (a) shall bear, on..two opposite sides, labels conforming to model No. 8, and if the substances it contains are enclosed in glass receptacles [marginal 2207 (2) (a)] it shall, in addition, bear a label conforming to model No. 9. Every package containing aerosol dispensers of 10° (b) 2., 10° (bt) 2., 10° (c) or 10° (et), or non. - refillable containers of gas under pressure of 11 ° (b), 11 ° (bt), 11 ° (c) or l lo (et), shall bear a label conforming to model No. 2A. B. Particulars in the transport.document • (1) The description of the goods in the transport doc­ ument must be: (a) in the case of pure and technically - pure gases of 1 °, 3°, 5°, 7° or 9°, of aerosol dispensers of 10°, of non refillable containers of gas under pressure of 11 ° one of the names underlined in marginal 2201; (b) in the case of mixtures of gases of 2°, 4°, 6°, 8°, 12° or 13° «mixture of gases». This description must be supplemented by an indication of the composition of the mixture of gases in volume per cent or weight per cent. Constituents below one per cent need not be indicated. In the case of mixtures of gases of 2° (a), 2° (b), 2° (bt), 4° (a), 4° (b), 4° (c), 6° (a), 8° (a) or 8° (b) the descriptions or names customary in the trade which are underlined in marginal 2201 may likewise be used, without indication of the composition. , 2222 2223 2224 2225 2226 Class 2 These descriptions must be underlined in red and follo­ wed by particulars of the Class, the item number .(together with the letter, if any), and the initials «ADR» or «RID• [e.g., 2, 5° (at), ADR] (2) In the case of consignments of gases which are listed among the chemically unstable gases the sender shall certify as follows in the transport document: • The necessary steps have been taken to satisfy the require­ ments of ADR marginal 2200 (4)». In the case of consig­ nments of mixtures of gases of 12° or test gases of 13°, the sender shall certify as follows in the transport doc­ ument: «The conditions laid down in ADR marginal 2201, 12° or 13°, have been complied with». • (3) In the case of consignments of chlorine trifluoride [3° (atj) the sender shall certify as follows in the transport document: «After filling with chlorine trifluoride, the re­ ceptacle has been kept under observation for not less than seven days and its leakproofness has been verified». (4) In the case of tanks containing gases of 7° (a) or 8° (a). other than carbon dioxide and nitrous oxide, the transport document shall bear the following entry: «The tank is •in permanent communication with the atmosphere•. C. Empty packagings (1) Receptacles and tanks of 14° shall be closed in the same manner as though they were full. (2) The description in the transport document must be: «Empty receptacle or («Empty tank-), uncleaned, 2, 14°, ADR (or Item 14, RID)». This text must be underlined in red. D. Transitional provisions The following transitional provisions shall apply to re­ ceptacles for compressed 'or liquefied gases or gases dis­ solved under pressure: (a) receptacles already in service shall, subject to the following exceptions, be accepted in international traffic so long as the requirements of the contracting country in· which the tests in accordance with marginal 2216 were carried out so permit and as the intervals prescribed in marginals 2216 (3) and 2217 for the periodic inspections are observed; • (b) in the case of receptacles manufactured under the previous system (permissible stress two - thirds, instead of three -quarters, of the yield stress), no increase in either the test pressure or the filling pressure shall be permitted [see marginal 2211 (l)]; (c) transitional measures for tanks: see marginal 211180; (d) transitional measures for tank-containers: see margi­ nal 212180. CLASS 3. INFLAMMABLE LIQUIDS 1. List of substances (1) Among the inflammable liquids and mixtures the­ reof, whether liquid or still pasty at a temperature not exceeding 15°C, the substances listed in marginal 2301 are subject to the provisions of this Annex and of Annex B. These substances to be accepted for carriage under certain conditions are to be considered as substances of ADR. (2) Inflammable liquids which at a temperature of 50° C have a vapour pressure not exceeding 3 kg/cm2 , except those listed in other Classes, are deemed to be inflammable liquids within the meaning of ADR. (3) Liquids of Class 3 which are liable to form peroxides easily (as happens with ethers or with certain heterocyclic oxygenated substances) are not to be handed over for carriage unless their peroxide content, reckoned as hydro­ gen peroxide H 2 0 2, does not exceed 0.3 per cent. ( 4) The peroxide content referred to above and the flash - point referred to below shall be determined as shown in Appendix A.3 (marginals 3300 - 3303). 2227 2236 9,300 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2193 (5) Substances of Class 3 which polymerize easily are to be accepted for carriage only if the necessary precau­ tions have been taken to prevent their polymerization during· carriage. (6) Solid substances soluble in liquids shall be deemed to include driers, fixed oils (boiled or blown linseed oils, etc.) or similar substances (nitrocellulose excepted) whose flash - point is above l00°C. lo (a) Liquids not miscible, or only partially miscible, with water· which have a flash - point below 21 ° C, also when they contain not more than 30 per cent solids (nitro­ cellulose excepted) either dissolved, or held in suspension in the liquids, or both, e.g. crude petroleums and other crude oils; volatile products from the distillation of petro­ leum and of other crude oils or of coal, lignite, shale, wood and peat tars, e.g. petroleum ether, pentanes, ben­ zine, benzol and toluene; condensation products of natural gas; ethyl acetate (acetic ester), vinyl acetate, diethyl ether ether (sulphuric ether) methyl formate and other ethers and esters; carbon disculphide; acrylaldehyde (acrolein); certain chlorinated hydrocarbons [e.g. 1,2 - dichloroe­ thane and chloroprene (chlorobutadiene)]; (b) mixtures of liquids having a flash - point below 21 °C and containing not more than 55 per cent nitrocell­ ulose with a nitrogen content not exceeding 12.6 per cent (collodions, semi - collodions and other nitrocellulose sol­ utions). Class 3 . For (a), see also marginal 2301a under (a), (b) and (d); for (b), see also marginal 2301a, under (a). Note: For mixtures of liquids having a flash - point below 21 °C and containing more than 55 per cent nitrocellulose, whate­ ver its nitrogen content, or containing not more than 55 per cent nitrocellulose with nitrogen content above 12.6 per cent, see Class la, marginal 2101, 1°, and Class 4.1, margi­ nal 2401 7° (a+. 2° Liquids not miscible, or only partially miscible, with water which have a flash - point below 21 ° C and contain more than 30 per cent solids (nitrocellulose excepted) either dissolved, or held in suspension in the liquids, or both, e.g.: certain colours for rotogravures and for lea­ thers, certain varnishes, certain enamel paints, and rubber solutions. See also marginal 2301a, under (c). 3 ° Liquids not miscible, or only partially miscible, with water which have a flash - point between 21 ° C and 55 ° C inclusive, also when they contain not more than 30 per cent solids either dissolved, or held in suspension in the liquids, or both, e.g.: turpentine: .semi - heavy products from the distillation of petroleum and of other crude oils, or of coal, lignite, shale, wood.and peat tars, e.g. white spirit (turpentine substitute), heavy benzols, petroleum oils (for lighting, heating or engines), xylene; styrene, cumene, solvent naphtha; butanol; butyl acetate; pentyl acetate (amyl acetate)! nitromethane (mononitromethane) and ce­ tain mononitro - paraffins; certain chlorinated hydrocar: bons (e.g. chlorobenzene). See also marginal 2301a, under (c) and (d). 4° Liquids not miscible, or only partially miscible, with water which have a flash - point above 55 °C but not exceeding 100 ° C, also. when they contain not more than 30 per cent solids either dissolved, or held in suspension in the liquids, or both, e.g.: certain tars and their distillation products: heating oils, diesel oils, certain gas oils; tetrahyd­ ronaphthalene (tetralin); nitrobenzene; certain chlorinated hydrocarbons (e.g. 1 - chloro - 2 - ethylhexane). See also marginal 2301a, under (c) and (d). 5 ~ Liquids miscible in all proportions with water which have a flash - point below 21 °C, also when they contain ' not more than 30 per cent solids either dissolved, or held in suspension in the liquids, or both, e.g.: methanol (methyl alcohol, wood spirit), denatured or not; Class 3 Ethanol (ethyl alcohol, ordinary alcohol), denatured or not; acetaldehyde; acetone and acetone mixtures; pyridine. See also marginal 2301a, under (a) and (c). 6° Empty receptacles, uncleaned, and empty tanks, uncleaned, which have contained inflammable liquids of Class 3. Substances handed over for carriage in conformity with 2.3 01 b.. the following provisions are subject neither to the provi sions for this Class contained in this Annex nor to those contained in Annex B: (a) liquids of I O (except those mentioned under (b) below), and acetone and acetone mixtures (5°): in quanti­ ties not exceeding 200 g per receptacle, in receptacles . made of sheet - metal, glass, porcelain, stoneware or a suitable plastics material,· these receptacles, with a total content not exceeding I kg, being placed together in an outer packaging made of sheet - metal, wood or fibreboard and fragile receptacles being suitably secured in the packa ging to prevent their beakage; . (b) carbon disulphide, diethyl ether, petroleum ether, pentanes, methyl formate: 50 g per receptacle and 250 g per package, these substances being packed in the same way as those of (a); (c) liquids of 2° - 5°, except acetaldehyde, acetone and acetone mixtures: I kg per receptacle and I 0 kg per package, these substances being packed in the same way as those of (a); • (d) the motor - fuel contained in the tanks of motor driven vehicles or in closed auxiliary tanks firmly fixed to the vehicles. If there is a cock between the tank and the engine it must be closed; the electric circuit m·ust also be disconnected. Motor cycles and motor - assisted pedal cycles whose tanks contain motor - fuel must be loaded upright on their wheels, secured against falling. 2. Provisions A. Packages I. General conditions of packing 2302 (I) Receptacles shall be so closed and l~ak - proof as to prevent any loss of the contents, and particularly any evaporation. (2) The materials of which the receptacles and their closures are made must not be liable to attack by the contents nor form harmful or dangerous compounds there with. Class 3 (3) Packagir,gs, including their closures, must be suffi­ ciently, ·rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require­ ments of carriage. In particular, receptacles and their closures must, unless the section headed «Packing of a single substance» provides otherwise, be able to withstand any pressure which, the presence of air also being taken into account, may arise inside the receptacles in normal· carriage. For this purpose a free space must be left, ac­ count being taken of the difference between the temperat­ ure of the cubstances at the time of filling and the highest mean teaperature which they are likely to reach during carriage (see also marginal 2305). Inner packagings shall be firmly secured in outer packagings. Unless otherwise specified in the section entitled «Packing of a single substance», inner packagings may be enclosed in outer packagings, either singly or in groups. • (4) Bottles and other glass receptacles must be free from faults liable to impair their strength; in particular, internal stresses must have been suitably relieved. The walls must be not less than 3 mm thick in the case of receptacles weighing, with their contents, more than 35 kg and not less than 2 mm in the case of other receptacles. The tightness of the closure system must be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preventing any loosening of the closure system during carriage. (5) Cushioning materials shall be suited to ·the nature of the contents and, in particular, shall be absorbent. Suitable materials must be used to secure receptacles in the protective packaging; this securing must be carried out with care and he checked periodically (possibly before each fresh filling <:>f the receptacle). 2194 E<l>HMEPl:r TH:r KYBEPNH:rBU (TEYXO:r nPOTO) 2. Packing of a single substance (1) Substances of·l 0 5° must be packed in suitable 2303 receptacles made of metal or of glass, porcelain, stoneware or similar materials. Substances of 4° and corrosive liquids of 1 ° (a), 3° and 5° may also. be packed in receptacles made of a suitable plastics material. [For the special provi sions concerning chloroprene and nitromethane, see under . (8) and (9), respectively, below]. (2) Fragile receptacles (glass, porcelain, stoneware or similar materials) may not contain-more than the following quantities of substances of 1 °: • carbon disulphide . . . . . . . . . . . . . . . . . . . . . . . 1 litre; diethyl ether, petroleum ether, pentanes ...... 2 litres; other substances of 1 ° • • • • • • • • • • • • • • • • · · · · 5 litres; Clase 3 (3) Tin- plate receptacles having a capacity not excee- 2303 ding 10 litres must have a wall thickness of not less than 0.25 mm; those having a capacity exceeding 10 litres but not exceeding 60 litres must have a wall thickness of not less than 0.3 mm and their joints shall be double-seamed by welting, or soldered, or produced by a process ensuring a similar degree of strength and tightness. (4) Receptacles made of sheet-steel (for tin-plate recep­ tacles having a capacity not exceeding 60 •litres, see also (3)) must be welded or ~ard-soldered, and the quantities of substances of 1 °-5° they may contain, according to the thickness of their walls, are. as follows: if the wall thickness is not less than 0.5 mm: not more than 30 litres; if the wall thickness is not less than 0. 7 mm: not more than 60 litres; if the wall thickness is not less than 1.5 mm: over 60 litres. Packages weighing more than 100 kg shall be fitted with rolling hoops. (5) Receptacles made of sheet-metal other than steel must be designed and manufactured in such a way that they possess the same strength as the sheet-steel receptac­ les referred to under (4). (6) Liquids whose vapour pressure at 50°C does not exceed 1.5 Kg/cm2 , with the exception of carbon disulph­ ide, may also be carried in metal drums complying with the following provisions: • The body joints of the drums must be welded and the end joints welded or double-seamed by welting. The drums must be fitted with rolling hoops or strengthening ribs. Every drum must have undergone the leakage test prescri­ bed in marginal 3502 of Appendix A.5. The drums must be of a type of construction which has satisfied the other tests prescribed in the aforesaid Appendix A.5. and must bear the mark assigned at the time of type approval. (7) For the carriage in non-returnable metal packagings (new packagings intended to be used only once) of inflam­ mable products whose vapour pressure at 50°C does not exceed 1.1 kg/cm2 it is not necessary, in the case of a package whose unit weight must not exceed 225 kg, for the end of the receptacle to be welded to the body and for the wall thickness to be greater than 1.25 mm, but the receptacle must be able to withstand, without leakage, a hydraulic pressure of 0.3 kg/cm2 at least, and its body and ends must be equipped with devices (such ae ribs or rolling hoops), whether detachable or not, ensuring rigi­ dity. (8) Chloroprene [l O (a)] shall be packed: (a) in hermetically-closed metal receptacles, suitably lined if necessary, having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or other outer packaging of adequate strenght; or (b) in sheet-steel canisters, welded or hard-soldered, having a capacity not exceeding 60 litres, hermetically closed and fitted with means of handling. •. (9) Nitromethane (3°) must be contained: (a) in frapile receptacles containing not mo~e than 1 litre; or (b) in sheet-steel receptacles in conformity with (4) above having a capacity not exceeding 10 litres; or (c) in metal drums each having two hermetic closures, one of them screwthreaded, each drum being fitted with -~ rolling hoops and having a capacity not exceeding 200 lit­ res. • (1) Fragile receptacles containing substances of 1 ° to 5°, receptacles made of a plastics material and containing corrosive liquids of 1 ° (a), 3° and 5°, tin-plate receptacles containing substances of 1 ° and-5°, tin-plate receptacles having a wall thickness of less than 0.5 mm and containing substances of 2° -4°, and sheet-steel receptacles containing nitromethane in conformity with marginal 2303 (9) (b), shall be secured by cushioning materials in protective packagings. If receptacles made of a plastics material are secured separately in protective packagings, cushioning materials are not necessary. Protective packagings enclosing fragile receptacles co­ ntaining substances of 1 ° and 5° and protective packagings enclosing receptacles containing nitromethane (3°) must have complete sides and be made of wood, sheet-metal or a similar material. The closure of fragile receptacles placed in open protec­ tive packagings must be provided with a protective cover shielding them from damage. If the packages are loaded on an open vehicle, the protective cover must be incapable of igniting on contact with a flame. (2) The following are to be accepted for carriage without protective packaging: (a) receptacles made of a plastics material in conformity with marginal 2304 (1), containing substances of 4°; (b) receptacles made of tin-plate not less than 0.5 mm thick, containing substances of 2°-4°; (c) sheet-metal receptacles in conformity with marginal 2303 (4) to (7); ~) metal canisters in conformity with marginal 2303 (8) ·(b) containing cloroprene [l O (a)]; (e) metal drums in conformity with marginal 2303 (9) (c) containing nitromethane (3°). (3) The following packages must not exceed the ma­ ximum weights indicated below: (a) (b) (c) (d) (e) (f) (g) (h) packages of fragile receptacles containing substances of 1 ° • • • • • • • • • • • • • • • packages of fragile receptacles containing substances of 2° - 5° • • • • • • · · • • • • • packages of receptacles made of a plastics material and containing substances of 1 ° (a) and 3°-5°, and of tin-plate receptacles containing substances of 1 °-5° • • • • • • • • • • packages of receptacles containing chlo­ roprene in conformity with marginal 2303 (8) ...................... : ....... . packages of sheet-steel receptacles contai­ ning nitromethane in conformity with mar ginal 2303 (9) (b) .................. . .dru ms tested in conformity with marginal 2303 (6) ......................... . receptacles in conformity with marginal 2303 (7) ......................... . drums containing nitromethane in confor mity with marginal 2303 (9) (c) ....... . ( 4) Packages other than cases and metal drums shall be fitted with means of handling. Metal receptacles intended to contain liquids of 1 °, nitromethane (3°).- or acetaldehyde, acetone, or acetone mixtures (5°), shall not be filled beyond 93 per cent of their capacity. Nevertheless, receptacles containing hydro­ carbons other than petroleum ether, pentanes, benzene and toluene may be filled to 95 per cent of their capacity. 3. Mixed packing (l) Substances grouped under the same item number may be included in the same package. The inner packa 2304 30 kg; 75 kg; 75 kg; 75 kg; 75 k,g; 250 kg; 225 kg; 275 kg; 2305 <l>EK 225 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTOI 2195 gings shall conform lo what is prescribed for each ;11bstance, and the outer packaging shall be that laid down for the substances of the item number in question. (2) If smaller quantities are not prescribed in the section entitled «Packing of a single substance», substances of this Class may be enclosed in the same package either with dangerous substances of other Classes (if mixed packing , ' Item Description per No. of substances fragile receptacle lo (a) Carbon disulphide 0.3 1itre . l 0 3a)and l" (b) All substances except car bon disulphide 1 litre 2" All substances 1 litre 30 All substances 3 litres 40 All substances 5 litres 50 Liquids having a boiling point,;;; 50°C 1 litres Other substances 3 litres 4. Marking am;! danger labels on packages (see Appen- . dix A'.) • (1) Packages containing liquide of 1 ° to 3° and 5° shall bear a label conforming to modes) No. 2A. However, if substances of 2°, 3° or 5° are packed in receptacles made of glass, porcelain, stoneware or similar material, of a capacity exceeding 5 litres, the packages shall bear two labels conforming to model No. 2A. Packages containing acrylaldehyde or chloroprene (ch­ lorobutadiene) [l O (a)] or methanol (methyl alcohol) (5 °) shall in.addition bear a label conforming to model No. 4. (2) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9. If the fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampoules, bear labels conforming to model No. 8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when othe packagings are used. (3) In the case of consignments carried as a full load, labels Nos. 2A and 4, as prescribed under (1), need not be affixed to the packages if the vehicle bears the marking prescribed in Annex B, marginal 10 500. B. Particulars in the transport document (1) The description of the goods in the transport doc­ ument must conform to one of the names underlined in marginal 2301. If the latter does not contain the name of the substance, the trade name shall be used. The descrip­ tion of the goods must be underlined in red and followed by particulars of the Class, the item number (together with the letter, if any), and the initials •ADR» or •RID• [e.g. 3, 1 °(a), ADR]. 2307 2308 2309 is likewise permitted in the case of such substances) or with other goods, as indicated below. The inner packagings must satisfy the general and spe­ cial conditions of packing. In addition, the general provi­ sions contained in marginals 2001 (5) and 2002 (6) and (7) must be observed. A package must not weigh more than 150° kg, or more than 75 kg if it contains fragile receptacles. Maximum quantity per per Special other package provisions receptacle 1 litre 1 litre Liquids of Class 3 nust not be packed together with substances of Class 4.2, hydrogen peroxide or perchloric acid of Class 5.1, or substances of Class 8, 2°(a), 3"(a), 4°, 7° and 41 °. : 5 litres 5 litres ? 5 litres 10 litres ' 5 litres 10 litres 5 litres 10 litres .. ' ~ -,.". ', . 5 litres 5 litres 5 litres 10 litres ' (2) In the case of all consignments of substances which polymerize easily,' the following must" be certified in the transport document: «The necessary steps have been taken to prevent polymeri~tion during carriage•. 2310 C. Empty packagings (1) Receptacles and ·tanks of 6° must be closed in the same, manner and leak-proof in the same degree as though . they were full. (2) The description in the transport document.must be: «Empty receptacle (or empty tank), 3, 6° ADR (or RID)•. This description must be underlined in red. • (3) Empty receptacles, uncleaned; of 6° which have contained substances of 1 ° to 3° and 5° shall bear a label conforming to model No. 2A. Those which have contained acrylaldehyde or chloroprene (chlorobutadiene) (1 °(a)) or methanol (methyl alcohol) (5 °) shall in addition bear a label conforming to model No. 4. CLASS 4.1. INFLAMMABLE SOLIDS 1 ; List of substances Among the substances covered by the heading of Class 4.1, those listed in marginal 2401 are subject to the provisions of this Annex and of Annex B. These substances to be accepted for carriage under certain conditions are to be considered as substances of ADR. 1 ° Substances which can easily be ignited by sparks, such as wood flour, sawdust, wood shavings, wood fibre, wood charcoal, wood parings and wood cellulose, old"pa­ per and waste paper, paper fibres, cane (except Spanish broom), reeds, hay, straw, also when damp (including 2315 2316 2317 2399 2400 2401 2196 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) maize, rice and flax straw), vegetable textile substance~ and waste of vegetable textile substances, cork in powder or granular form, expanded or not, with or with?ut an admixture of tar or of other substances not subject to spontaneous oxidation, and cork waste in small lumps. See also Class 4.2, marginal 2431, 8°-10°, and marginal 2'43la, under (b). Note: 1. These substances are included in the list only for the purposes of the prohibitions on mixed loading. For this purpose the provisions of marginal 2416 (1) appl~. No other clause, either of this Annex or of Annex B, 1s applicable to them. 2. Hay still having a degree of ~umidity which. might lead to fermentation is not to be accepted for carnage. 3. Wrappings and slabs of expanded cork, manufact­ ured under pressure, with or without an admixture of tar or of other substances not subject to spontaneous oxida­ tion, are not subject to any of the provisions of ADR. 4. Cork impregnated with substances still subject to spontaneous oxidation is a substance of Class 4.2 (see marginal 2431, 9°). 2° (a) Sulphur (including flowers of sulphur); 3° (b) sulphur in the melted state. 3° Celloidin, produced by incomplete evaporation of the alcohol contained in collodion and consisting mainly of collodion cotton. 4° Celluloid in slabs, sheets, rods or tubes, and fabrics coated with nitrocellulose. 5° Film celluloid, i.e. the raw material for films, without emuls1~n, in ·rolls, and developed celluloid films. 6° Celluloid waste and celluloid-film waste. . Note: Nitrocellulose-film waste, free from gelatine, in rll'els, sheets or strips, is a substance of Class 4.2 (see marginal 2431, 4°) 7° (a) Weakly nitrated nitrocellulose (such as collodion cotton), i.e. with a nitrogen content not-axceeding 12.6 per cent, well stabilized and containing in addition not less than 25 per cent water or alcohol (methyl, ethyl, normal propyl or isopropyl, butyl or amyl alcohol, or mixtures thereof), also if denatured, solvent naphtha, ben­ zol, toluene, xylene, mixtures of denatured alcohol and xylene, mixture water and alcohol or alcohol containing camphor in solution; Note: 1. Nitrocellulose with a nitrogen content excee­ ding 12.6 per cent is a substance of Class la (see marginal 2101, 1°). 2. When the nitro~ellulose is wetted with denatured alcohol, the denaturing substance must not have a detrime­ ntal.effect on the stability of the nitrocellulose. (b) plasticized nitrocellulose, non-pigmented, contai­ ning not less than 18 per cent plasticizer (butyl phthalate or a plasticizer at least equivalent 'in effect) and in which the nitrocellulose has a nitrogen content not exceeding 12.6 per cent; the nitrocellulose may be in the form of ch­ ips; Note: Plasticized nitrocellulose, non-pigmented, contai­ ning not less than 12 per cent and less than 18 per cent butyl phthalate or a plasticizer at least equivalent in effect is a substance of Class la (see marginal 2102, 4°). (c) plasticized nitrocellulose, pigmented, containing not less than 18 per cent plasticizer (butyl phthalate or a plasticizer at least equivalent in effect), in w hich the nitro­ cellulose has a nitrogen content not exceeding 12.6 per cent and which contains not less than 40 per cent nitrocell­ ulose; the nitrocellulose may be in the form of chips. Note: Plasticized nitrocellulose, pigmented, containing less than 40 per cent-nitrocellulose is not subject lo the provisions of ADR. For (a), (b) and (c): weakly-nitrated nitrocellulose and plasticized nitrocellulose, pigmented or not, are not to be accepted for carriage unless they satisfy the stability and safery conditiom of Appendix A. I or the conditions set forth above regarding the nature and quantity of the addi­ tional substances. For (a), see also Appendix A.I, marginal 3101, for (b) and (c), see also Appendix A.I, marginal 3102, 1. 8" Red phosphorus (amorphous), phosphorus sesquisu lphide and phosphorus pentasulphide. . Note: Phosphorus pentasulphide not free from white or yellow phosphorus is not to be accepted for carriage. 9° Ground rubber, rubber dust. 10° Dust or' coal, lignite, lignite coke and peat, artifi­ cially prepared (e.g. by pulverization or other processes), and coke from carbonized lignite rendered inert (i.e. not liable to spontaneous ignition). MNote: 1. Natural dusts obtained as .residues in the productioo ~f coal, coke, lignite or peat are not subject to the provisions of ADR. 2. Coke from carbonized lignite not rendered comple­ tely inert is not to be accepted for carriage. 11 ° (a) Crude naphthalene with a melting point below 1s 0 c· (b)' pure naphthalene and crude naphthalene with a melting point of 75°C or over; • (c) Naphthalene in the melted state. for (a) and (b), see also marginal 2401a. Naphthalene in balls offlakes [11 ° (a) and(~) is s ubje~t 2401a neither to the provisions for this Class contamed m this Annex nor to those contained in Annex B if it is packed, • not more than 1 kg per box, in tightly-closed fibreboard or wooden boxes and these boxes are enclosed, not more ·than 10 per case, inwooden cases. • 2. Provisions A. Packages 1. General conditions of packing ( 1) Packagings shall be so closed and arranged as lo 2402 prevent any loss of the contents. (2) The materials of which the packagings and their closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there­ with. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require­ ments of carriage. Solid substances shall be firmly secured in their packagings, and inner packagings shall be firmly secured in outer packagings. Unless otherwise specified in the section entitled «Packing of a single substance», inner packagings may be enclosed in outer packagings, either singly or in groups. (4) Cushioning materi~ls shall be suited to the nature of the contents; in particular, they must be absorbent when the contents are liquid or might exude liquid. 2. Packing of a single substance (1) Sulphur of 2° (a) sh,all be packed in stout in stout 2403 bags made of paper or of closely-woven jute. (2) Sulphur in the melted state, of 2° (b), may not be carried otherwise than in tanks. Celloidin (3°) shall be so packed as to prevent its desic- 2404 cation. (1) Celluloid in slabs, sheets, rods or tubes, and fabrics 2405 coated with nitrocellulose, ( 4°), shall be enclosed: (a) in firmly-closed wooden packagings, or • (b) in strong paper wrappings which shall be placed 1. in crates; or 2. between frames made of boards, the edges of the frames extending beyond the paper wrapping and the frames being bound together with iron bands; or 3. in wrappings of closely-woven fabric. (2) A package must not weigh more than: 75 kg in the case of celluloid in !!labs, sheets or tubes and of fabrics coated with nitrocellulose, if the outer packa­ ging is made of in fabrics conformity with (1) (b) 3; 120 kg in all other cases. Film celluloid in rolls and developed celluloid films (5°) 2406 shall be enclosed in wooden packagings or in fibreboard boxes. E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2197 (1) Celluloid waste and celluloid-film waste (6°) shall he enclosed in wooden packagings or in two· strong bags 111ade of coarse, closely woven jute canvas, the bags being fireproofed so as not to ignite even on contact with a flame and having strong and continuous seams, These bags shall be placed one inside the other; after filling, their openings shall be • separately and several times folded over and closely stitched so as to prevent any escape of the contents. However, celluloid waste may be packed in a single bag if the celluloid waste is first packed in strong packing paper or in a suitable plastics material and it is certified in the transport document that the celluloid waste does not contain any waste in the form of dust. (2) Packages having a raw-canvas or jute packaging must not weigh more than 40 kg in single packaging not more than 80 kg in double packaging. (3) For the particulars in the transport document, see marginal 2416(2). ( 1) Substances of 7°(a) shall be packed: (a) in wooden receptacles or in drums made of imperme­ able fibreboard; these receptacles and drums shall have a lining impermeable to the liquids they contain; their closures must be leak-proof: or (b) in bags impermeable to the vapours from the liquids they contain (e.g. bags made of rubber or of a suitable plastics material not readily inflammable), placed in a wooden case or in a metal receptacle; or (c) in zinc-lined or lead-lined iron drums; or (d) in receptacles made of tin-plate, zinc sheet or alumi­ nium sheet and secured by cushioning materials in wooden cases. (2) Nitrocellulose of 7°(a), if petted exclusively with water, may be packed in fibreboard drums; this fibreboard must have undergone a special treatment to render it completely impermeable; the closures of the drums shall be water-vapour proof. (3) Nitrocellulose of 7°(a), with added xylene, may not be packed otherwise than in metal receptacles. (4) Substances of 7"(b) and (c shall be packed: (a) in wooden packagings lined with stout paper or zinc sheet or aluminium sheet; or (b) in strong fibreboard drums or provided that the substances are dustfree and that this is certified in the transport document, in fibreboard cases which have been rendered impermeable; or (c) in sheet-metal packagings. (5) For substances of 7°, metal receptacles must be so constructed that, by reason of the method of assembly of their walls, of their mode of closure, or of the presence of a safety device, they yield when the internal pressure reaches a value not greater than 3 kg/cm2 ; the presence of these closures or safety devices must not impair the strength of the receptacle nor impair its closure. (6) A package must not weigh more than 75 kg or, if it can be rolled, not more than 300 kg; however, a fibre board drum must not weigh more than 75 kg and a fibrebo­ ard case not more than 35 kg. (7) For the particulars in the transport document, see marginal 2416(3). (1) Red phosphorus and phosphorus pentasulphide (8°) shall be packed: Item Description of No. substance 2"(a) Sulphur 7°(a) Weakly-nitrated nitrocellulose (such as collodion cotton) 8" Red (emorphous phosphorus) ' ·8" Phosphorus sesquisulphide 2407 2408 2409 (a) in receptacles made of sheet iron or tin-plate, which shall be placed in a strong wooden case; a package must not weigh more than l 00 kg; or (b) in receptacles made of glass or stoneware not less than 3 mm thick, or of a suitable plastics m~terial, each containing not more than ] 2.5 kg of substance. These receptacles shall be secured with cushioning materials in a strong wooden case; a package must not weigh more than l 00 kg; or (c) in metal receptacles which, if with their contents they weigh more than 200 kg, shall be fitted with reinfor­ cing hoops at their ends, and with rolling hoops. (2) Phosphorus sesquisulphide (8°) shall be packed in leak-proof metal receptacles, which shall be secured by cushioning materials in wooden cases wit~ closely-fitting sides. A package must not weigh more than 75 kg. Substances of 9° shall be packed in firmly-closing leak­ proof receptacles. (l) Substances of 10° shall be packed in metal or wooden receptacles or in strong bags. (2) Wooden receptacles and bags are not, however, to be accepted for coal dust, lignite dust or peat dust artifi­ cially prepared unless the dust has been completely cooled after drying by heat. 1 (3) For the particulars in the transport document, see marginal 2416(4). (1) Naphthalene of 11 °(a) shall be packed in firmly­ closed wooden or metal receptacles. (2) Naphthalene of 11 °(b) shall be packed in wooden or metal receptacles, or in stout fibreboard cases, or in strong bags made of textile or of four-ply paper or of a suitable plastics material. Where fibreboard cases are u·sed, a package must not weigh more than 30 kg. (3) Naphthalene in the melted state [11 °(c)] must not be carried otherwise than in tanks. 3. Mixed packing ·- •. ;,,r,, • (1) Substances grouped under the same item number may be included in the same package. The inner packa­ gings shall conform to what is prescribed for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. A package containing celluloid rods and tubes packed-toge­ ther in a textile wrapping must not weigh more than 75 kg. (2) If smaller quantities are not prescribed in the section entitled "Packing of a single substance", substances of this Class, in quantities not exceeding 6 kg for all of the substances listed under the same item number or the same letter, may be enclosed in the same package either with substances of another item number or of another letter of the same Class, or with dangerous substances belonging to other Classes (if mixed packing is likewise allowed in the case of such substances), or with other goods, subject to the following special conditions. The inner packagings must satisfy the general and spe­ cial conditions of packing. In addition, the general provi­ sions contained in marginals 2001 (5) and 2002 (6) and (7) must be observed. A package must not weigh more than 150 kg, or more than 75 kg if it contains fragile receptacles. Special conditions: 2410 2411 2412 2413 Maximum quantity per per Special provisions recentacle nacka!!e 5 kg 5 kg Must not be packed together with chlorates, permanganates, perchlora le~, or peroxides (other than solutions of hvdro!!:en neroxide) 100 g 1 kg Must not be packed together with substances of Classes 4.2 and 5.1 5 kg 5 kg Mixed packing not allowed 2198 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 4. Marking and danger labels on packages (see Appen­ dix A.9) (1) Packages containing substances of 4° to 8° shall bear a label conforming to model No. 28. However, if substances of 4° to 7° are packed in wrap­ pings made of closely ,woven fabric in accordance with marginal 2405 (1) (b) 3., in fibreboard boxes or cases in accordance with marginals 2406 and 2408 (4) (b), in jute bags in accordance with marginal 2407 (1) or in fibrebo­ ard drums in accordance with marginal 2408 (1) (a), (2) and 4 (b), the packages shall bear two labels conforming to model No. 28. (2) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9. If the fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampoules, bear labels conforming to model No. 8; • these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. (3) In the case of consignments carried as a full load, label No. 28 need not be affixed to the packages. B. Particulars in the transport document (1) The description of the goods in the transport document must conform to one of the names underlined in marginal 2401. Where the name of the substance is not indicated in the case of 1 °, the trade name must be used. The description of the goods must be underlined in red and followed by particulars of the Class, the item number (together with the letter, if any), and the initials "ADR" or "RID" [e.g. 4.1, 7° (a), ADR). (2) In the case of celluloid waste (6°) packed in stout packing paper or in a suitable plastics material and placed, so packed, in bags made of closely-woven raw canvas or jute, the following must be certified in the transport doc­ ument: "Contains no waste.in dust form". (3) In the case-of-su~t3nces of 7° (b) and (c) packed in fibreboard cases, the following must be certified in the transport document: "Substances free from dust". ( 4) In the case of coal dust, lignite dust or peat dust (10°) artificially prepared and packed in wooden receptac­ les or in bags [see marginal 2411(2)), the following must be certified in the transport document: "Substances com­ pletely cooled after drying by heat". Empty packagings No provisions.· CLASS 4.2 SUBSTANCES LIABLE TO SPONTANEOUS COMBUSTION 1. List of substances Among the substances and articles covered by the hea­ ding of Class 4.2 only those listed in marginal 2431 are to be accepted for carriage, and then only subject to the provisions of this Annex and of Annex B. These substances and articlC's to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. 1 ° White or yellow phosphorus. 2° Compounds of phosphorus with alkali metals or alka­ line-earth metals, e.g., sodium phosphide, calcium phos phide, strontium phosphide. . Note: Compounds of phosphorus with the so-called he­ avy metals, such as iron, copper, tin,· etc., but with the exception of zinc (zinc phosphide is a substance of Class 6.1 - see marginal 2601 33°), are not subject to the provisions of ADR. ~ 0 Zinc alkyls, magnesium alkyls, aluminium alkyls and hahdes and hydrides of aluminium alkyls. See also margi­ nal 2431a under (a). 4° Nitrocellulose-film waste, free from gelatine, in reels, sheets or strips. 2414 2415 2416 2417 2423 2424 2425 2429 2430 2431 Note: Nitrocellulose-film waste free from gelatine is not to be accepted for carriage if it is dusty or includes dust'y portions. 5° (a) Used rags and waste; (b) Greasy or oily fabrics, wicks, cord or thread; (c) The following greasy or oily substances: wool, hair (and horsehair), artificial wool, reclaimed wool (also called wool shoddy), cotton, recarded cotton, artificial fibres (rayon, etc.), silk, flax, hemp and jute, also in the form of spinning or weaving waste. For (a), (b) and (c), see also marginal 2431a under (b). Note: Wetted substances of 5° (b) and (c) are not to be accepted for carriage. • 6° (a) Dust and powder of aluminium or zinc and mixt­ ures of dust of powder of aluminium and zinc,;also when greasy or oily; powder of zirconium and titanium; dust from blast-furnace filters; (b) Dust, powder and fine shavings of magnesium and of magnesium alloys with a magnesium content of more than 80 per cent, all free from particles likely to promote ignition; (c) The following salts of dithionous (hydrosulphurous) acid (H 2 SO 4 ): dithionites (hydrosulphites) of sodium, po­ tassium, calcium and zinc; (d) Metals in a pyrophoric form. For (a), see also marginal 2431a under (b) and (c); for (b) and (c), see also marginal 243 la under (b). 7° Freshly calcined soot. See also marginal 2431a under (b). 8° Newly-quenched charcoal, powdered, granulated or in lumps. See also marginal 2431a under (b) and Class 4.1, marginal 2401, 1°. Note: By "newly-quenched charcoal" is meant: in the case of charcoal in lumps, charcoal which has been quenched less than four days previously; in the case of powdered charcoal and of granulated charcoal in a granule size of less than 8 mm, charcoal which has been quenched less than eight days previously and has been air-cooled in thin layers or by a process ensuring an equivalent degree of cooling. 9° Mixtures of granulated or porous combustible substances with constituents still liable to spontaneous oxidation, such as linseed oil or other natural drying oils, boiled or with added drying compounds, resin, resin oil, petroleum residues, etc. (e.g. the substance known as cork waste, lupuline), and oily residues from the bleaching of soya oil. See also marginal 2431a under (b) and Class 4.1, marginal 2401, 1°. 10° Paper, cardboard and products made of paper or cardboard (e.g. cardboard wrappings and cardboard rings), wood-fibre sheets, skein of thread, fabrics, string, thread, spinning or weaving wastes, are impregnated with oils, greases, natural drying oils, boiled or with added drying compounds or other impregnating substances liable to spontaneous oxidation. See also marginal 2431a under (b) and Class 4.1, marginal 2401, 1°. Note: Substances of 10° are not to be accepted for carriage if their humidity exceeds the hygroscopic humi­ dity. · 11 ° The substance wjth an iron oxide base having been used for purifying lighting gas (spent oxide of iron). Note: If the substance which has been used for purifying lighting gas (spent oxide of iron} is,· after storage and aeration, no longer liable to spontaneous ignition, and if this is certified in the transport document by the entry: "Substance not liable to spontaneous ignition", it is not subject to the provisions of ADR. 12° • Used yeast bags, uncleaned. See also marginal 2431a under (b). 13° Empty sodium nitrate bags made of a textile fabric. Note: Textile bags from which all the nitrate impregna­ ting them has been completely removed by washing are not subject to the provisions of ADR. E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2199 14° Empty iron drums, uncleaned, and empty tanks, uncleaned which have contained phosphorus of 1 °. 15° Ern'pty. receptacles, uncleaned, which have contai­ ned substances of 3°. Note: re 14° and 15°: Empty packagings which h~ve contained other. substances of Class 4.2 are not subJect to the provisions of ADR. . . . Dangerous substances hande~ ~ver for ca~age in ~on­ formity with the following prov1s1ons ~e s?bJec t neither to the provisions for this Class contained in this Annex nor to those. contained in AnnelC B: (a) solutions of substances of 3° i~ a con~~ntrati?n not exceeding 10 per cent in solvents with a boiling pomt not lower than 95°C, if their condition is such as to exclude any danger of spontaneous ignition and if "this is certified in the transport document by the entry: Substance not liable to spontaneous ignition"; see, however, Class 3; (b) substances of 5°- 10° and 12° (excluding, however, those of 6° (d)), if their ~ondition is such as to exc!ude any danger of spontaneous ignition and if this is certified in the transport document by the entry: "Substance not liable to spontaneous ignition"; for the substances of ~0 certain substances of 9° and 10°, however, see Class 4.1 marginal 2401, 1 °; (c) dust and powder of aluminium or zinc [6°(a)], e.g. packed together with varnish f?r use ~. the manufact~re of colours, if packed with care in quantities not exceeding 1 kg. 2. Provisions A. Packages 1. General conditions of packing 2431a (1) Packagings shall be so closed and arranged as to 2432 prevent any loss of the contents. . . (2) The materials of which the packagings and their closures are made, must not be liable to attack by the contents nor form harmful or dangerous compounds there­ with. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong 'in all their parts to prevent ~ny loosing during carriage and to meet the normal reqmre­ ments of carriage. In particular, in the case of substances in the liquid state of immersed in a liquid or in soluti?n, receptacles and their closures must, unless the section headed "Packing of a single substance or of articles of the same kind" provides otherwise, be able to withstand any pressure which, the pressure of air also b~ing taken into account, may arise inside the receptacles in normal carriage. For this purpose a free space must be left, ac­ count being taken of the difference between the temperat­ ure of the substances at the time of filling and the highest mean temperature which they are likely to reach . durin g carriage. Solid substances shall be firmly secured in theJr packagings, and inner packagings sh~ be fin nly s~cured in outer packagings. Unless ~therw1se specified m t~e section entitled "Packing of a single substance or of art11::a . les of the same kind", inner packagings may be enclosed in outer packagings, either singly or in groups. (4) Bottles and other glass receptacles- must be free from faults liable to impair their strength; in particular, internal stresses must have been suitably relieved. The thickness of the walls must be not less than 3 mm in the case of receptacles which, with their contents, weigh more than 35 kg, and not less than 2 mm in the case of other re­ ceptacles. The tightness of the closure system must. be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preventing any loosening of the closure system during carriage. (5) When receptacles made of glass, porcelain, stone­ wave of similar materials are prescribed or allowed, they must be secured by cushioning materials in protective pac­ kagings. Cushioning materials shall be suited to the nature of the··contents; in particular, they shall be dry and absorbent when the content are liquid or might exude liquid. 2. Packing of a single substance or of articles of the same kind ( 1) Phosphorus of 1 ° shall be packed: (a) in leak-proof tin-plate receptacles hermetically clo sed and placed in wooden cases; or • (b) in sheet-iron drums closing hermetically. Press-on lids shall not be allowed. The sheet-iron constituting the body, bottom and lid shall not be less than 1.5 mm thick. A package must not weigh more than 500 kg. If it weighs more than 100 kg, it shall be fitted with rolling hoops or strengthening ribs, and shall be welded; or (c) not more than 250 g per receptacle, in hermetically­ closed glass receptacles secured by cushioning materials in leak-proof tin-plate receptacles closed by soldering and secured, likewise by cushioning materials, in wooden ca­ ses. (2) Receptacles and drums containing phosphorus shall be filled with water. (2) Receptacles and drums containing phosphorus shall be filled with water. (1) Substances of 2° shall:be packed in leak-proof tin­ plate receptacles hermetically closed and placed in wooden cases. (2) Substances of 2° may also be packed, not more than 2 kg per receptacle, in receptacles made of glass, porcelain, stonew !lre or similar materials, secured by cush­ ioning materials in wooden cases. (1) Substances of 3° shall be packed in receptacles made either of metal or of glass, porcelain, stoneware or similar materials, hermetically closed. Receptacles must not be filled beyond 90 per cent of their capacity. • • (2) Metal receptacles shall be secured by cushioning materials in protective packagings which, if they are not · closed, shall l}e covered. If the covering consists of readily-· inflammable substances, it shall be rendered sufficiently fire-resistant to prevent its catching alight in coilt~ct with· a flame. If the protective packaging is not • cl6sed, the· package shall be fitted with means of handling natl shall • • not weigh more than 7 5 kg. • (3) Receptacles made of glass, porcelain, stoneware or similar materials shall have a capacity of not more than 5 litres and shall be secured by cushioning materials in leak-proof sheet-metal receptacles hermetically closed. ( 4) Substances of 3° may also be packed in hermetically- • closed drums made of corrosion-resistant steel and having a capacity of not more than 300 litres and a wall thickness of not less than 3 mm. The drums must withstand a test pressure of 10 kg/cm2 and satisfy the conditions of marginal 2211 (1) and (2) (b). The closure of the filling and em­ ptying device must be ensured by a protective cap. Recep­ tacles must not be filled beyond 90 per cent of their capacity; however, with the liquid at a mean temperature of 50 ° C, a free space of 5 per cent must remain for safety purposes. When handed over for carriage, the liquid must be under a layer of inert gas at a pressure not exceeding 0.5 kg/cm2 • Receptacles shall be tested in. conformity with the provisions of marginal 2216 (2) and (3). The tests shall be repeated every 5 years. The recep­ tacles shall bear the following particulars in clearly legible and indelible characters: 1. the name of the substance in full, the name or mark of the maker or owner, and the number of the receptacle; 2. the tare of the receptacle, including fittings and ac­ cessories; 3. the test pressure, the date (month, year) of the last test undergone, and the stamp of the expert who carried out the tests and inspections; 4. the capacity of the receptacle and the maximum filling allowed; 5. the wording: «Do not open during carriage; liable to spontaneous ignition». A package must not weigh more than 400 kg. (1) Substances of 4° shall be packed in bags plac~d in drums made of impermeable fibreboard or in receptacles 2433 2434 2435. 2436 2200 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) made of zinc sheet or aluminium sheet: The sides of metal receptacles shail be lined with fibreboard. The bottoms and lids of fibreboard drums and metal receptacles shall be lined with. wood. (2) Metal receptacles shall be fitted with closures or. safety devices yielding when the internal pressure reaches a value not greater than 3 kg/cm2; the presence of these closures or safety devices must impair the strength of the receptacle nor impair its closure. (3) A package must not weigh more than 75 kg. (1) Substances of 5° (a) shall be tightly compressed and be placed in leak-proof metal receptacles. (2) Substances of 5° (b) and (c) shall be tightly compres­ sed and be packed either in wooden or fibreboard cases or in paper or textile wrappings firmly secured. (1) Substances of 60 (a) shall be enclosed in tightly­ closing leak-proof receptacles made of wood or metal. However, zirconium shall be enclosed only in metal or glass receptacles, which shall be secured by cushioning materials in strong wooden cases. If the cushioning mate­ rials are inflammable, they shall be fireproofed. (2) Substances of 60 (b) shall be enclosed in tightly­ closing leak-proof iron drums or in wooden cases with a sheet-metal lining rendered leak-proof (by soldering, for example) or in boxes made of tin-plate or thin aluminium sheet and so closing as to be leak-proof; these drums, cases or boxes shall be placed in wooden cases. For substances of 60 (b) handed over individually for carriage in boxes made of tin-plate or aluminium sheet, a wrapping of corrugated fibreboard will suffice instead of a w@oden case; a package of this nature must not weigh more than 12 kg. (3) Substances of 60 (c) shall be packed in air-tight sheet-metal receptacles or air-tight iron drums. In the case of sheet-metal receptacles, a package must not weigh more than 50 kg.· , .. ,,. (4) Substances of 60 (d) shall be packed in receptacles made of metal, glass or a suitable plastics material and so closing as to be gas-tight. The stoppers used for closure shall be held in position by an additional device (such as a cap, crown, seal or binding) capable of preventin~ any loosening during carriage. The substances shall be dispat­ ched under a protective liquid (such as. methanol) or a protective gas. Description of Item No. substance lo White or yellow phosphorus 2o Phosphides 3o Zinc alkyls, etc. 60 (a) (b) and (d) Dust and powder of aluminium or zinc Dust, powder and fine shavings of magnesium . Metals in a pyrophoric form 4o, So, 60 (c) all substances 7o - 120 2437 2438 Metal receptacles shall be placed in a wooden packing case. A package must not weigh more than 50 kg. Glass receptacles shall be secured by cushioning mate­ rials in fibreboard or metal packagings; the cushioning materials must be incombustible. Receptacles made of a plastics material shall be placed in fibreboard or metal packagings. Packagings containing receptacles made of glass or a· plastics material shall be placed in a wooden packing case. A package must not weigh more than 25 kg. Substances of 7o - l0o and 120 shall be enclosed in 2439 tightly-closing packages. Wooden packagings used for substances of 7 o and 80 shall be provided with a leak-proof lining. The substance having been used for purifying lighting · 2440 gas (spent oxide of iron) (l lo) shall be packed in tightly closing sheet-metal receptacles. Empty sodium nitrate bags (130) shall be made up into 2441 tightly-packed bundles securely fastened· with string and placed either in a wooden case or in a wrapping consisting either of several thicknesses of stout paper or of waterproo fed fabric. 3. Mixed packing (1) Substances grouped under the same item number 2442 may be included in the same package. The inner packa gings shall conform to conform to what is prescribed for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. (2) If smaller quantities are not prescribed in the section entitled «Packing of a single substance or of articles of the same kind substances of this Class, in quantities not exceeding 6 kg in the case solids or 3 litres in the case of liquids for all of the substances listed under the same item number or the same letter, may be enclosed in the same package either with substances of another item number or of another letter of the same Class, or with dan­ gerous substances delonging to other Classes (if mixed packing is likewise allowed in the case of such substances), or with other goods, subject to the following special condi­ tions. . The in~~r packagin~ must satisfy the general and spe­ cial condillons of packmg. In addition, the general provi­ sions of marginal 2001 (5) and 2002 (6) and (7) must be observed. A package must not weigh more than 150 kg, or more than 7 5 kg if it contains fragile receptacles. . Special conditions: . Maximum quantity Special per receptacle per package nrovision" Mixed packing not allowed 3 kg 3 kg Must not be packed loge ther with weakly•nitrated nitrocellulose and red phosphorus of Class 4.1, nor with bifluorides • ECl>HMEPII: THI: KYBEPNHIEQI: (TEYXOI nPQTO) 2201 4. Marking and danger labels on packages (See Appendix A.9) (1) Packages containing substances of lo to 4o oro6o shall bear a label conforming to model No. 2C. However, if substances of 4o are packed in drums made of impermeable fibreboard in conformity with marginal 2436 (1), the packages, shall bear two labels conforming to model No. 2C. (2) Drums containing phosphorus of lo and having a screw-cap lid shall, unless they are fitted with a device maintaining them upright, bear in addition, high up in two diametrically opposite places, two labels conforming to model No. 8. \ (3) Packages containing fragile receptacles not visible from the outside shall bear labels conforming to model No. 9. If the fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampoules, bear labels conforming to model No. 8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. (4) In the case of consignments carried as a full load, label No. 2C as prescribed under (1), need not be affixed to the packages if the vehicle bears the. marking prescribed in Annex B, marginal 10500. B. Particulars in the transport document The description of the goods in the transport document must conform to one of the names underlined in marginal 2431. Where the name of the substance is not indicated in the case of 2 °, 3 °, 9° and 10°, the trade name must be used. The description of the goods must be underlined in red and followed by particulars of the Class, the item number (together with the .letter, if any), and the initials «ADR» or •RID» [e.g. 4.2,5 ° (a), ADR]. C. Empty packagings {l) Heceptacles and tanks of 140 and receptacles of 150 must be closed in the same manner and leak-proof in the same degree as though they were full. (2) The description in the transport document must be: «Empty receptacle (or empty tank), 4.2, 140 (or 150), ADR (or RID)». This description must be underlined in red. • CLASS 4.3 SUBSTANCES WHICH GIVE OFF INFLAMMABLE GASES ON CONTACT CT WITH WATER 1. List of substances Among the substances and articles covered by the hea­ ding of Class 4.3 only those listed in marginal 24 71 are to be accepted for carriage, and then only subject to the provisions of this Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considerer as substances and articles of DR. 1 ° (a) Alkali and alkaline-earth metals, e.g. sodium, potassium, calcium, as well as alkali metal alloys, alkaline~ earth metal alloys and alloys of alkali and alkaline-earth metals; (b) alkali-metal amalgams and alkaline-earth metal amalgams; (c) alkali-metal <!lspersions. 2° (a) Calcium carbide and aluminium carbide (b) alkali-metal and alkaline-earth metal hydrides (e.g. lithium hydride, calcium hydride), mixed hydrides, and boron hydrides and aluminium hydrides of alkali metals and alkaline-earth metals; ( c) alkali silicides; (d) calcium silidde; in powder, grains or lumps, contai­ ning more than 50 per cent silicon, manganese calcium silicide (silicomanganese-calcium); (e) alloys of magnesium with manganese. 3° Amides of alkali metals and alkaline-earth metals, 2443 2444 2445 2446 2452 2453 2454. 2469 2470 24'V e.g. sodamide (sodium amide). See al~o marginal 24 7 la. Note: Calcium cyanamide is not subject to the provisions of DR. • 4° Trichlorosilane· (silicochloroform). 5° Empty receptacles, uncleaned, and empty tanks, uncleaned, which have contained substances of Class 4.3. Sodamid~ (3°) in quantities not exceeding 200 g per 2471a package is not subject to the provisions for this Class contained in this Annex or in Annex B if it is packed in receptacles which are so closed as to be leak-proof and which cannot be attacked by the contents, and if these receptacles are packed with care in a strong, leak-proof wooden packaging with a leak-proof closure. 2. Provisions A. Packages 1. General conditions of packing (1) Packagings shall be so closed and leak-proof as to 2472 prevent the ingress of moisture and any Joss of the conte ntes. (2) The materials of which the receptacles and their closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there­ with. Receptacles must in all cases be free from moisture. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent any . loosening during carriage and to meet the normal require­ ments of carriage. In particular, in the case of solids immersed in a liquid, receptacles and their closures must, unless the section headed •Packing of a single substance» provides otherwise, be able to withstand any pressure which, the presence of air also being taken into account, may arise inside the receptacles in normal carriage: For· this purpose a free space must be left, account being taken of the difference between ~he temperature of.the substan­ ces at the time of filling and the highest mean temperature which they are likely to reach . during carriage. Solid substances shall be firmly secured in their packagings; and inner packagings shall be firmly secured in outer pac kagings. • Unless otherwise specified in the section entitled «Pac­ king of a single substance», inner packagings may be enclosed in outer packagings, either singly or in groups. ( 4) Bottles and other glass receptacles must be free . from faults liable to impair their strength; in particular, internal stresses must have been suitably relieved. The thickness of the walls must in no case be less than 2 mm. The tightness of the closure system must be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preventing any loosening of the closure system during carriage. 35) Cushioning materials shall be suited to the nature of the contents. 2. Packing of a single substance (1) Substances of lo shall be packed: 2473 (a) in receptacles made of sheet-iron, lead-lined sheet iron or tin-plate. For substances of lo (b), however, recep tacles made of lead-lined sheet-iron or of tin-plate are not to be accepted. These receptacles, with the exception of iron drums, must be placed in wooden packing cases or in protective iron hampers; or • (b) not more than 1 kg per receptacle, in receptacles made of glass or stoneware. Not more than 5 of these receptacles shall be packed in a wooden packing case having a leak-proof lining of ordinary sheet-iron, lead­ lined sheet-iron, or tin-plate, assembled by soldering. For glass receptacles containing quantities not exceeding 250 g, the lined wooden case may be replaced by an outer receptacle made of ordinary sheet-iron, lead-lined sheet­ iron, or tin-plate. Glass receptacles shall be secured in the outer packagings by incombustible cushioning mate rials. • (2) If a substance of lo (a) in not packed in a welded metal receptacle with a lid hermetically closed by • solde­ ring, then: i202. .!:'.E..:::::<l>.!...!H"-!M..:..:E~P-'.:II:=--=-T.!...!Hc-=r,...:.K., ,Yc..::B=..=E:.:...P..:...:N:.:...H=r=E=Q=I:'--'( ;: T=EY.:...:Xc..::.O=r-=-n:.:...P~Qe....:T~O:.L..) • (a) it must be completely covered by mineral oil whose flash-point is above 50° C, or-be sufficiently sprinkled to ensure that the lumps are coated with this oil; or • (b) the air in the receptacle must be completely replaced by a protective gas (e.g. nitrogen) and the receptacle so closed as to be gas-tight; or (c) the substance must be poured into the receptacle, which must be filled to the brim and so closed, after cooling, as to be gas-tight. (3) Iron receptacles must have sides not less than 1.25 mm thick. If, with their contents, they weigh more than 75 kg, they must be hard-soldered or welded. If they weigh more than 125 kg, they must in addition be fitted with end and rolling hoops or with rolling flanges. (1) Substances of2o shall be packed: (a) in receptacles made of sheet-iron, lead-lined sheet­ iron or tin-plate. For substances of 2o (b) and (c) a recep­ tacle must not contain more than 10 kg. Those receptacles, with the exception of iron drums, must be placed in wooden packing cases or in protective iron hampers; or (b) not more than 1 kg per receptacle, in· receptacles made of glass or stoneware or of a suitable plastics mate­ rial. Not more than 5 of these receptacles shall be packed in a wooden packing case with a leak-proof lining of ordi­ nary sheet-iron, lead-lined sheet-iron or tin-plate, assem­ bled by soldering. For glass receptacles containing quanti­ ties not exceeding 250 g, the. lined wooden case may be replaced by an outer receptacle made of ordinary sheet­ iron, lead-lined sheet-iron or tin-plate. Glass receptacles shall be secured in the packing cases by incombustible cuchioning materials. (2) A package must not weigh mor than 75 kg if it contains substances of 2° (b) or (c) and not more than 125 kg if it contains substances of 2° (d) or (e). Amides (3°) shall be packed, not more than 10 kg per box or drum, in hermetically-closed metal boxes or drums which shall be placed· in wooden cases. A package mus; not weigh more than 75 kg; (1) Trichlorosilane (4°) must be packed in receptacles made of corrosion-resistant steel and having a capacity Item No. • 1 Description of substance l 0(a) 2°(a) 2°(b) I Alakli and alkaline - earth metals (e.g. sodium, po­ tassium, calcium, barium in fragile receptacles in other receptacles Calcium carbide Alkali metal and alkaline earth metal hydrides (e.g. lithium hydride, calcium hydride), mixed hydrides, boron hydrides and alumi­ nium hydrides in fragile receptacles in other receptacles Trichlorosilane 2474 2475 2476 not exceeding 500 li1res. The receptacles must be hermeti­ cally closed; the closing device must be specially protected by a cap. The receptacles must be constructed as pressure vessels for a working pressure of 4 kg/ cm2 and be tested in conformity with the regulations governing pressure ves­ sels in force in the c ountry of departure. Receptacles with a capacity not exceeding 250 litres must have a wall thickness of not less than 2.5 mm, and those with a higher capacity a wall thickness of not less than 3 mm. (2) If filling is based on weight, the degree of filling must not exceed 1.14 kgjl. If it is carried out by visual check, the degree of filling.shall not exceed 84.5 per cent. 3. Mixed packing (1) The substances grouped under the same item number may be included in the same package. The inner packagings shall conform to what is prescribed for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. • (2) If smaller quantities are not prescribed in the section entitled «Packing of a single substance•, substances of this Class, in quantities not exceeding 6 kg in the case of solids or 3 litres in the case of liquids for all of the substances listed under the same item number or the same letter, may be enclosed in the same package either with substan­ ces of another item number or of another letter of the same Class, or with dangerous substances belonging to other Classes (if mixed packing is likewise permitted in the case of such substances), or with other goods, subject to the following special conditions. Class 4.3 . The in~~r packagings must satisfy the general and s c!al cond11I~ns of packing. In addition, the general pr~­ s1ons contained in marginals 2001(5) and 2002(6) and (7) must be observed. A packag~ 1!1ust not weigh more than 150 kg, or more than 75 kg if it contains fragile receptacles. Special conditions: Maximum quantity Special provisions per per receptacle package 500 g 1 kg 500 g 1 kg Mixed packing not allowed 500 g 1 kg 500 g 1 kg Mixed packing not allowed The limits of 500 g or 1 kg apply to alkali metals and alkaline - earth me . tals of 1 °(a), and to alkali metal and alkaline - earth metal hydrides of 2°(b), in respect of the aggregate weight of these substances. Alkali metals and alkaline ea,th metals, and su­ bstances of 2 ° (b), may not be packed together with acids, nor with liquids co­ ntainign water. • 2477 2477 <l>EK 225 E<J>HMEPl:r TH:r KYBEPNHrEQr (TEYXO:r nPQTO) 2203 4. Marking and danger labels on packages (see Appendi~ A.9) (1) Every package containing substances of Class 4.3 24 78 shall bear a label of model No. 20 and a label conforming to model No. 7. (2) Every package containing trichlorosilane of 4° shall bear in add'ition a label conforming to model No. 2A. (3) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9. If the fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampou­ les, bear labels conforming to model No.8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. B. Particulars in the transport document 2479 The description of the goods in the transport document 2480 must conform to one of the names underlined in marginal 24 71. Where the name of the substance is not indicated in the case of 1 •, the trade name must be used. The description ·of the goods must be underlined in red and followed by particulars of the Class, the itein number (together with the letter, if any), and the initials «ADR• or «RID» [e.g.4.3 2°(a), ADR]. C. Empty packagings 2481 2497 (1) Receptacles and tanks of So must be closed in same 2498 manner and be leak-proof in the same degree·as though they were full. (2) The description in the transport document must be: «Empty rece·ptacle (or empty tank), 4.3. 5°, ADR (or RID)». This·descpription must be underlined in red. CLASS 5.1 OXIDIZING SUBSTANCES 1. List of substances 2499 Among the substances and articles coverd by the hea- 2500 ding of Class 5.1, those listed in marginal 2501 are subject to the provisions of this Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considered a' substan ces and articles of ADR. Note: Unless specifically listed in class la or Class Le, mixtures of oxidizing substances with combustible sustan­ ces are not to be accepted for carriage if they are capable of exploding on contact with a flame or are more sensitive to shock and to friction than dinitrobenzene. lo Stabilized, aqueous solutions of hydrogen peroxide containing more than 60 per cent hydrogen peroxide, and stabilized hydrogen peroxide. Note: 1. For aqueous solutions of hydrogen peroxide co­ ntaining not more than 60 per cent hudrogen peroxide, see marginal 2801, 41°. 2. Aqueous solutions of hydrogen peroxide containing more than 60 per cent hydrogen peroxide, not stabilized, and hydrogen peroxide, not stabilized, are not to be accep­ ted for carriage. 2o Totranitromethane, free from combustible impuri­ ties. Note: Tetranitromethane not free from combustible imp­ urities is not to be accepted for carriage. 3° Perchloric acid in aqueous solutions containing more than 50 per cent but not more than 72,5 per cent perchlo­ ric acid (HC10) 4 • See also marginal 2501a, under (a). Note: Perchloric acid in aqueous solutions containing not more than 50 per cent perchloric acid (HC10) 4 in a substance of Class 8 (see marginal 2801, 4°). Aqueous solutions of perchloric acid containing more than 72.5 per cent perchloric acid are not to be accepted for car­ riage; the same applies to mixtures of perchloric acid with any liquid other than water. 4o (a) Chlorates; inorganic chlorate weed - killers con­ sisting of mixtures .of sodium chlorate, potassium chlorate of calcium chlorate with a hygroscopic chloride (such as magnesium chloride or calcium chloride); Note: Ammonium chlorate is not to be accepted for car­ riage. (b) perchlorates (with the exception of ammonium perchlo­ rate, see 5°) (c) sodium and potassium chforites; (d) mixtures of chlorates perchlorates and chlorites of (a), (b) and (c) with one another. For (a), (b), (c) and (d), see also marginal 2501a, under (b). 5° Ammonium perchlorat~. See also marginal 2501a, under (b). 6° (a) Ammonium nitrate not containing combustible substances in a higher proportion than 0.4 per cent; Note: Ammonium nitrate containing more• than 0.4 per cent combustible substances is not. to be accepted for carriage unless it is a constituent of an explosive of 12° or 140 of marginal 2101. (b) mixtures of ammonium nitrate with ammonium sulphate or ammonium phosphate containing more than 40 per cent nitrate but not more than 0.4 per cent combu­ stible substances;. , ( c) mixtures of ammonium nitrate with an inert substance· (e.g. infusorial earth, calcium carbonate, potassiumchlo­ ride) containing more than 65 per cent nitrate but not more than 0.4 per cent combustible substances. For (a), (b), see also marginal 2501a, under (b). Note: 1. Mixtures of ammonium nitrate with ammonium sulphate or ammonium phosphate containing not more than 40 per cent nitrate, and mixtures of: ammonium nitrate with an inert inorganic substance containing not more than 65 per cent nitrate, are not subject to the provisions of ADR. 2. In the mixtures referred to under (c), only inorganic substances which are neither combustible .not, oxidizing may be considered as inert.· • .,..-,", 3. Compound fortilizers in which the total content of nitrogen as nitrate and as ammonia does not exceed 14 per cent or in which the nitrogen content as nitrate does not exceed 7 per cent are not subject to the prosivions of ADR. 7° (a) Sodium nitrate; (b) mixturen of ammonium nitrate with nitrates of sodium, potassium, calcium or magnesium; (c) barium nitrate, lead nitrate. For (a), (b) and (c), see also marginal 2501a, under (b). Note: 1. If they do not contain more than 10 per cent ammonium nitrate, mixtures of ammonium nitrate with calcium nitrate or with magnesium nitrate or with both are not subject to the provisions of ADR. 2. Empty textile bags which have contained sodium nitrate and have not been entirely freed from the nitrate impregnating them are articles of Class 4.3 (see marginal 2431, 13°). 8° Inorganic nitrites. See also marginal 2501a, under (b). Note: Ammonium nitrite and mixtures of an inorganic nitrite with an ammonium salt are not to be accepted for carriage. • 9° (a) Peroxides of alkali metals and mixtures contai­ ning peroxides of alkali metals which are not more dange­ rous than sodium peroxide; (b) dioxides and other peroxides of alkaline - earth metals, e.g. barium dioxide; (c) permanganates of sodium, potassium, calcium and ba rium. • For (a), (b) and (c), see also marginal 2501a, under (b). Note: Ammonium permanganate, and mixtures of a per­ manganate with an ammonium salt, are not to be accepted for carriage. 10° Chromium trioxide (chromic anhydride; also called chromic acid). See also marginal 2501a, under (b). 11 ° Empty packagings, uncleaned, and empty timks, uncleaned, which have contained substances of Class 5.1. 2501 2204 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Note: Empty packagings and empty tanks. whi\:h have 'contained a chlorate, a perchlorate, a chlorite (4° and 5 "), an inorganic nitrite (8°) or substances of 9° ~nd 10°, with residues from their previous contents adhering to the ou­ tside, are not to be accepted for carriage. Class 5.1 Substances handed over for carriage in conformity wit~ the following provisions are subject neither to the provi­ sions for this Class contained in this Annex nor to those contained in Annex B. (a) substances of 3o, in quantities not exceeding 2~0 g per receptacle, on condition that they are . packed in receptacles so closed as to be leak-proof and not capable of being attacked by the contents, and that receptacles are packed, not more than 10 per case, in a wooden case with inert absorbent cushioning materials; (b) substances of 4°-10°, in quantities not exceedi~g 1 0 kg, packed not more than 2 kg per receptacle in receptacles so closed as to be leak-proof and not Cll1)a ble of being attacked by the contents, these receptacles being • enclosed in strong, leak - proof packagings made of wood or sheet - metal and having leak - proof closures. 2. Provisions . A. Packages 1. General conditions of pagking (1) Receptacles shall be so closed and arranged as to prevent any loss of the contents. (2) The materials of which the packagings and their closures are made must not be liable to attack by the contents, or cause the contents to decompose, . or form harmful or dangerous compounds therewith. (3) Packagings, including their closures, must be suffi­ ciently rigid and storng in all their parts lo prevent any loosening during carriage and lo meet the normal require­ ments of carriage. In particular, where substances are in the liquid stale, receptacles and their closures must, unless the section headed «Packing of a single substance» pr~~ides otherwise, be able lo withstand any pressure which, the presence of air also being taken into account, may arise inside the receptacles in normal carriage. For this purpose a free space must be left, account being taken of the difference between the temperature of the substan­ ces at the time of filling and the highest mean temperature which they are likely to reach during carriage. Unless otherwise specified in the section entitled «Packing of a single substance», inner packagings may be enclosed in outer packagings, either singly or in groups. (-4) Bottles and other flass receptacles mu~t be free from faults liable to impair their strength, in particular, internal .stresses must have been suitably relieved. The walls must be not less than 3 mm thick in the case of receptacles weighing, with their contents, more than 35 kg and not less than 2 mm in the case of other receptacles. The tightn·ess of the· closure system must be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preventing any loosening of the closure system during carriage. (5) When receptacles made of glass, porcelain, stone­ ware or similar materials are prescribed or allowed, they must be secured by cushioning materials in protective packagings, Gushioning materials must be incombustible (asbestos, glass wool, absorbent earth, infusorial earth, etc.) and incapable of forming dangerous compounds with the contents of the receptacles. If the contents are liquid, the cushioning materials shall also be absorbent and pro­ portionate in quantity lo the volume of the liquid; this interior absorbent layer must not, however, be less than 4 cm thick al any point. lacking of a single substance ( 1) Aqueous solutions of hydrogen peroxide, and hydro­ gen peroxide of lo, shall be packed in drums or other 2501a 2502 2502 2503 · receptacles· made of aluminium of al least 99.5 per cent purity or of special steel not liable to cause the hydrogen peroxide to decompose. These receptacles ~hall be fitt~d with means of handling; they must be a!Jle to remain upright in a stable fashion and must:. . . (a) be fitted in their upper part with a closin? device ensuring equality of the internal and the atmospenc press­ ure; this closing device must in all circumstanc~s prevent any escape of the liquid and any entry of foreign matter into the receptacle and must be protected by a vented cap; or (b) be able to withstand an internal pressure of 2.5 kg/cm? and be fitted in the ~pper part with a s~fety devic~ yielding when the excess of internal pressure IS 1 kg/ cm at most. (2) Receptacles shall not be filled beyond 90 per cent of their capacity. (3) A package must not weigh more than 90 kg. Tetranitromethane (2o) shall be contained in bottles made of glass, porcelain, stonewa~e ~r similar ~aterials or of a suitable plastics material, with incombusl!ble stop­ pers, placed inside a wooden case with complete sides; fragile receptacles shall be secured therein by absorbent earth cushioning. Receptacles shall not be filled beyond 93 per cent of their capacity. Perchloric acid in aqueous solutions (3o) shall be co­ ntained in glass receptacles, which shall be filled to not more than 93 per cent of their capacity. The receptacles shall be secured by absorbent and incombustible cushio­ ning materials in incombustible protective packagings im­ permeable to liquids and capable of retaining the contents of the receptacles. The closure of the receptacles shall be protected by caps if the protective packagings are not completely closed. Glass bottles closed by glass stoppers may also be secured by absorbent and incombustible cushioning mate­ rials in wooden cases with complete sides. Packages containing fragile receptacles and carried otherwise than as a full load must not weigh more than 7 5 kg and shall be fitted with means of handling. ( 1) Substances of 4° and 5° and solutions of substani::es of 4° shall be packed in receptacles made of glass, of a suitable plastics material, or of metal; solid substances of 4 ° (b) may also be enclosed in hardwood casks. (2) Fragile receptacles and receptacles made of a plas­ tics material must be secured by cushioning materials in wooden or metal protective packagings. They may also be secured separately by incombustible cushioning materials in non-fragile intormediate receptacles which must in, turn . be firmly placed or secured by cushioning materials in protective packagings. Each receptacle must contain not more than 5 kg of substance. In the case of receptacles whose contents are liquid, the cushioning materials must be absorbent. (3) In the case of receptacles made of a plastics material and containing solutions of substances of 4o, the protec­ tive packagings may be dispensed with if the walls are not less than 4 mm thick at every point, the walls are stren­ gthened by strong reinforcing rims, the ends are strengthe­ ned, the upper part is provided with two strong handholds, and the opening is fitted with a screw-threaded closure. (4) Receptacles for liquids shall not be filled beyond 95 per i;el)t of their capacity. • • (5) Packages containing fragile receptacles or receptac­ les made of a plastics material [see (2) and (3)], if they contain liquids, and packages containing fragile receptac­ les or receptacles made of a plastical material [see (2)], if they contain only solid substances and are carried other­ wise than as a full load, must not weigh more than 75 kg. Packages carried otherwise than as a full load shall be fitted with means of handling. (6) Packages which can be rolled must not weigh more than 400 kg; if they weigh more than 275 kg they shall be fitted with rolling hoops. (7) Receptacles containing solid chlorales other than those referred to under (8) must not contain any combu­ stible material other than a small pad of waxed paper. 2504 2505 2506 2506 E<J>HMEPII TH:[ KYBEPNHIEQI (TEYXOI nPQTO) 2205 (8) If the chlorate is in the form of tablets, with or without a suitable binder, and is packed in bottles contai­ ning not more than 200 g, a sufficient quantity of c~tton wool may be used to prevent excessive no ement of the tablets in the bottle. The bottles shall be packed in fitrebo­ ard boxes placed in an intermediate packaging separate from the outer packaging. An intermediate packaging may not contain more than 1 kg or a package more than 6 kg of chlorate. (1) Substances of 6°, 7°, and 8° shall be packed: (a) in drums or cases; or ' (b) in strong bags made of closely - woven fabric or of stout paper of at least five plies or, in quantities not exceeding 50 kg, in bags made of a suitable plastics material sufficiently thick and strong to prevent any loss of the contents. If the substance is more hygroscopic than sodium nit­ rate, bags made of closely - woven fabric or of stout paper of five plies must be lined with a suitable plastics material or be rendered impermeable by suitable means. Packages which can be rolled must not weigh more than 400 kg; if they weigh more than 275 kg they shall be fitted with rolling hoops. (1) Substances of 9° (a) shall be packed: (a) in steel drums; or (b) in receptacles made of sheet-metal, lead-lined sheet­ iron, or t!n?late, secured in wooden packing cases having a metal lmmg rendered leak-proof, e.g. by soldering. When carried as a full load, substances of 9°(a) may be packed in tin-plate receptacles placed solely in protec­ tive iron hampers. (2) Receptacles containing substances of 9°(a) must be so closed and leak-proof as to prevent moisture from ente­ ring. (3) Substances of 9°(b) and (c) shall be packed: (a) in incombustible receptacles fitted with an incombu­ stible h~rmetic closure. If the incombustible receptacles are fragile, each shall be secured separately by cushioning materials in a wooden case lined with stout paper; or (b) in hardwood casks with closely-fitting stave, lined with stout paper. (4) Packages containing fragile receptacles and carried otherwise than as a full load must not weigh more than 7 5 kg and shall be fitted with. means of handling. Packages capable or rolling must not weigh more than 2508 400 kg; they must be fitted with rolling hoops if they weigh more than 275 kg. (1) Chromium trioxide (10°) shall be packed; 2509 (a) in receptacles made of glass, porcelain, stoneware or similar materials, tightly stoppered, and ~ecured in a wooden case by inert and absorbent cushioning materials; or (b) in metal drums. (2) Packages containing fragile receptacles carried otherwise than as a full load must not weigh more than 7 5 kg and shall be fitted with means of handling. Packages capable of rolling must not weigh more than 400 kg; they must be fitted with rolling hoops if they weigh more than 275 kg. 3. Mixed packing ( 1) Substances grouped under the same letter may be 2510 included in the same package. The inner packagings shall conform to what is prescribed for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. (2) If smaller quantities are not prescribed in the section entitled «Packing of a single substance», substances of this Class, in quantities not exceeding 6 kg in the case of solids or 3 litres in the case of liquids for all of the substances listed under the same item number or the same letter may be enclosed in the same package either with substan: ces of another item number or of another letter of the same Class, or with dangerous substances belonging to other classes (if mixed packing is likewise allowed in the case of such substances), or with other goods, subject to the following special conditions. Class 5.1 The inner packaging must satisfy the general and spe- 2510 cial conditions of packing. In addition, the general provi sions of marginals 2001 (5) and 2002 (6) and (7)) must be observed. ' . A package must not weigh more than 150 kg, or more than 75 kg if it contains fragile receptacles. Special conditions: Maximum quantity Item No. lo 2o 3o 4o 4o(a) Description of substance Hydrogen peroxide and aqueous solutions of hydro­ gen peroxide containing more than 60% hydrogen peroxide. Tetranitromethane Perchloric acid Solutions of substances of 4o Chlorates in fragile receptacles in other receptacles per receptacle Mixed packing 1 kg 5 kg per package not allowed. 2.75 kg 5 kg Special provisions Must not be packed together with weaklynitrated nitrocellulose, red phosphorus, bifluorides, liquid halogenated irritants, hydroch­ loric acid, sulphuric acid, chlorosulphonic acid, . acetic acid, benzoic acid, salicylic acid, formic acid, nitric acid, free sulphonic acids, mixed nit­ rating acids, sulphur, hydrazine. Must be separa­ ted from uncombined carbon .. 2206 E<l>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) · (•' \I Maximum quan.tity Item Description per No. of substance receptacle .... 4o(b) Perchlorates 5 kg and So 4o(c) All substances and 6o,7o, 80 9o(a) Peroxides and -in fragile (b) receptacles 500 g in other receptacles 5 kg 9o(c) Permanganates 5 kg l0o Chromic anhydride 4.5 kg (chromic acid) , Class 5.1 4. Marking and danger labels on packages (see Appen­ dix A.9) (1) Packages containing substances of Class 5.1 shall bear a label of model No. 3. However, packages contai­ ning substances of lo to So or 80 to l0o shall bear two labels conforming to model No.3. Packages containing substances of 3o shall in addition bear a label conforming to model No. 5. (2),Packages containing fragile receptacles not visible from the outside shall bear a Jabel conforming to model No. 9. If the fragile rereptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampou­ les, bear labels conforming to model No. 8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. (3) In the case of consignments carried as a full load, labels Nos. 3 and 5, as prescribed under (1), need not be affixed to the packages if the vehicle bears the marking prescribed in Annex B, marginal 10 500. B. Particular in the transport document The description of the goods in the transport document must conform to one of the names underlined in marginal 2501; it must be underlined in red and followed by partic­ ulars of the Ciass, the item number (together with the letter, if any), and the initials «ADR» or «RID» [e.g. 5.1, 4o (a) ADR] C. Empty packagings (1) Packagings and tanks of llo must be closed in the same manner and leak-proof in the same degree as though they were full. 2511 2512 2513 2514 2520 2521 I per Special provisions package (in any form), hypopnosphites, ammoma ana its compoun ds, triethanolamine, aniline, xylidine, toluidine, or inflammable liquids having a flash point below 21 °C. 5 kg Must not be packed togetfier w1tfi we~· nitrated nitrocellulose, red phosphorus, bibluorides, liquid halogenated irritants, hydroch loric acid, sulphuric acid, chlorosulphonic acid, nitric acid, mixed nitrating acids, aniline, pyri dine xvlidine. toluidine, sulehur, hi:drl!,zin e · Must not be packed together with weakly-nitrated nitrocellulose or red phosphorus. .. , Same substances prohibited as in tne case of perchlorates, 2.5 kg and also: aluminium dust, powder or granules, acetic acid; aqueous liquids, inflammable liquids of Classes 3 and 6.1 5 kg substances of Class 4.1; metallic peroxides must not be packed in the same package with solutions of hydrogen peroxide. The limitation of 2.5 kg applies to peroxides of 9o(a) and (b) for all of these substances. The use of sawdust or other or ganic filling materials'is prohibited. 5 kg Same substances prohibited as in the case of eh !orates, and also: solutions of hydrogen peroxide, glycerine, glycols. Must be separated from the same substances as indicated in the case of chlo rates. 4.5 kg The use of sawdust or other organic filling materials is prohibited. (2) The description in the transport document must be: «Empty packaging, 5.1, 11 °, ADR (or RID)». This des­ cription must be underlined in red. (3) Empty textile bags, uncleaned, which have contai­ ned sodium nitrate [7 o (a)] are subject to the provisions of Class 4.2 (see marginal 2441). CLASS 5.2 ORGANIC PEROXIDES 1. List of substances Among the substances and articles covered by the hea­ ding of Class 5.2, only those listed in marginal 2551 are to be accepted for carriage, and then only subject to the provisions of this Annex and of Annex B. These substan­ ces and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. Note: Organic peroxides which may explode on contact with a flame or which are more sensitive to shock and to frict!on than dinitrobenzene are not to be accepted for carn~ge unless they are specifically listed in Class la (see marginal 2101, l0o and Appendix A.1, marginal 3112; also marginal 2551, Group E, below) ..... Group A • lo Ditertiary butyl peroxide. 2o Tertiary butyl hydroperoxide with not less than 20 per cent ditertiary butyl peroxide and not less than 20 per cent phlegmatizer. Note: Tertiary butyl hydroperoxide with not less than 2522 2549 2550 2551 EO>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) ~ 2207 20 per cent ditertiary butyl peroxide but without phlegma­ tizer is listed under 3 lo. 3o Tertiary butyl peracetate with not less than 30 per cent phlegmatizer. 4o Tertiary butyl perbenzoate. So Tertiary butyl permaleate with not less than 50 per cent phlegmatizer. 60 Ditertiary butyl diperphtalate with not less than 50 per cent phlegmatizer. 7o 2,2-bis (tertiary butyl peroxy) butane with not less than 50 per cent phlegmatizer. 80 Benzoyl peroxide: (a) with not less than 10 per cent water; (b) with not less than 30 per cent phlegmatizer. Class 5.2 Notes: 1. Benzoyl peroxide in the dry state or with less than 10 per cent water or less than 30 per cent phlegmati­ zer is a substance of Class 1 a [ see mar gm al 2101 lOo (a)]. 2. Benzoyl peroxide containing not less· than 7~ yer cent dry and inert solids is no subject to the prov1s10ns of ADR. 9o Cyclohexanone peroxides [l-hydroxy-1-hydropero­ xydicyclohexyl peroxide and bis (1-hydroxycyclohexyl) peroxide and mixtures of these two compounds]: (a) with not less than 5 er cent water; . (b) with not less than 30 per cent phlegmatizer. • Notes: 1. Cyclohexanone peroxides and their mixtures in the dry state or with less than 5 per cent water or less than 30 per cent phlegmatizer are substances of Class la [ see marginal 2101, 1 0o (b )]. 2. Cyclohexanone peroxides and their mixtures contai­ ning not less than 70 per cent dry and inert sohds are • not subject to the provisions of ADR. l0o a, a - Dimethylbenzyl hydroperoxide (cumyl hydro­ peroxide) with a peroxide content not exceeding 95 per cent. llo Dilauroyl peroxide. . 120 1, 2, 3, 4-Tetraxxdro-1-naphtyl hydroperoxide. 130 2,4-Dichlorobenzoyl peroxide: (a) with not less than 10 per cent water; (b) with not less than 30 per cent phlegmatizer. 140 p-Menthanyl hydroperoxide with a peroxide co­ ntent not exceeding 95 per cent (remainder alcohols and ketones). • • 150 2,6,6-Trimethyl norpinanyle hydroperoxide (pi~a­ nyl hydroperoxide; pinane hydroperoxide) with a peroxide content not exceeding 95 per cent (remainder: alcohols and ketones). 160 Di-(a, a - dimethylbenzyl) peroxide with a peroxide content not exceeding 95 per cent. Note: Di-(a, oc-dimethylbenzyl) • Dicumyl peroxide containing 60 per cent or more dry . and inert solids is not subject to the provisions of ADR. Class 5.2 1 7 o Parachlorobenzoyl peroxide: (a) with not less than 10 per cent water; (b) with not less than 30 per cent phlegmatizer. Note: 1. Parachlorobenzoyl peroxide in the dry state or with less than I 0 per cent water or less than 30 per cent phlegmatizer is a substance of Class 1 a [ see marginal 2101, lOo(c)]. 2. Parachlorobenzoyl peroxide containing 70 per cent or more dry and inert solids is not subject to the provisions of ADR. 180 Di-isopropylbenzene hydroperoxide (isopropylc­ umyl hydroperoxide) with 45 per cent of a mixture of alcohol and ketone. 190 4-Methylpentan-2-one peroxide (isobutylmethyl­ ketone peroxide) with not less than 40 per cent phlegmati­ zer. 2551 2551 200 Tertiary butyl (a, a-1-dimethylbenzyl) peroxide with not more thary 95 per cent peroxide. 210 Diacetyl peroxide with not less than 75 per cent phlegmatizer. 220 Acetyl benzoyl peroxide with not less than 60 per cent phlegmatizer. Note: re lo to 220. Substances which are inert to organic peroxides and have a flash-point not lower than 100°C and a boiling-point not lower than 150°C are deemed to be phlegmatizing substan~es. Substances of Group A may also be diluted with solvents which are inert to these substances. Group B 300 Butanone peroxide (ethyL methyl ketone pero­ xide): (a) with no~ less than 50 per cent. phlegmatizer; •(b) in solutions containing not more than 12 per cent of this peroxide in solvents which are inert to it. 310 Tertiary butyl hydroperoxide: (a) with not less than 20 per cent tertiary butyl pero­ xide, without phlegmatizer; (b)in solutions containing not more than 12 per cent of this hydroperoxide in solvents which are inert to it. Class 5.2 Note: re 300 and 3 lo. Substances which are inert to organic peroxides and have a flash-point not lower than 100°C and a boiling-point not lower than 150°C are deemed to be phlegmatizing substances. Group C . 350 Peracetic acid containing not more than 40 per cent peracetic acid and not less than 45 per cent acetic acid and not less than 10 per cent water. Note: re Groups A, Band C. Mixtures of products listed in Groups A, and C are to be accepted for carriage subje~t to the conditions laid down for Group C if they contam peracetic acid, and in other cases subject to the conditions laid down for Group B. Group D 400 Sampels of phlegmatized organic peroxides not listed in Groups A, B or C, or of their solutions, are to be accepted in quantities not exceeding 1 kg per package on condition that their stability in storage is at least equal to that of the substances listed in Groups A and B. Group E Note: Group E comprises organic peroxides which de­ compose easily at normal temperatures and must there­ fore be carried only under conditions of adequate refrige­ ration. Although of an explosive nature as defined by the Note on Class 5.2, a few organic peroxides are included. in Group E because they can be safely carried in a refrige­ rated state and in order to avoid any confusion regarding their handling. • 450 Dioctanoyl peroxide ( dicapryly 1 peroxide) of tech nical purity. 460 Acetyl cyclohexane sulphonyl peroxide: (a) containing not less than 30 per cent water; (b) in solution with not less than 80 per cent solvent; • (c) in solution with not less than 70 per cent phlegmati zer. 4 7 o Diisopropyl peroxydicarbonate: (a) of technical purity; (b) in solution with not less than 50 per cent phlegmati­ zer or solvent. Class 5.2 480 Dipropionyl peroxide in solution with not less than 75 per cent solvent. / 2551 2551 2208 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOr nPQTO) 490 Tertiary butyl perpivalate: (a) of technical purity; (b) in solution with not less than 25 per cent phlegmati­ zer or solvent. 500 Bis-(3,5,5-trimethylhexanoyl) peroxide in solution with not less than 20 per cent phlegmatizer. 510 Dipelargonyl peroxide of technical purity. 520 Tertiary butyl per-2-etl'iylhexanoate of technical purity. . . . 530 Di-2-ethylhexyl-peroxydicarbonate m solullon with not less than 55 per cent phlegmatizer or solvent. 540 Didecancyl peroxide of technical purity. 550 Tertiary butyl perisobutyrate in solution with not less than 25 per cent solvent. Notes: 1. Substances which are inert to organic peroxi­ des and have a flash-point not lower than 100°C and a boiling point not lower than 150°C are deemed to be phlegmatizing substances. 2. The solvents referred to are substances which are inert to organic peroxides and which also satisfy one of the following conditions: (a) they are not inflammable and have a boiling point of not less than 85 ° C; or (b) they are not inflammable and have a boiling point of less than 85 ° C but not less than 60 ° C, in which case • hermetically closed containers must be used; or (c) they have a flash-point of not less than 21 °C and a boiling point of not less than 85 ° C; or (d) they have a flash-point of less than 21 °C but not less than 5 ° C and a boiling point of not less than 60 ° C, in which case hermetically closed containers must be used. Class 5.2 Group F 990 Empty packagings, uncleaned, and empty tanks uncleaned, which ~ave contained substances of Class 5.2. 2. Provisions A. Packages 1. General conditions of packing (1) The materials of which the packagings and their closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there with. • (2) Packagings; including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require­ ments of carriage. Inner packagings shall be firmly sec­ ured in outer packagings. Unless otherwise specified in the section entitled •Packing of a single substance», inner packagings may be enclosed in outer packagings, either singly or in groups. (3) Cushioning materials must not be readily inflam­ mable; in addition they shall be suited to the nature of the contents and must not cause the peroxides to decom­ pose. 2. Packing of a single substance a. Packing of substances of Group A Receptacles shall be so closed and leak-proof as to prevent any loss of the contents. (1) Substances of 1 ° to 7°, 8°, 9° (b) 10" to 12°, l3°(b), 14° to 16°. l7°(b) and 18° to 22° and their solutions must be packed: (a) in hot-dipped tinned receptacles or in receptacles made of aluminium not less than 99.5 per cent pure; or (b) in receptacles, made of a suitable plastics material, which shall be placed in protective packagins; or (c) not more than 2 litres per bottle, in tightly-closing glass bottles which shall be secured by cushioning mate­ rials in a protective packaging so as to be protected against breakage. (2) Substances of lo to 3o, 5o to 7o, 80 (b), 9o (b), l0o to 12°, 13° (b), 16°, 18° and 20° may also be packed in hot-tipped galvanized receptacles. (3) Substances of 80 (a), 9o (a), 13 (a) and ~ 7o ~a) shall be contained, not more than 5 kg per pagkagmg, m water tight pagkaking placed in a wooden case. (4) Pasty and solid per9xi~es may ~lso be pac~ed i~ bags, made of a suitable plastics matenal, placed m ~UI­ table protective packagings. The thickness of the packmg material shall be sufficient to prevent any loss of the contents from the bags in normal carriage. Solid peroxides may be packed, not more than 1 kg per receptacle, in paraffin - waxed fibreboard receptacles placed in a ~oo­ den case; however, in the case of cyklohexanone peroxides of 9o (a) the contents of a receptacle shall be limited to 500 g. (5) Substances of lOo and of 140 to 180 may also be packed in receptacles made of sheet - steel. ( 6) with the exception of bags made of a suitable plastics material, receptacles containing liquid or pasty organic peroxides must not be filled beyond 93 per cent of their capacity. (7) A package must not weigh more than 50 kg. Packa­ ges weighing more than 15 kg shall be fitted with means of handling. b. Packing of substances of Group B 2555 (1) Receptacles filled with substa~ces of ~0° (a) ~nd 31 ° (a) shall be fitted with a ventmg device allowmg compensation .between the internal pressure and the atmospheric pressure and in all circumstances - even in the event of expansion of the liquid through heating preventing the liquid from splashing out and impurities from entering the receptacle. For substances· of 300 (b) and 310 (b), only receptacles so closed and leakproof as to prevent any loss of the contents shall be accepted. (2) Packages shall be fitted with a base which keeps them securely upright without danger of falling. 2551 (1) Substances of 300 (a) and 310 (a) shall be packed: '2556 (a) in not - dipped tinned or hot - dipped galvanized receptacles or in receptacles made of aluminium not less than 99 - 5 per cent pure; or (b) in receptacles, made of a suitable plastics material, placed in protective pagkagings. The strength of these receptacles shall be sufficient to prevent any' loss of the contents in normal carriage; or 2552 (c) not more than 2 litres per bottle, in glass bottles, which shall be secured by cushioning materials in protec­ tive packagings so as to be protected against breakage. (2) Receptacles containing liquid or pasty organic pero­ xides must not be filled beyond 90 per cent of their capa­ sity. (3) A package must not weigh more than 40 kg. Packa­ ges weighing more than 15 kg shall be fitted with means of handling. (4) Sustances of 300 (b) and 3 lo (b) may be forwarded only in quantities not exceeding 5 kg in receptacles as specified in (1 but not equipped with a venting device (in glass bottles, only in quantities not exceeding 1.5 litre) The receptacles must not be filled beyond 75 per of their capasity. c. Packir{g of substances of Group C 2557 1. Substances of 350 and mixtures containing peracetic acid shall be packed, not more than 25 kg per receptacle, 2553 in thick walled glass receptacles, or in receptacles made of a suitable plastics material, fitted with a special closure 2554 made of a suitable plastics material, capable of being sealed, in communication with the atmosphere through an opening situated above the level of the liquid, and in all circumstances - even in the enent of expansion of the liquid through heating - preventing the liquid from splash­ ing out and impurities from entering the receptacle. (2) Glass receptacles shall be firmly secured, by clean mica powder or glass wool used as cushioning materials, in protective pagkagings made of sheet - steel or of alumi­ nium, capable of being closed, and fitted with means of handling and with a base which keeps them securely upri­ ght without risk of falling; the receptacles shall be secured even if the walls of the protective packagings are not complete. Receptacles made of a suitable plastics material ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2209 mljit be placed in close - fitting protective packagings made of sheet - steel and capable of being closed. d. Packing of substances of Croup D Substances of Crour D shall be packed, in quantities not exceeding 1 kg per package, in hot - dipped tinned receptacles, or in receptacles made of aluminium not less than 99.~ per cent pure, or in bottles made of a suitable plastics material injection - moulded or blown and having a sufficient wall thickness, or in glass bottles placed in protective packagings made of sheet - steel, aluminium or wood. The glass bottles shall be firlmy secured in the protective packagings by clean mica power or glass wool used as cushioning materials. Solid compounds may also be packed in bags, made of a suitable plastics material of sufficient thickness, likewise placed in protective packa­ gings made of sheet - steel, aluminium, or wood. If the peroxides give off gases at temperatyre lower than 40 ° C, the receptacles must satisfy the conditions of marginal 2555. e. Packing of substances of Group E 1. Packages containing substances of Croup E shall be fitted with a venting device allowing compensation between the internal pressure and the atmospheric pressure and in all circumstances - even in the event of expansion of the liquid through heating preventing the liquid from spla­ shing out and impurities from entering the receptacle. 2. Receptacles containing liquid organic peroxides must not be filled beyond 95 per cent of their capacity. 1. Substances of 450, 510 and 540 shall be packed, not more than 50 kg per receptacle or bag, in receptacles or bags, made of a suitable plastics material, which shall • be placed in suitable protective pagkagings in quantities not exceeding 50 kg per packaging. 2. Substances of 460 (a) shall be p11-cked, not more than 5 kg per bag, in bagks made of a suitable plastics material, which shall be placed, not more than 20 kg packaring and either singly or in groups, in suitable protec­ tive packagings. 3. Substances of 470 (a) shall be packed. a) not more than 1 kg per receptacle, in receptacles, made of a suitable plastics material; b) not more that 3 kg per bowl, in bowls made of aluminium not less than 99.5 per cent pure, with plastics lids. The protective packagings must not contain more than 10 kg of the substance. 4. Substances of 460 (b) and (c), 470 (b), 480, 49o(b), 500, 520, 530 and 550 shall be packed, not more than 25 kg per receptacle, in receptacles made of a suitable plastics material, which shall be placed not more than 50 kg per packaging (but not more than 25 kg per packaging in the case of substances of 520), in protective packagings. 5. Substances of 490 (a) shall be packed, not more than 10 kg per receptacles, in receptacles made of a suitable plastics material, which shall be placed, not more than 40 kg per packaging, in protective packagings. 6. Packages weighing more than 35 kg which contain substances of Group E shall be fitted with means of han­ dling. f. Packing of substances in small quantities. Substances of 1 ° to 22 °, 30 ° and 31 °, forwarded in small quantities, may also be packed as follows: a) Liquids not more • than 1 kg per package, in bottles, made of aluminium, a suitable plastics material, or glass, with stop­ pers, made of a suitable plastics material or with yoke or screw closures having, in either case, an elastic gasket. The bottles shall be secured, by clean mica powder or glass wool used as cushioning materials, in fibreboard or wooden boxes. The filling material must be sufficient in quantity to absorb the whole of the liquid. The bottles must not be filled beyond 75 per cent of their capasity; b) pasty or powdered substances not more than 1 kg per package, in aluminium boxes or in fibreboard or wooden boxes (the two latter being lined with aluminium or with a suitable plastics material) with 2558 2559 2561 a strong closure. A free space of 10 per cent shall be left in the packagings. 3. Mixed packing Substances of Class 5;2 may not be included in the same package either with other substances or articles of ADR or with other goods. Substances of Grour C Must not be included in the same package with substances of Groups A, B or E. 4. Marking and danger labels on packages (see Appen­ dix A. 9) 1. Every package containing substances of Class 5.2. shall bear a label conforming to model No 3. Packages containing substances of 460 (a), 470 (a) and 490 (a) shall also bear a label conforming to model No 1. 2) Packages containing fragile receptacle!! not visible from the outside shall bear a label conforming to model No 9. If the fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampoules, bear labels conforming to model No 8; packages contai­ ning substances ·of 306, 310, 350, 400 and 450 to 550 shall also bear label conforming to model No 8; these iabels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. B. Particulars in the transpost document The description of the goods in the transport document must conform to one of the names underlined in marginal 2551; it must be underlined in red and followed by partic­ ulars of the Class, the item number (together with the letter, if any), and the initials «ADR» or «RID• (e. g. 5.2., 80 (a) ADR). C. Empty packagings L Peleptacles ant tanks of 990 must be closed in the same manner and leak - proof in the same degree as though they were full. , ..... 2. The description in the transport document must be «Empty receptacle, 5.2, 990 ADR (or RID)». This desprip­ tion must be underlined in red. CLASS 6.1. TOXIC SUBSTANCES 1. List of substances 1. Among the substances and articl~s covered by the heading of Class 6.1, those which are listed in marginal 2601 or are covered by a collective heading of that margi­ nal are subject to the provisions of this Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. 2. Substances of Class 6.1. which polymerize easily are not to be accepted for carriage unless the necessary pre­ cautions have been taken to prevent their polymerization during carriage. 3. The flash 6 point referred to below shall be determi­ ned in the mariner described in Appendix A.3. A. Toxic substances having a flash - point below 21 ° C and a boiling point below 200° C 1. Hydrocuanic acid and inflammable volatile substan­ ces having a similar toxic effect, such as: a) hydrocyanic acid containing not more than 3 per cent water (absorbed by an inert porous substance or in the liquid state), on condition that. the filling of the recep­ tacles was carried out less than one year previously; Note: Hydrocyanic acid not satisfying these conditions is not to be accepted for carriage. b) aqueous solutions of hydrocyanic acid containing not more than 20 per cent hydrocyanic acid (HCN). Note: Solutions of hydrocyanic acid containing more than 20 per cent hydrocyanic acid (HCN) are not to be accepted for carriage. 2. Nitriles (organic cyanides), such as: a) actylonitrile; b) acetonitrile (methyl cyanide); c) isobutyronitrile (isobutyric nitrile). 3. Other nitrogenous organic substances, such as: 2562 2563 2564 2565 2566 2569 2570 2600 2601 2210 ECJ>HMEPlr THr KYBEPNHI:EQI: (TEYXOr nPQTO) ethyleneimine and propyleneimine containing not more than 0.003 per cent total chlorine, and their aqueous solutions; normal butyl isocyanate, tertiary butyl isocya­ nate, isobutyl isocyanate and isopropyl isocyanate. Note: Ethyleneimine and propyleneimine of any other nature are not to be accepted for carriage. 4. Halogenated organic, substances such as: a) ally! chloride; b) methyl chloroformate; c) ethyl chloroformate. 5. Metal carbonyls, such as: a) nickel carbonyl (nickel tetracarbonyl l); b) iron. carbonyl (iron pentacarbonyl). B. Toxic substances having a flash - point of 21 ° C or a over, and non - inflammable toxic substances, both having a boiling point below 200° C 11 ° Nitrogenous organic substances, such as: a) 2 - cyanopropan - 2 - 01 (acetone cyanohydrin); b) aniline 12 ° Halogenated organic substances. suC'h as: a) 1 - chloro - 2, 3 - epoxypropane (ep.l!'hlorohydrin); b) glycol chlorohydrin (2 - chloroethanol); c) acetylene tetrachloride (1, 1, 2, 2-tetrachloroe­ thane); d) chloropicrin; Note: Mixtures of chloropicrin with methyl chloride or methyl bromide are substances of Class 2 if the vapour pressure of'the mixture at 50° C exceeds 3 Kg/cm2 [see marginal 2201 4o (bt)]. e) trichloromethanesulphenyl chloride; f) 2, 2-dichlorodiethyl ether, (chloroethyl ether, 2-ch Ioroetyl ether. 13 ° Oxyrenated organic substances, such as: a) ally! alcohol; b) dimethyl sulphate; c) phenol."···-'" 14 ° Lead all {yls, such as tetraethyl lead, tetramethyl lead and mixtures of lead alkyls with halogenated organic compounds, e.g. ethyl fluid. C. Toxic organic substances having a boiling point of 200 ° C or over. 21. Nitrogenous organic substances, such as: a) 2-bromophenylacetonitrile (bromobenzyl cyanide); b) phenylcarbylamine chloride; c) 2, 4-diisocyanatotoluene; d) ally! isothiocyanate; e) chloroanilines; f) mononitrionalines and dinitroanilines; g) naphthylamines; • h) 2, 4-diaminotoluene; i) dinitrobenzenes; k) chloronitrobenzenes; I) mononitritoluenes; m) dinitrotoluenes; n) nitroxylenes; o) toluidines; p) xylidines 22 ° Oxygenated organic substances not covered by 2 lo and 230, such as: a) cresols; b) xylenols. 23° Halogenated organic substances not covered by 210; such as: a) xylyl bromide: b) phenacyl chloride (w-chloro aceto phenone); c) phenacyl bromide (w-bromoacetophenone); d) 4-chloro aceto phenone (methyl p-chlorophenylke­ tone); e) symmetical • dichloroacetone. D. Inorganic substances which may release toxic gases on contact with acids (but see under E for silicon alloys). 31 ° Inorganic cyanides a) cyanides and complex cyanides in a solid form; 2601 b) solutions of inorganic cyanides; c) preparations of inorganic cyanides. Note: Ferrocyanides and ferricyanides are not subjest to the provisions of ADR. 32 ° The following azides: a) sodium azide; b) barium azide with not less than 50 per cent water or alcohols, and aqueous solutions of barium azide. Note: Barium azide in the dry state or with less than 50 per cent water or alcohols is not to be accepted for car­ riage. 33. Zinc phosphide Note: Zinc phosphide capable of spontaneous ignition or, under the effect of moisture, of releasing toxic gases is not to be accepted for carriage. ' E. Silicon alloys capable of releasing toxic gases. 41 ° (a) Ferro - silicon and mangano - silicon with more than 30 per cent and less than 70 per cent silicon; (b) ferro-silicon alloys with aluminium, manganese, cal­ cium or more than one of these metals, with a total content of silicon and of elements other than iron and manganese greater than 30 per cont but less than 70 per cent, all the substances of 41 ° having been stored for not less than three days in a dry place open to .the air. Note: 1. Ferro-silicon and mangano-silicon briquettes, whatever their silicon content, are not subject to the provi­ sions of ADR. 2. Substances of 41 ° are not subject to the provisions of ADR if they are not liable to release dangerous gases under the effect of moisture during carriage ahd the sender so certifies in the transport document. 3. Substances of 41 ° which have not been stored for not less than three days in a dry place open to the air are not to be accepted for carriage. F. Other toxic inorganic substances. 51 ° Beryllium in powder form; beryllium compounds in powder form. 52° Arsenical compounds, such as: (a) oxides of arsenic; (b) sulphides of arsenic. Note: With regard to arsenical substances and prepara­ tions used as pesticides, see under 81 ° (i), 82° (i) and 83° (i). 53° mercury compounds, such as: Mercuric chloride (corrosive sublimate), except cinna bar and mercurous chloride (calomel). Note: With regard to mercurial substances and prepara­ tions used as pesticides, seeunder 81 ° (f), 82° (f) and 83' (f). 54° Thallium compounds Note: With regard to substances and preparations co­ ntaining thallium and used as pesticides, see under 81 ° (h), 82° (h) and 83° (h). . G. Halogenated organic substances having a harmful or irritant effect. 61 ° Halogenated organic substances, volatile, inflam­ mable or non-inflammable, having a flash-point of 21 °C or over and a boiling point below 200°C, such as: (a) ethylene dibromide (symmetrical dibromoethane); (b) chloroacetone; (c) bromoacetone; (d) 1,2 -dibromobutan-3-0ne; (e) methyl chloroacetate; (f) ethyl chloroacetate; (g) methyl bromoacetate; (h) ethyl bromoacetate; (i) 1,1--dichloro- 1-nitroethane; (k) benzyl chloride; (I) 1-chloro- 1-nitropropane. ~2• Hal~~enated org~nic substances of low volatility havmg a bodmg point of 200°C or over and not covered by 23°, such as: • (a) benzyl iodide; <I>EK 225 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2211 (b) acetylene tetrabromide (1, 1, 2, 2-tetrabromoe­ thane). H. Inorganic substances having a harmful effect. 71 ° Barium compounds, such as barium oxide, barium hydroxide, barium sulphide and other barium salts (except barium sulphate and barium titanate). Nc,te: Barium chlorate, perchlorate, nitrate, nitrite; dio­ xide and permanganate are substances of Class 5.1 (see marginal 2501 under 4°(a) and (b), 7°(c), 8° and 9° (b) and (c)]. 72° Lead compounds, such as lead oxides, lead salts including lead acetate, lead pigments (e.g. white lead and lead chromate), except lead titanate and lead sulphide (ga­ lena). Note: Lead chlorate, lead perchlorate and lead nitrate are substances of Class 5.1 (see marginal 2501 4° (a) and (b) and 7° (c)J. . 73° Residues and wastes containing compounds of anti­ mony or oflead or of both, e.g. ·ashes oflead or of antimony or of lead and antimony: lead sludges containing less than 3 per cent free acid. Note: Lead sludges containing 3 ~r cent or m~re free acid are substances of Class 8 (see marginal 2801, 1 ° (e)]. 74° Vanadium compounds in powder form, such as vanadium pentoxide and the vandates. Note: Vanadium chlorate and vanadium perchlorate are substances of Class 5.1 (see marginal 2501, 4° (a) and (b)l. • 75° Antimony compounds, such as antimony oxides and antimony salts, except stibnite. Note: Antimony chlorate and antimony 'perchlorate are substances of Class 5.1 [see marginal 2501, 4° (a) and (b). Antimony pentachloride, antimony trichloride and antimony pentafluoride are substances of Class 8 [ see marginal 2801 11 ° (a), 12° and 15° (b)]. f. Substances and preparations used as pesticides 81 ° Substances and preparations presenting a risk of very severe poisoning: (a) organo-phosphorus compounds, such as: azinphos­ ethyl, azinphosmethyl, demeton-O+S, dimefox, endoth­ ion, HETP, mecarbam, methylparathion, mevinphos, pa­ rathion, phosphamidon, sulfotep and TEPP, and prepara­ tions containing more than 10 per cent of these substances. (b) Halogenated organic compounds, such as: aldrin, dieldrin, heptachlor, and preparations containing more than 10 per cent of these substances. (c) Nitrated organic compounds, such as: 4,6 -dinitrope­ nol, dinoseb, dinitrohenyl acetate: dinotro-ci0cresol, and preparations containing more than 50 per cent of these substances. (d) Carbamates and derivatives of urea, such as: ANfU, isolan, and preparations containing more than 25 per cent of these substances. • ( e) Alkaloids, such as: nicotine, brucine; strychnine,' 'or . • their salts, and preparations containing more than 10 per cent of these substances. (f) Organic compounds of metals, such as: 1. organic mercurial compoundes, and preparations containing more than 5 per cent of these substances; 2. trialkyl and triaryl compounds of tjn, and prepara­ tions containing more than 25 per cent of these substances. (g) Other organic compounds, such as: cumachlor, so­ dium fluoracetate, fluoracetamide, pindone, warfarin, and preparations containing more than 5 per cent of these substances. (h) Inorganic compounds of metals, such as: thallium compounds, and preparations containing more than 10 per cent of these substances. (i) Other inogranic compounds, such as: compounds of arsenic, and preparations containing more than 10 per cent of these substances. 82° Substances and preparations presenting a risk of severe poisoning: (a) Organo-phosphorus compounds, such as: .. 1. demeton-O+S-methyl, dioxathion, ethion, fenthion, phenkapton, thiometon, and preparations containing more than 25 per cent of these substances; 2. proparations of azinphos-ethyl, azinphos-methyi, de­ meton-O+S, dimefox, endothion, HETP, mecarbam, me­ thylparathion, mevinphos, parathion, phosphamidon, sulfotep and TEPP, containing more than 2.5 per cent but not more than 10 per active substance. (b) Halogenated organic compounds, such as: 1. toxaphene, pentachlorophenol, and preparations co­ ntaining more than 20 per cent of these substances; 2. gamma?BHC (gammexane), DDT, and preparations containing more than 50 per cent of these substances. (c) Preparations of nitrated organic compounds,such as: 1. preparations of 4,6-dinitrophenol, dthoseb, dinitro­ phenyl acetate and dinitro-o-cresol, containing more than 10 per cent but not rriore than 50 per cent active substance;. • 2. preparations of binapacryl, containing more than 50 p er cent active substance. • ( d) Carbamates and derivatives of urea, such as: 1. dimethan, urbazid, and preparations containing more than 25 per cent of these substances; 2. preparations of ANTU and isolan, containing more than 5 per cent but not more than 25 per cent active substance. • (e) Preparations· of alkaloids, such as: preparations of nicotine, brucine, and strychnine, or their salts, containing more than 2.5 per cent but not more than 10 per cent active substance. • (f) Preparations of organic compounds of metals, such as: 1. organic mercurial preparations, containing more than 1 per cent but not more than 5 per cent active substance; 2. preparat.ions of trialkyl and triaryl compounds of tin, containing more than 5 per cent but not more than 25 per cent active substance. (g) Preparations of other organic compounds,,such as: 1. preparations of cumachlor, sodium huaracetate, pin­ done and warfarin, containing more than 1 per cent but not more than 5 per cent active substance; 2. preparations of fltioracetamide, containing not more than 5 per cent active substance; (h) Preparations of inorganic compounds of metals, such as: Preparation of thallium compounds, containing more than 2.5 per cent but not more than 10 per cent active substance. (i) Preparations of other inorganic compounds, such as: Preparations of compounds· of arsenic, containing more t han 2.5 per cent but not more than 10 per cent active substance. 83° Harmful substances and preparations: (a) Organo-phosphorus compounds, such as: 1. diazinon, dimethoate, trichlorfon, malathion, and preparation containing more than 5 per cent of these substances; • 2. preparations of demeton-O+S-methyl, dioaxathion, ethion, fenthion, phenkapton and thiometon, containing more than 2.5 per cent but not more than 25 per cent active substance; 3. preparations of azinphos-ethyl, azinphos-methyl, de­ meton-O+S, dimefox, endothion, HETP, mecarbam, me­ thylparathion, mevinphos, parathion, phosphamidon, sulfotep and TEPP, containing not more than 2.5 per cent active substance. (b) Preparations of halogenated organic compounds, such as: 1. preparations of toxaphene and pentachlorophenol containing more than 5 per cent but not more than 20 per cent active substance; 2. preparations of g~mma-BHC (gammexane) and DDT, containing more than 10 per cent but not more than 50 per cent active substance. 3. preparations of aldrin, dieldrin and heptachlor, co­ ntaining more than 2. 5 per cent but not more than 10 per cent active substance. (c) Preparations of nitrated organic compounds, such as: 2212 E<l>HMEPII THI KYBEPNHIEQI (TEVXOI nPQTO) 1. preparations of binapacryl, contai~ing more than 10 per cent but not more than 50 per cent active substance; 2. preparations of 4,6 -dinitrophenol, dinoseb, dinitro­ phenyl acetate and d,initro-o-cresol, containing more than • 2.5 per cent but not more than 10 per cent active substance. ( d) Preparations of carbamates and derivatives of urea, such as: 1. preparations of ANTU and isolan, containing more than 1 per cent but not more than 5 per cent active substance; 2. preparations of dimethan and urbazid, containing more than 2.5 per cent but not more than 25 per cent active substance. (e) Preparations of alkaloids, such as: preparations of nicotine, brucine and strychnine, or their salts, containing not more than 2.5 per cent active substance. ( f) Preparations of organic compounds of me tails, such as: 1. preparations of organic mercurial compounds, co­ ntaining not more than :t per cent active substance; 2. preparations of trialkyl and riaryl compounds of tin, containing more than l per cent but not more than 5 per cent active substance. (g) Preparations of other organic compounds, such, as: preparations of cumachlor, sodium fluoracetate, pin­ done and warfarin, containing not more than 1 per cent active substance. (h) Preparations of inorganic compounds of metals, such as: preparations of thallium" compounds, containing not ·more than 2.5 per cent active substance. (i) Preparations of other inorganic compounds, such as: preparations of compounds of arsenic, containing not more than 2.5 per cent active substance. 84° (a) cereal grains and seeds impregnated with one or more of the pesticides'of other toxic substances· of Class 6.1, used as pesticides; · (b) dressed seeds treated with pesticides or with other toxic substances of Class 6.1, but not used as pesticides. K. Empty packagings: • 91 ° Empty packagings, uncleaned, empty tanks, uncle­ aned, and empty bags, uncleaned, which have contained substances of 1 °-5°, 11 °-14°, 21 °-23°, 31 °-33°, 41 °, 51 •. 54°, 81 ° and 82°. 92°. Empty packagings, uncleaned, empty tanks, uncle­ aned, and empty bags, uncleaned, which have contained substances of 61°, 62°, 71°-75°, 83° and 84°. Note: 91° and 92°. Empty packagings with residues from their previous contents adhering to the outside are not to be accepted for carriage. Class 6.1 2. Provisions A. Packages I: General conditions of packing (1) Packagings shall be so closed and arranged as to prevent any loss of the contents. For the special provision relating to subs~nces of 41 ° see marginal 2618. (2) The materials of which the packagings and their closures are made must not be liable to attack by the contents or form harmful or dangerous compounds there­ with. (3) Packagings, including their closures, must be suffi. ciently rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require­ ments of carriage. In particular, where substances are in the liquid state or in solution, or have been wetted by a liquid, the receptacles and their closures must, unless the section headed «Packing of a single substance» provides otherwise, be able to withstand any pressure which, the presence of air also being taken into account, may arise inside the receptacles in normal carriage. For this purpose a free space must be left, account being taken of the difference between the temperature of the substances at the time of filling and the highest mean temperature which 2602 they are likely to reach during carriage. Inner packagings shall be~ firmly secured in outer packagings. Unless other­ wise specified in the section entitled «Packing of a single substance•, inner packagings may be enclosed in outer packagings, either singly or in groups. ( 4) Bottles and other glass receptacles must be free from faults liable to impair their strength; in particular, internal stresses must have been suitably relieved. The thickness of the walls must be not less than 3 mm in the case of receptacles which, with their contents, weigh more than 35 kg, and not less than 2 mm in the case of other receptacles. The tightness of the closure system must be ensured by an additional device (cap, crown, seal, binding, etc.) capable of preventing any loosening of the closure system during carriage, unless the said closure comprises two plugs, one placed over other, one of them being screw threaded. • (5) When receptacles made of glass, porcelain, stone­ ware or similar materials are prescribed or allowed, they must be secured by cushioning materials in protective packagings. Cushioning materials shall be suited to the nature of the contents; in particular, they shall be absor­ bent when the contents are liquid. (6) When handed over for carriage, packages must not be contaminated on the outside by toxic substances. 2. Packing of a single substance (1) Hydrocyanic acid and inflammable volatile substan­ ces having a similar toxic effect [l O (a)] shall be packed: (a) when completely absorbed by an inert porous mate­ rial: in strong sheet-steel boxed, with a capacity of not more than 7 .5 litres, entirely filled with the porous mate­ rial, which must be of such a nature that it does not shake down or form dangerous spaces, even after prolonged use or under impact, at temperatures up to 50°C. The boxes must be able to withstand a pressure of 6 kg/cm2 and must, when filled at 15 °C, still be leak-proof at 50°C. The date of filling shall be stamped on the lid of each box. The boxes shall be placed in packing cases with sides not less than 18 mm thick in such a manner that they • cannot come into contact with one another. The total capa­ city of the boxes in one packing case must not e?(ceed 120 litres and the package must not weigh more that 120 kg; (b) When liquid bu! not absorbed by a porous material: in carbon-steel receptacles. These shall conform to the spirit of the provisions relating to such receptacles in Class 2, marginals 2211, 2212(1), 2213, 2215 and 2218, with the following derogations and special requirements: The internal pressure to be applied for the hydraulic pressure test must be 100 kg/ cm2• The pressure test shall be repeated every two years, when a meticulous inspection of the inside of the receptacle shall also be carried out and the receptacle's weight deter­ mined. In addition to the marks prescribed in marginal 2218(i) (a)-(c) and (e)-(g), the receptacles must bear the date (month, year) of the most recent filling. The maximum filling allowed for the receptacles is 0.55 kg liquid per litre of capacity. (c) With regard to the parti~lars in the transport doc­ ument, see marginal 2634(2). (2) Aqueous solutions of hydrocyanic acid [lo (b)] shall be packed in flame-sealed glass ampoules containing not more than 50 g, or in glass-stoppered glass bottles so closed as to be leak-proof and·containing not more than 250 g. The ampoules and bottles shall be secured by absorbent cushioning materials in soft-soldered tin-plate boxes or in protective cases with a soft-soldered tin-plate lining. A pac,age comprising a tin-plate box must not Weigh more than 15 kg or contain more than 3 kg hydro­ cyanic acid solution; a package comp~ing a case must not weigh more than 75 kg. (1) Substances of 2o shall be packed: (a) 1. in sheet-steel canisters with walls not less than 1 mm thick an a capacity not exceeding 60 litres, the 2603 2604 E(t)HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2213 openings being closed two plugs, one placed over the other, one of them being screwthreaded. The sheet-steel canisters must have welded lengthwise seams, two reinfor­ cing ribs in the walls, and a protective rim below. the joint recessed at the bottom. Canisters with a capacity of 40 to 60 litres must have their bottoms welded on and be fitted with means of handling on the side; or 2. in all-welded steel drums with walls not less than 1.25 mm thick fitted with rolling hoops and reinforcing ribs and having the openings closed by two plugs, one placed over the other, one of them being screw­ threaded; (b) acrylonitrile may also be packed: 1. in aluminium bottles of a capacity not exceeding 2 litres, secured by infusorial-earth cushioning in sheet­ metal receptacle whose lids shall be firmly stuck down by means of suitable adhesive strips. The sheet-metal recep­ tacles shall be placed, with filling material, in wooden cases. A package must not weigh more than 7 5 kg; or 2. in non-returnable metal drums (new packagings intended to be use only once); these drums, whose walls shall not be less than 1.2 mm thick, shall be provided with a screw-threaded plug fitted with a gasket. The plug shall be situated on one of the ends be protected by the rim of the drum. The drums ·may have a body• with ends recessed, the joints being strengthened by chimb reinfor­ cements; if they do not possess rolling hoops they must provided with reinforcing ribs. A package must not weigh more than 200 kg. Carriage in non-returnable drums shall take place only as a full load on open vehicles; or 3. in non-returnable steel drums (new packagings inten­ ded to be use only once) having sides made of sheet steel 1.24 mm thick, end made of sheet steel 1.5 mm thick, and a tare weight of 22.5 kg; the drums must be provided with reinforcing ribs. The body sea shall be welded and the ends shall be double-seamed by welting the body, with a polyethylene liner in~erted. Two screw-plug clos~re units, one of 50.8 mm (2 ??) and one of 19.05 mm (3/4 ??) shall be double-seamed by welting to one of the ends, with a synthetic-rubber liner inserted. "Thin sheet­ steel caps shall placed over the closure units; Class 6.1 (c) acetonitrile may also be packed in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of capacity not exceeding 1 litre, with the openings closed by two plugs, one placed over the other, one of them being screw - threaded. These receptacles shall be secured by absorbent cushioning ma­ terials in a wooden case or some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling. (2) Receptacles containing acrylonitrile or acetonitrile must not be filled beyond 95 per cent, and receptacles containing lsobutyronitrile not beyond 92 per cent, of their ca­ pacity. (l) Substances of 3o shall be packed in receptacles ?.60!) made of sheet - steel of sufficient thickness, which shall be closed by a screw - threaded bung or plug rendered leak - proof both to liquid and to vapour by means of a suitable gasket. The receptacles must be capable of withs tanding an internal pressure of 3 kg/cm2. Each receptacle shall be secured by absorbent cushioning materials in a strong and leak - proof protective metal packaging. The protective packaging shall be hermetically closed and its closure shall be secured against any inadvertent opening. The degree of filling shall not exceed 0.67 kg per litre of capacity of the receptacle. (2) A package must not weigh more than 75 kg. Packa­ ges weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling. Substances of 4° shall be packed: 2. 601:> (a) in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres, with t~e openings closed by two plugs, one placed over the other, one of t~m being screw - threaded. These receptacles small be secured by absorbent cushioning materials in a wooden case or some other outer packaging of sufficient strength. The receptac­ les shall not be filled beyond 93 per cent of their capacity. Such a package must not weigh more than 75 kg. Package weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in flame - sealed glass. ampoules containing not more than 100 g, which shall be secured by absorbent • cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules must not be filled beyond 93 per cent of their capacity. Such a pl\ckage must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with ll).eans of handling; or (c) in metal receptacles having, if necessary, a suitable lining, the receptacles having a capacity not exceeding 15 litres and having the openings closed by two plugs, one placed over the other, one of the being screw - threaded. These receptacles shall be secured by absorb cushioning materials in a wooden case or some other outer packaging sufficient strength. The receptacles must not be filled bey­ ond 93 per cent of their capacity. Such a package must not weigh more than 100 kg; or (d) in welded metal drums having, if necessary, a sui­ table lining, the drums having the openings closed by two plugs, one placed over the other, one of them-being screw threaded. The drums must not be filled beyond 93 per . cent of their capacity. If, with their contents, they weigh more than 275 kg, they shall be equipped with rolling ho-. ops; (e) in receptacles made of strong black sheet - iron or tin - plate and hermetically closed. A tin - plate receptacle must not, with its contents, weigh more than 6 kg. These receptacles shall be secured by absorbent cushioning ma­ terials, either singly or in groups, in a wooden packing case. Such a package must !}Ot weigh more than 75 kg. (1) Substances of So shall be packed in nietal receptac- 2607 les. The receptacles must be fitted with completely leak proof closing devices, which shall be secured against mechanical damage by protective caps. Steel receptacles must have walls not less than 3 mm thick and receptacles made of other materials must have walls· at least thick enough to ensure equivale mechanical strength. A package must not contain more than 25 kg of liquid. The maximum filling allowed ,,hall be 1 kg of liquid per litre of capacity. (2) Receptacles shall be tested· before being put into service for the first time. The test pressure to be applied for the hydraulic pressure test shall be not less than 10 kg/ cm2 • The pressure test shall be repeated every five years and shall include a meticulous inspection of the inside of the receptacle and a check of the tare weight. Metal receptacles shall bear the following particulars in clearly legible and indelible characters: (a) the name of the product in full (the names of both substances may al be shown side by side); • (b) the name of the owner of the receptacle; (c) the tare of the receptacle, including such fittings and accessories valves, protective caps, etc.; (d) the date (month, year) of the acceptance test and the subsequent tests, and the expert' s stamp; Class 6.1 ( e) the maximum permissible filling per r~ceptacle in kg; ( f) the internal pressure ( test pressure) to be applied for the hydraulic pressure test. • 2608 (1) Substances of 11 ° (a) sh~ be packed: (a) in sheet - steel canisters with walls not less than 1 mm thick and a capacity not ~xceeding 60 litres, the openings· being closed by two plugs, one placed over the other, one of them being screw - threaded. The sheet steel· canistern must 'have welded lengthwise seams, two reinforcing ribs in the walls, and a protective rim below the joint recessed at the bottom. Canisters ·with a capacity of 40 to 60 litres must have their bottoms welded on and be fitted with means of handling on the side; or 2214 l;<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) (b) in all - welded steel drums, with walls not less than 1.25 mm thick, fitted with rolling hoops and reinforcing ribs and having the openings closed by two plugs, one placed over the other, one of them being screw - threaded. (2) Substances of 11 • (b) shall be packed: (a) in hermetically - closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not • exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 7 5 kg. Packages weigh­ ing more than 30 kg. other than those forwarded as a full load, shall be fitted with means of handling; or (b) in metal receptacles having, if necessary, a suitable lining, the receptacles having a capacity not exceeding 15 litres and having the openings closed by two plugs, one placed over the other, one of them being screw - threaded. These receptacles shall be· secured by absorbent cushio­ ning. materials in a wooden case or some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or ( c) in hermetically - closed metal drums having, if neces­ sary, a suitable lining. The drums must not be filled beyond 95 per cent of.their capacity. II If they weigh, with their contents, more than 275 kg they shall be fitted with rolling hoops; or Class 6.1 (d) in hermetically - closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg. (1) Substances of 12• (a) and (b) shall be packed: 1 €,oc:t (a) not more than 5. litres per bottle, in glass bottles placed separately with. 11;bs~rbent materials, in a strong tin plate receptacle; in~ the case of 1 - chloro - 2, 3 epoxypropane, black sheet - iron may be used instead of tin - plate. The receptacles shall be secured by absorbent cushioning materials in a wooden packing case. A package must not weigh more than 75 kg; or (b) not more than 5 litres per receptacle, in receptacles, made of stout tin - plate, with leak - proof closures; in the case of 1 - chloro - 2, 3 - epoxypropane black sheet iron may be used instead of tin -· plate. The receptacles shall be secured by absorbent cushioning materials or wood - wool cushioning in a wooden packing case. A package must not weigh more than 75 kg; or (c) in welded steel drums with the openings closed by two. plugs, one placed over the other, one of them being screw~ threaded, the drums being fitted with rolling hoops. In the case of glycol chlorohydrin (2 - chloroethanol) it is also permissible to use welded canisters with the openings closed by two plugs, one placed over the other, one of them being screw - threaded, the canisters being fitted with means of handling, being of sheet steel 1 mm thick galvanized on both sides, and having a capacity not excee­ ding 60 litres; (d) the receptacles must not, be filled beyond 93 per .cent of their capacity. (2) Substances of 12• (c) shall be packed: (a) i~ hermetically - closed receptacles made of glass, porcelam, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling· or (b) in fla]lle - sealed glass ampoules containing not more than 109 g, which shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of su~ficient strength. The ampoule must not be filled beyond 95 per cent of their capacity. Such a package ll!Ust not weigh more than 7 5 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or Class 6.1 (c) in hermetically - closed canisters made of a sutable metal, welded or hard - soldered, having a capacity not exceeding 60 litres, and fitted with means of handling. The canisters must not be filled beyond 95 per cent of their capacity; or ( d) in hermetically - closed metal drums having, if ne­ cessary, a suitable inner lining. The drums must not be filled beyond 95 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. (3) Substances of 12° (d) and (e) shall be packed: (a) in hermetically - closed receptacles made of glass, porcelain, stone - ware or similar materials, or of a suitable •,plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package ·must nor weigh more than 75 kg. Packages weighing more than 30 kg. other than those forwarded as a full load, shall· be fitted with means of handling; or • (b) in flame sealed ~ ampoules containing not more than 100 g, which shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules must not be filled beyond ,95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (c) in hermetically - dossed metal receptacles having, if necessary, a suitable lining, and having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (d) in hermetically -closed metal drums havi11g, if necessary, a suitable lining. The drums must not be filled be~ond 95 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. ( 4) Substances of 12° ( e) may also be packed in hermeti­ cally - closed canisters made of a suitable metal, welded ~r hard - soldered, having a capacity not exceeding 60 hires, and fitted with means of handling. The canisters must not be filled beyond 95 per cent of their capadty. Class 6.1 (5) Substances of 12• (f) shall be packed: (a) in hermetically - closed metal receptacles having, if necessary, a suitable lining; and having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushionin·g materials in a wooden case or in some other outer packaging of sufficient strength. The recep~acles must not be filled beyond 93 per cent of their capacity. Such a package must not weigh more than 100 kg; or (b) in hermetically - closed canisters made of a suitable metal, welded ~r hard - soldered, having a capacity not exceedmg 60 litres, and fitted with means of handling The canisters must not be filled beyond 93 per cent of their capacity; or (c) in hermetically - closed metal drums having, if neces­ sary, a suitable linin~. The dr:ums must not be filled beyond 93 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. (1) Substances of 13° (a) and (b) shall be packed: 2610 (a) m flame - sealed glass ampoules or in hermetically . closed glass bottles for this purpose a 'stopper made of cork coated with paraffin wax, or ground - glass stopper, E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) '2215. may be used. The ampoules and booties muit not be filled beyond 93 per cent of their capacity and must not weigh, with their contents, more than 3 kg. They shall be wrapped in corrugated fibreboard and secured by a sufficient qua­ ntity of inert and absorbent cushioning materials (infusorial earth or similar materials) in soft - soldered tin - plate boxes or in wooden cases lined with a tin - plate lining assembled by soft soldering. A package comprising a tin plate box must not weigh more than 15 kg and a package comprisirig a wooden case not more than 7 5 kg; or (b) in soldered or seamless· sheet metal receptacles or in receptacles made of a suitable plastics material. These receptacles shall be hermetically - closed; they must not be filled beyond 93 per cent of their capacity and must not weigh, with their contents, more than 50 kg; if they are made of thin sheet - metal, e.g. tin - plate, they must not weigh, with their contents, more than 6 kg. The sheet metal or plastics receptacles shall be secured by a suffi­ cient quantity of inert and absorbent cushioning materials ((e.g. infusorial earth or similar materials) in protective receptacles fitted with means of handling. Such a package must not weigh more than 100 kg; or ·(c) in hermetically - closed welded or seamless metal drums fitted with bands and rolling hoops and not filled beyond 93 per cent of their capacity. Class 6.1 (2) Substances of 13° (c) shall be packed: (a) in hermetically - closed receptacles made of glass, porcelain, stone - ware or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in hermetically - closed metal receptacles having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or ,(c) in hermetically - closed metal drums having, ifneces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops· or (d) in hermetically - closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg· or (e) in bags made of a suitable plastics material, so closed as to be leak - proof, and placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 7 5 kg. Substances of 14 ° sall de packed: (a) in welded steel drums with openings closed by two plugs, one placed over the other, one of them being screw· threaded, the drums being fitted with rolling hoops. The drums must not be filled beyond 95 per cent of. their capacity; or (b) in receptacles made of strong black sheet - iron or of tin - plate and hermeticaly closed. A tin - plate recep­ tacle must not, with its content, weigh more than 6 kg. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden packing case. Such a package must not weigh more than 7 5 kg. (1) Substances of 21 ° (a), (b), (c) and (d), and liquids of 21 ° (e) and (f), shall de packed: Class 6.1 (a) in hermetically - closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a 2611 2612 package must a not weigh more than 75 kg. Packages wighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in flame - sealed glass ampoules containing not more than 100 g, which shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules mu~t not be filled beyond 95 per cent of their' capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means. of handling, or (c) in hermetically - closed metal receptacles having, if .necessary, a suitable lining, and having a capacity not exceeding ~ 5 litres. These receptacles shall be secured • by absorbent cushioning materials in a wooden case or in some other outer outer packaging of sufficient strength. The receptacles must nCJt be filled beyond 95 per cent of their capacity. Much a package must not weigh more than 100 kg; or • (d) in hermetically - closed metal drums having, if neces­ sary, a suitable lining. The drums must mot be filled beyond 95 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. • (2) Substances of 21 ° (h), (c) and liquids of 21 ° (e) and (f) may also be packed in hermeti~ally - closed ca~isters made of a suitable metal, welded or hard - soldered, having a capacity not exceeding 60 litres, and fitted with means of handling. The canisters must not be filled beyond 95 per cent of their capacity. (3) Substances of 21° (e) and (f) in the solid state, and substances of 21 • (g), (h), (i) and (k), shall be packed:. ·(a) in hermetically - closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics matedal, which must not contain more. than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substange. These. receptacles shall be secured by cushioning materialiin' a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in hermetically - closed metal receptacles having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh. more than 100 kg; or (c) in hermetically - closed metal drums having, if neces­ sary, a suitable lining. If the drums weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. (4) Substances of 21 ° (e) and (f) in the solid state, and substances of 21 ° (g) and (h),-may also be packed: (a) in bags mad~ of a suitable plasti~s material, so closed as to be leakproof, and placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 7 5 kg; or (b) in hermetically - closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg. ( 5) Substances of 21 ° (g) may also be packed in hermeti­ cally - closed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of • some other material of sufficient strength. ,,. (6) Substances of 210 (1), (m), (n), (o) and (p) ~hall be packed: • (a) in hermetically - closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must n! >t be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 3, kg, other than those forwarded as a·foll 2216 E<l>HMEPlr THE KYBEPNHEEQE (TEYXOr nPQTO) load, shall be fitted with means of handling; or (b) in flame - sealed glass ampoules containing not more than 100 g, which shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (c) in hermetically - closed metal receptacles having, if necessary, a suitable lining, and having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some oth~r outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package ·must not weigh more than 100 kg; or {d) in hermetically - closed canisters made of a suitable metal, welded or hard - soldered, having a capacity not exceeding 60 litres, and fitted with means 1,>f handling. The canisters must not be filled beyond 95 per cent of their capacity; or (e) in hermetically - closed metal drums having, if neces­ sary, a suitable lining. The drums must not be filled beyond 95 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. (7) 4 - nitrotoluene [21 ° (1)] may also be packed: (a) in bags made of a suitable plastics material, so closed as to be leak - proof, and placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in hermetically - closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg; or (c) in bags made of stout paper of four plies, lined with a bag made of a suitable plastics material, so closed as to be leak - proof. Such a package must not weigh more than 55 kg. (8) Substances of 21 ° (o) in flakes may also be packed in bags made of stout paper of four plies, lined with a bag made of a suitable plastics material and so closed as to be leak - proof. Such a package must not weigh more than 55 kg. Substances of 22° shall be packed: (a) in hermetically - closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptaclei, made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 7 5 kg; or (b) in hermetically-closed metal receptacles having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg or (c) in hermetically-closed metal drums having, if neces­ sru:y, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (d) in hermetically:closed receptacles, made of a sui­ t~ble plastics material, of a capacity not exceeding 60 htres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength; or (e) in bags made of a suitable material, so closed as to be leak-proof, and placed in a wooden case or in some other outer packaging of sufficient strength. Such a pac­ kage must not weigh more than 75 kg; or (I) in hermetically-closed wooden casks of sufficient 2613 strength, with a suitable lining. Such a package must not weigh more than 250 kg. • (1) liquids of 23° shall be packed: (a) in hermetically-closed receptacles made of glass~ porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a · package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or • (b) in flame-sealed glass ampoules containing not more than 100 g, which shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules must not be filled beyond 95 per cent of their capacity. Such a pac~age must not weigh more than 75 kg. Packages weigh­ ting more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or ' (c) in hermetically-closed metal receptacles having, if necessary, a suitable lining, and having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning material in a wooden case or in some other outer packaging of sufficient strength. The receptacles must no t be filled beyond 95 per cent of their capacity. Such a package must not weigh more than l00 kg; or ( d) in hermetically-closed metal drums having, if neces ' sary, a suitab}e lining. The drums must not be filled beyond 95 per cent of their capacity. If they weigh, with their contents, more than 275 kg, they shall be fitted with rolling hoops. (2) ·solids of 23° shall be packed in the same way as substances of 22° .. (1) Substances of 31 ° (a) and solid preparations of 31 ° (c) shall be packed: (a) in hermetically-closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaginp: of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in hermetically-closed metal receptacl~s having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or (c) in hermetically-closed metal drums having, if neces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (d) in hermetically-closed receptacles, made of a sui­ t~ble plastics material of a capacity not exceeding 60 ~•Ires. These receptacle~ shal~ be placed singly and tightly m a protective packagmg with complete sides, made of paperboard or of some other material of sufficient strength; or (e) in hermetically-closed wooden casks of sufficient strength, with suitable lining. Such a package must not weigh more than 250 kg. (2) Substances of 31 ° (b) and liquid preparations of 31° (c) shall be packed: (a) i~ hermetically-closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres. T hese recertac)es shall be secured by absorbent cushio­ nmg matenals m a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh- • mg more than 30 kg, other than those forwarded as a full 2614 2615 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2217 load, shall be fitted with means of handling; or· (b) in flame-sealed glass ampoules containing not more than 100 g, which shall be secured by absorbent cushio­ ning materials in a wooden case or in some outer packaging of sufficient strength. The ampoules must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means 9f handling; or (c) in hermetically-closed metal receptacles having, if necessary, a suitable lining, and having a capasity not exceeding 15 litres. These receptacl~ shall be secured . by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must •not weigh more than 100 kg; or (d) in hermetically-closed clinisters made of a suitable metal, welded or hard-soldered, having a capacity not exceeding 60 litres, and fitted with means of handling. The canisters must not be filled beyond 95 per cent of their capacity; or . (e) in hermetically-closed metal drums having, if neces­ sary, a suitable lining. The drums must not be filled beyond 95 per cent of their capacity. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops. (1) Sodium azide [32°(a)] shall be packed in receptacles made of black sheet-iron or tin-plate. (2) Substance of 32°(b) shall be packed in receptacles made of glass or of a suitable plastics material. A recep­ tacle must not contain more than 10 kg of barium azide nor more than 20 litres of barium azide solution. The receptacles shall be secured separately, by absorbent cushioning materials, in case or .in iron hampers with complete sides; the volume of the cushioning material must.be at least equal to that of the content of the recep­ tacle. Where hampers are used, the cushioning materials, if readily inflammable; shall be fireproofed sufficiently to prevent ignition on contact •with a flame. Zinc phosphide (33°) shall be packed in metal receptac- • 2617 les secured in wooden cases. A package must not weigh more than 7 5 kg. Substances of 41 ° shall be enclosed in wooden or metal 2618 packaging which may be fitted with a device allowing gases to escape. Finely granulated substances may also be pac ked in bags. Substances of 51 ° shall be packed: 2619 (a) in hermetically-closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured bv cushioning mate.rials in a wooden case or in some other outer packaging of sufficient strength. Such a package must 11ot weigh more than 75 kg; or (b) in hermetically-closed metal receptacles having, if necessary, a suitable lining, and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or • (c) in hermetically-closed metal drums having, if neces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (d) in hermetically-closed receptacles, made of a sui­ table plastics material, of a capacity not' exceeding 60 • litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength; or (e) in bags made of a suitable plastics material, so closed as t.o be leak-proof, which shall be placed in a wooden.case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (f) in hermetically-closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg. (1) Substances of 52° shall be packed: 2620 (a) in hermetically-closed receptacles made of glass, porcelain, stoneware, or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each; receptacles made plastics material may, if forwarded as a full load, contain up to 10 kg of substance. The receptacles shall be secured by cushioning materials in. a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in hermetically-closed metal receptacles having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or (c) in hermetically-closed metal drums having, if neces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (d) in hermetically-closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength; or (e) in bags made of a suitable .plastics material, so closed at to be leak-proof, which shall be j:>\aced in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (I) in receptacles made of wood or paperboard,J~~ed with a vapour-tight plastics material and hermetically clo- • sed. Such a package must not weigh more than 75 kg; or (g) in hermetically-closed metal receptacles. Such a package must not weigh more than 7 5 kg. (2) When forwarded as a full load, the substances may also be packed: (a) in hermetically-closed wooden casks of sufficient strength, with a suitabl~ lining. Such a package must not weigh more than 250 kg; or (b) in bags made of stout paper of four plies, lined with a bag made of a suitable plastics material, so closed as to be leak-proof. Such a package must not weigh more than 55 kg. (1) Solids of 53° shall be packed: 2621 (a) not more than 10 kg per bag, in bags made of paper of two plies; or (b) in bags made of a suitable plastics material; or ( c) in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material; or (d) in steel receptacles or in strong wooden casks or in wooden cases fitted with strengthening bands. Re (a), (b) and (c): The receptacles and bags shall be secured by cushioning materials in wooden outer packa­ gings. (2) Liquids or substances in solution of 53° shall be pac­ ked: (a) in receptacles made of glass, porcelain, stoneware or similar materials. These receptacles' shall be secured by cushioning materials in protective packagings which, if not cases, shall be fitted with means of handling; or (b) in metal receptacles. (3) A package containing fragile receptacles or bags made of a plastics material must not weigh more than 75 kg. . Thallium compounds (54°) shall be pa~ked: 2622 (a) in hermetically-closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material which· must not contain more tl1an 5 kg each. Receptacles made of plastics material may, if forwitr 2218 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured by cushioning materials in a wooden ·case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in tin-plate receptacles; or (c) in wooden cases fitted with strengthening bands; or (d) in wooden cases fitted with iron hoops or strong wooden hoops. . (1) Substances of 61° and 62°, other than those of 61 °(1 ), shall be packed: (a) in hermetically-closed receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding five litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more.than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in flame-sealed glass ampoules containing not more than 100 g, which shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The ampoules must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (c) in hermetically-closed metal receptacles having, if necessary, a suitable lining, and having a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (d) ii'! hermetically-closed canisters made of a suitable metal, welded or hard-soldered, having a· capacity not exceeding 60 litres, and fitted with means of handling. The canisters must not be filled beyond 95 per cent of their capacity; or (e) in hermetically-closed metal drums having, if neces­ sary, a suitable lining. The drums must not be fiJled beyond 95 per cent of their capacity. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (f) in hermetically-closed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper­ board or of some other material of sufficient strength. The receptacles must not be filled b eyond 95 per cent of their capacity. (2) Substances of 61 ° (1) shall be packed: (a) in all-welded steel drums with walls not less than 1.25 mm thick, fitted with rolling hoops and reinforcing ribs and having the openings closed by two plugs, on~ placed over the other, one of them being screw-threaded; or (b) in sheet-steel canisters with walls not less than 1 mm thick and a capacity not exceeding 60 litres, the openings being closed by two plugs, one placed. over the other, one of them being screw-threaded. The sheet-steel canisters must have welded lengthwise seams, two reinforcing ribs in the walls, and a protective rim below the joint recessed at the bottom. Canisters with a capacity of 40 to 60 litres must have their bottoms welded on and be fitted with means of handling on the side; or (c) in aluminium bottles of a capacity not exceeding 2 litres, secured by infusorial-earth cushioning in sheet­ metal receptacles whoce lids shall be firinly stuck down by means of suitable adhesive strips. The sheet~metal receptacles shall be placed, with filling materials, in woo­ den cases. A package must not weigh more than 75 kg; or (d) in non-returnable metal drums (new packagings 2623 intended to be used only once); these drums, whose walls shall be not less than 1.2 mm thick, shall be provided with a screw-threaded plug fitted with a gasket. The plug shall be situated in one of the ends of the drum and be protected by the rim. The drums may have a body with ends recessed, the joints being strengthened by climb . reinforcements; if they do not possess rolling hoops they must be provided with reinforcing ribs. A package must not weigh more than 200 kg. Carriage in non-returnable drums shall take place only as a full load on open vehicles; or (e) in non-returnable steel drums (new packagings inte11ded to be used only once) having sides made of sheet steel 1.24 mm thick, ends made of sheet steel 1.5 mm thick, and a tare weight of 22.5 kg; the drums must be provided with reinforcing ribs. The body seam shall be welded and the ends shall be double-seamed by welting to the body, with a polyethylene liner inserted. Two screw­ plug closure U!1its, one of 50.8 ·mm (2) and one of 19.05 mm (3/4), shall be double-seamed by welting to one of the ends, with a synthetic-rubber liner inserted. Thin-sheet~steel caps shall be placed over the closure units. (3) The receptacles referred to under (2)(2) to (e) must not be filled beyond 93 per cent of their capacity. Substances of 71 ° shall be packed: (a) in iron or wooden packagings; or (b) in bags made of stout paper of at least two plies, or made of jute, lined with a bag made of a suitable plastics ml!,terial, so closed as to be leak-proof. • (1) Substances of 72° and 73° shall be packed: (a) in hermetically-closed receptacles made of glass, porcelain, stoneware or similar· materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substance. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or • (b) in steel or wooden packagings; or (c) in bags made of stout paper of at least 2 plies. However, bags for lead acetate must be made: 1. of hemp lined with a suitable plastics material or with stout crepe paper stuck on with bitumen; such a bag, with its contents, must not weigh more than 30 kg; or 2. of stout paper of at least two plies, lined with a bag made of suitable plastics material; such a bag, with its contents, must not weigh more than 30 kg; or 3. of stout paper of at least five plies, lined with a bag made of suitable plastics material; such a bag, with its contents, must not weigh more than 55 kg; or • 4. of stout paper of at least three plies, placed in jute bags; such a bag,' with its contents, must not weigh more than 55 kg; or (d) in bags made of suitable plastics material, so closed as ·lo be leak-proof, which shall be placed in a wooden case or in some other outer packaging of sufficient stren­ gttri. Such a package must not weigh more than 75 kg. (2) Substances of 72° may also be packed in receptacles made of tin-plate or of sheet-steel. Substances of 74° and 75° shall be packed: (a) in hermetically-closed receptacles made of glass, porcelain stoneware or similar materials, or of a suitable plastics material, which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full load, contain up to 10 kg of substance. These receptables shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (b) in steel or wooden packagings; or (c) in bags made of stout paper of at least 2 plies or in jute bags; or ' (d) in receptacles made of tin-plate !?r sheet-steel. Pesticides of 81 ° shall be packed: .~ 2024 2625 2626 2627 <l>EK 225 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2219 (a) in solid or paste form: 1. in hermetically-closed receptacles: made ·of glass, porcelain stoneware or similar materials, or of a -suitable plastics material , which must not contain more than 5 kg each. Receptacles made of plastics material may, if forwar­ ded as a full l<;1ad, contain up to 10 kg of substance. These receptables shall be secured by cushioning materials in a wooden case o~ in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or 2. in hermetically-closed metal receptacles having, if necessary, a suitable lining and which must not contain more than 15 kg each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient sirength. Such a package must not weigh more than 100 kg; or Class 6.1 3. in hermetically - closed metal drums having, if neces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; 4. in hermetically - closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient stren­ gth; or 5. in bags made of a suitable plastics material, so closed as to be leak-proof, which shall be placed in a wooden case or in some other outer packaging of sufficient stren­ ght. Such a package must not weigh more than 75 kg; or 6. in receptacles made of wood or paperboard, lined with a vapour-tight plastics material and hermetically clo­ sed. Such a package must not weigh more than 75 kg; or 7. in hermetically-closed metal receptacles. Such a pac­ kage must not weigh more than 75 kg; 8. arsenical compounds forwarded as a full load may also be packed in hermetically-closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh more than 250 kg; 9. preparations may also be enclosed in packagings ready for use, which shall be firmly packed in a wooden case or in some other outer packaging of sufficient stren­ gth. Such a package must not weigh more than 75 kg; (b) in liquid form: 1. in receptacles made of glass, porcelain, stoneware or similar materials, or of a suitable plastics material, of a capacity not exceeding 5 litres, with the opening closed by two plugs, one placed over the other, one of them being screw-threaded. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 93 per cent of their capacity. Such a package must not weigh more tnan 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or 2. in flame-sealed glass ampoules containing not more than 50 g; which shall be secured by absorbent cushioning materials in a wooden case or in some other outer packa­ ging of sufficient strength. The ampoules must not be filled beyond 93 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or 3. in metal receptacles having, if necessary, a suitable lining, the receptacles having a capacity not exceeding 15 litres and having the openings closed by two plugs, one placed over the other, one of them being screw-threaded. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles must not be filled beyond 93 per cent of their capacity. Such a package must not weigh more than 100 kg; or 2627 2627 4. in canisters made of a suitable metal, welded or hard-soldered, with walls not less than 0.5 mm thick and a capacity not exceeding 60 litres, the openings being closed by two plugs, one placed over the other, one of them being screw-threaded, the canisters being fitted with means of handling. The canisters must not be filled bey­ ond 93 per cent of their capacity; or 5. in hermetically-closed metal drums having, if neces­ sary, a suitable lining. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops. The drums must not be filled beyond 93 per cent of their capacity; or • 6. in receptacles made of a suitable plastics materiai, of a capacity not exceeding 60. litres, the openings being closed by two plugs, one placed over th other, one of them being screw-threaded. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength: The receptacles must not be filled bey ond 93 per cent of their capacity. • Pesticides of 820 shall be packed: (a) in solid form: 1. in the same way as solids of 810; 2. when forwarded as a full load, also in bags made of stout paper of four plies, lined with a bag made of a suitable plastics material, so closed as to be leak-proof. Such a package must not weigh more than 55 kg; (b) in liquid form: in the same way as liquids of 810. Pesticides of 830 sh~ll be packed: (a) in solid form: 1. in the same way as solids of 810; or 2. in jute bags ·rendered impermeable to moisture by a lining made of a suitable material, stuck on with bit­ umen, or in jute bags lined with a bag made ·of a suitable plastics material, so closed as to be leak-proof. Such a package rr;;.ist not weigh more than 55 kg; or • 3· in the case of preparations, and of other pesticides if they are forwarded as a full load, in bags made of stout paper of four plies, lined with a bag made of a suitable plastics material and hermetically closed. Such a package must not weigh more than 55 kg; or 4. in the case of solid arsenical • compounds: i. in double-walled wooden casks lined with stout paper; or ii. in fibreboard boxes placed in a wooden case; or iii. not more than 12.5 kg per bag, in double bags, made of stout paper or of a suitable plastics material, which shall be placed either in a wooden case lined with stout paper or tightly in a stout case made of double-faced corrugated fibreboard or of solid fibreboard of equivalent strength, the case being lined with stout paper. All joints and flaps shall be covered over with adhesive strips. A package comprising a fibreboard case must not weigh more than 30 kg. . 5. in the case of arsenical compounds forwarded as i> complete load: i. in ordinary wooden packagings lined with stout paper; or ii. not more than 25 kg,per bag, in two-ply paper bags, or in bags made· of a suitable plastics material, which shall . be plac ed separately in bags made of jute or of a similar material lined with crepe paper; or iii. in bags made of paper of at least three pli~s or in ~wo-ply paper bags lined a bag made of a suitable plastics material. Such a package must not weigh more than 20 kg; or iv. in two-ply paper bags or in bags made of a suitable plastic material, which shall be placed in four-ply paper bags. Such a package must not weigh more than 60 kg. In cases as referred to under iii. and iv. above, each consignment must be accompanied by empty bags in the proportion of 1 for every 20 bags coiitaining arsenical substances, these empty bags being intended to accommo­ date such quantity of substances as may escape from bags damaged during carriage. 2628 2629 2220 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) (b) inliquid form: 1. in the same way as liquids of 810; or 2.' in the case of preparations: i. in hermetically-closed cylindrical receptacles made of glass, porcelain, stoneware or similar materials, of a capacity not exceeding 25 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient stren­ ght. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 7 5 kg; or ii. in hermetically-closed glass carboys, of a capacity not exceeding 25 litres, which shall be secured by absor­ bent cushioning materials in a wooden case or in some other outer packaging of sufficient strength, or which shall be well secured in iron or wicker hampers. The carboys must not be filled beyond 95 per cent of their capacity. Such !I packag~ must not weigh more than 75 kg; or iii. in receptacles, made of a suitable plastics material, with walls not less than 4 mm thick and a capacity non exceeding 60 litrs, the openings being closed by two plugs, one placed over the other, one of them being screw­ threaded, the recepatcles having to protective packaging if the competent authority of the country of departure so allows. The receptacles must not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Substances of 84° shall be packed: (a) in the same way as solids of 81 °; or (b) in the case of substances of 84° (a) very conspicuously· 2630 coloured, in hags made of paper of al least two plies, or of a suitable plastics material, which shall be placed in textile bags; or (c) in the case of substances of 84°(b), in closely-woven jute bags. 3. Mixed packing (1) Substances grouped under the same item number may be included i!l the same package. The inner packa­ gings shall conform to what is prescribed for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. . • (2) If smaller quantities are not prescribed in the section headed •Packing of a single substance», substances of this Class, in quantities not exceeding 6 kg in the case of solids or ·3 litres in the case of liquids for all of the substances listed under the same item number or the same letter, may be enclosed in the same package either with substan­ ces of another item number or of another letter of the same Class, or with dangerous substances belonging to other Classes (if mixed packing is likewise allowed in the case of such substances), or with other goods, subject to the following special conditions: The inner packagings must satisfy the general and spe­ cial conditions of packing. In addition, the general provi­ sions of marginals 2001 (5) and 2002 (6) and (7) must be observed. • A package must not weigh more than 150 kg, or more than 75 kg if it contains fragile receptacles. Special conditions: Maximum quantity Item Description of • per ~\ per Special provisions No Substance receptade package 1 °(a) Hydrocyanic: acid mixed pacuing not allowed 1 °(b) Solutions of hydrocyanic 1 litre llitre Must not be packed togeffier acid containing not more with any other acid than 4% hydrocyanic acic (solutions containing mon than 4% are prohibited) 20 Acrylonitrile, acetonitrile, 1 litre 1 litre Must not be packed together isobutyronitrile with substances of Classes 5.1 and 8. Glass receptacles must be secured by cushio ning materials in protective receotacles 5°(a) Nickel carbonyl mixed pacuing not allowed 11 °(a) 2-cyanopropan-2-ol 1 litre 1 litre Must not be packed togeilier with substacnes of Classes 5.1 and 8. Glass receptacles must be secured by cusioning materials in protective recep tacles 13°(6) Dimentyl sulphate 1 litre 3 litres · 31 °(a) Cyanides in a solid form Must not be packed together with substances of an acid nature in fragile receptacles 500g 500g in other receptacles 5 kg 5 kg 31 °(b) Solutions of inogranic cya 1 litre 3 litres nides 41 °(b) Ferro-silicon alloys with 2.5 kg 2.5 kg, aluminium '-· 2631 E<l>HM.EPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2221 4. Marking and danger labels on packages (see Appen­ dix A.9) (1) Packages containing substances of 1 ° - 5°, 11 ° 14°, 21° - 23°, 31° - 33°, 41°, 51° - 54°, 81° and 82° shall bear a label conforming to model No. 4; packages containing substances of 2°, 4°(a), 5° and 11 °(a) shall bear, in addition a label conformating to model No. 2A. Packages containing substances of 61 °, 62°, 71°-75°, 83° and 84° shall bear a label conforming to model No. 4A. (2) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9, If the-fragile receptacles contain liquids, the packa­ ges shall in addition, except in the case of sealed ampou­ les, bear labels conforming to model No. 8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. (3) In the case of consignments forwarded as a full load, labels Nos. 2A, 4 or 4A need not be affixed to the packages if the vehicle bears the marking prescribed in Annex B, marginal 10500. B. Particulars in the transport document (1) In the case of substances which are referred to by name in the list of substances (marginal 2601), the des­ cription of the goods in the transport document must con­ form to the name underlined in marginal 2601. The des­ cription of the goods must be underlined in red and follo­ wed by particulars of the Class, the item number (together with the letter, if any), and the initials «ADR» or «RID» [e.g. 6.1, lo(a), ADR]. In the case of substances which are not referred to by name in the list of substances (marginal 2601), the trade name or the chemical name must be used. This description must be underlined in red and followed by particulars of the .-Class and item number (together with the letter, if any) of the substance presenting a comparable degree of danger, and the initials «ADR» [e.g. 6.1, 21°(m), ADR). (2) In the case ofhydrocyanic acid [lo(a)] the following must be certified 1n the transport document: «The nature of the goods, and the packaging, are in conformity with the provisions of ADR». (3) In the case of substances of 41 °, the following must be certified in the transport document: «Stored in the open air and in a dry place for not less than three days». (4) In the case of consignments of substances which polymeriz easily, the following must be certified in the transport document: «The necessary steps have been ta­ ken to prevent polymerization during carriage», C. Empty packagings 2632 2633 2634 2634 2635 2642 (1) Bags of 91 ° and 92° must be packed in cases or in 2643 impermeable bags preventing any loss of substances. (2) Other packagings and tanks of 91 ° and 92° must be closed the same manner and leak-proof in the same degree as though they were full. • • (3) Packagings of 91 ° forwarded otherwise than as a full load, tanks, and packed bags of 91 ° shall bear lab~ls conforming to model No. 4; packed bags of 92° shall bear labels conforming to model No. 4A (see Appendix A.9). (4) The description in the transport document must be: «Empty packaging, 6.1, 91 ° (or 92°), ADR (or RID). This description must be underlined in red. 2644 2649 CLASS 6.2 REPUGNANT SUBSTANCES AND SUBSTANCES LIABLE TO CAUSE INFECTION 1. List of substances Among the substances and articles covered by the hea 1 2650 ding of Class 6.2, only those listed in marginal 2651 are to be accepted for carriage, and then only subject to the· provisions of this Annex and of Annex B. These substan­ ces and articles to be accepted for carriage under certain conditions are to be considered as substances and articles of ADR. • 1 ° (a) Fresh tendons, clippings of fresh skins not limed or salted, trimmings from fresh tendons or from dippings of fresh skins; Note: Clippings of wet fresh skins, limed or salted, are not subject to the provisions of ADR. (b) fresh horns, claws or hoofs not cleansed ·of bone and soft adhering parts, fresh bones not cleansed of ·flesh or other soft adhering parts; • • (c) undressed pig's bristles and hair. 2° Fresh skins, unsalted or salted, from which effensive quantities of blood or brine drip. Note: Properly salted skins containing only a small qua­ ntity of moisture are not subject to the provisions of ADR. 3° Cleaned or dried bones, cleaned or dried horns, claws or hoofs. Note: Dry bones divested of fat, not giving off any putrid odour, are not subject to the provisions of ADR. 4° Fresh calf rennets, cleansed of all traces of edible matter. Note: Dried calf rennets not giving of an offensive odour are not subject to the provisions of ADR. 5° Compressed residues arising from the manufacture of skin glue (calcareous residues, residues from the liming of skin clippings, or residues used as fertilizers). 6° Non-compressed residues arising from the manufact­ ure of skin glue 7° Non-infected urine protected against decomposi­ tion. 8° Anatomical pieces, entrails and glands. (a) non infected (b) infected 9o Manure. 10° Excrement. 11 ° Other animal substances, repugnant or liable to cause infection, not already specifically mentioned in 1 ° to 10°. 12° Empty packagings and empty bags which have contained substances of 1° to 8°, 10° and 11°, and sheets which have been used to cover substances of Class 6.2. Note: If uncleaned, these packagings, bags and sheets are not to be accepted for carriage. 2. Provisions .A. Packages 1. General conditions of packing (.1) Packagings shall be so closed and leak-proof as to prevent any loss of the contents. (2) Packagings, including their closures, ~ust be suffi­ ciently rigid and strong in all their parts to prevent any loosening during carriage and to meet the normal require­ ments of carriage. In particular where substances are in the liquid state or are liable to ferment, receptacles and their closures must, unless L'1e section headed «Packing of a single substance• provides otherwise, be able to withs­ tand any pressure which, the presence of air also being taken into account, may arise inside the receptacles in normal carriage. For this purpose a free space must be left, account being taken of the • difference betwen the temperature of the substances at the time of filling and the highest mean temperature which they are likely to reach during carriage. (3) No trace of the contents must adhere to the outside of packages. 2. Packing of a single substance Substances of lo shall be packed: {a) if forwarded otherwise than as a full load: 1. in metal receptacles fitted with a safety closure ca­ pable of yielding to internal pressure, or in casks, small vats or cases; or 2651 2651 2652 2653 2222 E<I>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2. in the case of substances of lo (c) in the dry state, also i bags; on condition that the bad odour can be removed by disinfection. In the case of substances not in the dry state, packing in bags is allowed only from 1 November to 15 April; (b) if forwarded as a full load: 1. in the packagings specified in (a) 1. above; or 2. on condition that the bad odour can be removed by di­ sinfection,. in bags impregnated with suitable disinfec­ tants. Substances of 2 ° shall be packed: (a) if forwarded otherwise than as a full load: 1. in casks, small vats or cases; or 2. during the months from November to February incl­ usive, in bags impregnated with suitable disinfectants, on condition that the bad odour can be removed by disinfec­ tion; (b) if forwarded as a full load: 1. in the packagings specified in (a) 1. above; or 2. on condition that the bad odour be removed by disin­ fection,- in bags impregnated with suitable disinfectants. Substances of 3 ° shall be packed in casks, small vats, cases, metal receptacles or bags. Substances of 4 ° shall be packed: (a) if forwarded otherwise than as a full load: in casks, small vats, cases, metal receptacles or bags; (b) if forwarded as a full load: in any suitable packa­ gings. Substances of 5 ° and 60 shall be packed in casks, small vats, cases or metal receptacles. Substances of 7 ° shall be packed in hermetically closed receptacles made of galvanized sheet-steel. (1) Substances of 8° shall be packed in metal recep­ tacles fitted with a safety closure capable of yielding to internal pressure, in casks or small vats; substances of 80 (a) may also be packed in cases. (2) Substances of 8 ° may also be packed as follows: (a) substances of 8° (a), in rec.eptacles made of glass, porcelain, stoneware, metal or a suitable plastics material.. These receptacles shall be placed, either singly or in groups, in a strong wooden case, with absorbent cushio­ ning materials if the receptacles are fragile. If the substances to be carried are immersed in a preserving fluid, the absorbent materials shall be sufficient in quantity to absorb all the fluid. The preserving fluid must not be in­ flammable. Packages weighing more than 30 kg shall be fitted with means of handling; (b) substances of 8 ° (b ), in suitable receptacles placed with cushioning materials in a strong wooden case having a metal lining rendered leak-prood e.g. by soldering. Pac­ kages weighing more than 30 kg shall be fitted with means of handling; Substances of 9° shall be forwarded only in bulk. Substances of 10° shall be packed in receptacles made of sheet-metal. Substances of 11 ° shall be packed in metal receptacles fitted with a safety closure capable of yielding to internal pressure, or in casks, small vats or cases. 3. Mixed packing Substances listed under an item number of marginal 2651 may be included in the same package only with substances listed under the same item number,and then only on condition that the packagings prescribed in sec­ tions A. l and 2 above are used. 4. Marking and danger labels on packages (see Ap­ pendix A.9) Packages containing fragile receptacles not visible from the outside shall bear a label conforming to model No. 9. If the fragile receptacles contain liqnids, the packages shall in addition, except in the case of sealed ampoules, bear la 2654 2655 2656 2657 2658 2659 2660 2661 2662 2663 2664 bels comforming to model No.8; these labels shall be af­ fixed high up on two opposite sides of cases or in an equiva­ lent manner ,with other packagings are used. B. Particulars in the transpori document The description of the goods in the transport document must conform to one of the names underlined in marginal 2651. Where the name the substance is not indicated, the trade name must be used. The description of the goods must be underlined in red and followed by particulars of the Class, the item number (together with the letter, if any), and the initials «ADR» or t•RID• [d.g. 6.2, lo (a), ADR]. Empty packagings ( 1) Articles of 120 shall be cleaned and treated with sui­ table disinfectants. (2) The description in the transport document must be: «Empty packaging (or empty bag, or sheet), 6.2, 120, ADR (or RID)». This des~ription must be underlined in red. CLASS 7 RADIOACTIVE SUBSTANCES Introduction 2665 2666 2667· 2672 2673 2674 2699 (1) Scope iloo (a) Among the substances with a specific activity of more than O. 002. microcurie per gramme and articles containing such substances, only those indicated in the schedules of marginal 2703 are to be accepted for carriage and then only under the conditions set out in the appropriate sched­ ules of the said marginal and in appendix A.6 (marginals 3600 to 3699). • (b) The substances and articles referred to in (a) are substances and articles of ADR NOTE. Cardiac pacemakers containing radioactive substances, when they have been surgically implanted in medical patients, or radiopharmaceuticals being carried inside patients in the course of medical treatment, are not subject to ADR. (2) Definitions and explanations A1 and A2 •A1• means the maximum activity of special form radio­ active substances permitted in a Type A package. «A • means the maximum activity of radioactive substance~, other than special form radioactive substances, permitted in a Type A package. These values either are listed in Ap­ pendix A.6 table XXi or may be derived in accordance with the procedure described in marginals 3690 and 3691 of Appendix A.6. Allowable number of packages «Allowable number1 of packages• means the maximum number of Fissile Class II or Fissile Class III packages wich may be grouped together in one place during carriage or during transit storage. * 1) When the group is made up of packages of different designs, the maximum number of packages shall be such that the following formula is satisfied: n1 + h2 + ~ +.... shall not exceed 1. In this l'ormula, NI N2 N3 n1, n2, n3 ... are the numbers of packages for which the corr~sponding allowable numbers are NI' N 2 , N 3 ... res­ pectively. Ea>HMEPll: THl: KYBEPNHl:EQl: (TEVXOl: nPQTO) 222,'3 Containment system «containment system» means the components of the packaging specified by designer as intended to retain the radioactive substance during carriage. Design «Desing» means the description of a special form substance, or of a package or a packaging of a particular kind, which enables it to be fully identified. The descrip­ tion ·may include specifications, enginnering drawings, reports demonstrating compliance with regulatory requi­ rements, and other relevant documentation. Fissile substances «Fissile substance» means plutonium-238, pluto­ nium-239, plutonium-241, uranium-233, uranium 235, and all substances containing any of these radionu­ clides. Unirradiated natural and depleted uranium do not come under this definition. Low-level solid radioactive substances «Low-level solid radiactive substance» (LLS) means any of the following: (a) Solids (e.g. consolidated wastes, activated substances) in which: . (i) the activity in normal carriage is and remains dis­ tributed throughout the solid or the collection of solids or is and remains uniformly distributed in a solid compact binding agent (such as concrets, bitumen, ceramic); (ii) the activity is and remains insoluble so that even under loss of packaging the loss of radioactive substance per package resulting from the effects of wind, rain, etc., of from total immersion in water is limited to less than 0.1 A2 in a period of one week; and . (iii) the activity averaged· throughout the radioactive subtance does not exceed 2x10-3 A/g. (b) Articles of non-radioactive substance which are contaminated with a radioactive substance, provided that the radioactive contamination is in a non-readily­ dispersible from and that the level of contamination ave­ raged over 1 m2 (or over the area of the surface if that area is less than 1 m2) does not exceed 20uCi/cm2 for beta and gamma emitters and the low-· toxicity alpha emitters indicated in Table XIX of Ap­ pendix A.6; and 2 uCi/cm2 for other alpha emitters. Low specific activity substances (1) «Low specific activity substances (l)» (LSA) means any of the following: (a) Uranium or thorium ores and physical or chemical concentrates of those ores: (b) Unirradiated natural or depleted uranium or unir­ radiated natural thorium;. (c) Tritium oxide in aqueous solutions, provided that the concentration· does not exceed 10 Ciflitre; (d) Substances in which the activity is uniformly dis­ tributed and which if they were reduced to their mi­ nimum volume in conditions likely to be encountered in carriage, such as dissolution in water with subsequent recrystallization; precipitation; evaporation; combu­ stion; abrasion; etc., would have an average specific acti­ vity of not more than 10-4 \/ g; (e) Articles on non-radioactive substance which are contaminated with a radioactive substance, provided that the non-fixed surface contamination does not ex­ ceed ten times the values in Table XIX of Appendix A,.6 and that the contaminated article or the contamination on the article, if it was reduced to its minimum volume in conditions likely to be encountered in carriage, such as dissolution in water with subsequent recrystallization; precipitation; evaporation; combustion; abrasion; etc., would have an average specific activity of not more than 10-4 A/g. Low specific activity substances (II) «Low specific activity substances (II)» (LSA) means any of the following: (a) Substances in which the activity in nor~al carriage is and remains uniformly distributed and in which the average specific activity does not exceed 10-4 A/g; (b) Articles of non-radioactive substance which are contaminated with a radioactive substance, provided that the radioactive contamination is in a non-readily­ dispersible form and that the level of contamination ave­ raged over 1 m2 ( of over the area of the surface if that area is less than 1 m2) does not exceed 1 uCif cm2for beta and gramma emitters and the low­ toxicity alpha emitters indicated in Table XIX of Ap­ pendix A.6; and 0.1 uCijcm2 for other alpha emitters. Maximum normal operating pressure «Maximum normal operating pressure» means the maximum pressure above atmosplieric pressure at mean sea-level that would develop in the containment system in a period of one year in conditions of temperature and solar radiation corresponding to environmental condi­ tions of transport in the absence of venting, external coo­ ling by an ancillary system, or operational controle during carriage. Multilateral approval «Multilateral approval» means approval by the com­ petent authority of the country of origin and by the com­ petent authority of each country in whose territory the consignment is to be carried. . .. ,. • Package . «Type A package» means a type A packaging together with its limited radioactive contents. As the contents of a Type A package are limited to A 1 or A 2 , such a package does not require approval by the competent authority. «Type B(U) package» means a Type B packaging, to­ gether with its radioactive contents, which since it is de- • signed in accordance with specified design and contain­ ment criteria requires .unilateral approval only of the package design and of any stowage provisions that may be necessary for heat dis~pation. «Type B(M) package» means A Type B packaging, to­ gether with its radioactive contents, which sirice its de­ sign fails to meet one or more of the specific additional design criteria for Type B(U) packages (see marginal 3603 of Appendix A.6) requires multilateral approval of the package design and, in certain circumstances, of the conditions of despatch. Packaging «Packaging» means the assembly of components ne­ cessary to ensure compliance with the packaging requi­ rements of this Class. It may, in particular, consist of one or more receptacles, absorbent materials, spacing structures, radiation shielding, and devices for cooling, for absorbing mechanical shocks and for thermal insula­ tion. These devices may include the vehicle with the tie­ down system when these are intended to form an integral part of the packaging. «Type A packaging» means a packaging which in normal carriage is able to prevent any loss or dispersal of the radioactive content and to retain its shielding function. The conditions of normal carriage shall be rep­ roduced by the tests prescribed in marginal 3635 and 3636 of Appendix A.6, which tests the packaging shall be shown to have passed. «Type B packaging» means a packaging.which is able 2224 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO} to withstand not only the conditions of normal carriage, as a Type A packaging does, but also a transport acci­ dent. The conditions of such an accident shall be reprod­ uced by the tests prescribed in marginals 3635 to 3637 of Appendix A.6, which tests the packaging, shall shown to have passed in the conditions likewise prescribed. Radiation leve «Radiation level» means the corresponding radiation dose-equivalent rate expressed in millirem per hour. Ra­ diation levels may be determined by instruments, com­ bined with the use of conversion tables where necessary of by calculation. Measured or calculated neutron flux densities may be converted into radiation levels by using the date given in the following table. Neutron flux densities to be regarded as equivalent to a radiation level- cif 1 mrem/h Energy of neu­ • tron Thermal 5 keV 20 keV 100 keV 500 keV 1 MeV 5 MeV 10.MeV , Flux density equivalent. to 1 mrem/h (n/cm2•s) 268 228 112 32 12 7.2 7.2 6.8 Note: Equivalent flux densities for energies between those listed above should obtained by linear interpola­ tion. Radioactive contents «Radioactive· contents» means the radioactive substance together with any contaminated solids, liquids or gases in the package. Special form radioactive substance «Special form radioactive substance» means either a non-dispersible solid radioactive substance or a sealed capsule containing a radioactive substance. The sealed capsule shall be so constructed that it can be opened only by destroying it. The special form radioactive substance shall meet the following requirements: (a) It shall have at least on dimension of not less than 5 mm; and (b) It shall comply with the relevant test requirements specified in marginals 3640 to 3642 of Appendix A.6. In general, the «special forrri» concept enables substances exhibiting a higher activity level to be incl­ uded in a Type A package. Specific activity The «specific activity» of a radionuclide means that ra­ dionuclide's activity per unit mass. The specific activity of a substance in which the radionuclides are essentially uniformly distributed is that substance's activity per unit mass. Trasnport index The «transport index» of a package means: (a) The number expressing the maximum radiation level in millirem per hour at i m from the external surface of the package; or (b) In the case of packages of Fissile Class II or Fissile Class III, the higher of the following numbers: the number expressing the maximum radiation level as under (a) above; and the number obtained by dividing 50 b the allowable number of such packages. The «transport index» of a container means either; the sum of the transport indices of all packages within the container, except that for containers carrying Fissile Class III packages, the transport index shall be 50 .unless the sum of the transport indices of the packages necessitates a higher figure. or for containers not carrying Fissile Class II or III packages and under full load, the number expressing the maximum radiation level in mrem/h at I m from the external surface of the container multiplied by the value in the following table appropriate to the maximum cross­ sectional area of the container. Multiplication factors Size of load Multiplication factor Measurement (cross-sectional area measurements of the load perpendicular to the direction of inte rest). I m2 and less fzf 1 m2 to 5 m2 fzf 5 m2 to 20 m2 fzf 20 m2 to 100 m2 I 3 6 19 (c) The figure expressing the transport index shall be rounded upwards to the first decimal place. Uncompressed gas «Uncompressed gas» means a gas at a pressure not exceeding the ambient atmospheric pressure at the time when the containment sytem is closed. Unilateral approval «Unilateral approval» means approval by the compe­ tent authority of the country of origin only. If the country of origin is not a party" to ADR, the approval shall require validation by the competent authority of the first ADR country reached by the consignment. Unirradiated uranium «Unirradiated uranium» means uranium containing not more than 10·6 g plutonium per g uranium-235 and a fission product activity of not more than 0.25 mCi per g uranium-235. • Unimidiated thorium «Unirradiated thorium• means thorium containing not more than 10·7 g of uranium-233 per g of thorium-232. Uranium; natural, depleted, enriched «Natural uranium» means chemically-separated ura­ nium with the naturally-occurring distribution of uranium isotopes (appromixately 99.28 per cent urani~m-238 and 0.72 per cent uranium-235). «Depleted uramu~• means uranium containing less than 0. 72 per cent uramum-235, the remainder being uranium-238. «Enriched uranium• means uranium containing more than 0. 72 per cent ura­ nium-235, the remainder being uranium-238. In all cases a very small amount of uranium-234 is present. 2700 Ecr>HMEPII: THI: KYBEPNHI:EQI: {TEYXOr nPQTO) 2225 (3) Prohibitions on mixed loading Si,bstances of class 7 contained in packages bearing a label conforming with models Nos. 6A, 6B or 6C shall not be loaded in the same vehicle together with substances and articles of Classes la (marginal 2101), lb (marginal 2131) or le (marginal 2171) contained in packages bea­ ring one or two labels conforming with model No. 1. The substances and articles of this class contain one or more of the radionuclides referred to in chapter VI of Appendix A.6 (marginals 3690 and 3691). The list hereunder specifies the different types of con­ signment: 1. Empty packages which have contained radioactive substances; , 2. Articles manufactured from natural or depleted ura nium or natural thorium; 3. Small quantities of radioactive substances; 4. Instruments and manufactured articles; 5. Low specific activity substances LSA (I) 6. Low specific activity substances LSA (II) 7. Low-level solid radioactive substances; 8. Radioactive substances in Type A packages; 9. Radioactive substances in Type B(U) packages; 10. Radioactive substances in Type B(M) packages; 11. Fissile substances; 12. Radioactive substances carried under special arran­ gement. 1. Substances Empty packages: with have contained radioactive substances. 2. Packaging/Package (a) Packaging shall be in accordance with the require­ ments given in marginal 3600 of Appendix A.6, and shall be securely closed and in good condition. (b) Permitted internal contamination levels: not more than 100 times those levels set out in paragraph 5. (c) Where an empty packaging includes natural or dep­ leted uranium or natural thorium in its structure its surface shall be covered with a substantial, inactive sheath made of metal or some other resistant material. Schedule 1 Danger labels on package. None Note: Anty labe indicating a danger shall be covered or removed. 3. Packages maximum radiation level 0.5 mrem/h at the surface of the package. 4. Mixed packing No provisions. 5. Contamination on packages Non-fixed external contamination limits: Beta/ gamma/low-toxicity alpha emitters 10·4 uCi/cm2 Natural/depleted uranium/ natural thorium 10·3 uCifcm2 Other alpha emitters 10·5 uCi/ cm2 For full details, see marginal 3651 of Appendix A.6. 6. Marking on packages (a) Packages shall be plainly and durably marked with the weight if over 50 kg. (b) Any marking indicating a radioactive danger shall not be visible. 7. Transport documents The transport document shall include the description «Radioactive substances (Empty packages), 7, schedule 1, ADR», with the name underlined in red. 8. Storage and despatch No provisions. 9. Carriage of packages in vehicles and' containers No pr<'visions. 10. Carriage in bulk iri vehicles and containers Not applicable. 2701 2702 2703 11. Carriage in lank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and containers None. 13. Prohibitions on mixed loading No provisions. 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers No provisions. 15. Other provisions None. 1. Substances Articles manufactured from natural or depleted ura­ nium or natural thorium. The outer surface of the uranium or thorium shall be covered by a substantial, inactive sheath made of metal or some other resistant material. Schedule 2 Danger labels on packages. None. NOTE: Such articles may for example be unused packa­ gings intendeded for the transport of radioactive substan­ ces. 2. Packaging/Package Packaging shall be in accordance with the requirements given in marginal 3600 of Appendix A.6. 3. Package maximum radiation level 0,5 mrem/h at the surface of the package. 4. Mixed packing No provisions. 5. Contamination on packages Non-fixed external contamination limits: Beta/ gamma/low-toxicity alpha emitters 1()·4 uCi/crri2 Natural/depleted uranium/ natural thorium 10·3 uCif cm 2 Other ~lpha emitters 10·5 uCifcm 2 For full details see marginal 3651 of Appendix A.6. 6. Marking on packages None. 7. Transport documents The transport document shall include the description «Radioactive substances (Manufactured articles), 7, sched­ ule 2, ADR», with the name underlined in red. 8. Storage and despatch No provisions. 9. Carriage of packages in vehicles and containers No provisions. 10. Carriage in bulk in vehicles and containers Not applicable. 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and containers None. 13. Prohibitions on mixed loading No provisions. 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers No provisions. 15. Other provisions None. 1. Substances Small quantities of radioactive substances in amounts which do not exceed those given in the table below and which do not contain more than 15 g of uranium-235. 2226 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Schedule 3 : ;,, Danger labels on packages. None (but see paragraph 15). Nature of ubstances So ids and gases Special form Other forms Tritium Liquids Tritium oxide in aqueous solutions less than 0.1 Ci/1 • between 0.1 Ci/1 and 1.0 Cijl greater than 1.0 Ci/1 Other Ii uids ac age limits 10-3 Al 10·3 A2 20 Ci* lO00Ci 100 Ci I Ci 104 A2 For mixtures o ra ionuc i es, see margma o AppP.ndix A.6. 2. Packaging/Package (a) Packaging shall be in accordance wi th the require ments given in marginal 3600 of Appendix A.6. . (b) During transport there shall be no leakage of radw­ active substances. 3. Package maximum radiation level 0.5 mrem/h at the surface of the package. 4. Mixed packing No provisions. 5. Contamination on packages Non-fixed external contamination limits: Beta/ gamma/low-toxicity alpha emitters 10·4 uCijcm2 Natural/depleted uranium/ natural thorium 10·3 uCijcm2 Other alpha emitters 10·5 u Ci/cm2 For full details, see marginal 3651 of Appendix A.6. 6. Marking on packages The outermost surface of the containment system shall be marked «RADIOACTIVE» as a warning on opening the package. . 7. Transport documents . . The transport document shall include the descnption «Radioactive substances (Small quantities), 7, schedule 3, ADR», with the name underlined in red. 8. Storage and despatch No provisions. 9. Carriage of packages in vehicles and containers No provisions. 10. Carriage in bulk in vehicles and containers Not permitted. 11. Carriage in tank vehicles and tank containers Not permitted. 12. Placards and labels on vehicles tank vehicles, lank containers and containers None. 13. Prohivitions on mixed loading No provisions. 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers See marginal 3695 (3) of Appendix A.6. 15. Other provisions (a) Accident provisions - see marginal 3695 (1) of Appendix A.6. (b) Decontamination in storage - see marginal 3695 (2) of Appendix A.6. (c) Radioactive substances which possess other hazar­ dous properties shall also comply with the provisions of the appropriate class. ,* The values for tritium also apply to tritium in activated luminous paint and tritium adsorbed on solid carriers. 1. Substances Instruments and Manufactured articles such as clocks, electronic tubes or apparatus, having radioactive substan­ ces as a component part, whose activity does not exceed the amounts given in the table below and which do not contain more than 15 g. of uranium-235 .. Nature of Item Package substances limits limit~ !Solids 10-2 Al Al Special form A2 Other forms 10-2 A2 Liquids 10-3 A2 10-1 A2 Gases Tritium 20 Ci* 200 Ci* Special form . 10-3 Al 10-2A1 Other forms 10·3 A2 10-2 A2 For mixtures of radionuclides, see marginal 3691 of Appendix A.6. ,. 2. Packaging/Package (a) Packaging shall be in accordance with the require­ ments given in marginal 3600 of Appendix A.6. (b) The instruments and articles shall be securely pac­ ked. 3 Package maximum radiation level 0.5 mrem/h at the surface of the package and 10 mrem/h at 10 cm from any point on the external surface of any unpacked instrument or article. 4. Mixed packing No provisions. 5. Contamination on packages Non-fixed external contamination limits: Beta/gamma/ low-toxicity alpha emitters 10·4 uCi/cm2 Natural/depleted uranium/ natural thorium 10-3 uCi/cm2 Other alpha emitters 10·5 uCi/cm2 For full der.ails, see marginal 3651 of Appendix A.6. 6. Marking on packages Each instrument or article (except radioluminescent ti­ mepieces or devices) shall bear the marking «RADIOAC­ TIVE». 7. Transport Documents The transport document shall include the description «Radioactive substances· (Instruments) or (Manufactured articles), 7, schedule 4, ADR», with the name underlined in red. 8. Storage and despatch No provisions. 9. Carriage of packages in vehicles and containers No provisions. 10. Carriage in bulk vehicles and containers Not applicable. 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and Labels on vehicles tank vehicles, tank ' containers and containers None. 13. Prohibitions on mixed loading No provisions. . 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers See marginal 3695 (3) of Appendix A.g, 15. Other provisions (a) Accident provisions - see marginal 3695 (1) of Appendix A.6. (b) Decontamination in storage - see marginal 3695 (2) of Appendix A.6. * The values for tritium also apply to tritium in activated luminous paint and tritium adsorbed on solid carriers, «l>EK 225 E<r>HMEPlr THr KYBEPNHl:EOr (TEYXOl: nPOTO) • 2227 Class 7 1. Substances Lo'w specific activity substances LSA(I), belonging to one of the following groups as defined fully in marginal 2?00(2): (i) uranium or thorium ores or concentrates (sub-papa (a) of definition) (ii) unirradiated natural or depleted uranium or unirra­ diated natural thorium (sub-papa (b) of definition) (iii) tritium oxide in aqueous solutions - concentration 10 Ci/l or less. (sub-para (c) of definition) (iv) substances with uniform activity under minimum volume conditions of not more than 10-4 A2/g (sub-para ( d) of definition). (v) Non-radioactive articles contaminated to not more than 10 times the package limits set in para 5 below and so that the specific activity under minimum volume conditions never exceeds 10-4 A2/g (sub-para (e) of definition). Schedule ·5 Danger labels on packages (see Appendix A. 9). Unless transported as a full a load, labels to models 6A, 68 or 6C shall be affixed externally to two opposite sides, see marginals 3653 to 3655 of Appendix A.6 for package category. The contepts shall be described on the labels as «Radioactive LSA•. Subsidiary labelling: (i) for thorium nitrate and uranium nitrate - model No. 3 la­ bels are required. (ii) for uranium hexafluoride - model No. 4 labels are req­ uired. If fissile substances are present the requirements of schedule II shall be met in addition to the requirements of this schedule. 2. Packaging/Package Packages transported other than as full load-packaging· shall be in accordance with the requirements of marginal 3600, marginal 3650 to 3655 and marginal 3656(1) to (4) of Appendix A.6. Substances of paragraph l(ii) above in massive solid form shall be packed so as to prevent abrasion, and in other solid forms shall be contained in a substantial sheath. 3. Package maximum radiation level 200 mrem/h at the surfate of the package and 10 mrem/h at 1 metre from that surface (see marginals 3653 to 3655 of Appendix· A.6). Except in the case of a full load when the limit ·is 1,000 mrem/h at the surface of the package and may exceed I 0 mrem/h at I metre from that surface (see m~rginal 3659(7) of Appendix A.6). 4. Mixed packing See marginal 3650 of Appendix A.6. 5. Contamination on packages . (a) Non-fixed external contamination limits for packages carried other than full load. Beta/gamma/low-toxicity alpha emrpiters 10·4 1,1Ci/cm2 • Natural/depleted uranium/natural thorium 10·3 1,1Ci/ cm2 Other alpha emitters 1 o-s 1,1Ci/ cm2 For full details, see marginal 3651 of Appendix A.6. (b) For packages carried in a full load - No provisions. 6. Marking on packages Packages transported as full load - stencilled or other­ wise marked «RADIOACTIVE LSA». Package transported other than full load - plainly and durably marked with the weight if over 50 kg. 7. Transport documents The transport document shall include the description «Radioactive substances (Low specific activity LSA (I)), 7, 2703 2703 schedule 5, ADR», with the name underline in red. and the details specified in marginals 3680 and 3681 of Appendix A.6. s: Storage and despatch (a) Storage and segregation from other dangerous goods see marginal 3658 (1) Appendix A.6. (b) Storage and sepregation from packages labelled «FOTO» - see marginal 240000 of Appendix 8.4 for seg­ regation table. (c) Total transport index limitation for storage, no limit except in the case Fissile Class II or III packages, see mar­ ginal 3658 (2) to (5) of Appendix. 9. Carriage of packages in vehicles and containers (a) Segregation from packages labelled «FOTO• - see marginal 240001 of Appendix 8.4 for segregation Table. (b) Total transport index limitatiQn - 50. This limit does not apply to a load, provided that if Fissile Class II or III packages are present the allowable number is not ex­ ceeded, (see marginal 3659(5) of Appendix A.6). (c) Maximum radiation levels for vehicles and large co­ ntainers in 'the case of a full load 200 mrem/h at surface 10 mrem/h at 2 metres from surface (see marginal 3659(1) of Appendix A.7) Also, for veh~cles - 2 mrem/h in any normally occupied position - see marginal 3659(8) of Appendix A.6. ( d) Packages not in conformity with the requirements of marginal 3600 shall be transported as full load, and the li­ mits in the following table shall not be exceeded: • Nature of substances Solids Tritium oxide in aqueous ·solutions Other liquids and gases Vehicle or large container activity limit N,.o.,limit 50,000 Ci 100 X A2 10. Carriage in bulk· in vehicles and containers • Permitted under full load provided that, after loading, external surfaces of vehicles are carefully cleaned by the consignor and provided that no leakage can occur under normal transport. Quantity limits as in the table in parag raph 9 above. • 11. Carriage in tank-vehicles and tank-containers (a) Carriage in tank-vehicles: permitted for liquids or so­ lids other than uranium hexafluoride and substances liable to sportaneous ignition (see Appendix A.6, marginal 3660); (b) Carriage in tank-containers: permitted for liquids 9r solids, including natural or depleted uranium hexafluoride (see Appendix A.6, marginal 3661). 12. Placards and labels on vehicles, tank vehicles, tank co­ ntainers and containers (see Appendices A.9 and 8.4) Containers - labels to models 6A, 68 or 6C'on all four sides. Vehicles and large· contaiers - placards to model in Appendix 8.4 marginal 240 010 on each lateral side and on rear wall of vehicle (see marginals 3659(6) and 71 500). Subsidiary labelling (i) for thorium nitrate and uranium nitrate - model No. 3 la­ bels are required (ii) for uranium hexafluoride - model No. 4 labels are req­ uired. 13. Prohibitions on mixed loading See marginal 2700(3). 14. Decontaminated of vehicles, tank vehicles, tank contai ners and containers • (a) For full load consignments, after unloading, vehicles to be decontaminated by the consignee to the levels in Table XIX.of Appendix A.6 unless to be used for carrying 2703 2703 2228 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) the same substances. See also marginal 3695( 4) of Ap­ pendix A.6. (b) For non-full load consignements, see marginal 3695(3) of Appendix A.6. 15. Other provisions .(a) Accident provisions - see marginal 3695(1) of Ap ~~ix ~ • ~ (b) Decontamination in storage - see marginal 3695(2) • of Appendix A.6. 1. Substances Low s~cific activity substances LSA(II) belonging to ei­ ther of the following groups as difened fully in marginal 2700(2): (i) substances with uniform activity of not more than 10-4 A2/g. (sub-para (a) of definition). (ii) non-radioactive articles contaminated non-dispersibly to a level not exceeding 1 µCi/ cm2 for beta and gamma emitters and low toxicity alpha emitters, or 0.1 µCijcm2 for other alpha emitters (sub-para (b) of definition). If fissile substances are present the requirements of schedule 11 shall be met in addition to the requir.ements of this schedule. 2. Packaging/Package Packaging shall be in accordance with the requirements of marginal 3600, marginal 3650 and marginal 3651 of Appendix A.6. 3. Package maximum radiation level Closed vehicles under conditions of marginal 3659(7) (a) of Appendix A.6 - 1000 mrem/h at the surface of the package and may exceed 10 mrem/h at one metre from that surface. All other vehicles not under the conditions of marginal 3659 (7)(a) of Appendix A.6 - '200 mrem/h at the surface of the package and 10 mrem/h at one metre from that surface. 4. Mixed packing See marginal 3650 of Appendix A.6. 5. Contamination on packages Non-fixed external contamination limits: Beta/gamma/low toxicity alpha emitters 104 UCi/cm2 • Natural/depleted uranium/natural tho-· rium l0·3UCi/cm2 Other alpha emitters 10·5UCijcm2 For full details, see marginal 3651 of Appendix A.6 Schedule 6 Danger labels on packages 2703 None required unless fissile substances are present (see Schedule 11 ). • 6. Maruing on packages Packages shall be stencilled or otherwise marked «RA­ DIOACTIVE LSA•. 7. Transport documents The transport document shall include the description «Radioactive substances (Low specific activity LSA (II)), 7, schedule 6, ADR, «with the name underlined in red, and the details specified in marginals 3680 and 3681 of Ap­ pendix A.6. 8. Storage and despatch Only under full load 9. Carriage of packages in vehicles and containers (a) Carriage only by full load (b) If the consignment includes Fissile Class II or III pac­ kages the allowable number shall not be exceeded. (see Schedule 11 ). (c) Maximum. radiation levels for vehicles and large conta i­ ners 2703 200 mrem/h at surface 10 mrem/h at 2 metres from surface (see marginal 3659(7) of Appendix A.6) Also, for vehicles - 2 mremjh in any normally occupied position - (see marginal 3659(8) of Appendix A.6) ( d) The limits in the following table shall not be exceeded: Nature of substances Vehicle or large container activity limit Solids Tritium ixode in aqueous solutions Other liquids and· gases No limit 50000 Ci 100 X A2 10. Carriage in bulk in vehicles and containers Not permitted. 11. Carriage in tank vehicles and tank containers Not permitted. 12. Placards and labels on vehicles, tank vehicles, tank co­ ntainers and containers (see Appendices A.9 and B.4) Containers - labels to 6A, 6B or 6C • on all four sides. Vehicles and large containers - placards to model in Ap­ pendix B.4, marginal 240 010 on each lateral side and on rear wall or vehicle (see marginals 3659(6) and 71 500). 13. Prohibitions on mixed loading See marginal 2700(3). 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers See marginal 36953(3) and (4) or Appendix A.6. 15. Other provisions Accident provisions - see marginal 3695 (1) of Ap­ pendix A.6. 1. Substances Low level solid radioactive substances LLS belonging t.o either of the following groups as defined fully in marginal 2700(2): . (i) substances with uniform activity of not more than 2 X 10·3 A2/g. (sub para (a) of definition). (ii) non-radioactive articles contaminated to a level not ex­ ceeding 20 UCijcm2 for beta and gamma emitters and low toxicity alpha emitters or 2. UCljcm2 for other alpha emit­ ters. (sub-para (b) of definition). , If fissile substances are present the requirements of schedule 11 shall be met' in addition to the requirements of this schedule. 2. Packaging/Package (a) Pac~aging shall be in accordance with the requirements ofmargmals 3600 and 3650 of AppendixA.6.and shall be capable of withstanding the tests set out- in marginal 3635(4) and (5) of Appendix A.6. (b) Under the conditions of the tests set out in (a) there shall be • (i) no loss or dispersal of the radioactive contents (ii) no increase of the maximum radiation level recorded or calculated at the external surface for the condition before the test. • 3. Package maximum radiation level • Closed vehicles under conditions of marginal 3659(7) (a) of Appendix A.6 - 1000 mrem/h at the surface of the package and may exceed 10 mrem/h at one metre from that surface. All other vehicles not under the conditions of '' marginal 3659(7) (a) of Appendix A.6 - 200 mrem/h at the surface of the package and 10 mrem/h at one metre from that surface. ·:b 2703 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2229 4. l\1ixed packing See marginal 3650. of Appendix A.6. Schedule .7 Danger labels· on packages None required unless fissile substances are present. (see schedule 11). 5. Contamination on packages No provisions. 6. Marking on packages Packages shall be stencilled or otherwise marked «RA­ DIOACTIVE LLS». 7. Transport documents The transport document. shall include the description «Radioactive substances (Low • level solid (LLS), 7, schedule 7, ADR», with the name underlined in red, and the details specified in marginals 3680 and 3681 of Ap­ pendix A.6. 8. Storage and· despatch Only under full load. 9. Carriage of packages in vehicles and containers (a) Carriage only by full load (b) If the consignment contains Fissile Class II or III pac­ kages the allowable number shall not be exceeded (see schedule 11 ). (c) Maximum radiation levels for vehicles and large contai­ ners. 200 mrem/h at surface 10 mrem/h at 2 metres from surface see marginal 3659(7) of Appendix A.6. Also, for vehicles - 2 mrem/h in any normally occupied positic;m - see marginal 3659(8) of Appendix A.6. • 10. Carriage in bulk in vehicles and containers, Not permitted. 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank co­ ntainers and containers (see Appendices A.9 and B.4) Containers - labels to model 6A, 6B or 6C on all four si­ des. Vehicles and large containers - placards to model in Ap­ pendix B.4, marginal 240 010 on each lateral side and on rear wall of vehicle (see marginals 3659(6) and 71 500). 13. Prohibitions on mixed loading See marginal 2700(3). 14. Decontamination of vehicles, tank vehicles, tank co~ . ntainers and containers After unloading, vehicles to becontaminated by the con­ signee to the level set in table XIX of Appendix A.6 unless to be used for carrying the same substances. See also mar­ ginal 3695(3) and of Appendix A.6. 15. Other provisions Accident provisions - see marginal 3695 (1) of Ap­ pendix A.6. Schedule 8 Danger labels on packages (see Appendix A.9) Labels to models 6A, 6B or 6C shall be affixed externally to two opposite sides, see marginals 3653 to 3655 of Ap­ pendix A. 6 for package category. 1. Substances Radioactive substances in Type A packages up to an acti­ vity per package of A 2 or A1 if in special form. • If fissile substances are present the requirements of schedule 11 shall be met in addition to the requirements of this schedule. • 2. Packaging/Package Type A, in accordance with the desigh requirements given in marginals 3600 and 3601 ofAppendic A.6. 3. Package maximum radiation level 2 00 mrem/h at the surface of the package and 10 mrem/h at 1 metre from that surface (see marginals 3653 to 3655 of Appendix A.6). except· in the case of a full load, when the limit is 1000 mrem/h at the surface of the package and may exceed 10 mrem/h at 1 metre from that surface (see marginal 3659 (7) of Appendix A?6). 4. Mixed packing See Marginal 3650 of Appendix A.6. 5. Contamination on packages Non - fixed extremal contamination limits: Beta/ gamma/ low - toxicity alpha emitters 10-4 µCij cm2 . Natural/depleted uranium/natural thorium 10·3 µCi/ cm2 Other alpha emitters 10·5 µCl/cm 2 For full details, see marginal 3651 or Append~x A.6 6 . Marking on packages Packages shall be plainly and dyrably marked externally with I. «Type A» II. the weight of the package, if over 50 kg. 7. Transport Documents a)For a summary of the approval and notification require ments - see marginal 2704. . • b) The transport document shoud include the description «Radioactive substances in Type A packages, 7, schedule 8, ADR», with the name underlined in red, and the details specified in marginals 3680 and 3681 of Appendix A.6. c) Where adv antage is taken of the increased activity per package permitted if the substance is in special form, the unilateral special form design approval certificate shall be in the consignor's possession before the first shipment (see marginal 3671 of Appendix A.6). 8. Storage and despatch a) Storage and segregation from other dangerous goods see marginal 3658 (1) of Appendix A.6. b) Storage and segregation from packages labelled «FOTO» see marginal 240 001 of Appendix B. 4 for segregation table . c) Total transport index limitation for storage - 50 per group with 6 metres between groups see marginal 3658 (2) to (5) of Appendix A.6. 9. Carriage of packages in vehicles and containers a) Segregation from packages labelled «FOTO» see marginal 240 001 of Appendix B.4 for segregation tables. b) Total transport index limitation - 50. This limitation does not apply to a full load, provided that if Fissile Class II or III packages are present the allowable number is not ex­ ceeded. See marginal 3659 (5) of Appendix A.6. c) Maximum radiation level for vehicles and large contai ners in the case of a full load. • 200mrem/h at surface 10 mrem/h at 2 metres from surface (See marginal 3659 (7) of Appendix A.6) Also, for yeh­ icles - 2 mrem/h in any normally occupied position - see marginal 3659 (8) of Appendix A.6. 2230 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 10. Carriage in bulk in vehicles and containers Not applicable. 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and containers (see Appendices A.9 and B.4) Containers - labels to model 6A, 6B or 6C on all four si­ des. Vehicles and large containers - placards to model in Appendix B.4, Marginal 240 1010 each lateral side and on rear wall of vehicle (see marginal 3659 (6) and 71 500). • 13. Prohibition on mixed loading See marginal 2700 (3). 14. Decontamination of vehicles, tank vehicles, tank co­ ntainers and containers See marginal 3695 (3) of Appendix A.6. 15. Other provisions (a) Accident provisions - see marginal 3695 (1) of Ap pendix A.6. • (b) Decontamination in storage - see marginal 3695 (2) of Appendix A.6. Schedule 9 Danger labels on packages (see Appenlix A.9) Labels to models 6A, 6B or 6C shall be affixed externally two opposite sides, see marginals 3653 to 3655 of Ap­ pendix A.6 for packages category. 1. Substances Radioactive substances in Type R (U) Packages No limit on the qu~ntity per package except as prescribed in the approval certificates. If fissile substances are pre­ sent, the requirements of schedule 11 shall be met in addi­ tion to the requirements of this schedule. 2. Packaging/Package Type B (U), in accordance with the design requirements given in marginals 3600 to 3603 of Appendix A.6 requi­ ring competent authority unilateral approval, see marginal 3672 of Appendix A.6. 3. Package maximum radiation level 200 mrem/h at the surface of the package and 10 mrem/h at 1 metre from that surface. (see Marginale 3653 to 3655 of Appendix A.6). except in the case of a full load, when the limit is 1000 mrem/h al the surcace of the package and may exceed I 0 mrem/h at 1 metre from that surface (see marginal 3659 (7) of Appendix A?6). 4. Mixed packing See Marginal 3650 of Appendix A.6. 5. Contamination on packages Non - fixed extremal contamination limits: Beta/gamma/ low - toxicity alpha emitters 10-4 Ci/cm2 Natural/depleted uranium/natural thorium 10·3 Ci/cm2 Other alpha emitters 10-5 C 1 / cm2 For full detaile, see marginal 3651 or Appendix A.6 , 6. Marking on packages Packages shall be plainly and durably marked extrer­ nally with: a) .TYPE B (U)». b) competent suthority identification mark. c) the weight if ove'r 50 kg. d) the trefoil symbol embossed or stamped on the outer­ most fire and water - resistant receptacle. 7. Transport Documents a) For a summary of the approval and notification requi­ rements, see marginal 2704. b) The transport document shall include the description «Radioactive substances in Type B (U) packages, 7, schedule 9, ADR», with the name underlined in red, and the details specified in marginals 3680 and 3681 of Ap­ pendix A.6. c) Unilateral package desigh approval certificate is req­ uired, see marginal 3672 of Appendix A.6. d) Before the shipment of any package the consignor shall be in possesion of all relevant approval certificates. e) Before the first shipment of a particular design of pac­ kage, if the activity is greater than 3 X 103 ~ or 3 X 103 A1 as appropriate, or 3xl04 Ci whichever is the lower, the consignor shall ensure than copies of the competent autho­ rity approval certificates have been supplied to the compe­ tent authorities of countries affected by the moyement, see marginal 3682 (1) of Appendix A.6. I) Prior to each shipment where the activity is greater than 3Xl03 A2 or 3xl03 A1 as appropriate, or 3xl04 Ci whichever is the lower, the consignor shall notify the com­ petent authorities of all countries affected by the move­ ment, preferably fifteen days in advance as detailed in marginal 3682 of Appendix A.6. g) Where advantage is taken of the increased activity per package permitted because the substance is in special form, see paras. (e) and (f) above, a unilateral spesial form design approval certificate is required ( see marginal 36 71 of Appendix A.6). 8. Storage and despatch a) Any instructions in the competent suthority approval certificate shall be observed. b) Storage and segregation from other dangerous goods see marginal 3658 (1) of Appendix A.6. c) Storage and segregation from packages labelled «FOTO» - see marginal 240 001 Appendix B.4 for segre­ gation table. d) Total transport index limitation for storage·- 50 per group with 6 metres between groups marginal 3658 (2) to (5) of Appendix A.6. e) The consignor shall have complied with the pre-use and pre-shipment requirements of marginal 3643 and 3644 of Appendix A.6. use an pre - shipment requirements of marginals 3643 and 3644 of Appendix A.6. I) The temperature of the accessible surfaces of the pac­ kage shall not exceed 50° in the shade unless transport is under full load conditions, in which case the limit is 82 ° C (see marginals 3602 (3) (b)and 3603 (8) of Appendix A.6). • g) If the average surface heat flux from a package ex­ ceeds 15W /m2 then the package shall be transported as a full load. ,., 9. Carriage of packages in vehicles and containers a) Segregation from package labelled «FOTO» see mar­ ginal 240. 001 of Appendix B.4 for segregation table. b) Total transport index limitation - 50. This limitation does not apply to a full load, provided that if Fissile Class II or III packages are present the allowable number is not ex­ ceeded. See marginal 3659 (5) of Appendix A.6. c) Maximum radiation levels for vehicles and large co ntainers in the case of a full load. 2 00 mrem/h al surface 10 mrem/h at 2 metres from surface See marginal 3659 (7) of Appendix A.6. Also for veh­ icles - 2 mrem/h in any normally occupied position - see marginal 3659 (8) of Appendix A.6. 10. Carriage in bulk in vehicles and containers Not applicable. 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and containers (see Appendices A.9 and B.4). Containers - Labels to model 6A, 6B or 6C on all four si­ des. ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2231 Vehicles and large containers - placards to model in Appendix B.4 marginal 240 10 on each lateral side and on rear wall of vehicle (see marginals 3659 (6) and 71 500). 13. Prohibition on mixed loading See marginal 2700 (3) 14. Decontamination of vehicles, tank vehicles, tank co ntainers and containers See marginal 3695 (3) of Appendix A.6. 15. Other. provisions a) Accident provisions - see marginal 3695 (1) of Ap­ pendix A.6. b) Decontamination in storage - see marginal 3695 (2) of Appendix A.6. Schedule · l 0 Danger labels on packages (see Appenlix A.9) Labels to models 6A, 6B or 6C shall be affixed externally two opposite sides, see marginals 3653 to 3655 of Ap­ pendix A.6 for package category. 1. Substances Radioactive substances in Type B (M) Packages that is a Type B package design which fails to·meet one or more of the specific additional requiremets for Type B (U) packages (see marginal 3603 of Appendix A.6). No limit on the quantity per package except as prescribed in the ap­ proval certificate. If fissile substances are present, the req­ uirements of schedule 11 shall be met in addition to the requirements of this schedule. 2. Packaging/Package Type B (M), in accordance with the design requirements given in· marginal 3604 of Appendix A.6 requiring compe­ tent authority multilateral approval, see marginal 3673 of Appendix A.6. 3. Package maximum radiation level 200 mrem/h at the surface of the package and 10 mrem/h at 1 metre from that surface. (see Marginals 3653 to 3655 of Appendix A.6). except in the case of a full load, when the limit is 1000 mrem/h at the surface of the package and may exceed 10 mrem/h at 1 metre from that surface (see marginal 3659 (7) of Appendix A?6). 4. Mixed packing See Marginal 3650 of.Appendix A.6. 5. Contamination on packages Non - fixed extremal contamination limits: Beta/ gamma/ low - toxicity alpha emitters 104 ~Ci/ cm2 . Natural/depleted uranium/natural thorium 10·3 1,LCi/ cm2 • Other alpha emitters 10·5 fJ,Cl/cm2 For full detaile, see marginal 3651 or Appendix A.6 6. Marking on packages Packages shall be plainly and durably marked externally with: I) •Type B (M)» II) competent suthority identification mark III) the weight of the package if over 50 kg IV) the trefoil symbol embosed or stamped on the outer­ most fire and water - resistant receprace. 7. Transport Documents a) For a summary of the approval and notification requi­ rements, see marginal ·2704. b) The transport document shall include the description •Radioactive substances in Type B (M) packages, 7, schedule 10, ADR•, with the name underlined in red, and the details specified in marginals 3680 and 3681 of Ap­ pendix A.6. c) Multilateral package design approval certificates are required, see marginal 3673 of Appendix A.6. d)If the package is designed to allow for continuous ve­ nting or if the total activity of the contents exceed 3X 103 A 2 or 3xl03 A1 as appropriate, or 3Xl04 Ci whichever is the lower, multilateral shipment certificates are required unless a competent authority authorizes transport by a spe­ cific pro\'.ision in its package design certifficate, see mar ginal 3675 of Appendix A.6. • e) Where advantage is taken of the increased activity per package permitted if the subtstance is in special form, see para. ( d) above, a unilateral special form design approval certicate is required (see marginal 3671 of Appendix A.6). I) Prior to each shipment the consignor shall notify the competent authorities of all sountries affected by the move­ ment preferably fifteen days in advanse as detailed in mar­ ginal 3682 (2) to (4) of Appendix A.6. g) Before the shipment of any package, the consignor shall be in possesion of all relevant approval cerfificates. 8. Storage an despatch a) Any instructions in the competent suthority approval certificates shall be observed. b) Storage and segregation from other dangerous goods see marginal 3658 (1) of Appendix A.6. c) Storage and segregation from package labelled «FOTO» - see marginal 240 001 Appendix B4 for segre gation table. • d) Total transport index limitation for storage - 50 per group with 6 metres between groups - see marginal 3658 (2) to (5) of Appendix A.6. e) The consignor shall have complied with the pre ·- use and pre - shipment requiremets of marginals 3643 and 3644 of Appendix A.6. I) If the surface temperature of the package exceed 50 ° C in the shade the package shall be transported as a full • load - see marginal 3602 (4) (b) of Appendix A:6·:· g) if the average surface heat flux from a package ex­ ceeds 15W /m2 , then the package shall be transported as a full load. h) Packages specially designed to allow continyo4s ve­ nting - see marginal 3604 (2) of Appendix A.6. shall only be transported under full load. 9. Carriage of packages in vehicles and containers a) Segregation from packages labelled «FOTO• - see marginal 240 001 of Appendix B4 for segregation table. b) Total transport index limitation - 50. This limitation does not apply to a full load, provided that if fissile class II or III packages are present.the allowable number is not ex-· ceeded - see marginal 3659 (5) of Appendix A.6. c) Maximum tadiation levels for vehicles and large co­ ntainers in the case of a full load. 200 mrem/h at surface 10 mrem/h at 2m from surface see marginal 3659 (7) of Appendix A.6. Also, for vehicles 2 mrem/h in any normally occupied position - see mar­ ginal 3659 (8) of Appendix A.6. 10. Carriage in bulk in vehicles and containers. Not applicable. 11. Carriage in tank vehicles and tank containers. Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and containers (see Appendix A9 and B4) Containers - labels to model 6A, 6B or 6C on all four si­ des. Vehicles and large containers - pla9ards to model in Ap­ pendix B4 marginal 24 010 on each lateral side and on rear wall of vehicle (see marginals 3659(6) and 71 500). 13. Prohibition on mixed,Joading See marginal 2700 (3). 14. Decontamination of vehicles, tank vehicles, tank co 2232 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI m::iQTO) ntainers and containers. See marginal 3695(3) of Appendi~ A.6. 15. Other provisions (a) Accident provisions - see marginal 3695 (1) of Ap­ pendix A.6. (b) Decontamination in storage - see marginal 3695(2) of Appendix A.6. Schedule 11 Danger labels on packages (see Appendix A9) Fissile Class I - labels to mo­ dels 6A, 68 or 6C. Fissile Class II - labels mo­ dels 68 or 6C Fissile Class III - labels to model 6C only. Labels be af­ fixed externally to two oppo­ site sides, see marginals 3653 to 3655 of Appendix A6 for package category. 2. Packaging/Package 1. Substances Fissile substances that is ura­ nium - 233, uranium - 235, plutonium - 238, plutonium 239, plutonium - 241, or any substance containing any of the foregoing, except unirra­ diate d natural and • depleted uramum. Fissile substances shall also be consigned in full com­ pliance with the require­ ments of one of the other schedules, as appropriate to the radioactivity. (a) The following substances specified fully in mar­ ginal 3610 of Appendix A6 are exempt from the special packaging requirements of this schedule: (i) Fissile substances in quantity not exceeding 15 g. (ii) Natural or depleted uranium irradiated in a thermal reactor. , (iii) Dilute hydrogenous solutions in limited conce­ ntrations and quantities. (iv) Enriched uranium with not more than 1 per cent of uranium , 235, which should not form a lattice arrange ment if metal or oxide. (v) Substances distributed at not more than 5 g per 10 litre volume. (vi) Plutonium where less than 1 kg per package and where not more than 20 per cent by mass consists of pluto­ nium - 239 or 241. . (vii) Enriched uranyl nitrate solution containing ura­ nium with not more than 2 per cent uranium - 235. (b) Otherwise, packages shall be in accordance with the design requirements of Fissile Class I, II or III given in marginals 3611 to 3624 of Appendix A6 and have compe~ tent authority approval, where necessary, as detailed in marginal 3674 of Appendix A6. 3. Package maximum radiation level See appropriate schedule. 4. Mixed packing See marginal 3650 of Appendix A6 5. Contamination on packages See appropriate schedule. 6. Marking on packages See appropriate schedule. 7. Transport documents (a) For a summary of the approval and notification req­ uirements - see marginal 2704. 1 (b) The transport document shall include the details spe­ cified in the schedule appropriate to the nature of the co­ ntents with the word «Fissile» prefixed to the description and underlined in red. (c) Unilateral or multilateral package design approval certificates may be required, see marginal 3674 of Ap­ pendix A6. (d) Fissile Class II package designs complying with mar ginal 3620 of Appendix A6 shall have multilateral ship­ ment approval certificates. Such a package design requires no prior notification unless specified in the competent au­ thority's shipment approval. (e) Fissile Class III package designs shall have multila­ teral shipment approva) certificates unless a competent 11.u­ thority a uthorizes transport by a specific provision in its package design certificate, see marginal 36 75 ofAppendix A6. (f) Prior to each shipment of a Fissile Class III package which requires multilateral package design approval, see marginal 3674 of Appendix A6 the consignor shall notify the competent authorities of all countries affected by the movement preferably fifteen days in advance as detailed in· marginal 3682 (2) to (4) of Appendix A6. (g) Before the shipment of any package the consignor shall be in possession of any relevant approval certificates. 8. Storage and despatch (a) Any instructions in the competent authority approval certificates must be observed. (b) Total transport index limitation for storage - 50 per group with 6 metres between groups - see marginal 3658 (2) lo (5) of Appendix A6. (c) The consignor shall have complied with the pre - use requirements of marginal 3643 of Appendix A6. 9. Carriage of packages in vehicles and containers (a) Any instruction in the competent authority approval certificates shall be observed. (b) Total transport index limitation - 50. This limitation does not apply to a full load, provided that if Fissile Class II or III packages ate present the allowable number is not ex­ ceeded. See marginal 3659(5) of Appendix A6. 10. Cariage in bulk in vehicles and containers (a) No restrictions for fissile material up to 15 g total or for solutions within certain concentration and quantity Ii-· mits, see paragraph 2 (a) (i), (iii) and (vii) and marginal 3610 of Appendix A6. (b) Not applicable for Fissile Class I or ·II packages. (c) Permitted under Fissile Class III only if so specified in the competent authority certificate. • 11. Carriage in tank vehicles and tank containers Not applicable. 12. Placards and labels on vehicles, tank vehicles, tank containers and' containers • (see Appendices A9 and 8.4) Containers - labels to models 6A, 6B or 6C on all four. sides. • Vehicles and large containers - placards to model in Ap­ pendix B4 marginal 240 010 on each lateral side· and on· rear wall of vehicle (see marginals 3659 (6) and 71500). 13. Prohibitions on mixed loading See marginal 2700 (3) 14. Decontamination of vehicles, tank vehicles, tank co ntainers and containers See appropriate schedule. 15. Other provisions Accident provisions - see marginal 3695 (1) of Ap­ pendi~ A6. Schedule 12 Danger labels on packages (see Appendix A9) Labels in conformity with model no. 6C shallo be af­ fixed externally to two oppo­ site sides unless otherwise prescribed in the competent authority certificate. See marginal 3655(1) of Ap­ pendix A6. 1. Substances Radioactive substances car­ ried under special arrange­ ment If it is not possible to comply with the package design or shipment requirements, con­ signments shall be tran­ sported under a special ar­ rangement which will ensure that the over - all safety level E<l>HMEPII THI KYBEPNHIEQI (TEYXOr nPQTO) 2233 is no less than it would have been had all the applicable requirements been met. See marginal 3676 of Ap­ pendix A6. NOTE For a summary of the approval and notification requirements, see marginal 2704. Summary of approvals and pri\)r notification requirements (a) Approval of special form substance~, and package designs . Competent authority whose Subject of approval approval· is required 1 Special form substance excepting those items spe cified in Schedules 3 and 4. Country of origin . 2 Type A, LSA and LLS. None unless contents are £is sile and/not exempted from the fissile requirements under marginal 3610 of·Ap, pendix A6: Country of origin 3 Type B (U) Country of origin 3 Type B (M) Country of origin and all countries en route 5 ,Fissile package~ Package designs corn plying with marginal 3620, 3623 or 3624 of Appendix A6 None· Package designs corn plying with marginal 3616 or 3622 of Ap pendix A~ Country of origin All other package designs Country of origin and all countries en route Note: «Country of origin• refers to the country where the design originated. Packages in the fissile classes also fall into one or other of package design categories 2, 3 or 4 above and the relevant provisions also apply to them. (b) Approval of shipments and prior notification Package Competent authority Prior notification of whose approval is required each shimpent for each shipment 1. r, Type A, LSA None and LIS None 3. 4. Type B (U) None Country of origin and all countries en route when co­ ntents exceed 3 x 103 A1 or 3 X 103 A2, as appropriate or 3 X 104 C. whi­ chever is low~r. Type B(M) - Country of origin· Country of origin Continuously and all countries en and all countries venting Type B(M) Not continuou­ sly venting route. en route. Country of origin Country of origin and all countries en and all countries route when contents en route. exceed 3 X 103 A 1 or 3 x 103 A , as ap propriate or 3 X 104 C. whichever is lo ' wer. 5. Fissile packa­ ges Fissile Class l None • None Fissile Class ll Packages complying None unless speci­ with marginal 3620 fied in the compe~ of Appendix A6 on- tent authority ship­ ly: Country of ori- ment approval gin and all countri es eri route. Fissile Ill Class Country of origin Country of origin and lilt countries en and.;all countries route. en route. Packages subject to tran­ sport under­ special arran­ gements Country of origin Country of origin and all countries en and all countries . route. en route. Note: Before shipping a Type B(U) package the contents of which exceed 3 X 103A1 or 3 x 103A 2 , as appropriate, or 3 X 104C. whichever is lower, for the first time, the consignor shall ~nsure that copies of each applicable competent autho­ rity certificate applying to the design have been submitted to the competent authority of those countries in whose territory it is to be transported. Country of origin refers to the country where the shipment originated. Packages in the fissile classes also fall into one or other of the other headings of this Table and the relevant provisions also apply to them. CLASS 8 CORROSIVE SUBSTANCES 1. List of s~bstances Among the substances and articles covered by th e hea­ ding of Class 8 those which are listed in marginal 2801 or are covered by a collective heading of that marginal are subject to the provisions of this'1Annex and of Annex B. These substances and articles to be accepted for carriage under certain conditions are to be ~onsidered as substances and articles of ADR. 2705 2799 2234 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) A. Acid substances (a) Inorganic acids 1 ° Sulphuric acid: (a) sulphuric acid containing more than 95 per cent pure acid (H2SOJ, and oleum (fuming sulphuric acid); (b) sulphuric acid containing more than 75 per cent but not more than 85 per cent pure acid (H2SO J; (c) sulphuric acid containing not more than 75 per cent pure acid (H2SO J; (d) waste sulphuric acid, completely denitrated; Note: Incompletely denitrated waste sulphuric acid is not to be accepted for carriage. (e) lead sludge containing sulphuric acid; Note: Lead sludge containing less than 3 per cent free acid is a substance of Class 6.1 (see marginal 2601, 73°). (f) storage batteries filled with sulphuric acid. For (a) to (d), see also marginal 2801a, under (a). 2° Nitric acid: (a) nitric acid containing more than 70 per cent pure acid (HNO3; (b) nitric acid containing more than 55 per cent but not more than 70 per cent pure acid (HNO3; (c) nitric acid containing not more than 55 per cent pure acid (HNO3). For (a) to (c), see also marginal 2501a, under (a) and (~. • 3° Mixed nitrating acids (sulphuric and nitric acids): (a) mixed nitrating acids containing more than 30 per ceat pure nitric acid (HNO3); (b) mixed nitrating acids containing not more than 30 per cent pure nitric acid (HNO3); Note: For waste mixed nitrating acids, see lo (d). ·For (a) and (b) see also marginal 2801a, under 3a) and (b). 4° Perchloric acid in aqueous solutions containing not more than 50 per cent pure acid (HCLO J. See also mar ginal 2801a under (a). • . . Note: Aqueous solutions of perchloric acid containing more than 50 per cent but .not more than 72.5 per cent pure acid HCLO,) are substances of Class 5.1 (see mar­ ginal 2501, 3 °). Solutions containing more than 72.5 per cent pure acid are not to be accepted for carriage; the same applies to mixtures of perchloric acid with any liquid other than water. 5° Solutions of hydrochloric acid, solutions ~f hydrob­ romic acid, solutions of hydriodic acid, and mixtures of sulphuric acid and hydrochloric acid. See also marginal 2801a, under (a). • Notes: 1. Mixtures of nitric acid with hydrochloric acid are not to be accepted for carriage. 2. Liquefied anhydrou·s hydrobromic acid and liquefied hydrochloric acid are substances of Class 2 (see m~rginal 2201, 3° (at) and 5° (at). 6° Hydrogen fluoride (anhydrous hydrofluoric acid) and aqueous solutions of hydrofluoric acid: (a) hydrogen fluoride (anhydrous hydrofluoric acid); (b) aqueous solutions of hydrofluoric acid containing more than 85 per cent hydrogen fluoride; (c) aqueous solutions of hydrofluoric acid containing more than 60 per cent but not more than 85 per cent hyd­ rogen fluoride; ( d) aqueous solutions of hydrofluoric acid containing not more than 60 per cent hydrogen fluoride .. For (c) and (d), see also marginal 2801a under (a). 7° Fluoboric acid (aqueous solutions containing not more than 78 per cent pure acid (HBF JJ. See also mar­ ginal 2801a under (a). Note: Solutions of fluoboric acid containing more than 78 per cent pure acid (HBF J are not to be accepted for carriage. 8° Fluosilicic acid (hydrofluosilicic acid (H2SiF JJ. See . also marginal 2801a, under (a). 9° Stabilired sulphur trioxide. See also marginal 2801 a, under (a) and (c). Note: Unstabilized sulph~r trioxide is not to be accepted for carriage. (b) Inorganic halides, acid salts and similar halogenated substances. 11 ° Liquid halides and similar halogenated substances (except compouds of flourine) which, in contact with .moist air or water, give off acid fumes, such as: • (a) antimony pentachloride (SbC15), chlorosulphonic acid [SOz(OH)Cl], disulphur dichloride (stabilized) (S :zCl2), ch­ romyl chloride (chromium oxychloride) (CrO Cl2), phos­ pheryl chloride (phosphorus oxychloride) (P6Cl3), phos­ phorus trichloride (PC! ), silicon tetrachloride (SiCIJ, • sulphuryl chloride (S0/12), thionyl chloride (SOC12), tita­ nium tetrachloride (TiL14) and stannic chloride (SnClJ; Note: Unstabilized disulphur dichloride is not to be ac­ cepted for carriage. (b) phosphorus tribromide (PBr3), pyrosulphuryl chlo­ ride (SzD5Cl2) and thiophosphoryl chloride (PSC13). For (a) and (b),.see also marginal 2801a, under (a). 12° Solid halides and similar halogenated substances (except compounds of fluorine) which, in contact with moist air or water, give off acid fumes, such as: aluminium chloride (anhydrous) (A1Cl3), antimony trich­ loride (technical) (SbC13), phosphorus pentachloride (PC15) and zinc chloride (Zncl2). See also marginal 2801a, under (a) and (d). Note: Non-anhydrous aluminium chloride is not to be accepted for carriage. 13° Bisulphates. See also marginal 2801a, under (a). Note: Bisulphates are not subject to the provisions of ADR if the sender certifies in the transport document that the products are free from free sulphuric acid and are dry. 14° Bromine. See also marginal 2801a, under (a). 15° The following compounds of fluorine: (a) difluorides; (b) ammonium fluoride, chromic fluoride, antimony pe­ ntafluoride; (c) boron trifluoride-acetic acid complex, boron trifluo ridepropioi;iic acid complex; ' (d) bromine trifluoride (BrF3), bromine pentafluoride (BrF5). For (a) to (d), see also marginal 2801a, under (a). (c) Organic substances: 21 ° The following acids: (a) chloracetic acids: 1. monochloroacetic and trichloroacetic acids (solid); • 2. dichloroacetic acid (liquid) and mixtures of chloroa­ cetic • acids; (b) formic acid containing not less than 70 per cent pure acid; (c) glacial acetic acid and its aqueous .solutions contai­ ning more than 80 per cent pure acid; ( d) propionic acid containing more than 80 per cent pure acid;• • (e) acetic anhydride. For (a) to (e), see also marginal 2801a, under (a). 22° Liquid acid halides, such as: acetyl chloride and benzoyl chlodire. See also marginal 2801a, under (a). 23° Alkyl and aryl chlorosilanes: (a) alkyl chlorosilanes and aryl chlorosilanes having a point below 21 °C; . (b) alkyl chlorosilanes and aryl chlorosilanes having a point of 21 •c or above; <!'El:: 'J.'2.5 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 22.15 '.'lote: Substances of this item number which give off in­ narnrnable gases on contact with water, are not to be ac­ cepted for carriage. For (a) and (b), see also margina l 2801a, under (a). B. Substances of basic character. 31" (a) Sodium hydroxide and potassium hydroxide (caustic soda, caustic potash), in lumps, in flakes or in powder form: See also marginal 2801a, under (a); (b) Sodium hydroxiqe filled in the niolten state. 32" Sodium hydroxide and potassium hydroxide in sol­ utions (soda lye, potash lye), also in mixtures (caustic lyes), alkaline solutions of phenol, cresols and xylenols, alkaline residues from oil refineries. See also marginal 2801a, under (a). 33" Storage batteries filled with alkaline solutions. See also marginal 2801a, under (e). 34~ Hydrazine in aqueous solutions containing not more than per cent hydrazine (N2HJ See.also marginal 2801a, under (a). • Note: Aqueous solutions containing more than 72 per cent hydrazine (N2H 4) are not to be accepted for carriage. 35" Alkyl and aryl amines and polyamines, such as: 1,2-diaminoethane (ethyle'nediamine), hexamethylene­ diamine, triethylenetetramine. See also marginal 2801a, under (a). 36" Sodium sulphide containing not more than 70 per cent Na2S. . Note: Sodium sulphide containing more than 70 per cent Na2S is not lo be accepted for carriage. 3 7° Hypochlorite solutions: (a) hypochlorite solutions containing more than 50 g available chlorine per litre; (b) hypochlorite solutions containing not more than 50 g available chlorine per litre. • For (a) and (b), see also marginal 2801a, under (a). C. Other corrosive substances. 41° Solutions of hydrogen peroxide: (a) aqueous solutions of hydrogen peroxide containing more than 40 per cent but not more than 60 per cent hyd­ rogen peroxide; (b) aqueous solutions of hydrogen peroxide containing more than 6 per cent but not more than 40 per cent ltyd­ rogen peroxide. For (a) and (b), see also marginal 280~a,- under (a). Note: Hydrogen per<?xide and its aqueous solutions co­ ntaining more than 60 per cent hydrogen peroxide are su bstances of Class 5.1 (see marginal 2501, 1°). ; D. Empty receptacles and empty tanks , 51 ° Empty packagings, uncleaned, and ~mpty tanks, uricleaned, except those which'have contained substances of 13° and 36°. Substances handed over for carriage in conformity with 2801a the following provisions are not subject to the provisions relating to this Class contained in this Annex or in Annex 8: (a) substances of 1 ° (a) to (d), 2° (b) and (c), 3° (b), 4°, 5°, 6° (c) and (d), 7°10 9°, 11°1015°, 21°10 23°, 31°(a), 32°, 34°, 35°, 3 7° and 41 ° in quantities not exceeding 1 kg for each substance, on condition that they are packed in leak­ proof receptacles incapable of being attacked by the co­ ntents and that these receptacles are packed with care in strong, leak-proof wooden packagings with leak-proof closures; (b) substances of 2° (a) and 3° (a), in quantities not ex­ ceeding 200 g for each substance, on condition that they are packed in leak-proof receptacles incapable of being at­ tacked by the contents and that these receptacles are sec­ ured, not more than 10 per case, in wooden cases with inert absorbent cushioning materials; (c) sulphur trioxide (9°), whether or not mixed with a small quaPtity of phosphoric acid, on condition that it is packed in strong sheet-metal boxes weighing not more than 15 kg, hermetically closed and fitted with a handle; (d) phosphorus pentachloride (12°) compressed into blocks weighing not more than 10 kg each, on condition that these blocks are packed in welded and air-tight sheet­ metal boxes placed, either singly or in groups, in a crate, a case or a container; (e) metal-cased storage batteries filled with an alkaline solution (33°), on condition that they are so closed as to pre\'ent leakage of \he solution and are protected against short circuits. 2. Provisions A. Packages 1. General conditions of packing ( 1) Packagings shall be so closed and arranged as to prevent any loss of the conte!]ts. For the special provision relating to storage batteries (1 ° (I) and 33°], see marginal 2804 and 2816; for hypochlorite solutions of 37° and hyd­ rogen peroxide of 41 °, see marginals 2820 and 2821 res­ pectively. (2) The materials of which the packagings and their clos­ ures are made must not be liable to attaek by the contents, or cause the contents to decompose, or form harmful or dangerous compounds therewith. (3) Packagings, including their closures, must be suffi­ ciently rigid and strong in all their parts to prevent any loo­ sening during carriage and to meet the normal reauire­ rnents of carriage. In particular, where substances are in the liquid state or in solution, receptacles and their clos­ ures must, unless the section headed «Packing of a single substance or of articles of the same kind» provides other­ ·wise, be able to withstand any pressure which, the pre~ sence of air also being taken into account, may arise inside the receptacles in normal carriage .. For this purp"5~ta free space must be left, account being taken of ihe difference between the temperature of the substances at the time of filling and the highest mean temperature which they are Ii-. kely to reach during carriage. Inner packagings shall be· firmly secured in outer packagings. Unless otherwise spe­ cified in the section entitled «Packing of a single substance or of articles of the same kind», inner packagings may be . enclosed in outer packagings, either singly or in groups. (4) Bottles and other glass receptacles must be free from faults liable to impair their strength; in particular, internal s~r<:!sses must have been suitably relieved. The walls must be not less than 3 mm thick in the case of receptacles wei­ ghing, with their contents, more than 35 kg and not less tha~ 2 mm in the case of other receptacles. The tightness of the closure system must be ensured by an additional device (cap, crown, seal, binding, etc.) ca­ pable of preventing any loosening of the closure system during carriage. (5) When receptacles niade of glass, porcelain, stone­ ware or similar materials, or of a suitable plasticl? material, are prescribed or allowed, they must, in the absence of any provision to the contrary, be provided with protective pac­ kagings. Receptacles made of glass, porcelain, stoneware or similar materials shall be carefully secured therein by cushioning materials. Cushioning'materials shall be suited to the nature of the contents. 2. Packing 9f a single substance or of articles of the same kind (1) Substances of-1 ° (a) to (c) and 2° to 5° shall be pack­ ed: (a) in hermetically closed receptacles made of glass, porcelain, stoneware or similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio ning materials in a wooden case or other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 2802 2803 2236 ECDHMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 50 kg, other those forwarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed cylindrical receptacles made of glass, porcelain, stoneware or similar material. These receptacles shall be secured by absorbent cushioning ma­ terials in a wooden case or other outer packaging of suffi­ cient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 7 5 kg; or (c) in hermetically closed glass carboys, which shall be secured by absorbent cushioning materials in a wooden case or other outer packaging of sufficient strength, or firmly fixed in iron or wicker hampers. The carbons shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. (2) Substances of 1 ° (a) to (c), 2° and 3° may also be packed in hermetically closed metal drums having a sui­ table lining in the case of substence of 1 ° (b), (c), (d) and (e) and a lining only if necessary in the case of substances of 2° and 3°. The drums shall not be filled beyond 95 per cent of their capacity. If, with their contents, they weigh more than 275 kg shall be fitted with rolling hoops. (3) Substances of 1 ° (a) to (e), 2° and 5° may also be packed in hermetically closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 lit- • res. These receptacles shall be placed singly and tightly in a protective-packaging with complete sides, made ()f paper­ board or of some material of sufficient sterngth. The recep­ tacl6S shall not be filled beyond 95 per cent of their capa­ city. Such a package must not weigh more than 100 kg. (4) Substances of 5° may also be packed in hermetically. ilosed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litres, with walls of sufficient thickness, which shall be not less than 4 mm in the case of receptacles of 50 litres, or over; the openings shall be closed by two plugs, one placed over the other, one of them being screw-threaded. These receptades need have no protective packaging if the competent authority of the country of departure so allows. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a pac­ ~age must not weigh more than 100 kg. (5) In the case of substances of 2° (a), 3° (a) and 4°, the absorbent cushioning materials must be incombustible; in the case of substances of 2° (b ), they shall be fire-resistant. Storage batteries filled with sulphuric acid [l 0 (1)] shall be secured in battery cases. The batteries shall be pro­ tected against short circuits and be secured by absorbent cushioning materials in a wooden packing case. Packing cases shall be fitted with means of handling. Nevertheless, if the storage batteries are made of a shock-resistant material and their upper part is so designed that the acid cannot splash out in dangerous quantities, the batteries need not be packed, but they must be protected against any short circuits sliding, falling or damage, and be fitted with means of handling. No dangerous quantities of acid must appear on the outside of packages. Similarly, storage batteries forming part of the equip­ ment of vehicles need not have special packaging if the ve­ hicles are loaded upright on their wheels and secured against falling. (1) Substances of 6° (c) and (d), 7° and 8° shall be pac­ ked. (a) in hermetically closed metal receptacles, with a sui­ table lining if necessary, of a capacity not exceeding 15 lit­ res. These receptacles shall be secured by absorbent cush­ ioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 90 per cent of their capacity. Such a pac­ kage must not weigh more than 100 kg; or (b) in hermetically closed metal drums, with a suitable li­ ning if necessary. The drums shall not be filled beyond 90 per cent of their capacity. If, with their contents; they weigh more than 275 kg, they shall be fitted with rolling hoops; or ( c) in hermetically closed receptacles, made of a suitable 2804 2805 plastics ·material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper­ board or of some other material of sufficient strength. The receptacles shall not be filled beyond 90 per cent of their capacity. Such a package must not weigh more than 100 kg. (2) Substances of 6°, (a) and (b), shall be packed in re­ ceptacles made of carbon steel of suitable alloy steel. The receptaclef must be able to withstand a test pressure of 10 kg/cm . The following kinds of receptacle shall be ac­ cepted: (a) cylinders with~ capacity not exceeding 150 litres; (b) cylindrical receptacles equipped with rolling hoops and having a capacity of not less than 100 litres and not more than 1,000 litres. At the test pressure, the stress in the metal at the most severely point of the receptacle shall not exceed three­ quarters of the yield stress. By "yield stress" is meant the stress at which a permanent elongation of 2%o (i.e. 0.2 per cent) of the gauge length on the test-piece has been prod­ uced. In addition, the material used for the receptacles must have adequate impact strength down to a temperature of -20°C. • The receptacles must be of seamless construction or welded. For welded receptacles, a steel of fully satisfactory weldability must be used. Welded receptacles are to be ac­ cepted only on condition that the manufacturer guarantees the workmanship of the welding and that the competent au­ thority of the country of origin has given its approval. The wall thickness of the receptacles must not be less than 3 mm. Openings for filling and discharging receptacles shall be fitted with flap valves or needle-valves. Valves (cocks) of other types may however be accepted if they present equi­ valent guarantees of safety and have been approved in the country of origin. Nevertheless, whatever the type of valve adopted, its system of attachment shall be strong and such that its satisfactory condition can be verified easily before each filling. Apart from a manhole, which if provided shall be closed by an effective closure, receptacles shall not be equipped with more than two openings, for filling and discharge. Valves (cocks) shall be protected by caps having vents. Valves placed inside the neck of the receptacles and pro­ tected by a screw-threaded plug, and receptacles carried packed in protective cases, shall not require a cap. Receptacles shall be subjected, under the supervision of an expert approved by the competent authority, to a hyd­ raulic pressure test at an internal pressure of not less than 10 kg/cm2 before being placed in service, and subseque­ ntly to the following periodic tests: The pressure test shall be repeated every eight years and shall be accompanied by an internal inspection of the receptacles and a check of their equipment. In addition, the resistance of the receptacles to corrosion shall be checked by means of suitable instruments (e.g. by ultra­ sound), and the condition of the equipment verified, every two years. Receptacles shall bear in clearly legible and d1Jrable characters: • (a) the name of the substance in full, the name or mark of the maker and the manufacturer's identification number of the receptacle; (b) the tare of the receptacle, including fittings other than the protective cap; (c) the test pressure, the date (month, year) of the most recent test undergone and the stamp.J)f the expert who car­ ried out the test and inspections; ( d) the capacity and permissible maximum load of the receptacle. The permissible maximum weight shall be 0.84 kg per litre of capacity. (1) Sulphur trioxide (9°) shall be packed: 2806 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) (a) in sold~red receptacles made of black sheet-iron or tin-plate, or in hermetically closed bottles made of black sheet-iron, tin-plate or copper; or (b) in flame~s~aled glass receptacles, or in hermetically closed receptacles made of porcelain, stoneware or similar materials; or (c) in steel drums which have been pressure-tested at 1.5 kg/cm2 . (2) The receptacles referred to in (a) and (b) above shall be sucured by incombustible and absorbent cushioning materials in packagings made of wood, black sheet-iron or tin-plate, Substances of 11 ° shall be packed: (a) in hermetically closed receptacles made of glass, porcelain, stoneware or similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer pac­ kaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weighing more than 30 kg, other than those forwarded as a full load, shall be fitted w ith means of handling; or (b) in hermetically closed metal drums, with a suitable li­ ning if necessary. The drums shall not be filled beyond 95 per cent of their capacity. If, with their contents, they weigh more tlian 275 kg, they shall be fitted with rolling hoops; or (c) in hermetically closed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper­ board or of some other material of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. ;,uch a package must not ~eigh more than 100 kg; or ' (d) in hermetically closed glass carboys, which shall be secured by absorbent cushioning material in a wooden case or in some other outer. packaging of sufficient stren­ gth. The carboys shall not be filled beyond· 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Substances of 120 shall be packed: (a) in hermetically closed receptacles made of glass, porcelain, stone-ware or similar material, or of a suitable plastics material, which must not contain more than 5 kg of substance each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strenght. Such a package must not weigh more than 7 5 kg; or (b) in hermetically closed metal receptacles, with a suitable lining if necessary, which must not contain more than 15 kg of substance each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strenght. Such a package must not weigh more than 100 kg; or (c) in hermetically closed metal drums, with a suitable lining if necessary. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (cl) in hermetically closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a potective packaging with complete sides, made of paperboard or of some other material of sufficient strength. Such a package must not weigh more than 100 kg; or (e) in hermetically closed wooden casks of sufficent strength, with a suitable lining. Such a package must not weigh more than 250 kg; (f) zinc chloride may also be packed in hermetically closed bags, made of a suitable plastics material, which shall b,;; placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 7 5 kg. 2807 2808 substances of 13 ° and 15 ° shall be packed: (a) in hermetically closed receptacle~ made of glass, porcelain, stoneware or similar material, or of a suitable plastics material, which must.not contain more than 5 kg of substance each; however, glass receptacles are not ac­ cepted for fluoride of 150. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or • (b) in hermetically closed metal receptacles, with a lead lining if necessary, which must not contain more than 15 kg of substance each. These receptacles shall be secured • by cushioning materials in a wooden case or in some other outer packaging of sufficient.strength. Such a package must not weigh more than 100 kg; or (c) in hermetically closed metal drums, with a lead lining if necessary. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or ( d) in hermetically closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength. Such a package must not weigh more than 100 kg; or (e) in hermetically closed bags, made of a suitable plastics material, which shall be placed ina wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (f) in hermetically closed wooden casks of sufficient strength, with a suitable lining. Such a package must not weigh mor than 250 kg; or. • (g) in stout paper bags of four plies, lined with a hermeti­ cally closed bag made of a suitable plastics material. Such a package must not weigh more than 55 kg. (1) Bromine"{l4o) shall be packed in suitable receptac-. Jes containing not more than 7. 5 kg of substance ·pet re­ ceptacle. (2) Bromine containing less than 0.005 per cent water, or between 0.005 per cent and 0.2 per cent water provided that in the latter case measures are taken lo prevent corro­ sion of the lining of the receptacles, may also be carried in receptacles satisfying the following conditions: (a) the receptacles shall be made of steel and be equip­ ped with a leak-proof lining made of lead or of some other material affording equivalent protection, and with hermetic closures; receptacles made of monel metal or nickel, or equipped with a nickel lining, shall also be permitted; (b) their capaciy must not exceed 1250 litres; (c) the receptacles shall not be filled beyond 92 per cent of their capacity or beyond 2.86 kg per litre of capa­ city; (d) the receptacles shall be welded and designed for a pressure of not less than 21 kg/cm2 . The materials and workmanship must in other respects meet the requirements of marginals 2211 (1) and (2) (b). The initial test of unlined steel receptacles shall be subject to the provisions of marginals 2215 (1) and 2216 (1), A and B. (e) the closing devices must project as little as possible from the receptacle and be fitted with a protective cap. The closing devices and the cap shall be fitted with gaskets made· of a material not capable of being attacked by bro­ mine. The closing devices must be in the upper part of the receptacles, so that they can in no case·be in permanent contact with the liquid; (f) the lead lining must be leak-proof and be not less than 3 mm thick. If some other material is used, it must provide protection equivalent to that provided by lead; (g) the receptacles must be provided with fittings enab­ ling them to stand stably upright, and with lifting attach­ ments (rings, flanges, etc.) at the top, which must be tested at twice the working load. (3) Receptacles in conformity with (2) above shall, be­ fore being put into service, be subjected to a thightenss test at a pressure of 2 kg/ cm2 • The tightness test shall be 2237 2809 2238 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) repeated every two years and shall be accompanied by an internal inspection of the receptacle and a check of its tare. This test and this inspection shall be supervised by an expert approved by" the competent authority. (4) The receptacles must bear, in clearly legible and indelible characters: (a) the name or mark of the maker and the number of the receptacle: (b) the word •Bromine•; (c) the tare of the receptacle and its maximum weight when filled; ( d) the date ( month and year) of the last test undergone; (e) the stamp of the expert who carried out the test and the inspections. (1) Substances of 210 (a) 1 shall be packed: (a) in hermetically closed receptacles made of glass, porcelain, stone-ware or similar material, or of a suitable plastics material, which must not contain more than 5 kg of substance each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or •. (b) in hermetically closed metal receptacles, with a suitable lining if necessary, which must not contain more than 15 kg of substance each. These receptacles shall be • secured with cushioning material sin a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or (c) in hermetically closed metal drums, with a suitable lining if necessary. If the drums, with their contents, weigh more than 275 kg, they shall be fitted with rolling hoops; or (d) in hermetically closed receptacles, made of a sui­ table plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper board of of some other material of sufficient stren­ gth. Such a package must not weigh more than 100 kg; or (e) in hermetically closed bags, more of a suitable plas­ tics material, which shall be placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 75 kg; or (I) in hermetically closed wooden casks of sufficient strenght, with a suitable lining. Such a package must not weigh mor than 250 kg; or (g) in stout paper bags of four plies, lined with a hermeti­ cally closed bag made of a suitable plastics material. Such a package must not weigh more than 55 kg; or (h) in jute bags r~ndered moisture-proof by a lining made of a suitable material, coated with bitumen, or in jute bags lined with a hermetically closed bag made of a suitable plastics material. Such a package must not weigh more than 55 kg. • (2) Substances of 21 ° (a)2., (b), (c), (d) and (e) shall be packed: • • (a) in hermetically closed receptacles made of glass, porcelain, stone-ware or similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These ·receptacles shall be secured by absorbent cushio• ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those fowarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed glass carboys, which shall be secured by absorbent cushioning materials in wooden case or in some other outer packaging of sufficient strength. The carboys shall not be filled beyond 95 per cent of • their capacity. Such a package must not weigh more than 75 kg; or (c) in hermetically closed metal receptacles, with a sui­ table lining jf necessary, of a capacity not exceeding 15 litres. these receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles 2811 shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (d) in hermetically closed canisters made of a suitable metal, welded or hard-soldered, of a capacity not excee • ding 60 litres and fitted with means of handling. The canisters shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg; or (e) in hermetically closed metal drums, with a suitable lining if necessary. The drums shall not be filled beyond 95 per cent of their capacity. If, with their contents, they weigh more than 275 kg, they shall be fitted with rolling hoops; or (I) in hermetically closed receptacles made of a suitable plastics material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly iri a protective packaging with complete sides, made of parer­ board or of some other material of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (g) in hermetically closed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litres, with walls of sufficient thickness, which shall be not less than 4 mm in the case of receptacles of 50 litres or over; the openings shall be closed by two plugs, one placed over the other, one of them being screw-threaded. These receptacles need have no protective packagings if the com­ petent authority of the country of departure so allows. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg. Substances of 220 shall be packed: (aJ in hermetically closed receptacles made of glass, porcelain, stone-ware or similar rmaterial, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be recured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed metal drums, with a suitable lining if necessary. The drums shall not be filled beyond 95 per cent of their capacity. If, with their contents, they weigh more than 275 kg, they shall be fitted with rolling hoops; or (c) in hermetically closed receptacles, made of a suitable plastics· material, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper­ board or of someother material of sufficient strength. Re­ ceptacles shall not be filled beyond 95 per cent of their capacity. Such a package must ·not weigh more than 100 kg; or • (d) in hermetically closed glass carboys, which shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient stren­ gth. The carboys shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than. 75 kg. (1) Substances of 230 shall be packed: (a) in hermetically closed receptacles made of glass, porcelain, stoneware or similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, except those forwarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed metal receptacles, with a 2812 2813 EG>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2239 suitable lining if necesary, of a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning mat~rials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (c) in hermetically closed metal drums, with a suitable lining if necessary. Drums intended to hold substance of 23 ° (a) must satisfy the requirements of Appendix A.5. the drumsshall not be filled beyond 95 per cen of their capacity. If, with their contents, they weigh more than 275 kg, they shall be fitted with rolling hoops. • (2) Substances of 23 ° (b) may also be packed: (a) in hermetically closed canisters m~de of a suitable metal, welded or hard-soldered, of a capacity not excee­ din~ 60. litres and fitted with means of handling. The camst~rs shall not be filled beyond 95 per cent of their capacity. Such package must not weigh more than 75 kg; or (b) in hermetically closed receptacles, made of a sui­ t~ble pl~stics material, of a capacity not exceeding 60 litres, with walls of sufficient thickness, which shall be not • less than 4 mm in the case of receptacles of 50 litres of over; the openings shall be closed by two plugs, one placed over the other, one of them being screwthreaded. These receptacles need have no protective packaging if the com­ petent authority of the country of departure so allows. The recep~acles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg. (1) Substances of 310 (a) shall be packed: 2814 (a) i~ hermetically closed receptacles made of glass, porcelam, stone-ware or similar material, or of a suitable plastics material, which must not contain more than 5 kg of su bst:ince eac~. T~ese receptacles shall be secured by cushtonmg matenals m a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh mor than 7 ~ kg; or (b) in hermetically closed metal receptacles,with a sui­ table lining if necessary, which must not contain more than 15 kg of substance each. These receptacles shall be secured by cushioning materials in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 100 kg; or (c) in hermetically closed metal drums, with a suitable lining if necessary. If the drums, with their contents, weigh more than 275 kg. they shall be fitted with rolling hoops; or ( d) in hermetically closed receptacles, made of a sui­ table plastics metarial, of a capacity not exceeding 60 litres. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paperboard or of some other material of sufficient strength. Such a package must not weigh more than 100 kg; or • (e) in hermetically closed bags, made of a suitable plastics material, which shall be placed in a wooden case or in some other outer packaging of sufficient strength. Such a package must not weigh more than 7 5 kg; or (f) in jute bags rendered moisture-proof by a lining made of a suitable material, coated with bitumen, or in jute bags lined with a hermetically closed bag made of a suitable plastics material. Such a package must not weigh more than 55 kg. (2) Substances of 31 ° (a) in flakes or in powdered form may also be packed in stout paper bags of four plies, lined with a hermetically closed bag made of a suitable platics material. Such a package must not weigh more than 55 kg. (3) Sodium hydroxide of 31 o (b) filled in a molten state shall be contained in steel drums with walls not less than 0.5 mm thick. The drums, with their contents, must not weigh mor than 450 kg. Substances of 32° shall be packed: 2815 (a) in hermetically closed receptacles made of glass, porcelain, stoneware of similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed metal receptacles, with a suitable lining if necessary, of a capacity not exceed.ing 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other . outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (c) in hermetically closed canisters made of a suitable metal, welded or hard-soldered, of a capacity not excee­ ding 60 litres, and fitted with means of handling. The canisters •shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg; or (d) in hermetically closed metal drums, with a suitable lining if necessary. The drums shall not· be filled beyond 95 per cent of their capacity. If, with their contents, they weigh more than 275 kg, they shall be fitted with rolling hoops; or . (e) in hermetically i1osed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litrtes. These receptacles shall be placed singly and tightly in a protective packaging with complete sides, made of paper­ board or of some other material of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or . (f) in hermetically closed receptacles,made of a.suitable plastics material, of a capacity not exceeding 60 litres•·and with walls of sufficient thickness, which shall be. not less than 4 mm in the case of receptacles of 50 litres or ove~; the openings shall be closed by two plugs, one· placed over the other, one of them being screw-threaded .. These receptacles need have no protective packaging if the com­ petent authority of the country of departure so allows. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or • (g) in hermetically closed cylindrical receptacles made of glass, porcelain, stoneware of similar material, of a capacity not exceeding 20 litres. These receptacles shall be secured by absorbent cushioning materials in .a wooden case or in some other outer packaging of sufficient stren­ gth. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 7 5 kg; or (h) ip hermetically closed glass carboys, which shall be securd by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient stren­ gth, or be firmly fixed in iron or wicker hampers. The carboys shall not be filled beyond 95 per cent of their capacity. Such a packag~ must not weigh more than 75 kg. ·storage batteries filled with alkaline soluti~ns (330) • 2816 shall be made of metal and the upper part shall be so designed that the lye cannot splash out in dangerous qua ntities. The batteries shall be protected against short circuits and be packed in a wooden packing case. (I) Hydrazine (34°) shall de packed: 2817 (a) in hermetically closed glass-receptacles, of a capacity not exceeding 5 litres, which shall be secured by suitable cushioning materials in boxes placed in a wooden case; or (b) in receptacles made of aluminium not less than 99.5 per cent pure or of stainless steel or of lead-lined iron· or (c) in r~ceptacles, made of a suitable plastics ma~erial, fitted with a screw closure and having a capacity not exceeding 65 litres, placed sinlgy in suitable protective packagings or secured in groups by suitable cushioning 2240 E(J)HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) materials in suitable protective packagings; a package must not weigh more than 100 kg, or more than 50 kg if th eprotective packaging consists of a fibreboard case; or ( d) in drums, made of a suitable plastics material, of a capacity not exceeding 220 litres and with walls not less than 1.5 mm thick, placed singly in drums fitted with rolling hoops. (2) No receptacle shall be filled beyond 93 per cent of its capacity. The receptacles under (b), (c) and (d) shall be pressure-tested at 1 kg/cm2 • ;Substances of 350 shall be packed: (a) in hermetically closed receptacles made of glass, porcelain, stoneware of similar material, or of a suitable plastics material, of a capacity not exceeding 5 litres. These receptacles shall be secured by absorbent cushio­ ning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 75 kg. Packages weigh­ ing more than 30 kg, other than those forwarded as a full load, shall be fitted with means of handling; or (b) in hermetically closed metal receptacles, with a suitable lining if necessary, of a capacity not exceeding 15 litres. These receptacles shall be secured by absorbent cushioning materials in a wooden case or in some other outer packaging of sufficient strength. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (c) in hermetically closed canisters made of a suitable metal, welded or hard-soldered, of a capacity not exc~e­ ding 60 litres, and fitted with means of handling. The canisters shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh mor than 75 kg; or (d) in hermetically closed metal drums, with a suitable lining if necessary. The drums shall not be filled beyond 95 per cent of their capacity. If with their contents, they weigh more than 275 kg, they shall be fitted with rolling hoops; or ( e) in hermetically closed receptacles, made of a suitable plastics material, of a capacity not exceeding 60 litrs. These receptacles shall be placed singly and tightly in a protective packaging with complete. sides, made of paper­ board or of some other material of sufficient strength. The receptacles shall mot be filled beyond 95 per cent of their capacity. Such a package must not weigh more than 100 kg; or (f) in hermetically closed receptacles, made of a suitable pl~tics material, of a capacity not exceeding 60 litres, with walls of sufficient thickness, which shall be not less than 4 mm in the case of receptacles of 50 litres or over; the openings shall be closed by two plugs, one placed over the other, one of them being screw-threaded. These receptacles need have no protective packaging if the com­ petent authority of the country of departure so allows. The receptacles shall not be filled beyond 95 per cent of their capacity. Such a package must not weigh mor than 100 kg. (1) Sodium sulphide (36°) shall be packed: (a) in lead-proof iron receptacles; or (b) in quantities not exceeding 5 kg, also in receptacles, made of glass or of a suitable plastics material, which shall be secured in strong wooden receptacles, glass receptacles being secured therein by cushioning materials. (2) Sodium sulphide in solid form may also be enclosed in other leak-proof receptacles. If carried as a full load, it may also be packed: (a) in stout paper bags of five plies, so closed as to be le­ ak-proof and lined with a bag made of a suitable plastics material; or ·(b) in bags made of a suitable plastics material equal in strength to the paper bags. Packages made up of bags must not weigh more than 55 kg. 2818 2819 (1) Hypochlorite solutions (37°) shall be packed: (a) in receptacles made of glass, porcelain, stoneware or • similar material, or of a suitable plastics material, secured in protective packagings; fragile receptacles shall be sec­ ured therein by cushioning materials; or (b) in metal drums, suitably lined. (2) In the case of hypochlorite solutions of 3 7° (a), the receptacles or drums shall be so· designed as to allow gases to escape, or shall be fitted with pressure-relief valves. . (1) Aqueo~s solutions of hydrogen peroxide containing more than 40 per cent but not more than 60 per cent hyd­ rogen peroxide [41 ° (a)] shall be contained: (a) in receptacles, which must be able to stand stably upright, made of aluminium not less than 99.5 per cent pure or of a special steel not liable to cause the hydrogen peroxide to decompose. The capacity of these receptacles must not exceed 200 litres; or (b) in receptacles, made of glass, porcelain, stoneware and suitable plastics material, of a capacity not exceeding 20 litres. Each receptacle shall be secured by absorbent, incombustill and inert cushioning materials in a sheet-steel packaging with complete sides, lined with suitable mate­ rials. This packaging shall be placed in a wooden packing case with a sloping protective cover. For closure and degree of filling, see under (3). (2) Aqueous solutions of hydrogen peroxide containing more than 6 per cent but not more than 40 per cent hyd­ rogen peroxide [41° (b)] shall be contained in receptacles made of glass, porcelain, stoneware, aluminium not less than 99.5 per cent pure, special steel not liable to cause ' the hydrogen peroxide to decompose, or a suitable plastics material. Receptacles of a capacity not exceeding 3 litres shall be secured by cushioning materials in wooden cas!!s; if the re­ ceptacles contain aqueous solutions of hydrogen peroxide containing more than 35 per cent hydrogen peroxide, the cushioning materials must be suitable fire-proofed. A pac­ kage must not weigh more than 35 kg. If the receptacles have a capacity of more than 3 litres they musty satisfy the following conditions: (a) receptacles made of aluminium or of special steel must be able to stand stably upright. A package must not weigh more than 250 kg; (b) receptacles made of glass, porcelain, stoneware or ·a suitable plastics material shall be placed in suitable strong protective packagings which will keep them securely upright; the packagings shall be fitted with means of han­ dling. Inner receptacles other than those made of a plastics material shall be secured in outer packagings by cushio­ ning materials. Where receptacles contain aqueous sol­ utions of hydrogen peroxide containing more than 35 per cent but not more than 40 per cent hydrogen peroxide, the cushioning materials shall be suitably fire-proofed. A pac­ kage of this kind must not weigh more than 90 kg; ho­ wever, it may weigh up to 110 kg if the protective packa­ gings are, in addition, packed in a case or crate; (c) aqueous solutions of hydrogen peroxide containing more than 6 per cent but not more than 40 per cent hyd­ rogen peroxide may also be contained, without protective packagings, in receptacles made of a suitable plastics ma­ terial, provided that the thickness of the walls (including areas recessed for labelling is not at any point less than 4 mm, the walls are protected by strong ribs, and the ends are reinforced. The receptacles shall be fitted with means of handling. The capacity must not exceed 60 litres. For closure and degree of filling, see under (3). (3) Receptacles of a capacity not exceeding 3 litres may have a hermetic closure. In such cases the receptacles shall be filled with a weight of solution which, expressed in grammes, in equel to not more than two-thirds of the figure expressing the capacity of the receptacle in cm3• Receptacles of a capacity exceeding 3 litres shall be fitted with a special closure preventing excess internal pressure, leakage of the liquid, ·and the entry of foreign 2820 2821 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2241 matter into the receptacle. Whore receptacles are packed separately, the outer packaging shall be fitted with a cover which, while protecting the closure, makes it possible to ve­ rify that the closure is directed upwards. These receptacles may not be filled beyond 95 per cent of their capacity. 3. Mixed packing ( 1) Substances grouped under the same item number may be included in the same package. The inner packa­ gings shall conform to what is prescribed • for each substance, and the outer packaging shall be that laid down for the substances of the item number in question. (2) If smaller quantities are not prescribed in the sectii,n entitled «Packing of a single substance or of articles of the same kind» and no special conditions are laid down below, substances of this Class, in quantities not exceeding 6 kg in the case of solids or 3 litres in the case of liquids for all of the substances listed under the same item number or the same letter, may be enclosed in the same package either with substances of another item number or of another letter of the same Class, or with substances or articles beloging to other Classes (if mixed packing is likowise allowed in the 2822 case of such substances or articles), or with other goods. subject to the following special conditions. The inner packagings must satisfy the general and spe­ cial conditions of packing. In addition, the general provi­ sions of marginals 2001 (5) and 2002 (6) and (7) must be observed. Mixed packing of· an acid substance with a basic substance in the same package is not allowed if both substances· are contained in fragile receptacles. A package must not weigh more than 150 kg, or more . than. 75 kg if it contains fragile receptacles. Maximum quantity Description of ,.. per per Item-No. substances receptacle package Special provisions 1 °(a) Oleum 3 litres · 12 litres Must not be packed together with chlorates, per mengenates, solutions of hydrogen peroxide, perch 1 ° (a) (b), Sulphuric acid other than lorates, peroxides or hydramine. The limitation of 18 litres applies to sulpharic, nitric and hydrochloric (c) oleum 3 litres 16 litres acids, and mixed nitrating acids, for aU of these substances. If the pac~age contains an acid subject to a limitation of 12 litres, this limitation inust be applied. ' 2° (a) Nitric acid containing more than 70% pure acid 3 litres 12 litres ... .;. Musi not be packed together with' formic acid,- tric 2° (b) and Nitric acid containing not • thanola-mine, aniline, ·xylidine, tolucline, chlorates, pannanganates, inflammable liquids with a flash more than 70% pure acid 3 litres 18 litres point below 21 ° C, solutions of hydrogen peroxide, perchlorates, peroxides, hydrozinc, glycerine, gly 30 Mixed nitreting acids 3 litres 18 litres cols; Onldy inert filling materials must be used. 40 Perchloric acid Mixed packing not allowed ' 50 Hydrochloric acid 5 litres 18 litres Must not be packed together with chlorates, per manganates, perchlorates peroxides (other than sol utions of hydrogen peroxide). 60 Solutions of hydrofluoric acid 1 litre 10 litres 11 ° (a) Disulphur dichloride 500 g 500 g 11 ° (a) Antimony pentachloride 2.5 kg 5 kg Must not be packed togegher ·with substances of 360 of Class 8 or with substances of Class 5.1; must be protected against ponetration of moisture Chlorosulphanic chloride Sulphuryl acid Thionylchloride Titanium tetrachloride '-tann;~ ~hl~r;..lo 12° Antimony trichloride 14° Bromine in fragile receptacles 500 g 500 g inother receptacles 1 kg 3 kg 15 ° (a) Difluorides 5 kg 15 kg Must not be packed together with substances of Classes 4.2, 4.3 and 5.1, or with nitric acid or 1", mixed nitrating acids. I 2242 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI: nPQTO) 21 ° (b) Nitric acid 5 litres 21°(c) Acetic acid 5 litres 34° Hydramine 5.5 kg 36° Sodium sulphide containing not more -than 70% Na2S 2.5 kg 41 ° (a) Solutions of hydrogen pero xide containing more than 35% hydrogen peroxide Mixed packing not allowed 41 ° (b) Solutions of hydrogen pero xide containing more than 15% hut not more than 35% hydrogen peroxide in fragile .receptacles 1 litres in other receptacles 3 litres Solutions of hydrogen pero • )(ide containing more than 6%-::but ncit more than 15% hydrogen peroxide 3 litres 4. Marking and c;langer labels on packages (see Appendix A.9) Cases containing storage batteries (1 ° (f) and 33°) shall be legibly and indelibly marked: «Storage batteries». This inscription shall be in an official languc1ge of the country of departure and also, if that language is not English or French, or German, in English, French or German, unless otherwise provided in agreements, if any, concluded bet­ ween t he countries concerned in the transport opera­ tion. (1) Packages containing substances of 1 ° to 7°, 9°, 11 °, 12°, 14°, 15°, 22°, 31°, 35°, or 41° (a) shall bear a label conforming to model No. 5. However, if liquids of 1 ° (a) to (e), 2° to 5°, 11 °, 22° or 32° are packed in receptacles made of glass, porcelain, stoneware or simi lar material, of a capacity exceeding 5 litres, the packages shall bear two labels conforming io model No. 5. (2) Packages containing fragile receptacles not visible from the outside shall bear labels conforming to model No. 9. If the fragile receptacles contain liquids, the packages shall in addition, except in the case of sealed ampoules, bear labels conforming to model No. 8; these labels shall be affixed high up on two opposite sides of cases or in an equivalent manner when other packagings are used. (3) Every case containing storage batteries [l O (f) and 33°], and packages weighing not more than 75 kg contai­ ning substances of 1° to 7°, 9°, 11°, 21°, 31° to 35° and 3 7°, shall, in addition, bear on two opposite sides labels conforming to model No. 8. (4) In the case of consignments carried as a full load, label No. 5, as prescribed under (1 ), need not be affixed to 2823 2824 15 litres Must not be packed together with chlorates, perman ganates solutions of hydrogen peroxide, nitric acid, mixed nitrating acids. 15 litres Must not be packed together with chloride or per maganates. 5.5 kg Must not be packed together with sulphuric acid, chlorosulphanic acid, nitric acid, mixed nitratin acids, chlorates, permanganates, sulphur, solutions of hydrogen peroxide, perchlorates and peroxides. Must be kept separate from caustic alkaline substances and strong oxidizing agents. 15 kg Must not be packed together with acid substances. Must not be packed t?gether with sulphuric acid, chlorosulphonic acid, formic acid, nitric acid, mixed nitrating acids, triethanolamine, aniline, xylidine, to! uidine, permanganates,inflammable liquids with a flash-point below 21 ° C, metallic peroxides, hydrazin~. 3· litres 12 litres 12 litres Only inorganic filling materials must be used. the packages i(the vehicle bears the marking prescribed in Annex B, marginal 10500. B. Particulars in the transport document , 2825 (1) The descri ption of the g?od~ in the lr!J,llsport doc ument must conform to one of the names underlined in marginal 280.1. Where the name of the substance is not in­ dicated in the case of 11 °, 12°, 13°, 15°, 22° and 35°, the trade name must be used. The description of the goods must be underlined in red and followed by particulars of the Class, the item number (together with the letter, if any), and the initials «ADR» or «RID» [e.g. 8.1 (a), ADR]. (2) In the case of brRmine containing 0.005 per cent to 0.2 per cent water, carried in receptacles in conformity with marginal 2810 (2), the following must be certified in the transport document: «Steps h~ve been taken to prevent corrosion of the lining of the receptacles». C. Empty packagings 2826 2827 2834 (1) Receptacles and tanks of 510 must be closed in the' 2835 same manner and leak-proof in the same degree as though they were full. (2) The description of the goods in the transport doc­ ument must be: «Empty receptacle, 8, 51, ADR (or RID)». This description must be underlined in red. (3) Uncleaned receptacles which have contained substances of 6° or bromine (14°) shall bear a label confor­ ming to model No. 5 (Appendix A.9). They must have to ,; traces of acid or bromine on the outside. 2836 3099 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2243 UNITED NATIONS PUBLICATION Sales No. E. 78VIII.I Price: SU.S. 25.00 (Vol. I. II and III) (or equivalent in other currencies) United Nations publications may be obtained from bookstores and distributors throughout the world. Consult your bookstore or write to: United Nations, Sales Section. New York or Geneva. FOREWORD The text below comprises, in addition to the Agreement itself and the Protocol of signature, the annexes in the form in which they entered into force on 29 July 1968 as well as the amendments there to up to 1 October 1978. Part III APPENDICES APPENDIX A. l A. Stability and safety conditions relating to expl~sive substances, inflammable solids and organic peroxides The conditions of stability set out below are the standard minima defining the stability required of substances to be accepted for carriage. These substances may be handed over for carriage only if they fully conform to the foll?wing requirements. Re marginal ~ 101, 1 °, marginal 21 71, 4 ° and margmal 2401, 7 (a): Nitrocellulose heated for half an h?ur at 132° C must not give off visible yellowish-brown. nitrous fumes. The ignition temperature must be above 180 ° C. Pyroxylin thread must satisfy the same conditions of stability as nitrocellulose. See marginals 3150, 315l(a) and 3153. Re marginal 2101, 3 °, 4° and 5°, and marginal 2401. 7 ° (b) and (c): ' 1. Nitrocellulose powders not containing nitroglycerine; plasticized nitrocellulose: . 3 g of powder or of plasticized nitrocellulose, heated for one hour at 132 ° C, must not give off visible yellowish­ brown nitrous fumes. The ignition temperature must be above 170° C. • 2. Nitrocellulose powders containing nitroglycerine: 1 g of powder heated for one hour at ll O ° C must not give off visible yellowish-brown nitrous fumes. The ignition temperature must be above 160° C. with regard to 1. and 2., see i:narginals 3150, 315l(b) and 3153. • Re marginal 2101, 6°, 7°, 8° (a) and (b) and 9° (a), (b) and (c): l:. Trinitrotoluene (Tolite), mixtures termed liquid tnmtr?tol~ene and trinitroanisole (6 ° ), hexyl (hexa~1trod1p~enylamme) and picric acid [7 ° (a)), pentohtes (mixtures of pentaerythritol tetranitrate ·and tr!n!troto)uene) and hexolites (mixtures of trimethylene­ tnmtramme and trmitrotoluene) [7°(b)], phlegmatized pe nt~rite and phlegmatized hexogen [7°(c)), tr~n 1troresorc1nol [8 ° (a)), tetryl (tnmt~ophenylmethylnitramine) [8 ° (b )], penthrite (l~e~ta~i,:thritol 0 tetranitrate) and ~exogen (trimethylene­ tr!n!tramme) [9 (a)], pentolites (mixtures of penthrite and tr!n!trotoluene) an~ hexolites (m!xtures of hexogen and tnmtrotoluene) [9 (b)] and mixtures of penthrite or 3100 3101 3102 3103 hexogen with wax, paraffin wax or substances similar to wax or paraffin wax [9° (c)), heated for 3 hours at a temperature of 90° C, must not give off visible yellowish­ brown nitrous fumes. See marginals 3150 and 3152 (a). 2. Organic nitro-compounds mentioned under 8 ° other than trinitroresorcinol and tetryl (trinitrophenylmethylnitramine), heated for 48 hours at a temperature of 7 5 ° C, must not give off visible yellowish­ brown nitrous fumes. See marginals 3150 and 3152 (b). 3. Organic nitro-compounds mentioned under 8° must not be more sensitive to ignition, shock or friction than: trinitroresorcinol, if they are soluble in water; tetryl (trinitrophenylmethylnitramine), if they are insoluble in water. See marginals 3150, 3152, 3154, 3155 and 3156. Re marginal 2101, ll 0 (a) and (b): '. 1. Black powder [11 ° (a)] must not be more sensitive to flame-ignition, impact or friction than the finest sporting powder having the following composition: 75 per cent potassium nitrate, 10 per cent sulphur and 15 per cent black alder charcoal. See marginals 3150, 3154, 3155 and 3156. 2. Slow mining powders similar to black powder [11 ° (b)] must not be more sensitive to flame-ignition, impact or fricti~~ than the standard explosive having the following compos1t1on: 75 per cent potassium nitrate, 10 per cent sulphur and 15 per cent lignite. See marginals 3150, 3154, 3155 and 3156. Re marginal 2101, 12°: Nitrate explosives in powder form [12 ° (a)], and explosives not containing inorganic nit~ates, in powder form [12° (b)]; must be capable of bemg stored for 48 hours at 7 5 ° C without giving off. visible yellowish-brown nitrous fumes. Before and, after storing they must not be more sensitive to flam~-i~ition, impact or friction than the standard explosive· having the following composition: . ~O per cent ammonium nitrate, 12 per cent tnmtrotoluene, 6 per cent nitroglycerine and 2 per cent wood flour. See marginals 3150, 3152 (b), 3154 (a) and (b), 3155 and 3156. A sample of. the standard explosive referred to above is held at the disposal of the Contracting States by La boratoire du Centre d' etudes et reclierches des charbonnages de France (CERCHAR), Boite postale No. 2, 80550 Verneuil-en-Halatte, France. Re marginal 2101, 13 °: Chlorate and perchlorate explosives must not contain any ammonium salt. They must not be more sensitive to flame ignition, impact or friction than a chlorate explosive having the following c?~position: 80 per cent potassium chlorate, 10 per cent dm1trotoluene, 5 per cent trinitrotoluene, 4 per cent castor oil and 1 per cent wood flour. See marginals 3150, 3154, 3155 and 3156. Re marginal 2101, 14° (a) and (b): Explosives of 14° ~a) and (b) '.11~st not be more sensitive to flame-ignition, 1mpac~ or fnct10 n than blasting gelatine containing 93 pet cent mtroglycerme or guhr dynamite.containing not more than 75 per cent nitroglycerine. They must satisfy the exudation test of marginal 3158. See marginals 3150, 3154 (b), 3155 and 3156. Re marginal 2101, 14° (c): Explosives of 14° (c) must be capable of being stored for 48 hours at 7 5 ° C without giving off visible· yellowish-brown nitrous fumes. Before and after storing they must not be more sensitive to flame­ igni!ion, impact or friction than the standard explosive h~vmg the following composition: 3 7. 7 per cent mtroglyco l or nitroglycerine or a mixture of the two, 1.8 per cent guncotton, 4 per cent trinitrotoluene, 52.5 per cent ammonium nitrate and 4 per cent wood flour. See~­ marginals 3150, 3152 (b), 3154 (a), (b), (c) and (d), 3155 and 3156. . 3104 3105 3106 3107 2244 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) ' Re marginal 2131, l 0 (b): The explosive substance must not be more sensitive to flame-ignition, impact or friction than tetryl.- See marginals 3150, 3154, 3155 and 3156. Re marginal 2131, 1° (c): The explosive substance must not be more sensitive to flame-ignition, impact or friction than penthrite. See marginals 3150, 3154, 3155 and 3156. Re marginal 2131, 5 ° ( d): 'J]ie transmission charge must not be more sensitive to flame-ignition, impact or friction than tetryl. See marginals 3'150, 3154, 3155 and 3156. Re marginal 2170 (2) (d): The explosive charge, after having been stored for four weeks at 50° C, must show no signs of deterioration due to insufficient stability. See marginals 3150 and 3157. Re marginal 2551, 1° to 50°: The substances shall be subjected to the test described in marginals 3154, 3155 and 3156. B. Rules for tests 1) The test procedures set out bel~w are to be applied when differences of opinion arise as to the acceptability • of substances for carriage by road. 2) If other methods or test procedures are used to verify the conditions of stability prescribed above in this , Appendix, those methods must lead to the same findings as could be reached by the methods specified below. '. 3) In carrying'out.the stability tests by heating described • below, the temperature of the oven containing the sample under test must not deviate by more than 2 ° C from the prescribed temperature; the prescribed duration of a 30 minute or 60 minute test must be observed to within two minutes, that of a 48-hour test to within one hour, and that of a 4-week test to within 24 hours. The oven must be such that the required temperature is restored not more than five minutes after insertion of the sample. . 4) Before undergoing the tests prescribed in marginals 3151, 3152, 3153, 3154, 3155 and 3156, the samples must be dried for not less than 15 hours at the ambient temperature in a vacuum desiccator containing fused ~nd granulated calcium chloride, the sample substance be~ng spread in a thin layer; for this purpose, substances which are neither in powder form nor fibrous shall be ground, or grated, or cut into small pieces. The pressure in the desiccator must be brought below 50 mm of mercury. 5) (a) Before being dried as prescribed in paragraph 4) above, substances of marginal 2101, 1 ° (expept those containing paraffin wax or a similar substance), 2 °, 9 ° (a) and (b), and those of marginal 2401, 7° (b), small undergo preliminary drying in a well-ventilated drying oven, with its temperature set at 70° C, until the loss of weight per quarter-hour is less than 0.3 per cent of the original weight. • b) For substances of marginal 2101, 1 ° (when they contain paraffin wax or a similar substance), 7° (c) and 9° (c), the preliminary drying must be carried out as prescribed in sub-paragraph (a) above, except that the temperature of the oven shall be set at between 40° and 45° c. 6) Nitrocellulose of marginal 2401, 7° (a) shall first undergo preliminary drying as prescribed in paragraph (5) (a) above; drying shall then be completed by keeping the nitrocellulose for at least 15 hours over concentrated sulphuric acid in a desiccator. Test of chemical stability under heat Re marginals 3101 and 3102 3108 3109 3110 3111 3112 3113 3149 3150 a) Test of substances listed in marginal 3101. . 1) In each of two glass test tubes having the following dimensions: length . . . . . . . . . . . . . . . . . . . . . . . . . . . . 350 mm .internal diameter ....... ~... . . . . . . . . 16 mm thickness of wall . . . . . . . . . . . . . . . . . . . 1.5mm is placed 1 g of substance dried over calcium chloride (if necessary the drying must be carried out after reducing the substance to pieces weighing not more than 0.05 g. each). Both test tubes, completely covered with loose­ fitting closures, are then so placed in an oven that at least four-fifths of their length ·is visible, and are kept at a constant temperature of 132° C for 30 minutes. It is observed whether nitrous gases in the form of yellowish­ brown fumes ·clearly visible against a white background are given off during this time. . 2) In the absence of such fumes the substance is deemed to be stable. b) Test of powders listed in marginal 3102. 1) Nitrocellulose powders not containing nitroglycerine, whether gelatinized or not, and plasticized nitrocellulose: 3 g of powder are placed in glass test tubes, similar to those referred to in a), which are then placed in an oven kept at a constant temperature of 132° C. 2) Nitrocellulose powders containing nitroglycerine: 1 g of powder is placed in glass test tubes, similar to those referred to in a), which are then placed in an oven kept at a constant temperature of 110° C. 3) The test tubes containing the powders referred to in (1) and (2) are kept in the oven for one hour. During this time no nitrous gases myst be visible. Observation and appraisal as in (a). • Re marginals 3103 and 3105 a) Test of substances listed in marginal 3103, 1. 1) Two samples of explosive each weighing 10 g are placed in cylindrical weighing bottles having an internal diameter of 3 cm and a height of 5 cm to the underside of the cover; the bottles are then firmly closed with their covers and heated for three hours at a constant temperature of 90 ° C in an oven in which they are clearly visible. 2) During this time no nitrous gases must be visible. Observation and appraisal as under marginal 3151 (a). b) Test of substances listed in marginals 3103, 2. and 3105. 1) Two samples of explosive each weighing 10 g are placed in cylindrical weighing bottles having an internal diameter of 3. cm and a height of 5 cm to the underside of the cover; the bottles are then firmly closed with their covers and heated for 48 hours at a constant temperature of 75 ° C in an oven in which they are clearly visible. 2) During this time no nitrous gases must be visible. Observation and appraisal as under marginal 3151 (a). Ignition temperature (see marginals 3101 and 3102) 1) The ignition temperature is determined by heating 0.2 g of substance enclosed in a glass test tube immersed in a Wood's alloy bath. The test tube is placed in the bath when the latter has reached 100° C. The temperature of the bath is then progressively increased by 5 ° C per • minute. 2) The test tubes must have the following dimensions: lenght ........................... . internal diameter .................. . thickness of wall .................. . and must be immersed to a depth of 20 mm. 125 mm 15 mm 0.5mm • 3) The test must be repeated three times, the temperature at which ignition of the substance occurs, i.e., slow or rapid combustion, deflagration or detonation, being noted each time. 4) The lowest temperature recorded in the three· tests is the ignition temperature. • 3151 3152 3153 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2245 Test of sensitivity to red heat and to flame~ignition (see marginals 3103 to 3110). a) Test in red-hot hemispherical iron crucible (see marginals 3103 to 3106 and 3108 to 3110). 1) Quantities of the explosive to be examined increasing from 0.5 g to 10 g are thrown into a red-hot hemispherical iron crucible I mm thick and 120 mm in diameter. The results of the test are to be classified as follows: 1. Ignition with slow combustion· (explosives with an ammonium nitrate base); 2. Ignition with rapid combustion ( chlorase explosives); 3. Ignition with violent combustion an ,deflagration (black powder), 4. detonation (fulminate of mercury). (2) The effect on the sequence of events of the amount of explosive used should be taken into account. (3) The explosive to be examined must not show any fundamental difference from the standard explosive. (4) The iron crucibles must be careffully cleaned before each test and replaced at frequent intervals. 3154 (b) Test of Case of ignition (see marginals 3103 to 3110). • (1) The explosive to be examined is placed in a small heap on an iron plate in quantities increasing - in the light of the results of the test under (a) - from 0.5 g to a maximum of l 00 g. (2) A burning match is applied to the apex of the small heap and note is taken whether the explosive ignites and burns slowly, deflagrates, or detonates, and whether, once ignition has occured, c;:ombustion continues even after the match has been removed. If no ignition takes place a similar test is made by bringing the explosive into contact with a gas flame and noting the same .points. (3) ,'he results of the test are compared with those obtained with the standard explosive. (c) Combustion test in conditions of enclosure in a sheet-steel box (see marginal 3107). ( 1) The c ombustion test is carried out in a cubical box, made of sheet steel with edges 8 cm long and a wall thickness of 1 mm .. The box is made of annealed mild steel sheet and closed in as tight a manner as possible by foldig the edge of the lid over (fig. 1 ). (2) In the case of explosives sensitive to friction, the top surface should be covered with a sheet of paper to prevent particles of explosive from finding their way between the edges and remaining trapped there when the edge of the lid is being bent over. The box is completely filled with the explosive so that the latter has as nearly as possible the same density as when in cartidges. The box is placed in the fire with care; it shall first be wrapped in, for example, several layers of packing paper to avoid immediate ignition of the explosive. A pile of wood 0.8 m high is prepared for the fire by first placing on the ground a thin layer of wood-wool and then on top of it, lying flat, three billets about 0.5 m long and 0.25 m in diameter. Across these are laid three more billets of similar size. On top of all are placed three layers of small sticks cut about 0.2 m long, with wood-wool between the layers. On each side, three or four pieces of wood about 0.5 m long are leant against the pile to prevent it from collapsing while it burns. The pile is ·set alight with a lighted fuse of wood-wool. (3) Observations are made to see whe ther the explosive flares or explodes; how long it burns and what phenomena accompany combustion; and what changes the box has undergone. (4) The test is carried out four times. A photograph is taken of the steel boxes after they have been used. (b) Test by heating in a confined spac~ in a steel tube with a calibrated orifice plate (steel tube test) (see marginals 3103 to 3110 and 3112). (1) The tests in (a) to (c) may be supplemented by the following test. (2) Description of the steel tube (fig. 2): The tube is made by pressing from sheet steel suitable for deep drawing1 • The dimensions are: inner diameter 24 mm; wall thickness 0.5 mm; lenght 75 mm. The open end is fitted with an outer flanqe. The tube is closed with a pressure-resistant central-orifice plate fixed tightly on the flange by an externally-threaded collar slipped over the tube and by a box nut screwed on to thiw collar. The plate is made from heat resisting chrome steel2 6 mm thick. To allow the escape of gases of decomposition, plates are used having cylindrical central orifices (a) with the following diameters: l.0-l.5-2.0-2.5-3-4-5-6-8-10-12-14-16-18-20 mm; a diameter of 24 mm is added when the tube is. used without orifice plate and closing device. Tme threaded collar and mut are made of manganese-chrome steel non­ scaling up to 800°C. 1 With orifice plates of from I to 8 mm diameter, nuts with a perforation (b) 10 mm in diameter must be used; if the diameter of the orifice is above 8 mm, that of the nut perforation must be 20 mm. Each tube is used for one test only. On the other hand, the orifice plates, threaded collars and nuts may be used again provided they are undamaged. As a check the orifice must be measured after each test. (3) Heating and protective device (fi?. 3): . • Heating is provided by town gas with. a net calorific value of 4,,000 Kcal/Nm3, from 4 burners producing about 2 .4 kc; ljsec for a consumption of 0.6 I/sec. As destruction of the tube is possible, heating is undertaken in a splinter-proof welded box, made of steel I 0 mm thick, open on one side and at the top. The tube is suspended between two rods 4 mm in diameter inserte d through holes drilled in opposite walls of the box, and 1s then heated by four Teclu burnes (external tube diameter 19 mm), the lowest heating the bottom·of the tube, those at the right a:nd left the walls, and that at the rear the closure. The burner tubes are inserted and secured in holes 20 mm in diameter drilled · in the walls of the splinter-proof box. The burners are lit siml.!ltaneously by a pilot jet and regulated to a plentiful supply of air so that the tips of the blue inner cones of the flames are almost touching the tube. • The whole installation is contained in a test stand separated froin the observation area by a strong wall i'! 1 e.g. Material Specification No. 1.0336.505 g, in accordance with DIN 1623 Sheet 1. . 2 e.g. Material Specification No. l.<!873, in accordance with Sheet •Stahl-Eisen-Werkstoff• 490-52. l e.g. Material Specification No.1.3817, in accordance with Sheet «Stahl-Eisen-Werkstoff• 490-52. 2246 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) which sight holes protected by armoured glass and slatted steel plates are arranged. The splinter-proof box is placed with its open side towards the observation area, care being takr~ that the flames are not affected by draughts. Equipment for extractmg gases of decomposition and smoke from the explosion is installed in the test room. If town gas is not av~ilable, propane can be used for heating. Is such a case the propane is taken from an industrial cylinder fitted with a pressure regulator (500 mm water gauge), through a meter (bellows-type meter w ith a capacity of 2 litres at 500 mm water gauge), and distributed by a manifold t1f the four burners, whose jets have a diameter of 0.8 mm. Each burner consumes not mo!e than about 1. 7 litres of propane a minute. The gas cylmders and the meter are placed outside the test stand. (4) Test procedure: The tube is filled with the explosive substance to within 15 mm of the top, i.e. to a height of 60 mm. If the substance . is in powdered form it is compressed by cautiously and gently tapping the tube and then pressing lightly with a small wooden rod. If the substance is gelatinous it is put ino the tube with the aid of a spatula; after each addition the substance is lightly pressed down with a small wooden rod to eliminate occlusions of air. When the quantity of substance inserted has been weighed, the threaded collar is slipped on to the tube, the required orifice plate is put in place, and the nut is tightened by hand. It is essential to make sure that none of the substance is trapped between the flange and the plate, or in the threads. The tube is then put in a rigidly mounted vice with shielding against inadvertent explosion, and the nut is fµlly tightened with a spanner. The tube, now ready for th~ te~t~- is suspended between the two rods in the splinter-proof-box; the pilot fet is lighted, and when the test stand has been closed the gas supply to the four burners is turned on. At the same time a· stop-watch is started to measure the time t1 elapsing between the lighting of the burners and the ignition of the substance, as shown by the escape of a flame from the orifice in the plat~, and the time t2 between lighting and explosion. On completion of the test the gas supply is shut off and exhaust system in the test stand is started up; no one must enter the stand until a sufficient period of time has elapsed. To make sure that the heating device is working satisfactorily, the tests must by preceded by a «dummy run•. (5) Interpretation of results: The relative degree of sensitivity of a substance to heating in the steel tube is expressed by the limiting diameter, this being the orifice with the largest diameter in millimetres with which, in three tests, at least one tube explodes, that is to say breaks up into at least three pieces. The thermal sensitivity increases with increasing limiting diameter and with decreasing times t and t . Organic peroxides ( except those w~tted oi diluted with volatile substances, e.g. water) for which the limiting diameter is not less than 2.0 mm i;hould be considered as explosive substances of Class la (see also note to marginal 2550). (e) Mealing test in a pressure vessel with an orifice plate and bursting disc (pressure vessel test) (see marginal 3112). (1) For organic peroxides, the tests shown under (a), (b) and (d) may be supplemented by the following test. (?) Description of the pressure vessel (fig. 4 to 6): • Figures 4 to 6 and the appropriate captions give tlie· details of the apparatus used and the dimensions and materials of the constituent parts. It should be noted that the use of 24 plates in provided for, the diameters of the orifices being: 1.0-1. 2-1. 5-2. 0-2. 5-3. 0-3. 5-4. Q-4. 5-5. 0-5. 5-6. 0-7. 0-8. 0-9. 0-10. 0-11. 0-12. 0-14. 0-16. 0-18. 0-20. 0-22.0 and 24.0 mm. These plates have a thi.ckness of 2 .0 mm :f. 0.2 mm. • The bursting disc is cut by a punch from a sheet of brass Q.05 mm thick with standing a bursting pressure of 5.4 ± 0.5 Kg/cm2 at normal temperature. Unannealed rolled brass containing 67 per cent copper is suitable. (3) Heating device: The pressure vessel is heated by technical-grade butane taken from a cylinder fitted with a pressure regulator. The heat output must be about 2,700 kcaljh. With a net calorific value of 27,000 kcal/m3 (at 1 atm and 20°C), the rate of gas supply must be about 100 1/h. A Teclu butane is used. The amount of gas used is measured by a rotameter or other meter and regulated by the burner valve. Instead of butane, town gas or propane may be used with a suitable burner, provided that the heat output of the gas is likewise about 2, 700 kcal/h (for example, in the case of town gas with a net calorific value of 4,050 kcaljm3 it would be necessary to supply about 670 ljh). The gas cylinder and the rotameter or other meter must be situated outside the,test area. • (4) Test procedure: For a normal test, 10 grammes of the substance are placed in the vessel. In the case of a: substance the sensitivity of which is unknown a start is made with smaller quantities: 1 gramme to begin with, then (if possible) 5 grammes, and finally 10 grammes. The bottom of the vessel must be evenly covered with the substance. The bursting disc, central orifice plate and retaining ring are then put in place. The wing nuts are tightened by hand and . the box nut with a spanner. The bursting disc is covered with enough water to keep it at a low temperature. The pressure vessel is placed on a tripod (with an inside ring diameter of 6 7 mm) which is inside a protective cylinder. The ring at the bottom of the vessel rests on the tripod. . The burner is lit, the flow of gas set at the required rate, and the flow of air so adjusted that the colour of the flame is blue and the inner cone of the flame light blue. The tripod must be of such a heigh that the inner cone almost touches the bottom of the vessel. Then the burner is placed under the vessel through a hole in the protective cylinder. The test area must be well ventilated and admission to it prohibited during the test. The vessel is observed from outside either by mirrors or through a sight hole in the wall, fitted with armoured glass. 1:he. time I ; betw~en the beginning of heating and the begmnmg ot reacllon (flame, production of smoke hissing) and the time t2 until the end of the reactio~ . ( detonation, end of hissing and production of smoke or· extinction of the flame) are measured. The vessel is then cooled with water and cleaned. (5) Interpretation of results: The relative degree of sensitivity of a substance to h~ating in the pre~ure vessel is expressed by the limiting diameter, this bemg the largest orifice diameter in millimeters with which the bursting disc is broken at least once in three tests while having remained intact during three tests with the next larger diameter. . ~~e t~ermal sensitivity increases with increasing hm1tmg diameter and with decreasing times t and t . Organic peroxides (except those wetted or ailutelwith v?latile s~bstances, e.g. water) for which the limiting diameter 1s not less than 9 mm should be considered as explosive substances of Class la (see also not to marginal 2550). Test of sensitivity to impact (see marginal 3103 to 3110 and 3112). (a) Fall-hammer test I (figs. 7 and 8) against a standard (control) explosive. (l) 1:he ex~losive, after drying as described in marginal 3150, 1s put mto the following form: . (a) Compact explosives are rasped fine enough to pass without residue throug~ a sieve of 1 mm mesh; only the 3155 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2247 residue remaining on a sieve of 0.5 mm mesh is kept for the following test; . (b) Explosives in powdered form are passed ~~ugh a sieve of l ·mm mesh; all that passes through this sieve 18 kept the impact test; Appendix A. l c) Plastic and .gelatinous explosives are formed into small, roughly spherical pills weighing between 25 and 35 mg. (2) The apparatus for carrying out the test consists of a weight which, sliding between two bars, is capable of being set to fall from a prearranged height and of being readily released for the fall. The weight does not fall directly onto the explosive, but falls onto a striker. Dresting on an anvil E, both in very hard steel and sliding easily in the guide ring F (fig. 7). The sample of explosive is placed between the striker and the anvil. The striker, anvil and guide ring are in a protective cylinder C made of hardened steel and placed on a steel block B embedded in a cement block A, (fig. 8). The dimensions of the various parts are given in the figures. . (3) The tests are carried out in tum on the explosive to be tested and, on the standard (control) explosive as follows: (a) The explosive, in the form of a spherical pill (if it is plastic) or measured with a measuring spoon of 0.05 cm3 capacity (if it is in the form of a powder or of raspings ), is arranged with care between the striker and the anvil, whose contact surfaces must not be moist. The ambien temperature must not exceed 30° C nor be less than 15 ° C. Each sample of the explosive must be subjected to one impact only. After each test the striker, the anvil and the guide ring must be carefully cleaned, any residue of explosive being removed. (b) Th~ tests must begin at heights of fall .likely to cause complete explosion of the explosives under test. The height of fall is reduced gradually until the resulting explosion is incomplete or no explosion results. At this height four impact tests are carried out, and if at least one produces a definite explosion, four further fall tests from a slightly lower height are carried out, and so on. (c) The lowest height or fall causing a definite explosion in a series of at least four tests at that height is taken as the limit of sesitivity. (d) The impact test is normally carried out with a ~rop weight of 2 Kg; however, if the sensitivity to impact with this weight requires a height of fall greater than 60 to 70 cm, the impact test must be carried out with a weight of 5 Kg. . (b) Fall-hammer test II (figs. 9 to 13) with numerical expression of impact sensitivity (impact energy in Kgm) (1) The test described in (a) may be replaced by the following test. Appendix A. I (2) Description of the apparatus: The essential parts of the apparatus are the impact device (see under (4), the cast steel block with base, the anvil, the column, the guides and the hammer with release devise (fig. 9). A steal anvil (100 mm in diameter, 70 mm hig.) is screwed on the steel block (230 x 250 x 200 mm) cast integral with the base (450 x 450 x 60 mm). Bolted to the back of the steel block is the supp~rt into which the column formed from a seamless-drawn steel tube (90 mm outside diameter, 75 mm inside diameter) is fixed. The two guides are fixed to the column by means of three cross-members and are fitted with a toothed rack to limit the tebound of the hammer and with a movable graduated scale for setting the height of fall. The hammer holding and releasing device is• adjustable between the guides and is clamped to them by the operation of a lever-nut on two jaws. The apparatus is so fixed on a concrete block (600 x 600 x 600 mm) by means of four anchoring screws sealed in the concrete that the base is iJl contact with the concrete over its whole area and the 3155 3155 guides are exactly vertical. A wooden splinter-proof box which has a lead lining 2 mm thick and opens easily surrounds the apparatus up to the level ·of the bottom cross-member. An exhauster enf11>les the explosion gases and dust from the substance to be fflmovect (3) Description of the fall-hammer: Each hammer is provided with two positiong grooves holding it between the guides as it drops and with a suspension spigot, a removable cylindrical striking head and a rebound catch which are screwed on to the hammer (fig. 11). The striking head is of hardened steel (HRC 60 to 63); its minimum diameter is 25 mm; it has a shoulder preventing it from being forced into the hammer by the impact. There are three hammers of different weights. The 1-Kg hammer is used for highly sensitivity the 5-kg hammer for substances of medium sensitivity and the 10-Kg hammer for substances oflow sensitivity. The 5-Kg and I 0-kg hammers are of massive and compact steel.• The 1-Kg hammer must have a heavy steel centre carrying the striking head and forming with it the main mass· of the hammer. The 1-Kg hammer is used for drop heights of 10 to 50 cm (impact energy 0.1 to 0.5 Kgm), the 5-Kg hammer for drop heights of 15 to 60 cm (impact energy 0.75 to 3 Kgm), and the 10-Kg hammer for drop heights of 35 to ;50 cm (impact energy 3·,5 to 5 Kgm). (4) Descriptions of the impact device: The sample to be examined is. enclosed in an impact device (fig. 11) consisting of two solid steel cylinders coaxially placed one above the other in a cylindrical guide ring likewise made of steel. The cylinders are steel rollers for anti-friction bearings and are 10 mm in diameter (type with a mean deviation of - 4 mic;:rons for a tolerance of - 2 microns, i.e. a diameter af 10-0.003 0.005 mm+, 10 mm high, with polished surfac~ ~n!J ; rounded edges (radius of curvature 0,5 mm) and an .HRC .hardness between 50 and 65 .. The guide ring has an outer • diameter of 16 mm. a lapped bore of 10 + 0.005+ 0.010 mm and a height of 13 mm. . . A cylindrical plug gauge may be used to check that the bore diameter is within the prescribed tolerances. The cylinders and the guide ring shall be degreased with acetone before use. The impact device is placed on an intermediate anvil 26 mm in diameter and 26 min high and centred by a locating ring provided with a ring of vent-holes to permit the escape of the gases (figs. 11 and 12). Each striking surface of the cylinders shall be used only once. If an explosion occurs, the guide ring shall not be used again. (5) Preparation of the samples The explosive substances are tested in the dry state. Substances of marginal 2101, 11 ° to 14 °, are tested as delivered provided that their water content agrees with the value indicated by the manufacturer. If the water content is higher, the mixtures must be dried before the test until their moisture content is that indicated. In addition, in· the case of solid substances other than those in paste-like. form ·the following points sh<?.t1ld be observed: (a) sybstances in powdered form are sieved (sieve mesh 0.5 mm); everything that passes through the sieve is used for the test; • (b) substances which have been compressed, cast ·or otherwise consolidated are broken into small pieces and sieved; the siftings from 0.5 mm to 1.0 mm in diameter are used for the test. (6) Test procedure: In the ~ of substances in powdered from, a sample is taken with a cylindrical measure of 40 mm3 c~pacity (3.7 mm diameter x 3.7 mm). • ~I least S1 37-1, in accordance with DIN 17000. ·3155 2248 ECl>HMEPII THI K'(BEPNHIEQI (TEYXOI nPOTO) ..:~::.:::....----------==--~ For substances in paste-like form, a cylindrical tube of the same capacity is used, which is plunged into the mass. After levelling off the excess extending beyond the measure, the sample is taken out by means of a wooden. 'l'Od. For explosive liquids a fine'-drawn piP,ette of 40 rnm~. ls used. • • The sample is placed on the open impact device, which is already in the locating ring on the intermadiate anvil, and in the case of sub.stances in powdered or paste-like form the upper steel cylinder is • lightly and carefully pressed with the forefinger until it touches the sample without flattening it. 1n the case of liquid substances the Upper steel cylinder is pressed down with the aid of the depth scale of a vernier gauge until it is 1 mm from the lower cylinder, and held in this position by a rubber ring previously slipped on to it (fig. 13). The device is placed centrally on. the anvil, the protective wooden box is closed, the hammer suspende d at the required height is released, and the exhauster IS then started up. The test is performed six times at each height of fall. . (7)1nterpretation of results . In inten>reting the results of the test of sensitivity to i!Jipact • a. distinction is made . between .. ~<>reaction "' "decomposition" (without flame or detonahon; recogmz­ able 'by colour-ehange or od~ur) and «explosion» (~di weak to strong detonation•. The de~ee of sens1hVIty to impact of a substance is measured by determing the weight of the hammer in kg and the lowest height of drop in cm with which an explosion occurs in at least one out of six tests, and the resultant impact energy in Kgm. The sensitivity of the substance to impact is greater the lower the impact energy in kgm. Test of sensitivity to friction (see marginals 3103 to 3110 and 3ll2) Friction test in a porcelain mortar · (1) The explosive is dried over calcium chloride. A saJJ lple of the explosive is compressed and ground in an unglazed porcelain mortar by means of a pestle, also ·unglazed. The mortar and pestle must have a temperature about 10 degrees higher than the ambient temperature (15° to 30° C). (2) The results of the test are compared with those obtained with the standard (control) explosive, and are classified as .follows: 1. no effect; 2. faint occasional crackling; 3. frequent crackling or very pronounced occasional crackling. Appendix A. l (3)Explosives which, under test, give the result set out in 1. are to be considered as practically insensitive to friction; if they give the result set out in 2. they are to be considered as moderately sensitive to friction; if they give the result set out in 3. they are to be considered as very sensitive to friction. (b) Test with the friction apparatus (figs.14 and 15) (1) The test described in (a) may be replaced by the followihng test. (2) Description of the apparatus: The friction apparatus is made up of the cast-steel base on which the friction device proper, comprising a fixed porcelain peg and movable porcelain plate (fig.14), is mounted. The porcelain plate is held in a carriage which runs 1n two guides. On operation of a push-button switch the carriage is moved by an electric motor through a • For some subsiances there is "ignition without detonation". This reaction is, however, regarded as an explosion (and designated by the terms in inverted commas) because it involves the entire sample and an explosion can also occur under indentical conditions. 3155 3156 3156 connecting-rod, an eccentric disc and suitable gearing in such a way that the porcelain plate moves back and forth once only beneath the porcelain peg, the distance of travel being 10 mm. The peg-holder pivots on an axis so that the porcelain peg can· be changed; it is extended by a loading arm with six notches for hanging a weight. Balance in the «zero» position (without weights) is a.chieved by adjusting a counter-weight. When the peg-holder · is . lowered on to the porcelain plate the longitudinal axis of the porcelain peg is perpendicular to the upper surface of the plate. One of the weights is hung by means of a ring and hook in the appropriate notch; the load on the peg can be varied from 0.5 to 36. Kg. •. . . (3) Description of the porcelain plate and peg: The flat porcelain plates are m(lde of .pure technical white porcelain and ~ave the following dimensions 25 mm X 25 mm X 5 mm. Before being fired, their two rubbing surfaces are thoroughly roughened by being rubbed with a SP,Onge. The sponge-marks are clearly visible. . The cylindrical porcelain pegs are also made of technical white porcelain; they are 15 mm long and 10 mm in diameter and their roughened ends are rounded, with a radius of curvature of 10 mm. . Samples of porcelain pegs and plates of the quality described above are deposited with the Bundesanstalt for Materialprufung, Berlin-Dahlem, which can supply the addresses of manufacturers. As the natural undamaged roughness of the plates and pegs is an essential condition for the reaction of the explosive substance, each part of the surface must be used only once. In conse g uence, the two end surfaces of. each peg are suffident for • two tests, and the two fricti~n surfaces of a plate will each serve for about three to six tests; (4) Preparation of samples: The explosive substances are tested in the dry state. Substances of marginal 2101, 11 ° to 14° are tested as delivered, provided that their W(lter content agrees with the value indicated by the manufacturer. If the water content is higher, the mixtures must be dried before the test until their moisture content is higher, the mixtures must be dried before the test until their moisture content is that indicated. In addition, for solid substances, except those in paste-. like form, the following points should be observed: (a) substances in powdered form are sieved (sieve mesh 0.5 mm); everything that passes through the sieve is used for the test; (b) substances which have been compressed, cast or otherwise consolidated are broken into small pieces and sieved; everything that passes through a sieve mesh of 0.5 mm is used for the test. (5) Test procedure: . A porcelain plate is fixed on the carriage of the friction apparatus so that the grooves of the sponge-marks on it run transversely to the direction of movement. The quantity to be tested, about 10 mrri3, is taken from substances in powdered form by means of a cylindrical measure (2.3 mm diameter X 2.4 mm); in the case of substances in paste-like form the sample is measured by a cylindrical tube which is plunged into the mass. Mter levelling off the excess extending beyond the measure, the sample is taken out by means of a wooden rod and . placed on the porcelain plate. The firmly-clamped porcelain peg is set on the heaped-up quantity as .shown in fig. 15; the loading arm is loaded with the required weight and the push-button switch is operated. Care must be taken that the peg rests on the sample and that there is enough of the substance in front of it to come under the peg as the plate moves. (6) Interpretation of results: In interpreting the results of the test a distinction is made between «no roaction», «decomposition» (change of colour, smell), «ignition», «crackling. and «explosion». The relative degree of sensitivity of a substance to friction in the friction apparatus as described is indicated (without taking the coefficient of friction into account) by EQ>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2249 the smallest load on the peg in Kg, with which ignitio~, crackling or an explosion occurs in at least one out o{ six tests. In this connection, even ignition and crackling are deemed to be dangerous reactions. The sensitivity of an explosive substance to friction is greater the lower. the ascertained load on the peg Qoading weight in relation to length of loading peg). . Explosive liquids and substances in paste-like form are not in general sensitive to friction under the conditions of this test; since because of the lubricating effect the slight frictional heat produced is insufficienno induce ignition. With such substances the absence of any reaction is no indication -that the substance is not dangerous. The stability of the products referred to in marginal 3111 is to . be checked by ordinary laboratory methods. Test of dynamite:for exudation (see marginal 3107) (1) The apparatus for testing dynamite for exudation (figs. 16 to 18) consists of a hollow bronze cylinder. This cylinder, which is closed at one end by a plate of the same metal, has an internal diameter of 15.7 mm and a depth. of 40 mm.: It is pierced by 20 holes 0.5 mm in diameter (4 sets of 5 holes) on the circumference. A bronze piston, cylindrical over 48 mm of its total length of 52 mm, can slide in the ·vertical .cylinder; this piston, whose diameter is 15.6 mm, is loaded with a weight of 2,220 g so as to produce a pressure of 1.2 Kg/cm2. • (2) A small plug of dynamite weighing 5 to 8 g, 30 mm long and 15 mm in diameter, is wrapped in very fine gauze and placed in the cylinder; the piston and its loading weight are then placed on it so that the dynamite is subjected to a. pressure of 1.2 Kg/cm2 •• The time taken for the appearance of the first si~ of oily droplets (nitroglycerine) at the outer orifices of the cylinder holes in noted. (3)The dynamite is considered-satisfactory if the time elapsing before the appearance of the liquid exudations is more than 5 minutes, the test having been carried out at a temperature of 15 ~ to 25 ° C. ~ Appendix A. l Combustion test Re marginal 3154 (c) ;EEE1= I . a ··----.--- ·-:·,o· --~-BIJ·-·s "' , IIO . ' ' ' a : I • I ' ·----· -- - -.. ., ---- ' ,, 3157 3158 3159 3199 Fig. l:. Steel box thickness of wall 1 mni· dimensions in mm • (1) general view (2) vertical section (3) section A~B ( 4) fabrication of wall ( 5) fabrication of base and cover ( 6) edges to be folded in Appendix A. l Test by heating in a s~eel tube with a calibrated .orifice plate He marginal 3154 ( d) Fig. 2: Steel tube and accessories Fig. 3: Heating and protective device dimensions in mm; for construction materials see marginal 3154 (d) (2) and (3) • (l) tube (la) outer flange (2) threaded collar; low-friction threa~ (3) orifice plate a = 1.0 ... 20.0 diameter. (4) nut b = 10 or 20 diameter (5) chamfe~ surface ( 6) 2 flats for spanner size 41 (7) 2 flats for spanner size 36 (8) splinter-proof box . (9) 2 • supporting rods for the tube (10) assembled tube . (11) position of rear burner; the other burners are visib)e (12) pilot jet • • • ·••---, ·. -nr- I· <5> 11-® ® Lr 11 •~ • ~J., r-1-..m•...J' H,S-l.;--1 .,, ... ' " ~ ,--,1~ G> ,~ n•O lO .1 • 2250 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 7 ""' 150 J 110 Appendix A.I Heating test in a pressure vessel with an orifice plate and bursting disc Re marginal 3154 (e) <S--,,.. 8-~~~:b.J !, ~~~ (9) ~"'~--' ~ -----.-IA!I✓ Fig. 4: Assembled pressure vessel; vertical section and plan (l) Pressure vessel (stainless steel) (la) welded joint (2) box nut (fully-killed weldable steel) (3) central-orifice plate (stainless steel) (4) inert retaining ring, 0.5 thick (5) pressure ring (stainlees steel) (6) brass handle (6a) brass screw (metetial M4 x 8 DIN 88) (7) bursting disc [for material see marginal 3154 (e) (2)] (8) wing nuts (brass M6 DIN 315) (Sa) washer (brass 6 DIN 125) (9) eye-bolt (stainless steel) ( 10) pivot for wing nuts (stainless steel) Note: Stainless steel having the folloving average composition is considered suitable: Cr 18%, Ni 9% Mn...;;2%, Si...;;1%, C...;;0.12%. f : ~ ... -- .. I Fig. 5: Pressure vessel dimensions in mm Appendix A. l Heating test in a pressure vessel with an orifice plate and bursting disc Re warginal 3154 (e) . . , ... Fig. 6: Pressure ring of the vessel; details in vertical section and plan view dimensions in mm E<l>HMEPII: THI KYBEPNHIEQI: (TEYXOI nPQTO) 2251 Appendix A. l Fall-hammer test I Re marginal 3155 (a) ..., .,00-----"'4 Fig. 7: Impact device, vertical section dimensions in· mm I • . . . •• I . . •, . . . .. . . . . -. r ... · .... . . : . ..... .. c. . . . .. • •------•dOO ------~ Fig. 8: Base for impact devise, vertical section dimensions in mm A. cement concrete block B. steel block C. protective cylinder D. striker E. anvil F. guide ring Appendix A. l Fall-hammer test II Re marginal 3155 (b) Fig. 9: Fall-hammer II, front and side, general view dimensions in mrr I F~. ·10, Foll-M~=• II !owe, p,rt dimeMWM io mm (1) base, 450x450x60 (2) steel block, 230x250X200 (3) anvil, 100 diameter x70 (4) column (5) median cross-member (6) 2 guides (7) toothed rack (8) graduated scale (9) fall-hammer (drop weight) (10) holding and releasing device ( 11) locating plate (12) intermediate anvil (interchangeable), 26 diameter X26 ( 13) locating ring with orifices (14) impact device 2252 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO} Appendix A. l • Fall-hammer test II Re marginal 3155 (b) Fig. 11: Hammer (drop weight) of 5 kg ( 1) suspension spigot (2) height marker (3) positioning groove ( 4) cylindrical striking head (5) rebound catch Appendix A. l Fall-hammer test II Re marginal 3155 (b) • ,o•.' ... r-'-1 <D-rro .,,::: flTI ~ IJ I .1--.. •--J <D Fig. 12: Impact device for substances in powered or paste-like form dimensions in mm Fig. 13: Impact device for liquid substances dimensions in mm (1) steel cylinders* (2) guide ring for steel cylinders* (3) locating ring with orifices (a) vertical section (b) plan ( 4) rubber ring (5) liquid substance (40 mm3) ( 6) space free from liquid • Steel can have the following composition: Cr ± 1.55%, C± 1 %, Si max 0.25% Mn ±0.35% HRC 58 ... 65 (heat-treated steel) Appendix A. l Test with friction apparatus Re marginal 3156 (b) Fig. 14: Friction apparatus; elevation. and plan view Fig. 15: Starting position of peg on sample ( 1) steel base (2) movable carriage (3) porcelain plate, 25x25x5 mm, held on the carriage • (4) fixed porcelain peg, 10 diameter xl5 mm (5) sample under test, approximately 10 mni3 (6) peg-holder (7) loading arm . (8) counterweight (9) switch (10) wheel for setting carriage at starting postion (11) dire~tion to electric drive motor E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2253 • • Appendix A. l Test of dynamite for exudation Re marginal 3158 Fig. 16: Hollow bronze cylinder, closed at one end; plan and vertical section dimensions in mm , • .. "" "' ] /J'-----(3) vn----® +••· .1 Fig. 17: Bell-shaped weight of 2220 g, capable of being suspended on 'the bronze piston ◄»' II Fig. 18: Cylindrical bronze piston dimensions in mm (1) 4 sets of 5 holes of 0.5 diameter (2) copper (3) lead plate with central tapered recess on underside (4) 4 openings, about 46 X 56, evenly spaced round periphery APPENDIX A.2 A. Provisions relating to the nature of aluminium - alloy receptacles for certain gases of Class 2 I. Quality of the material (1) The materials of aluminium - alloy receptacles which are to be accepted for the gases referred to in marginal 2203 (2) (b) shall satisfy the following requirements: A B C D Tensile strength, Rm, in krfmm2 5 to 19 20 lo 38 20 to 38 35 lo 50 Yield stres.s, Re, in krfmm2 (permanent sevtf 0,2%) 1 to 17 6 to 32 14 lo 34 21 to 42 Permanent elongation at fracture (l • = 5d) in per cent 12 lo 40 12 to 30 12 to 30 11 lo 16 Bend test ; n=5(Rm.;;IO) n=6(Rm.;;33) n=6(Rm.;;33) n=7(Rm.;;40) (diameter of fonner d= n.e, where e is the thicknes.s of the test - piece) n=6(Rm> 10) n=7(Rm>33)n=7(Rm>33) n=8(Rm>40) Aluminium Association Series Numher' 1000 5000 • 6000 2000 The actual properties will depend on the compos.ition of the alloy concerned and on the final treatment of the receptacle, but whatever alloy is used the thickness of the receptacle shall be calculated by the following formula: PxD e= 200Re + p 1.30 Where e = minimum thickness of receptacle wall, in mm; P = test pressure, in kg/cm2; D = nominal external diameter of the receptacle, in mm;, and Re = guaranteed minimum 0.2 - per cent proof stress, in kg/mm2 • In addition, the value of the minimum guaranteed proof stress (Re) introduced into the formula is in no case to be greater than 0.85 times the guaranteed minimum tensile strength (Rm), whatever the type of alloy used. Notes: 1. The above characteristics are based on previous experience with the following materials used for receptacles: Column A: Aluminium, unalloyed, 99.5 per cent pure; Column B: Alloys of aluminium and magnesium; Column C: Alloys of aluminium, silicon and magnesium, such as ISO/R209-Al-Si-Mg (Aluminum Association 6351 ). Column D: Alloys of • aluminium, copper and magnesium. 2. The permanent elongation at fracture (I = 5d) is measured by means of test-pieces of circular section in which the gauge length I is equal to five times the diameter d; if test-pieces of rectangular section are used . the gauge lenght must be calculated by the formula 1=5,65yFo, where Fo is the initial cross - sectional area of the test­ piece. 3. (a) The bend test (see diagram)•shall be carried out on specimens obtained by cutting into two equal parts of width 3e, but in no case less than 25 mm, an annular section of a cylinder. The specimens shall not be machined elsewhere than on the edges. (b) The bend test shall be carried out between a mandrell • of diameter (d) and two circular supports separated by a.distance of (d + 3e). During the test the inner faces shall be separated by a distance not greater than the diameter of the mandrel. (c) The specimen shall not exhibit cracks when it has been bent inwards around the mandrel until the inner faces are separated by a distance not greater than the diameter of the mandrel. • See ,Aluminium Standards and Data•, fifth edition, Ja~uary 1976, published by the Aluminium Association, 750 Third Avenue, New York. 320( 2254 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOr nPQTO) (d) The ratio (n) between the diameter of the mandrel and the thichkness of the specimen shall conform to the values given in the table. ,,...., I I I I i.-------i I ' I Diagram of bend test A lower minimum elongation value is acceptable on condition that in additional test approved by the competent authority of the country in which the receptacles are made proves that safety of carriage is ensured to the same extent as in the case of receptacles constructed to comply with the characteristics given in the table in paragraph (1). (3) The wall thickness of the receptacles at the thinnest point shall be the following: where the diameter of the receptacle is less than 50 mm: not less than 1.5 mm; where the diameter of the receptacle is from 50 to 150 mm: not less than 2 mm; and where the diameter of the receptacle is more than 150 mm: not less than 3 mm. (4) The ends of the receptacles shall have a semicircular, elliptical or «basket - handle» section; they shall afford the same degree of safety as the body of the receptacle. II. Additional official test for aluminium alloys. (1) In addition to the tests required by marginals 2215, 2216 and 2217, it is necessary to test for possible intercrystalline corrosion of the inside wall of the recep~a?le where use is made of an aluminium alloy contammg copper, or where use is made of an aluminium alloy containing magnesium and manganese and the magnesium content is greater than 3.5 per cent or the manganese content lower than 0.5 per cent. (2) In the case of an aluminium / copper alloy the test shall be carried out by the manufacturer at the time of approval of a new alloy by the competent authority; it shall thereafter be repeated, in the course of production, for each pour of the alloy. (3) In the case of an aluminium /magnesium alloy the test shall be carried out by the manufacturer at the time of approval of a ·new alloy and of the manufacturing process by the competent authority. The test shall be repeated whenever a change is made in the composition of the alloy or in the manufacturing process. (4) (a) Preparation of aluminium/copper alloys Before the aluminium/copper alloy is subjected to the corrosion test, the samples shall be cleansed of grease by means of a suitable solvent, and dried. (b) Preparation of aluminium/magnesium alloys Before the aluminium/magnesium alloy is subjected to the corrosion test, the samples shall be heated for seven days at 100 ° C; they shall then be cleansed of grease by means of a suitable solvent, and dried. (c) Performance of test The inner side fo a specimen measuring 1,000 mm2 (33,3 X 30 mm) of the material containing copper shall be treated at ambient temperature, for 24 hours, with 1,000 ml of an aqueous solution containing 3 per cent NaCl and 0,5 per cent HCI. 3201 (d) Examina-tion After being washed and dried, a section of the specimen 20 mm long shall be. examined mictographically at a magnification of 100 to 500 X, preferably after electropolishing. The depth of attack shall not go beyond the second layer of grains from the surfac e subjected to the corrosion test; in principle, if the entire first layer of grains is attacked, only part of the second row should be. In the case of sections, examination shall be performed at right angles to the surface. Where after electropolishing it is f!::iund necessary to render the grain boundaries particularly visible for subsequent examination, this shall be done by a method acceptable to the competent authority. Ill. Protection of the inner surface · The inner surface of aluminium - alloy receptacles shall be provided with a suitable anti-corrosion coating if the competent testing stations so ·consider necessary. B. Requirements concerning the materials and construction of receptacles intended for the carriage of deeply - refrigerated liquefied gases of Class 2 ( 1) Receptacles, tanks and shells shall be made of steel, aluminium, aluminium alloy, copper, or copper alloy, e.g. brass. However, receptacles, tanks and shells made of copper or copper alloy shall be accepted only for gases containing no acetylene; ethylene may however contain not more than 0.005 per cent acetylene. (2) Only materials appropriate to the lowest working . temperature of the receptacles, tanks and shells, and of their fittings and accessories, may be used. The following materials shall be accepted for the manufacture of receptacles, tanks and shells: (a) steels not subject to brittle fracture at the lowest . working temperature (see marginal 3265). The following may be used: 1. fine - grained unalloyed steels, down to a temperature of -60 ° C; 2. nickel steels (with a nickel content of 0.5 to 9 per cent), down to a temperature of -196° C, depending on the nickel content; 3. austenitic chrome - nickel steels, down to a temperature of -270° C (b) aluminium not less than 99.5 per- cent pure, or aluminium alloys (see marginal 3266); (c) deoxidized copper not less than 99.9 per cent pure, or copper alloys· having a copper content of over 56 per cent (see marginal 3267). (1) Receptacles, tanks and shells shall be either seamless or welded. (2) Receptacles under marginal 2207 made of austenitic steel, of copper or of copper alloy may alternatively be hard - soldered. The fittings and accessories may either be screwed to the receptacles, tanks and shells or be affixed there to as follows: (a) receptacles, tanks and shells made of steel, of aluminium or of aluminim alloy: by welding; (b) receptacles, tank~ and shells made of austenitic steel, of copper or of copper alloy: by welding or hard soldering. The construction or receptacles, tanks and shells and their mode of affixing to the vehicle, to the underframe or in the container frame shall be such as to preclude with certainty any such reduction in the temperature of the load - bearing components as would be likely to render them brittle. The fastenings of the receptacles, tanks and shells shall themselves be so designed that even when the receptacle, tank or shell is at its lowest working temperature the still possess the necessary mechanical properties. 3202 3203 3249 3250 3251 3255 3?64 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2255 1. Materials, receptacles, tanks and shells (a) Steel receptacles, tanks and shells The materials used for the manufacture of receptacles, tanks and shells, and the weld beads, shall at their lowest working temperature meet at least the following requirements as to impact strength. The tests may be conducted with test - pieces having either a U-shaped or a V-shaped notch. Material Impact strength 1 2 of sheet metal and weld beads at lowest working temperature 0 kgm/cm2 3 kgm/cm2 4 Unalloyed killed steel 3.5 2.8 Ferritic alloy steel Ni "55 % 3.5 2.2 F erritic alloy steel 5%;,.;;Ni~9% 4.5 3.5 ··· IAustenitic Cr-Ni steel 4.0 3.2 1 Impact strengths determined with different test - pieces • are not mutually comparable. 2 See marginals 3275 to 3277. 3 The values relate to test - pieces with a U-shaped notch as illustrated below. 4 The values relate to test-pieces with a V-shaJ)'ld notch conforming to ISO R 148. 1 0;; I "-; I 'It 0 ,-, ' I 55 - --'i' + 7 0,1 ,~· In the case of austenitic steels, only the weld bead need be subjected to an impact - strength test. For working temperatures below -196°C, the impact strenght test is not performed at the lowest working temperature, but at -196 ° C. (b) Receptacles, tanks and shells made of aluminium or aluminium alloy The seams of receptacles, tanks and shells shall at ambient temperature meet the following requirements as to bending coefficient: Thickness of sheet Bending coefficient K I for the seam e mmm Root in compression zone Root in tension- zone ~ 12 ~ 15 ~ 12 > 12 to 20 ~ 12 ~ 10 > 20 ~ 9 ~ 8 See marginal 3285. (c) Receptacles, tanks and shells made of copper or copper alloy It is not necessary to carry out tests to determine whether the impact strength is adequate. 3266 2. Tests (a) Impact-strength tests The impact strength shown in marginal 3265 relate to test-pieces measuring lOXl0 mm and having a U-shaped or a V-shaped notch. Notes: 1. With regard to the shape of the test-piece, see marginal 3265 (table), footnotes3 and 4• 2. For sheets less than 10 mm but not less than 5 mm thick, test-pieces having a cross-section of 10 X e mm, where «e» represents the thickness of the sheet, shall be used. Such impact-strength tests generally yield higher values than do such tests on standard test-pieces. 3. No impact-strength test shall be carried out on sheets less than 5 mm thick, or on their seams. (1) For testing sheet metal the impact strength shall be determined on three test-pieces. The test-pieces shall be removed at right angles to the direction of rolling in the case of test-pieces with a 1)-shaped notch and in the direction of rolling in the case of test-pieces with a 7 -shaped notch. (2) For testing seams the test-pieces shall be taken as follows: e ~ 10 Three test-pieces from the centre of the weld; three test-pieces from the zone of deformation created by the weld (the notch shall be completely outside the melted area but as near to it as possible); Centre of weld i.e. six test-pieces in all. □ u Zone of deformation The test-pieces shall be so machined as to have the maximum possible thickness. 10 < e ~ 20 Three test-pieces from the centre of the weld; three test-pieces from the zone of deformation; 3275 3276 l 5:-'---L---1 .) Centre of weld 2256 E<DHMEPII: THI: KYBEPNHI:EQI: {TEYXOI: nPQTO) Zone .of defo::mation i.e. six test-pieces· in all. e > 20 Two sets of three test-pieces (one set on the upper face, one set on the lower face) at each of the points indicated below: \ I r Centre of weld l l .... . . Zone of deformation i.e. twelve test-pieces in all. (1) For sheet metal the average of three tests shall meet the minimum values §iven in marginal 3265; none of the values may be more than 30 per cent below the minimum specified. (2) For welds the average values obtained from three the test-pieces taken at the different points, centre of weld and zone of deformation, shall correspond to the minimum values shown. None of the values may be more than 30 per cent below the minimum specified. (b) Determination of bending coefficient (1) The bending coefficient k referred to in marginal 3266 is defined as follows: • k = 50 ~, r where e = thickness of sheet in mm; and r = mean radius of curvature in mm of the test-piece when the first crack appears in the tension zone. (2) The bending coefficient k shall be determined for the seam. The width of the test piece shall be equal lo 3 e. (3) Four tests shall be performed on the seam, two with the root in the compression zone (fig. 1) and two with the root in the tension zone (fig. 2); all values obtained shall meet the minimum value requirements of marginal 3266. 3277 3278 3284 3285 e Fig. 1 Fig. 2 3286 3290 C. Provisions relating to tests on aerosol dispensers and non-refillable containers for gases under pressure of Class 2, 10° and 11 ° • 1. Pressure and bursting tests on receptacle model 3291 Hydraulic pressure tests shall be carried out on at least five empty receptacles of each model: (a) until the prescribed test pressure is reached, by which time no leakage or visible permanent deformation shall have occurred; and (b) until leakage or bursting occurs; the dished end, if any, should yield first and the receptacle should not leak or burst until a pressure 1.2 times the test pressure has been reached or passed. ?· Tightness (leakproofness) tests on all receptacles 3292 (1) For the test on aerosol dispensers (10°) and non­ refillable containers for gas under pressure (11 °) in a hot-water bath, the temperature of the bath and the duration of the test shall be such that the internal pressure of each receptacle reaches at least 90 per cent of the internal pressure that would be reached at 55 °C. However, if the contents are sensitive to heat or if the receptacles are made of a plastics material which softens at this test temperature, the temperature of the bath shall be from 20° to 30°C; in addition, one dispenser out of every 2,000 shall be tested at the temperature prescribed in the foregoing paragraph. (2) No leakage or permanent deformation of receptacles shall occur: The provision concerning permanent deformation is not applicable to receptacles which, being made of a plastics material, soften. APPENDIX A.3 Tests relating lo inflammable liquids of Classes 3 and 6.1 (1) The flash-point is determined by means of one of the following types of apparatus: (a) for use at temperatures not exceeding 50°C: Abel, Abel-Pensky, Luchaire-Finances, Tag; (b) for use at teperatures above 50°C: Pensky-Martens, Luchaire-Finances; (c) failing these, any other closed-cup apparatus capable of giving results within 2 ° C of these which an apparatus listed above would give at the same place. (2) To determine the flash-point of paints, gums and :similar viscous, products containing solvents, only apparatus and test methods suitable for determining the flash-point of viscous liquids may be used, such as method A of IP standard 170/59 or more recent IP standards, German standards DIN 53 213 and TGL 14 301, leaflet 2. 3293 3299 3300 E<DHMEPII: THI: KVBEPNHI:EQI: (TEYXOI: nPQTO) 2257 The test procedure shall be: (a) for the Abel apparatus, that of IP* standard 33/44; this standard may also be used for the Abel-Pensky apparatus; (b) for the Pensky-Martens apparatus, that of IP* standard 34/47, or that of ASTM* standard D.93/46; (c) for the Tag apparatus, that of ASTM** standard D.53/46; ( d) for the Luchaire apparatus, that of the Instruction annexed to the ministerial order (arrete ministeriel) (France) of 26 October 1925 issued by the Ministere du Commerce et de I' Industrie and published in the Journal Officiel of 29 October 1925. . If any other apparatus is used, the following precautions must be taken: 1. The test must be performed in a place free from draughts. 2. The rate of temperature increase of the liquid being tested must never exceed 5 ° C per minute. 3. The pilot-flame must be 5 mm ( ± 0.5 mm) long. 4. The pilot-flame must be applied to the opening of the receptacle after each rise of 1 ° C in the temperature of the liquid. In the event of a dispute as to the classification of an inflammable liquid, the item number proposed by the sender shall be accepted if a check-test of the flash-point, carried out on the liquid in question, yields a result not differing by more than 2 ° from the limits (21 °, 55 ° and 100°C respectively) stated in marginal 2301. If a check­ test yields a result differing by more than 2°C from these limits, a second check-test must be carried out, and the highest figure obtained shall be adopted. The peroxide content of a liquid shall be determined as follows: A quantity p (about 5 g, weighed to the nearest cg) of the liquid to be titrated is placed in an Erlenmeyer flask; 20 cm3 of acetic anhydride and about 1 g of powdered solid potassium iodide are added; the flask is shaken and, after ten minutes, heated for 3 minutes to about 60 ° C; it is then allowed to cool for 5 minutes, after which 25 cm3 of water are added. After being left standing for half an hour, the iodine liberated is titrated with a decinormal solution of sodium thiosulphate, no indicator being added. Complete decolorization indicates the end of the reaction. If n is the number of cm3 of thiosulphate solution required, the percentage of peroxide (calculated as H20 2 ) present in the sa~ple is obtained by the formula ~ . 100 p APPENDIX A.4 Reserved APPENDIX A.5 Provisions relating to tests on the metal drums referred to in marginals 2303 (6) and 2813 (1) (c) • I. Hydraulic pressure test This test shall be performed by an approved body. Number of samples Three drums per design type and per manufacturer. * The Institute of Petroleum, 61, New Cavendish Street, London, W.l. ** American Society for Testing and Materials, 1916 Race Street, Philadelphia 3, (pa.). 3301 3302 3303 3304 3399 3400 3499 3500 Test procedure and test pressure The drums shall be subjected to a hydraulic-gauge pressure of not less than 0. 75 kg/cm2 for five minutes, during which time the press~re must remain constant. The drums shall not be mechanically supported during the test. Criteria determining passing of test The drums must remain leak-proof. II. Drop test This test shall be performed by an approved body. Number of samples Six drums per design type and per manufacturer. Preparation of packages for testing The drums shall be filled to 98 per cent of their capacity. Target The target shall be ·a rigid, even, flat and horizontal surface. Height of drop If the test is carried out with water: (a) where the liquids to be carried have a specific gravity not exceeding 1.2 : 1.20 m; . (b) where the liquids to be carried have a specific gravity exceeding 1.2 a height expressed in metres by a number equal to the number expressing the specific gravity of the liquid to be carried rounded upwards to one decimal place. If the test is carried out with the liquid to be carried or with a liquid whose specific gravity is at least equal to that of the liquid to be carried : 1.20 m. Point of impact The test shall comprise drops of two kinds: • First drop (using three drums): The drum shall strike the target diagonally on the chime or, if it has no chime, on a circumferential seam. When dropped, the drum shall be so suspended that its centre of gravity is vertically above the point of impact. Second drop (using the other three drums): The drum shall strike the target horizontally on the welded longitudinal seam of the drum body. Criteria determining passing of test After the drop, all drums must be leak-proof when equilibrium between the external pressure and the internal pressure has been restored. If a drum is not leak-proof, twelve further drums shall be tested. None of these drums must show any leakage after the tests. If more than one in the first batch of six drums is not leak-proof, the type of drum in question shall be rejected. III. Leakage test Every drum shall be tested: (a) before being used in transport for the first time; and (b) after reconditioning, before being used again in transport. Tes.t procedure The drum shall be immersed in water; the manner of maintaining the drum under water shall be such as not to falsify the result of the test. Alternatively. the drum may be covered with a soap solution, heavy oil or other·suitable liquid on the seams and any other place where leakage could occur. Other methods at least as effective, such as the air pressure differential test ( •air-pocket tester»), may also be used. Air pressure to be applied The pressure shall not be less than 0.2 kg/cm2• Criteria determining passing of test There must be no air leakage. IV. Marking 3501 3502 2258 EG>HMEPII THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Drums of tested types of construction shall be durably marked with the impressed or printed sign of the State* in which· the test was carried out, with the mark «ADR» or .RID» and with a registration number assigned by the body which carried out the tests. V. Test report A test report must be drawn up, which shall include: 1. particular identifying the ~anufactur~r of the drum; 2. a description (e.g. matenal use?, thickness of walls and ends, joints, seams) and a drawmg; 3. the result of the tests; 4. the mark of the drum. A copy of the test report shall be sent to a bo~y designated by the competent authority of the State m which the test is carried out. 3503 3504 3505 3599 APPENDIX A.6. REGULATIONS RELATING TO RADIOACTIVE SUBSTANCES OF CLASS7 CHAPTER I - PACKAGING AND PACKAGE DESIGN REQUIREMENTS A. GENERAL DESIGN REQUIREMENTS FOR PACKACING AND PACKAGES ( 1) Th~ packaging shall be so designed that the package can be easily handled and can be properly secured during transport. (2) A package of gross weight 10 kg or more and up to 50 kg shall be provided with means for manual handling. (3) A package of gross weight in excess of 50 kg shall be so designed as to enable safe handling to be done by mechanical means. (4) The design shall be such that any lifting attachments on the package, when used in the intended manner, do not impose unsafe stresses on the structure of the package; assessment shall take account of appropriate safety factors to cover "snatch" lifting. (5) Attachments and any other features on the outer surface of the packaging which could be used to lift the packages shall be removable or otherwise rendered inoperable for transport or shall be designed to support the weight of the package in accordance with the requirements of paragraph ( 4) above. . (6) The outer layer of packaging shall be so designed as to avoid, as far as practicable, the collection and the retention of water. (7) The external surfaces of packaging shall, as far as practicable, be so designed and finished that they may be easily decontaminated. (8) Any features added to the package at the time of transport which are not part of the package shall not reduce the safety of the package. (9) The smallest overal external dimension of the packaging shall not be less than 10 cm. (10) Substances which have a critical temperature below 50°C or, at this temperature, a vapour pressure above 3 kg/cm2 shall be contained in receptacles which also comply with the regulations of marginals 2202 and 2211 to 2218. • The signs referred to are the national distinguishing signs for motor vehicles in international traffic. 3600 B. ADDITIONAL REQUIREMENTS FOR TYPE A PACKAGES (1) The outside of every package shall incorporate a feature such as a seal, which is not readily breakable and which, while intact, will be evidence that the package has not been opened. (2) As far as practicable, packaging shall be designed so that the external surfaces are free from protruding features. (3) The design of the packaging shall take into account the variations in temperature to which the packaging may be subjected during transport and st orage. In this respect, 40°C and 70°C shall be considered as satisfactory limits to be used in the selection of the materials; special attention, however, shall be given to brittle fracture over this temperature range. . (4) The design, fabrication and manufacturmg rechniques for welded, brazed, or other fusion joints shall be in accordance with national or international standards or with standards acceptable to the competent authority. (5) The package shall be capable of withstanding the effects of any acceleration, vibration or vibration resonance which may arise during normal transport without any deterioration in the effectiveness of thw closing devices on the various receptacles or in the integrity of the package as a whole. In particular, nuts, bolts and other securing devices shall be so designed as to prevent them from becoming loose or being released unintentionally, even after repeated use. (6) Special form radioactive substances may be considered as a component of the containment system. (7) The design shall include a containment system closed by a positive fastening device, that is a device which cannot open by itself, can only be opened intentionally and will resist the effect of a possible increase in pressure inside the vessel. (8) If a containment system forms a separate unit of the packaging, it shall be capable of being securely closed by a positive fastening device which is independent of any other part or the packaging. (9) The materials of the packaging and any components or structures shall he physically and chemically compatible with each other and with the package contents; account shall be taken of their behaviour under irradiation. (10) The design of any component of the containment system shall take into account, where applicable, the· radiolytic decomposition of liquids and other vulnerable materials and the generation of gas by chemical reaction and radiolysis. (11) The containment system shall retain its • radioactive contents under the reduction of ambient ·pressure to 0.25 kg/cm2• ( 12) All valves, other· than pressure relief valv~s, through which the radio.active contents could otherwise escape shall be protected against unauthorized operation and shall be provided with an enclosure to retain any leakage from the valve. • (13) A radiation shield which encloses a component of the packaging specified as a part of the containment system shall be so designed as to prevent the unintention~l release of that component from the shield. Where tlie radiation shield and such component within it form a separate unit, the radiation shield shall be capable of being securely closed by a positive fastening device which is independent of any other packaging structure. (14) Any tie-down attachments on the package shall be so designed that, under both normal and accident conditions, the forces in those attachm·ents shall not impair the ability of the package to meet the requirements of this Appendix. (15) Type A packaging shall be so designed that, if it were subjected to the rests specified in marginal 3635 it would prevent: (a) loss or dispersal of the radioactive contents, and 3601 ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOr riPQTO) 2259 (b) any increase of the maximum radiation level recorded or calculated at the external surface for the condition before the test. ( 16) Type A pack~ging designed for liquids shall, in addition, be adequate to meet the conditions prescribed in marginal (15) above if the package is subjected to the tests specified in marginal 3636. However, these tests are not required when enough absorbent material to absorb twice the volume of the liquid contents is within the' containment system and: (a) the absorbent material is within the radiation shield; or (b) the absorbent material is outside the radiation shield, provided that it can be shown that if the liquid contents were taken up by the absorbent material the resultant radiation level at the surface of the package would not exceed 200 mremjh. (17) Type A packaging designed for compressed or uncompressed gases shall, in addition, prevent loss or dispersal of the radioactive contents if .the package is subjected to the tests specified in marginal 3636. Packaging designed for tritium and argon-3 7, in gaseous form and in activities up to 200 Ci, shall be exempted from this requirement. C. BASIC ADDITIONAL REQUIREMENTS FOR TYPE B(U) AND TYPE B(M) PACKAGES (1) Except as provided in marginal 3603(1) (a) and 3604(2) respectively, Type B(U) and Type B(M) packages shall be designed to meet the additional requirements specified for Type A packages in marginal 3601(1) to (15) inclusive. (2) The packaging shall be so designed that if it were subjected to the tests in marginal 363 7 it would retain suffi cient radiation shielding to ensure that the radiation level at 1 m from the surface of the package would not exceed 1 rem/h had the package contained sufficient iridium-192 to produce a radiation level of 10 mrem/h at 1 m from the surface before the tests. Where the use of the packaging is to be restricted to particular radionuclides, those radionuclides may be used as the reference source in place of iridium-192. In addition, if the packaging is to be used for neutron emitters, an appropriate neutron referefice source should also be used. It is not required that a measurement necessarily be made with a test radiation source but only that calculations be made with respect to the particular· reference radiation source considered. (3) Type B(U) and Type B(M) packages shall be so designed, constructed and prepared for shipment that, under the ambient conditions specified in paragraph (4), they shall satisfy the conditions in (a) and (b) below: (a) Heat generated within the package by the radioactive contents will not, under normal conditions of transport (as demonstrated by the tests in marginal 3635) adversely affect the package in such a way that it will fail to meet the applicable requirements for containment and shielding if left unattended fo r a period of one week. Particular attention shall be paid to the effects of heat which may: (i) alter the arrangement, the geometrical form or the physical state of the radioactive contents or, if the material is enclosed in a can or receptacle (for example, clad fuel elements), cause the can, receptacle or material to melt; (ii) lessen the efficiency of the packaging through differential thermal expansion or cracking or melting of the radiation shielding material; (iii) in combination with moisture, accelerate corrosion. (b) The temperature of the accessible surfaces of a Type B(U) or Type B(M) package shall not exceed 50°C in the shade unless the package is transported as a full load. (4) In applying paragraph (3)(a), the following conditions shall be assumed: · 3602 (a) Ambient temperature 38°C. (b) lnsolation data according to Table I below. In applying paragraph (3)(b), the following condition. shall be assumed: Ambient temperature 38°C. In the case of Type B(M) packages to be transported exclusively between specified countries, alternative conditions may be assumed with the agreement of the competent authorities of these countries. TABLE I. INSOLATION DATA Form and location lnsolation in Gcal/cm2 for of surface 12 hours per day Flat surfaces transported horizontally: base none other surfaces 800 Flat surfaces not transported horizontally: each surface 200· Curved surfaces 400· a Alternatively, a sine function may be used, adopting an absorption coefficient and neglecting the effects of possible reflection from neighbouring objects. (5) Packaging which includes thermal protection for the purpose of satisfying the requirements of the thermal test specified in marginal 3637(3) shall be so designed that such protection will remain effective if the packaging is subjected to the tests specified in marginal 3635 and marginal 3637(2). Any such protection on the exte'rior of the package shall not be rendered ineffective by conditions commonly encountered in normal handling or in accidents and not simulated in the. tests referred to above, e.g. by ripping, cutting, skidding, abrasion or rough handling. D. SPECIFIC ADDITIONAL REQUIREMENTS FOR TYPE B(U) PACKAGES (1) The package shall be so designed that, if it were subjected to the 3603 tests referred to below, it would: (a) with regard to the tests specified in marginal 3635 restrict the loss of radioactive contents to not more than A 2 X 10·6 per hour. (b) with regard to the tests in marginal 3637, restrict the accumulated loss of radioactive contents to not more than A 2 X 10·3 in a period of one week. • Where mixtures of different radionuclides are present, the provisions of marginal 3691 shall apply. For (a) above, the evaluation shall take into account the external contamination limitations of marginal 3651. For both (a) and (b) above, the A 2 values for noble gases shall be those for the uncompressed state. (2) Compliance with the permitted activity release limits shall depend neither upon filters nor upon a mechanical cooling system. (3) A package shall not incorporate a feature which is intended to allow continuous venting during transport. (4) The package shall not include a pressure relief system from the containment system which would allow the release of radioactive substances to the environment under the conditions of the tests specified in marginals 3635 and 3637. (5) Where the maximum normal operating pressure (see marginal 2700(2)) of the containment system added . to any differential pressure below mean sea-level atmospheric pressure to which any component of the packaging specified as part of the containment system may be subjected exceed 0.35 kg/cm2 , that component shall be capable of withstanding a pressure of not less 3603 2260 E<DHMEPII THI KYBEPNHIEQI (TEVXOI nPQTO) than one and a half times the sum of those pressures; the stress at this latter pressure shall not be more than 7 5 per cent of the minimum yield strength and not more than 40 per cent of the ultimate strength of that component at the maximum expected operating temperature. (6) With the package at the maximum normal operating pressure (see marginal 2700(2) ) subjected to . the thermal test specified in marginal 363 7(3), the pressure in any component of the packaging specified as a part of the containment system shall be demonstrated not to exceed the pressure which corresponds to the minimum yield strength of that component at the maximum temperature which it would be expected to reach in the test. • (7) The package shall not have a maximum normal operating pressure (see marginal 2700(2)) in excess of · 7 kg/cm2 (gauge). (8) The maximum temperature of any surface readily accessible during transport of the package shall not exceed 82 ° C in the shade under normal conditions of transport (see also marginal 3602(3) (b) above.). (9) The containment system of a package containing liquid shall not be impaired if the PiCkage is subjected to a temperature of -40 ° C under normal conditions of transport. E. ADDITIONAL REQUIREMENTS FOR TYPE B(M) PACKAGES (1) In addition to the requirements of marginal 3602, Type B(M) packages shall, as far as practicable, meet the additional specific requirements for Type B(U) packages given in marginal 3603. (2) A type B(M) package shall be so designed that, if it were subjected to the tests referred to in Table II it would restrict the loss of radioactive contents to not more than the activity li'mits specified in Table II. The evaluation with respect to the tests specified in marginal 3635 shall take into account the external contamination limitations of marginar 3651. TABLE II. ACTIVITY LIMITS FOR LOSS OF RADIOACTIVE CONTENTS FROM TYPE B(M) PACKAGES Conditions Type B(M) packages Type B(M) packages not designed for specially designed continuous venting to allow continuous venting After the tests in A2 X 10·6 per hour A2x5xl0:5 per hour marginal 3635 After the tests in Krypton-85: 10 000 Krypton-85: 10 000 marginal 3637 Ci in 1 week Ci in 1 week Other radionuclides: Other radionuclides: A2 in 1 week A2 in 1 wekk • . The A 2 values used for noble gases shall be for the uncompressed state. Where mixtures of radionuclides are present the provisions of marginal 3691 shall apply. (3) If the pressure in the containment system of a Type .. B(M) package could result in a stress exceeding, under : the conditions of the tests in marginals 3635 and 363 7, : the minimum yield strength of any structural material of the containment system at the temperature which it would be expected to reach in the tests, the packaging shall be equipped with a pressure relief system to ensure that that minimum yield strength is not exceeded. 3604 3605 3609 CHAPTER II - FISSILE SUBSTANCES A. EXEMPTIONS OF FISSILE SUBSTANCES FROM FISSILE CLASS PACKAGE PRESCRIPTIONS Packages containing radioactive substances which are also fissile substances except for the cases specified in (a) to (g) below, shall be designed to comply with the requirements of this chapter. (a) Packages containing individually not more than 15 g of uranium-233, uranium-235, plutonium-238, plutonium-239, plutonium-241, or 15 g of any combination of these radionuclides, provided that the smallest external dimension of the package is not less than 10 cm. When material is transported in bulk, the quantity limitations shall apply to the vehicle. (b) Packages containing only natural or depleted uranium which has been irradiated in thermal reactors only. (c) Packages containing homogeneous hydrogenous solutions or mixtures satisfying the conditions listed in Table III. When material is transported in bulk, the . quantity limitations shall apply to the vehicle. TABLE III. LIMITATIONS ON HOMOGENEOUS HYDROGENOUS SOLUTIONS OR MIXTURES Parameters Any other fissile substances 235U only (including mixtures) Minimum HfX• 5200 5200 Maximum concentration of fissile nuclide in g/1 5 5 Maximum msss of f,ssile 500 SOOb nuclide in g,/package a Where. H /X . .is the ratio of the nu!l)ber of hydrogen atoms to the number of atoms of fissile nuclide. • b With a tolerance for Pu and 233U of not· more than 1 per cent of the mass of 235U. (d) Packages containing uranium enriched in uranium 235 to a maximum of 1 per cent by weight, and with a total plutonium and uranium-233 content of up to 1 per cent of the mass uranium-235, provided, that the fissile substances are distributed homogenc.ously throughout the material. In addition, if uranium-235 is present in metallic or oxide forms, it shall not form a lattice arrangement within the package. • (e) Packages containing any fissile substances provided that they do not contain more than 5 g of fissile substances in any 10-litre volume. The substances shall be packed in packages which will maintain the limitations on fissile substances distribution during normal transport. (f) Packages colltaining individually not more than 1 kg of total plutonium of which not more than 20 per cent by mass may consist of plutonium-239, plutonium-241, or any combination of thbse radionuclides. (g) Packages containing liquid solutions of uranyl nitrate enriched in uranium-235 to a maximum of 2 per cent by weight, with a tolerance for plutonium and uranium-233 of up to 0.1 per cent of the mass of uranium 235. The packages shall also comply with the other relevarit" parts of this Appendix. 3610 E<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) B. GENERAL .PROVISIONS FOR NUCLEAR SAFETY (1) All fissile substances shall be packed and shipped in such a manner that criticality1 cannot be reached under any foresseable circumstances of transport. In particular, the following contingencies shall be considered: (a) water leaking into or out of packages (b) the loss of efficiency of built- in neutron absorbers or moderators; • (c) possible rearrangement of contents into more reactive arrays, either within the package or as a result of loss from the package; ( d) reduction of spaces . between packages or contents; ( e) ·packages becoming immersed in water or buried in snow; (f) possible increase of reactivity du~ to temperature changes; (2) In addition, for irradiated nuclear fuel or unspecified fissile substances the following assumptions shall be made: • (a) Irradiated nuclear fuel for which the degree of irradiation is not known and whose reactivity decreases with burn-up shall be regarded as unirradiated for criticality control. If its reactivity increases with burn-up, it shall be regarded as irradiated to the point of maximum reactivity. The reactivity of nuclear fuel for which the degree of irradiation is known be assessed accordingly. (b) For unspecified fissile substances such as residues or scrap whose enrichment, mass, concentration, moderation ratio or density is not known or cannot be identified, the assumption shall be that each parameter that is not known has the value which gives the maximum reactivity under credible conditions. (3) Packages of fissile substances, except as provided in marginal 3610, shall be classified as follows: (a) Fissile Class I: packages which are nuclearly safe in any number and in any arrangement under • all foreseeable circumstances of transport; (b) Fissile. Class II: packages which, in limited number, are nuclearly safe in any arrangement under all foreseeable circumstances of transport; (c) Fissile Class III: packages which are nuclearly safe under all foreseeable circumstances of transport by reason of special precautions, or special administrative or operational controls imposed upon the transport of the consignment. C. PROVISIONS SPECIFIC TO FISSILE CLASS J PACKAGES (1) Each Fissile Class I package shall be so designed that, if it were subjected to the tests specified in marginal 3635: (a) water would not leak into or out of any part of the package unless water inleakage to, or outleakage from, that part, to the optimum foreseeable extent, has been assumed for the purposes of marginal 3614(1); and (b) the configuration of the contents and the geometry of the containment system would not be altered so as to increase the reactivity significantly. (2) Fissile Class I packages shall satisfy the nuclear safety criteria specified in marginals 3613 and 3614. 1. For the individual package considered in isolation (1) The following conditions shall be assumed: (a) the package is «damaged» (for this purpose 1. In· applying criticality data, obtained by eilher calculation or experiment, to the criticality clearance of lransporl packages, allowance shall be made separately for any inaccuracy in the data or uncertainty concerning their validity. 3611 3612 3613 «damage• shall mean the evaluated or demonstrated condition of the package if it had been subjected either to the tests specified in marginals 3635 and 3637(1) to (3), followed by that in marginal 3638 or to the tests specified in marginals 3635 and 3637(4), whichever combination is the more limiting); and (b) water can leak into or out of all void spaces of the packag~ including those within the containment system, except that, where the package design incorporates special features to prevent the leakage of water into or out of certain void spaces even ·as a result of human error, absence of leakage may be assumed in respect of those void spaces. Such special features may include either: (i) multiple high standard water barriers, each of which would remain leaktight if the package were subjected to the combinations of tests specified in paragraph ( 1 )(a); or (ii) high degree of quality control in the production and maintenance of packaging, coupled with special tests to demonstrate closure of each package qefore shipment. (2) The package shall be sub-critical by an adequate margin2 under the conditions specified in paragraph (1), the physical and chemical characteristics being taken into account, including any change in those characteristics which could occur under the conditions of paragraph (1), and with the conditions of moderation and reflection as specified below: (a) with the substances within the containment system: (i) the most reactive configuration and moderation foreseeable under the conditions of paragraph (l); (ii) close full water reflection of the containment system or such greater reflection of the containment system as may additionally be provided by the surrounding material of the packaging, and, in addition, (b) if any part of the substances escapes front th'!. containment system under the conditions of paragrap!t (l ): (i) the most reactive configuration and moderation considered credible; (ii) close full water reflection of the substances. 2. For consignments of one or more packages. (1) Any number of undamaged packages of one design in any arrangement shall be sub-critical; for this purpose «undamaged» shall mean the condition in which the packages are designed to be presented for transport. (2) 250 such packages when «damaged» shall be sub­ critical if stacked together in any arrangement and closely reflected on all sides of the stack by the equivalent of water (for this purpose «damaged» shall mean the evaluated or demonstrated condition of the package if it had been subjected either. to the tests specified in marginals 3635 and 3637 (1) to (3), followed by that in marginal 3638, .or to the tests specified in marginals 3635 and 3637 (4), whichever· combination is the more limiting). Hydrogenous moderation3 between packages, and water leakage into or out of the packages consistent with the test results shall be assumed to. the extent which results in the greatest reactivity. 3. Examples of package designs r equiring multilateral approval. . Example 1. The calculation shall be based on the following requirements: 2. For example, if mass of fissile substance is an appropriate parameter for control, an adequate margin would be represented by limiting the mass to 80 per cent of that mass which would be crilical in a similar system. 3. The hydrogenous moderation may be considered lo consist of either a uniform layer of full density water surrounding each package or water at an appropriate density homogeneously interspersed between packages. 2261 3614 3615 2262 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) (a) Each individual package shall comply with the criteria under marginals 3612 and 3613. (b) The package, whether damaged or undamaged, shall be such as to shield the fissile contents from thermal neutrons. (c) When a parallel beam of neutrons having an ·energy spectrum as specified in Table IV is incident at any angle on an undamaged package, the surface multiplication factor for epithermal neutrons, i.e. the ratio of the number of epithermal neutrons leaving the package to the number of epithermal neutrons entering the package, shall be less than one, and the evergy spectrum of the neutrons that are emitted by the package in an infinite array shall be no harder than that of the incident neutron. (d) The package design shall comply with the criteria in marginal 3614 (2). 4. Examples of package designs requiring unilateral approval. Example 1. (1) The packaging shall be constructed so that the fissile contents are surrounded by a layer of material capable of absorbing all thermal neutrons incident on it4 and this neutron absorbent layer is then surrounded by a thickness of at least 10.2 cm of wood having a minimum hydrogen content of 6.5 per cent by weight, so that the minimum external dimension over the wood is 30.5 cm. (2) The packaging shall be so constructed that when damaged» (for this purpose «damaged» shall have 'lhe meaning assigned in marginal 3613 (1)) the fissile contents will remain surrounded by the neutron absorbent layer, the neutron absorbent layer will remain surrounded by the wood, and wood will not be lost to an extent which would reduce the thickness of the remaining wood to less than 9.2 cm or reduce the minimum external dimension over the remaining wood to less than 28.5 cm. 4. This layer may consist of cadmium at least 0.38 mm thick equivalent to 0.325 g cadmium per cm2. 3616 (3) The contents shall not excedd that permissible mass of fissile substances shown in Tables V to XIII which is consistent with: (a) the nature of the substances; (b) the maximum moderation; and (c) the maximum diameter (or volume) which could occur if the package were «damaged» (for this purpose «damaged» shall have the meaning assigned in marginal 3613 (1) ). TABLE IV - NEUTRON ENERGY SPECTRUM" Neutron energy Fractions of neutrons E with energy less than E 11.0 MeV 1.000 2.4 ~1eV 0.802 1.1 MeV 0.590 0.55 MeV 0.460 0.26 MeV 0.373 0.13 MeV 0.319 43 keV 0.263 10 keV 0.210 1.6 keV 0.156 0.26 keV 0.111 42 eV 0.072 5.5 eV 0.036 0.4 eV 0 Note: ~·detailed calcu lation for a given package design m accordance with the method set out in marginal 3615 can give less restrictive values than those in Tables V to XIII. a. The spectrum is the epithermal portion of the equilibrium spectrum emergent from packages incorporating 5 cm thickness of wood in a critical array of such packages. Appendix A .6 TABLE V AQUEOUS SOLUTIONS OF URANYu!f FLUORIDE OR URA NYu!f NITRATE Pcrmissibl~ 111ase J>( uranium per package as a function of the packaging wood ,kr,:.ii ly I, Limited by maximum i~ternal diameter of inner receptacle Innl·r WooJ J~naity not exceeding 1,25 g/cm3 and not less than (g/cm3) receptacle 0,6 0,65 o. 7. o. 75 0.8 0.85 0,9 0.95 1,0 l, O'.i I.I diameter not l'XCccding· (cm) kg uranium per package 10.16 ' No limit No 1 imlt c,.004 0.120 0,157 o. 19} 0.2}1 0.267 0,}01 0.,,5 0.370 0.400 0.429 2. Limited ty maximum internal volume of inner receptacle Inner Wood dcr,sity not exceeding 1.25 g/cm3 and not lees than (g/cm3) receptacle ::. 6 0.65 0.1 o. 75 0.8 0.85 0.9 o.~5 1.0 1.U:, I.I v ol 1J.111e. 1,ot exc<.-eJing (1) kg ur~ium per package ;> u. 152 0.380 0.66 1.01 1.47 2.00 2.66 }.50 4.€4 t. ; 7 ,62 J. <,.(e4 0.22, 0.416 o.65 0.93 1. 25. 1.58 1.96 2.}4 2. ·:4 ,.11; 4. 0, 004 0.120 0.157 0.19} 0.2,1 0.2·14 0.}56 0,498 o.·i, 1. 'i 1.4·1 5 ·. ' o. 084 0.120 0.157 • 0.19} 0.2,1 0.267 0.301 0.495 , •. 0.57 c.t-r; u.-,4 7 O. l:64 0.120 0.157 o.19~ 0.2}1 0.267 o. }01 0,347 0,406 u. 4,.-, v.)3 llo limit 0.084 0.120 0.157 0.19} 0.2,1 o.?.67 0.}01 0.}}5 0.,10 l,4W 0.4:•~ !/ Uranium which inclu,lce no u23} and no more than 9}'" u2 '' by weight l,15 1,2 o,.456 0.478 1.15 1.2 9-}9 11.' }.'>: ,.')9 :?. ,'2 2.-,0 , .84 o. 92 0.6,:• o.66 (1,4)f o.47~ 1.2•; ; o. 4~JO, 1.2'> n., 4.4? }. ~•, l .ll:' o.n o. 491 m e :I: s: m "tl M I :I: M " -< CD m "tl 2 :I: M m :0 M =i m ~ 0 M :::::J "tl :0 I 0 ~ ~ 0) w A1,pen.dix A .G 'fAIIL.E VI 11011-ll'fllROCDiOUS \JRANil,ll (a) COMl'Olams UR IIJ.X'l'Ul!ES Ill \110:CII TIIE l•RANIUM-2}'., COJICEll'l'RATION LOES NOT ~;x::~D 4.,i r/c-m} (l,) (lncludinr, unmoderaled ur:inium melal of ur,u,ium-2}'., rnric-l;mcnt fl(Jl exceedir.1, 2' j-O· .·, , , i;, 'or•iri.l) PcnnicGible ~~or uranium ppr pack:y,:e BI~ 8 J\mction of ttr JJal"ka.,ir~r •.-·,f.•d 1:•11:·it~· ·r .. ; •. J,;imUeJ by maxiaiui:1 int .. n,:.1 ,iiamct.cr uf inner rectplar.lc I . ' lrin,:r \loo,I ,le11to1ty nol exceeding 1.25 g/f'fll, and n,>I ],,;;:· tl,an ().( r/•·m' f.,i.,ptnde .diam-:-U-r .not ,:X.'l'cdint: • ( ,-m) • - Ii,: uranium per pocknee ... . . • io.lL ffo 1 imi l lh i1m1 t · 0.19 ~--- Limfteil ·tiy"-maslmum 1 ntcmal volume· of inner receptacle Ji;r;1:r I \looJ 1irm1lty not. ucecdill£ 1.2~ g/cm'J and not le:••· lt,M (y./<:m}) • r~,:q,tii,·h - o.L~- -- 0,7 • 0.7~ o.o u.:•' vol~ 1:01 ' • l'X<'Cl~lr,t; (I) • - · kg uronlUIII per pa,·kage ' 1.0 10.0 12.2 14,'5 1.:. ~ ·4 4.& 1,8 7.:1 1.8 ·:.=J . ~ • ,.i) '·"' 3-0 ,.c, ~-'} 7. .1.41 1,41 1.41 1.41 1.41 N-·• . l-i m II 0.(9 • 0,69 0.(.9 -0,(9 O.('J .. ( ) - - · 2,, - - · tl 2, .. - a • Lra,; ;,.i:, 111.icl; i11c-l11J1:11 nu U . a,-,d n<> more lhan 972 pP.r cent U • by wei;t.t. (b) NiJl 11r.,, c•111lalnlne beeylllum or deuteiri1111 are excluded and lhP. mat1.s of carbon r-hall nol e:xc,•ed five ll111e,·· lh,• all""'"'' 111a,-~ ol' Hrar.i, .... "·: l •• . .. : • •4 ~-*'' 1.41 r-.t 'l l-,j l-,j 0:, ~ m e :::c 3: m ""C M i :::c M " -< CD m ""C 2 :::c M m :0 M ~ m < X 0 M ::::J ""C :0 i 0 Appendix A .6 TABLg VII NON-HYDROGENOUS URANIUl# Ca-lPOUHDS OR .MIXTURES JN VIIICH THE .• URANIUM-235 COHCl!:lfrRATION D<ES NOT EXCEED 9.6 g/c".D:5 !/, (Including unmoderated uranium metal of ·uranium-2:55 enrichment not exceeding ~ell, Ly veigl,t) Penni ssible mass of uranium per package as a function of the packap:in5 V<H•r1 d<·m:i t y ' ·l.· Limi led by maximum internal diameter. of inner receptacle Inner I Wood density not exceeding 1,25 g/cm3 and not less than (g/cm3) rcceptaclt: o.6 0'.65 o. 7 o. 75 o.a o.a5 0,9 0.95 1.0 1.0':, 1.1 di a:::l'I e.r nc, t cxcceJine; (cm) kg uranium per package I. 1 ~ 1.2 : 7.5 - !lo limit . 8 6 - No limit 8,5 6 7 8 - tlo limit 9 6 1 8 9.2 10 11 < No limit 9.5 6 7 8 9.2 10 11 12 14 15 - IL 1 iu;i t 10. 6 7 8 9.2 10 11 12 14 15 H. l'f 11 1·; No limit 0,69 0,69 0.69 0,69 0,69 0.69 0.69 0,69 0,69 (,,69 0,(;9 l', E) 0,£9 2. Lll::1i tcd b:, 11111ximum internal v.olume of inner recept·acle . lr . .nc:i I Wood density not ~xceeding 1,25 g/cm3 and not 0 less than (g/cm3) n·n:pl'acli, 0,65 0.7 0,75 • 0.8 0.85 0.9 ( -9'. v-.luz:,c 1,c,t . CXCL •.ding ( l) ~ '/ 8 9.2 10 11 12 i.l ~ 4 4,0 7,8 ·1 .a 7,13 7,f: ., ,<' .. ' . !,(3 3.63 . 3.63 ~.63 3.(3 3.( 3 1 • , . . . 7 l.~1 1,41 1.41 1, 41 l • -!~ . .. · 1. 41 JI .... N,, j lJT.i t . 0.(,9 O.f9 O,f9 o. fr) O,(.q C,(,::, ' . t ! y ,;n,.r:i:L~ ... .,i,ic1! i1,.·lude:': n,: u233 and ,w r.,or't' than 93½;, u23 '. by ,.,,,ii:;ht t,/ l~i~l~1·1•:1·c-onlainir,ir bt:1-vlli:um or :! 0 :11li,ri1.1111 ar•• PY.eluded an.I 11 :f•r:,a:,, of ~ad:r•r: ,-,hall I!,•· ,x,·r,., fiv,, ,,., ... ,, :,,,. tod .•. .·f 1:ra1:1 .c .. ,, 1.21, '' 19 0.69 1 • l• • ".P :·t. ,·• I -,l J ·~ .11 i. ••• , I m 8 :::c s: m "'tl M I :::c M " -< a, m "'tl 2 :::c M m :0 M ~ m < X 0 M ::I "'tl :0 I 0 ~ ~ 0:, CJ1 A l'Jl"nd 1 x A •. 6 TA?IIJ:: V 11 l UIR·!Oll~iiA'l'l,:il :mAil !UH Y tlETAL e Perrnisai l>le ma!Je of uranium per pa,·kaee a:i a fund ion of the Nlr.knging woo.J kn:li ly 1. Llmi lc:<1 by ;r.aximur.i internal :Jiamoter of inner recoptacl c Inner W'.lod density .:iot exceeding 1.25 g/cm1 and not lc:i:;. than (g/cm') r·et·eptac I e dlan,ct11r not o.6 o,65 0.7 0.75 o.e . o.ec; 0.9. • 0.95 1.0 ·1.05 ex..:ocliflB (cm) kg uranium per package .6 ;b lir.it ,. 6,5 l 7 ~ !lo limit ,. 7 6 7 8 9,2 10 - llo fimil . ·7,5 6 7 8 9.2 10 11 l;:, 14 l~ I(. ·-. tu • 6 7 8 9.2 10 11 12 14 15 16 • 11.J Hm.il.~ o.69 0.69 0.69 0.69 0.6') 0.69 0;69 0.69 0.69 0.6') lb llmitW 6 7 8 9.2 10 11 12 14 15 lb I 2- • . Li:rA tui' by :r..1.xir.;am internal volume of inner recepta..:lu . WooJ densit/not exceeding 1.25 g/cm' and not less tha~ (g/cm') . inner . receptac:;l'e o.6 0.65 0.7 0.75 o.e 0.85 0.9 0.95 1.0 1.05 .ilolull.l:·nu\ • exceeJing • (1.) kg uranium per.package • r . • 2 ; 6 1 8 9.2 10 11 12 14 15 16 5: 6 7 ·a 9.2 10 ·11 12 14 14.5 14.5 4 6 1 1.a 1.a 7.a 1.8 7,8 1.a 1.a -, .8 5 ,.6, ,.6, ,.6, ,.6, ,.6, ,.6, ,.6, ,.6, ,.6, ,.6) ., 1.41 1.41 1.41 1.41 ;.41 1.41 1.41 1.41 1.4i 1.41 ·uo i imi t o.69 0,69 0.69 0.69 0.69 o.69 0.69 0.69 0.69 o.69 II•• l i~I t°td '6 7 8 9.2 10 11 12 14 15 16 praniWli ilhich incluies no u2H and no more than 9l~ Jn5 by weight 1,1 1.15 1 ',) •· • . r . r . l'/ li I"( -· ~ 11 l / 11· o.£9 o.69 ~~(,) 17 17 l'/ 1.1 1.h 1 .2 17 17. I'( 1 4 .5 J.1.':> 14.5 • 1.a 7 .8 1.a ,.65 5.6} ).65 l.41 1 •. u 1 •. 11. 0.69 l)~(,9 o.G'} l'1 l'/ ·l"( !I ~l lriioae, enh11,11ced maauE:s apply where the fl.aaile substances are· in the form .or masoive metal rnd fre•· rro111 re-entrant surfaces. piece:; weighinc n:it !o:;.;; tlla.n :? kg ood1 1 ·11 1) l\r 0.6') 19 I •?5 19 14,5 7 .8 }.Gj 1.,11 0.6') 19 t,..? t,..? ~ m e •:J: s: m :E M f J: M "' -< CJ m ""O 2 ::I: M m :0 M ~ m < X 0 M ::::J ""O :0 f 0 Appendix A.6 TAllIE IX IIRAHI~ Cc»1POUNDS CR ~IXTilRES IN WHICH THE URANIUM CClfCENTRATIClf DOES Nor EXCEED 1v~6}t:i1 t/cm3 Pennissi ble niasa or llrl!J'lillll; per packape -~ a function of tl-.e packapinp ',I0Od density l . Limited by maximum internal. diam.eter of inner recept acle .. Inner I Wood density not exceedine 1.25 ,Jcm3 ~d not ieaa than (rJ~'> receptacle 0.6 0.65 0.7 0.75 O.J 0.85 0.9 0.95 1.0 -1.05 i.1 1.15 dilll:leter not . exceedinf ke uranium per packa@i! •; (cm) ' 6 I No limit ... E.5 2.80 . 6.0 ., llo li111i i .... 7. 2.80 6.0 6.o 6.o 6.o ., No lii..i t. ..... 7.5 2.80 6~0 6.0 6.o 6.o 6.0 6.o 14 15 15.2 15.2 15.2 ! 10 o.,,o o.87 1.10 1.80 2.50 :5.50 4.6 1.i 7.7 9.6 11.6 n.o ' ,llo 1 imi t· 0.084 o.i20 0.157 0.193 0.231· 0.267 o.,oi 0.}35 0.:570 0.400 0.429 0.456 2. l.imi tcd by maximum intei11al volume of inner re ceptaclo Inner I Wo~d den:iity not exceedi~e 1.25 e/cm} and not leas than (e/cm3) . •• r<·-::tJ,iaclc o.6 0.65 0.7 0.75 o.8 0.05 0.9 0.95 1.0 l. Cl'.; 1.1 1.1S • v,, 1 umc .not ,,x,·c1:<llnr (1) kt" urani cun per packaee 2 v.l'.:,2 o. }80 o.66 1.01 1.47 . 2.00 2.66 3.50 4.b4 6.1)4 '.(2 9. !:i .i. 0.084 0.416 3 0.22} 0.65 0.9} 1.25 1.58 i.96 2.34 2. ·14 ,. 1 i 3-'.•7 4 0.064 0.120 0.157 0.193 0.2}1 0.274 0.356 0.498 o.n 1.0C, 1.47 !:'.l'2 5 O.C84 o.i2q 0.157 ci. i 93 0.2}1 0.26? 0. }01 0.495 0.57 0.6(, , •. 'f.1 (. !•4 ., o .oa,1 . 0.120 o.'157 0.193 0.231 0.267 o. 301 .. 0.347' 0.406 {'·.,1~·.- 0.53 l·.t,' :; . l ! r..i t c,.c,a,1 0.120 0.157 .. 0.193 0.231 0.267 O. }Oi 0.335 0.370 0.40() o .. in c.~•,6 \.,. . . . . . 2}} . · I , ; .?. 7,·1 : • d· llran1u::. w111.:i: 11, :·h..J•·,;;nu ,.' anJ no more ,than.932 ~r ..:c1,1t t.,•, by ~e,1E'hl. 1.2 15.2 H,.1 u.4·1a 1.2 11. ~ 3.99 2. ·10 ('\.9:i l . t £ c·- .. 1·1:, 1.25 ... / ..... , ..... ./ 15.2 10.3 o.49~ ~ 1.21 , .! ; 1}.' 4 .. 1? 3 I,· . . . ,.,• 1.i:' ( ·p .. ,,, , --1'111 e t"1 :,,:: Nl Nl VI m e :I: '•S: m .,, M 4 :I: M " -< a, m .,, 2 :I: M m :0 M :;:j m < X 0 M :::J .,, :0 I 0 t,,;), ·•~;' '-'.J Appendix A .6 TABIE X Motf-HYDROCEHOUS PWTOMIUH COMPOUMDS OR MIXTURES IM WHICH THE PLUTOHI~2}9 COMCENTRATI0H liOES 101' EXCD:D 10 g/cm} !/ Permi~~!~le mass of plutonium per package as a function of the packaging woo4 d~nsity • 1. Limited by ir.axi11111m internal diameter of iMer rec~ptacle IMcr \ , Wood density not exc~eding 1.25 g/cm' and not leaa than (,/cm}) reccp"lacle o.6 0.65 0.7 0.75 o.a- 0.95 1 .05 1.1 diameter-not. -esc~.,j irig ''-: . . . (cm) - · kg, plutonium per package 6 ~ Ho lia.it ' -·- - - -- - - - --- - - --- - -- 6.5 ,~60 4.2 ~ Ho li.lllit --· ' 1 }.60 4.2 4.7 5., ~ llo 1 illli t ' 7.5 }.60 4.2 4.7 5.} 5.9 7,1 -... 10 }.60 4.2 4.7 5,.5 5.9 f.1 8.1 a:, llo l 1111i l II;. beat 0.405 0.40!) 0.405 0,405 0.405 0,405 0.405 0,405 2. Limited ty a-.aximum internal volume of inner receptacle lriner I Wood defieity not e%ceeding 1.25 g/cm.5 and not less than (g/cm}) recoiptacle u.6 0.65 0.1 o. 75 v:lu~,l not l·Xi.:t:.·C··llOg (I) kg plutonium per package ;. 3.60 4.2 4,7 5-! ,1 3.60 }.84 - }.84 3.i:,.; ' 2.44 2:44 2.44 2.-1-1 ; 1.20 . 1.20 1.20 1.2<' L lu:iit 0.405 0.405 0.405 o.~~~~-. 1.15 1 -~5 . • , ~ , . , I , ll.6 i<,9' Ci •• :05 l•~ .jl,5 v.O ' 5.1 ,; ·".; 2 .. :,1 : :2,1 o . .;05 ai i:1J<;l'1n:; c"r.ta1r.1r,e beryllium an,J dc>uterium are excluded and the mass of carbon sl:all n.lt ex,·,-,,.! 1/10 ..:J" Lt.,- a11~..-,.1 r..a:·, ~J" 1 !,,1.-m111:: .• I:,.;) I:,.;) O') 00 m e :I: s: m ""C M t :I: M " -< m m ""C 2 :I: M m :0 M =i m < X 0 M ::J ""C :0 t 0 Appendix A . 6 ·TABLE Xl UNMODERATED PLUTONIUM METAL Permissible mass of plutonium per package as a function of the packaging wood density , . l. Limited by maximum internal diameter of inner receptacle •.:~ lMer Wood density not exceeding 1.25 g/cm' and not lees than (g/cm}) receptacle o.6 0.65 0.7 0.75 o.a 0.85 diameter not exceeding (cm) kg plutonium per package 4 ,.20 ~ No limit . , , lO ,.20 ,.60 ,.90 4.2 4.4 4.5 No limit 0.405 0.405 0.405 o.40~ 0.405 0.:40':> Jfo Hmi tY ' ,.20 ,~60 ,.90 4.2 4.4 4.5 2. Limited by maxi11111111 internal volume of iMer receptacle Inner Wood density not exceeding 1.25 s/cm' and not leas than (g/cm}) receptacle o.6 • 0.65 0.7 0.75 o.8 . 0.85 VOlWlle not exceeding (1) '· kg plutonium per package ' ,.20 :,.60 ,.90 4.2 4.4 4.5 4 :,.20 :,.60 :,.84 ,.84 }.84 }.84 5 2.44. 2.44 2.44 2.44 2.44 2.44 1 1.20 1.20 1.20 1.20 1.20 1.20 No limit 0.405 0.405 • 0~405 0.405 0.405 0.405 No limit!/ :,.20 :,.60 f~90 4.2 4.4 4.5 !/ These enhanced masses apply vhere the fissile substances are in the form of massive metal pieces weighing not less than ·2 kg each and free from re-entrant surfaces m e ::I: s: m "'tJ M f ::I: M " -< tD m "'tJ 2 ::I: M m :0 M ~ m < X 0 M ::J "'tJ :0 f 0 b.:> b.:> 0) <:!:> Apvunuix A-~ ' Til~ Ul .'i .: r.Ll1!0111tni oo~uinls ~1 NiiTURES iN' ~1cu: :rHE· ,i.u10NTUN· ~N~i1ori ""'i;.,. NO EX- 2(•. ',{ I ., we,., T ......., Hf Pu~ 1. 35 g ,:m Penni,·i;ible ·111acs~f plu\oni\1111 per pa.:k&gl' nu ·a fur.et ion of the packaging"'"'" dc:r;: i l:f l. Limited by maxim11111 internal diameter of iMer receptacle Inner I Vood density not exceeding l.25 g/CZA} and not leSB than (g/,·m') ·receptacle c..c ·o.t') 0.7 0.75 o.8 • 0.85 0.9 0,95 1.0 1.0~ 1.1 di.aa.etcr not c:11<·,•cJing kg plutonium per package ,{,-m) 4 No limit 5 }.2 -,.ro :5.90 4.2 4.4 -· N~ limit 6 . 2.eo ,.e:o 3.90 4.2 4.4 4.5 4.5 4.5 4.5 t.:., 4-~ 6.5 2, ,:> :5.40 }.80 4.2 4,4 4.5 4.5 4.5 4-5 .;. 5 .:. ') 1 2.20 }.10 }.70 4.2 4.4 4.5 4.5 4.5 4.5 4.~ . ' • 7.5 1.90 2.70 ,.40 4.1 4.4 4.5 4.5 4.~ 4.5 4.; 4-~ ·8 1.ro 2.30 }.0 ,.ao 4.4 4.5 4.5 4.5 4.~ 4.~ 4. "; e.5 1. 30 1.80 2.4() ,.20 }.80 4.:5 4,5 4.5 4.5 4.5 4. ', .9 . 0~97 1. 30 1.80 2.40 }.00 }.40 }.£0 ,.eo 4.0 4.2 '}• ➔ 9.5 O.(~ o.88. 1.20 • 1.50 1.90. ~-20 2.40 2.fD 2.80 ,. 10 ;·.,o 10 o. 3!,0 0.42 0.50 o.sa 0.70 0.8} 0.99 1.20 l.~ 1.90 2.70 N; limit 0.022 0.05:5 0.084 0.114 0.14} 0.171 o.19~ 0,2?E 0.2~0 0.2"/4 0.294 • 2, Liau ted by 111&Xi111um internal volume of iMer receptacle Inner I Vood density not excet?dina 1.25 g/CZA} and not. l~s~ than (~/rr11,:5) ro,n,ptacle o.6 0.65 0.7 • 0.75 o.8 o.e~ 0.9 <',95 1.0 I.0~ I. l volume not · exccedin6 (1) ·kg plutonium per pac:lc:age • 2 0.1~2 0.309 0.52 0.80 1.16 1.~9 4.5 4.5 4 ,, :.' ... ·- .... ., 0.047 0.1}} 0.247 0.}80 0.700 0.76 4.~ 4.5 ,1.5 .:.•- .:." 4 0.022 o.07f 0.095 0.1}} 0.700 0.700 .o.·100 0.700 0.70l) C.S'·.' l .19 ; 0.022 0.0~} 0.085 0.118 0.700. 0.100 0.100 o.;oo <'. -;ri.'• Cl.;cr l • ;"('C' 1 0.02 • 0.05:5 o.os4 O.ll4 o.7ro 0.700 o.7c,o 0.700 o.-;n, e,.·;cc C • ''('( Ii-• ·Hl!II'. 0.():.>:.' 0.0•:5 0.084 0.114 c,.14:5 o·.1n 0.1'1': 0.2:f 0.:-''( ,,.~-'j4 0 .. , .. .... . 1.1~ l .2 . !.) . ' ~-, 4. ~ .i.~ 4.•, .i. '1 4.:; .i.~ 4. ~ .. -·. ... ~ ! .... 4-~ -·-.. ·· ,.~1.) ... -·. o. 31 i o. ~~·1 .. •;. ..... ' -.... .: . ~ . ' ~- . . ~. :. .. l. ~: ' • .:Of .: . ·:c0 (. 7(~ ~. ~·ol (; ... ()(, o. ~:; f'. ·~.:··; l .2~ .• . • L ~--.. ~-~ .: • ~1 .. ... , .:.: 4.~ ..... 1 • .i .:. ~ o.rn, 1.2~ .:.•· .:. : . ( .·.-.-, • .100 o. ~,~ ,-l~ c.., m e :c s: ·•m ""C M I :c M "' < OJ m ""C 2 :c M m lO M =t m < X 0 M ::::J ""C IO I 0 Ap~ndix A.6 TABLE XIII AQ~S SOLU'l'I~NS OF URANIUM-233 NITRATE OR URAHIUM-2'3 FLUORlllF.. Permiesible mass of uranium per package as a function of the packaging voorl Jr:neity 1.. Limited by mu:imu.111 internal di-ter of inner recept~cl, ·:··· IMer Wood denoity·not ·exceed~ng 1.25 g/cm3 and not less than (g/cm3) ,receptacle 0.6 0.65 0.7 0.75 0.8 0.85 0.9 · 0.95 1.0 1.05 1.1 11iemeter not • exc:eeJi'16 (cm) kg uranium per package 9 No limit ~ 9.5 0.0}5 0.067 - No limit 10 0.0:,5 0,067 0.100 - No limit No limit 0.0:,5 0,067 0.100 0.1}4 0.169 ·, 0.200 0.2:,1 0.261 0.289 o. }11, 0.:,40 2. Limited b,Y maximum internal volume of iMer receptacle Inner Wood density not exceeding 1.25 g/c~3 and not less than (g/cm3) ~receptacle 0.6 0.65 0.7 0.75 0.8 0.85 0.9 0.95 1.0 1.05 1.1 ·•1iol ,.me ·not '. e:rc1eedln1· (1). • kg uranium per package 2 0.152 0.,09 0.475 0.11 0.99 . l . :,:,. 1.71 2.11 2.54 2.99 3.44 ' (.,. 005 . o. n, ·o.1eo 0.228 0.285 0.}}2 0.}89 c.446 0.5iJ .... '>( o.c .. : 4 c,. (,85 0.109 0. l 33 0.175 0.213 0.256 0.}04 0.356 0.4,;e c;.4i.,: 0.51 .5 0.0}5 "'0.076 0.114 0.152 0.190 0.22, 0.256 u.292 0.}2} c·. :,~1 u.}89 7 0.0}5 o.on o.~09 0.142 0.175 0.204 0.2:,5 0.26} (.'1.289 c,. }10 0.:542 . llo limit 0.0}5 0.0.67 0.1 OC> 0.134 t), 169 .0.200 0.2:,1 0.2£1 0.289 C'.'lh, ll.}40 · 1.15 I.<' O.}bl o.r,1 1.15 1. 2 }.94 4.41 ('. il (. ·,3 ,.57 •. ,.(} 4.,., . . . • .4'.•l l•. 3(8 •. }'14 C.}(} ... :,·:·.• 1. :?'., , O. }'Jl 1.25 ~ . 4-~ • .• ·•0, 1·.,•1 ,4114 .,4;• , •. }'II · m e :c s: m :2 M t :c M ~ < gJ m 0 2 :c M m :0 M ~ m < X 0 M ::J 0 :0 d I,..:) I,..:) "-J .... 2272 ECJ;HMEPII: THI: 'KYBEPNHI:EQI: (TEYXOI: nPQTO ) D. PROVISIONS SPECIFIC TO FISSILE CLASS II PACKAGES (l)Each Fissile Class II package shllll: be ~esigne~ so that if it were subjected to the tests spec 1fied m margmal 3635: (a) Neither the volume nor any spacing on the basis of which nuclear safety for the purpose of marginal 3619(a) has been assessed • would suffer more than 5 per cent reduction, and the construction of the package wo~ld not permit the entry of a 100 cm cube. • .(b) Water would not leak into or out of any part of the package unless water inleakage to, or outleakage from, that part. to the optimum foreseeable extent had been assumed in assessing the allowable number for the purpose of marginal 3619(a). • (c) The configuration of the contents and tl1e geometry of the containment system would not be altered so as to increase the reactivity significantly. (2) Fissile Class II packages shall satisfy the nuclear safety criteria described in marginals 3618 and 3619. 1. The individual package considered in isolation. (1) The following conditions shall be assumed: (a) the package is damaged (for this purpose «damaged• shall mean the evaluated or demonstrated condition of the package if it has been subjected either to the tests specified in marginals 3635 and 3637 (1) to (3), followed by that in marginal 3638 or to tests specified in marginals 3635 and 3637 (4), whichever combination is the more limiting); and • (b) water can leak into or·out of all void spaces of the package, including those within the containment syste~, except that, where the package design incorporates special features to prevent the leakage of water into or out of certain void spaces even as a result of human error, absence of'lihlcage may be assumed iri respect of those void spaces. Such special features may include either: (i) multiple high-standard water barriers, each of which would remain leaktight if the package were subjected to the combinations of tests specified in paragraph (l)(a); or (ii) a high degree of quality control in the production and maintenance of packaging, coupled with special tests to demonstrate closure of each package before shipment .. (2) The package shall be sub-critical by an adequate margin (see footnote 2) under the conditions specified in paragraph ( 1 ), the physical and chemical charac teristics being taken into account, including any change ~~ those characteristics which could occur under the cond1t1ons of paragraph (1), and with the conditions of moderation and reflection as specified below: (a) with th~ substances within the containment system: (i) the most reactive configuration and moderation foreseeable under the conditions of paragraph (1 ); (ii) close full water reflection of the containment system or such greater reflection of the containment system as may additionally be provided by the surrounding material of the packaging and, in addition, (b) if any part of the substances escapes from the containment system under the conditions of paragraph ( 1 ); (i) the most reactive configuration and moderation considered credible; (ii) close full water reflection of the substances. 2. Consignments of one or more packages An «allowable number» shall be devised for each Fissile Class II package design, such that: (a) five times the allowable n umber of unda~aged packages shall be sub-critical if stacked together m: any arrangment without anything between the packages, close reflection on all sides of the stack by the equivalent or water being assumed; for this purpose «undamaged» shall mean the condition in which the packages are designed to be presented for transport; and (b) twice the allowable number of such packages when damaged shall be sub-critical if stacked together in any 3617 3618 3619 arrangement and closely reflected on all sides of the stack by the equivalent of water (for ~his purpose «damaged• shall mean the evaluated or demonstrated condition of each package if it had been subjected either to the tests specified in marginals 3635 and 3637 (1) to (3) followed by that in marginal 3638, or to the tests specified in marginals 3635 and 3637 (4), whichever combination is the more limiting); hydrogenous moderations3 between packages and water leakage into or out of the packages consistent with test results shall be assumed to the extent which results in the greatest·reactivity. 3. Examples of package designs requiring no competent authority approval Example I (requiring multilateral approval of shipment) Packages for Fissile Class II require no competent authority approval of package design provided that the following conditions are met; (a) Packaging: the criticality safety of these consignments does not depend upon the integrity of the packaging. Any packaging which complies with the other relevant requirements of Class IVb with respect to the non-fissile radioactive characteristics may, therefore, be used. • (b) Contents - uranium metal, compounds and/or mixtures; the contents of any consignment consisting of the «allowable number» of packages shall not exceed the permissible mass of uranium-235 given in Table XIV per consignment as a function of enrichment for substances satisfying the following conditions: (i) Uranium-233 shall not be present. (ii) Beryllium and hydrogenous material enriched in­ deuterium shall not be present. (iii) The total mass of graphite present shall not exceed 150 times the total mass of uraniumc235. (iv) Mixtures of fissile substances with substances having a higher hydrogen .density than water, e.g., some hydrocarbon· oils, shall not be present. This does not preclude the use of polyethylene for packing or wrapping. TABLE XIV. PERMISSIBLE MASS OF URANIUM 235 PER CONSIGNMENT Uramium enrichment in Permissible mass per weight per cent of uranium consignment grams of 235 not exceeding uranium-235 93 160 75 168 80 176 40 184 30 192 20 203 15 224 11 240 10 I 256 9.5 262 9 270 8.5 276 8 284 7.5 294 7 300 6.5 312 6 324 5.5 340 5 360 4.5 380 4 400 3.5 440 3 500 2.5 600 2 820 1.5 1360 1.35 1600 1 3400 0.92 6000 3620 E<DHMEPII THI KYBEPNHIEQI (TEYXOI ·nPQTO) 2273 (c) Conten~s - uranium metal, compounds and/or mixtures not forming a lattice: the contents of any consignment consisting of the allowable number of packages shall not exceed the permissible mass of­ uranium-235 given in Table XV per consignment as .a function of enrichment for substances satisfying the following conditions: (i) Uranium-233 shall not be present. (ii) Beryllium and hydrogenous· material enriched in deuterium sh~ll not be present. Appendix A.6 (iii) The total mass of graphite present shall not exceed 150 times the total mass of uranium-235. (iv) Mixtures of fissile substances with substances ha­ ving a higher hydrogen qensity than water. e. g. some hydrocarbon oils, shall not be present. This does not preclude the use of polyethylene (or packing or wrapping. (v) The fissile st1bstances shall be distributed homoge­ neously througho ut the contents, In addition, the substan­ ces shall not form. a lattice arrangement within the pac­ kage. TABLE XV. PERMISSIBLE MASS OF • URANIUM-235 PER CONSIGNMENT Uranium enrichment permissible mass per consignment in weight per cent ·of uranium-235 not ex grams of uranium-235 ceeding 4 ~ 420 3.5 460 3 560 2.5 740 2 1200 1.5 2800 1.35 4000 .. (d) Contents - uranium arid/or plutonium· metal, com0 pounds and/ or mixtures: the substances shall satisfy the following cqnditions: • (i) Beryllium and hydrogenous material enriched in deuterium'shall not be present. • (ii) The total m~ss of graphite present shall not exceed 150 times the total mass of uranium and plutonium. (iii) Mixtures of fissile substances· with substances ha­ ving· a higher hydrogen density than water, e.g., some hydrocardon oils, etc., shall not be present. This does not preclude the use of polyethylene for packing or wrapping. 3620 • The total mass of fissile substances per consignment shall be such that: • 235U(grams) • Pu(grams) +-=--....:. 160 ' 90 233 U (grams) . + . 1s not greater ·100 . than I. (e) Allowable numbe~:.th~ all.ow~ble number for a partic­ ular package to this specification will depend on the actual contents a nd is equal to. the fissile mass limit per consig­ nment· divided by the actual fissile mass present in the . package. In the case of the mixed nuqlides in (d) above the allowable number is: 160 235U + 1.6 X 233U + 1. 778 X Pu where 235U,' 233li and Pu are the number~,"of grams of 235U, 233U and Pu present in the package. Where the package forms part of..a mixed consignment the requirements of. footnote 1 to marginal 2700 (2) be met. (t) Shipment shall be subject to multilateral approval. E. PROVISIONS SPECIFIC TO FISSILE CLASS III PACKAGES • • 3620 Fissile Class I II packages shall mi:et the general requi7 rements of marginal 3611 and s ha,ll be approved in accor­ dance with marginals 3674 and 3675. 1. Examples of P.ackage designs requiring unilateral ap proval . Example 1 (requiring multilat eral approval 9f shipment) Packages to the following specification require only unilateral approval of the package de1?ign provided that the following conditions are fulfilled: (a) The number of packages in any one consignment· shall be so limited that: . (i) twice this number of undamaged packages shall be sub-critical if stacked together in a!ly arrangement without . anything between the packages, assuming close ~eflection on all sides of the stack by the equivalent of water; for this purpose "undamaged" shall mean· the condition in which the packages are designed to be presented for tra~s­ port; and (ii) this number of packages when "daniaged" shall be· sul.2 ~crit i<;aj if stacked together in any arrange~ent and cTosely reflected on all sides of the stack by the equivalent of water (for this purpose "damaged"shall mean the eval­ uated or demonstqi.ted condition of each package if it had been subjected either to the tests specified in marginals 3635 end 3637 (1) to (3) followed by that in marginals 3638 or the tests specified in marginals 3635 and 3637 (4), whichever combination is the more limiting). Hydrogenous monderation 3/between the packages and water leakage into or out of the packages consistent with test results shall be assumed to the extent which res~lts in the greatest reactivity. (b) Shipment of these packages shall be made only under arrangements approved by the competent authori­ ties in c~r:ifo~ity with marginal 3675, so as to prevent loading, transport or storage of these packages with!q.ther labelled packages of radioactive material. .... 2. Examples of fissile package design requiring no com­ petent authority approval Example 1 (requiring multilateral approval of shfp­ ment). Packages to the following specification for Fissile Class III require no competent authority approval of package design provided the following conditions are met: (a) The package is currently approved as a Fissile Class II package and the number in any one consignment does not exceed twice the. allowable number associated with the Fissile Class II approval. (b) Shipment of these packages shall be made only under arrang~ments approved by the competent authori­ ties in conformity with marginal 3675, so as to prevent loading, transport or storage of these packages with other Fissile Class II or Class III packages. Examples of such arrangements are: • (i) no other labelled packages of radioactive substances may be carried with the consignment' in the same vehicle, and (ii) either transport shall be direct to the consignee without any intermediate transit storage; or controls shall be imposed, by the provision of an escort, to prevent the packages of the consignment fron being stacked with or alongside any other packages of radioac­ tive substances after an accident, or at any other time. Thit·esc<>rt shall travel in a separate vehide. Example II (requiring multilateral approval of ship­ ment) Packages for Fissile Class III require no competent authority approval of package design provided that the following conditions are met (a) Packaging: the criticality safety of· these consig­ nments does not depend upon ,the integrity of the packa­ ging. Any packaging which cod"plies with the other relevant requirements of this .Appen 1x may therefore be used, provided it does .not incorporate lead exceeding 5 cm in thickness, tungsten or uranium shielding. • 3621 3622 3622 3623 2274 EG>HMEPII: THI: KYBEPNHIEQI (TEYXOI nPOTO) (b) Contents - uranium metal, compounds and/or mixt­ ures: the contents af any consignment shall not exceed the permissible mass of uranium-235 given in Table XVI per consignment as a function of enrichment for substan­ ces satisfying the following conditions: (i)Uranium-233 shall not be present. (ii) Berylliul!l and hydrogenous material enriched in deuterium shall' not be present. (iii) The total mass of graphite present shall not exceed 150 times the total mass of uranium-235. (iv) Mixtures of fissile substances with substances ha­ ving a higher hydrogen density than water e.g., some hydrocarbon oils, shall not be present. This does not precl­ ude the use of polyethylene for packing or wrapping. Appendix A.6 TABLE XVI. PERMISSIBLE MASS OF URANIUM-235 PER CONSIGNMENT. Uranium enrichment in weight Permissible mass per per cent of uranium-235 consignment grams of not exceeding uranium-235 93 400 75 420 60 440 40 460 30 480 20 520 15 560 11 600 10 640 9.5 655 9 675 8.5 690 8 710 7.5 730 7 750 6.5 780 6 810 5.5 850 5 900 4.5 950 4 1.000 3.5 1.100 3 1.250 2.5 1.500 2 2.050 1.5 3.400 1.35 4.000 1 8.500 0;92 15.000 • (c) Contents - uranium metal, compounds and/or mixtures not forming a lattice: Table XVII gives the permissible mass of uranium-235 per consignment as a function of enrichment, for substances satisfying the following conditions: (i) Uranium-233 shall not be present. (ii) Beryllium and hydrogenous material enriched in deuterium shall not be present. (iii) The total mass of graphite present shall not exceed 150 times the total mass of uranium-235. • (iv) Mixtures of fissile substances with substances having a higher hydrogen density than water, e.g., some hydrocarbon oils, shall not be present. This does not preclude the use of polyethylene for packing or wrapping. (v) The fissile s'ubstances shall be distributed homogeneously throughout the contents. In addition, the substances shall not form a lattice arrangement within the package. TABLE XVII. PERMISSIBLE MASS OF URANIUM-235 PER CONSIGNMENT Uranium enrichment in weight • Permissible mass per per· cent of uranium-235 consignment kilograms of not exceeding uranium-235 4. 1.05 3.5 1.15 3 1.4 2.5 1.8 2 3 1.5 7 1.35 10 (d) Contents - uranium and/or plutonium metal, compounds and/or·mixtures:· the substances shall satisfy the following conditions: (i) Beryllium and hydrogenous material enriched in ·deuterium shall not be present. (ii) The total mass of graphite present shall not exceed 150 times the total mass of uranium and· plutonium. .. (iii) Mixtures of fissile substances with substances having a higher hydrogen density than water.' e.g., some hydrocarbon oils, shall • not be present. This does. not preclude the use of polyethylene for packing or wrapping. The total mass of fissile substances per consignment shall be such that: 235U(grams) Pu(grams) 233U(grams)· + -=---'- + ---='-----=- , is not greater 400 225 250 than I. (e)·Conditions of transport: the following administrative controls shall be applied throughout the. transport of the consignment: (i) the quantity •Of substances in a consignment shall not exceed that defined in (b), (c) or (d) above; (ii) transport shall be direct to the consignee, without any intermediate transit storage. • (f) Shipment shall be subject to multilateral approval. CHAPTER III - TEST AND INSPECTION PROCEDURES A. DEMONSTRATION OF COMPLIANCE WITH THE TEST REQUIREMENTS (1) Demonstration of compliance .with the test requirements of this chapter may be accomplished by any of the methods listed below or by a combination thereof. (a) Performance of tests with prototypes or samples of the packaging as· normally presented for transport, in which case the contents of the packaging for. the test shall simulate as closely as practicable the expected normal radioactive contents. (b) Reference to· previous satisfactory demonstrations of sufficiently similar nature. (c) Performance of tests with models of appropriate scale incorporating those features which are significant with respect to the item under investigation, when engineering experience has •shown results of such tests to be suitable for design purposes. When a scale· model is used, the need for adjusting certain test parameters, such as the penetrator diameter or the compressive load, shall be taken into account. (d) Calculation, or reasoned argument, when the calculative procedures and parameters are generally agreed to be reliable or conservative. 3625 3629 3630 <J>.EK 225 E<J>HMEPlr THI: KYBEPNHI:EQr (TEYXOI: nPQTO) 227:J (2) With respect to the initial conditions for the tests of this chapter except those in marginals 3637 (4-) to 3639, the demonstration of compliance shall be based on the assumption that the package is in equilibrium at an ambient temperature of 38 ° C. With respect to the thermal test the effects of solar radiation can be neglected prior to and during that test but shall be taken into account in the subsequent evaluation of the test results. B. TESTS FOR PACKAGING 1. Number of specimens to be tested The number of specimens actually subjected, to the tests should be related to the number of packagings of t!-iat type which are to be produced, the frequency of use and the cost. The results of the tests may necessitate an increase in the number of specimens to meet the requirements of the test procedures in respect of maximum damage. • 2. Preparation of a specimen for testing (1) All specimens shall be examined before testing to identify and record faults or damage including the following: (a) divergence from the specifications or the drawings; (b) defects in construction; ( c) corrosion or other deterioration; and ( d) distortion of features. (2) The containment system of the packaging shall be clearly specified. (3) The external features of the specimen shall be clearly identified so that reference may be made simply and clearly to any part of such specimen. 3. Testing the integrity of containment and shielding After any of the applicable tests specified in marginals ~635 to 363 7, it shall be further demonstrated that the integrity of the containment, or of the containment and shielding, has been retained to the extent required in marginals 3601 (15) to (17), "3602 (2), 3603 (1) and 3604 (2) for the packaging under test. 4. Target for the drop tests specified in marginals 3635 (4), 3636 (2), 3637 (2) and 3641 (1) The target shall be a flat, horizontal surface of such a character that any increase in its resistance to displacement or deformation upon impact by the specimen would not significantly increase the damage to the SRecimen. 5. Tests for demonstrating ability to withstand normal conditions of transport (1) The tests are: the water spray test, the free drop test, the compression test and the penetration test. Prototypes of the package shall be subjected to the free drop test, the compression test and the penetration test, preceded in each case by the water spray iest. One prototype may be used for all the tests, provided that the requirements of paragraph (2) are complied with. (2) The time interval between the conclusion cif the water spray test and the succeeding test shall be s uch that the water has soaked in to the maximum extent, without appreciable drying of the exterior of the specimen;. In the absence of any evidence to the contrary, this interval-shall be taken to be about two hours if the water spray is applied from four directions simultaneously. No time interval should elapse, however, if the water spray is applied from each of the four directions consecutively. (3) Water spray test: Any water spray test shall be considered as satisfactory provided that: (a) the amount of water per uriit of ground area is approximately equivalent to a rainfall rate of 5 cm per hour; 3631 3632 3633 3634 3635 (b) the water impinges upon the specimen at an angle of approximately 45 ° from the horizontal; (c) the water is approximately uniformly distributed, as in .a rainfall, over the entire surface of the specimen in the direction of the spray; . (d) the duration of the spray is at least on hour; (e) the orientation of the packaging is such that the effects are expected to be the most severe for the features under investigation, and the specimen is supported so that it does not sit in a pool of water. . (4) Free drop test: The specimen shall fall onto the target so as to suffer maximum damage in respect of the safety features to be tested. . (a) The height of fall measured from the lowest point of the package to the upper surface of the target shall be as specified in Table XVIII. TABLE XVIII. FREE-FALL DISTANCE FOR PACKAGES Package weight l Free fall distance (Kg) (m) [ess than 5,000 1.2 5,000 to < 10,000. 0.9 10,000 to <:: 15,000 0.6 15,000 and greater 0.3 (b) For Fissile Class II packages, the free drop specified above shall be preceded by a free drop from a height of 0.3 m on each corner or, in the case of a cylindrical package, onto each of the quarters of each rim. (c) For ·fibreboard or wood rectangular packages not exceeding 50 kg in weight, a separate specimen shall be subjected to a free drop onto each corner from a height of 0.3 m. ., (d) For fibreboard cylindrical packages not exceeding 100 kg in weight, a separate specimen shall be subjected to a free drop onto each of the quarters of each rim from a height of 0.3 m. (5) Compression test: the specimen shall be subjected, for a period of 24 hours, to a compressive load equal to the greater of the following: (a) the equivalent of 5 times the weight of the actual package; (b) the equivalent of 1300 kg/m2 multiplied by the vertically projected area of the package. The load shall be applied uniformly to two opposite sides of the specimen, one of which shall be the base on which the package would normally stand. (6) Penetration test: the specimen shall be placed on a rigid, flat, horizontal surface which will not move significantly while the test is being carried out. (a) A bar of 3.2 cm diameter with a hemispherical end and weighing 6 kg shall be dropped and directed to fall, with its longitudinal axis vertical, onto the centre of the ,. weakest part of the specimen, so that, if it penetrates sufficiently far, it will hit the containment vessel. The bar shall not be significantly deformed by the test performance":· • (b) The height of fall of the bar measured from its lower end to the upper surface of the specimen shall be 1 m. 6. Additional tests for Type A packaging designed for liquids and gases ( 1) Separate specimens shall be subjected to each of the following tests unless it can be demonstrated that one test is rriore severe for the specimen in question than the other, in which case one specimen shall be subjected to the more severe test. (2) Free drop test: the specimen shall fall onto the target so as to suffer the maximum damage in respect of containment. The height of the fall measured from the lowest part of the specimen to the upper surface of the target shall be 9 m. C 3636 2276 E<l>HMEPlr THr KYBEPNHrEor (TEYXOr nPQTO) (3) Penetration test: the specimen shall be subjected to the test specified in marginal 3635 (6) except that the height of fall shall be increased to 1. 7 m from the 1 m specified in marginal 3635 (6) (b). 7. Tests for demonstrating ability to withstand accident conditions in transport (1) The specimen shall be subjected to the cumulative effects of the mechanical tests specified in paragraph (2) and the thermal test specified in paragraph (3) in that order. A separate specimen shall be subjected to the effect of the water immersion test in paragraph (4). (2) Mechanical test: the test shall consist of two drops onto a target. The order in which the specimen is subjected to the two drops shall be such that, on completion of the mechanical test, the specimen will have suffered stlch damage as will lead to the maximum· damage in the thermal test which follows. (a) For drop I, the specimen shall fall onto the target so as to suffer the maximum damage, and the height of fall measured from the lowest point of the specimen to the upper surface of the target shall be 9 m. (b) For drop II, the specimen shall fall onto the target so as to suffer the maximum damage, and the height of fall measured from the intended point of impact of the specimen to the upper surface of the target shall be 1 ~­ The target in this case shall be the upper end of a sol~d mild steel bar of circular section, 15 cm ± 0.5 cm m diameter. The target surface shall be flat and horizontal with its edges rounded off to a radius of not more than 6 mm. The bar shall be rigidly mounted perpendicularly ~n the foundation target described in marginal 3634 and shall be 20 cm long unless a longer bar would cause .. greater damage; in that case, a bar of sufficient length to cause maximum damage shall be used. (3) Thermal. test: any thermal test shall be considered as satisfactory provided that the heat flux incident on the specimen is not less than that which would result from exposure for 30 minutes of the whole specimen to a radiation environment of 800°C with an emissivity coefficient of at least 0.9. For purposes of calculation, the surface absorptivity shall be either that value which the package may be expected to possess if exposed to a fire or 0.8, whichever is greater. In addition, when significant, convective heat input shall be included on the basis of still ambient air at 800°C during the thirty-minute period. After c;:essation of the external heat input to the specimen: (a) the specimen shall not be cooled artificially until another· three hours have elapsed or until it has been demonstrated that all internal temperatures have begun to fall, whichever is the earlier; and • (b) any combustion of materials of the specimen shall be allowed to proceed for three hours after the cessation of external heating to the specimen unless it terminates earlier naturally. (4) Water immersion test: the specimen shall be immersed under a head of water of at least 15 m for a period of not less than eight hours. For test purposes, an external pressure of water of 1.5 ~g/cm2 (gauge) will be considered to meet these conditions. 8. Water in-leakage test for packages containing fissile substances ( 1) Packages ~ther than Fissile Class I or Fissile Class II packages and any packages for which water in-leakage or out-leakage to the extent which results in greatest reactivity has been assumed for purpose of assessment under marginals 3614 (2) and 3619 (b) shall be exempted from the test. (2) Before the specimen is subjected to the water in­ leakage test specified below, it shall be subjected to the tests in marginals 3637 (2) and (3). (3) The specimen shall be immersed under a head of water of at least 0.9 m for a period of not less than eight hours and in the attitude for which maximum leakage is 3637 3638 expected. For this test an ambient temperature of 38°C is not required. 9. Tests for integrity of containment and shielding Any test or inspection method may be employed to determine whether the requirements of this Chapter have been met after the specimen has been subjected to the tests in marginals 363 5 to 363 7, provided that the method can be demonstrated to meet the relevant requirements of marginals 3601 to 3604. C. TESTS FOR SPECIAL FORM RADIOACTIVE SUBSTANCES • • 1. General (1) The tests are: the impact test, the percussion test, the bending test and the. heat test. (2) Specimens· (solid radioactive substances or capsules) to be tested shall be prepared as normally presented for transport. The radioactive substances shall be duplicated as closely as practicable. . (3) A different specimen may be us~d for each of the ~~ ' (4) The specimen shall not break or shatter when subjected to the impact, percussion or bending tests. (5) The specimen shall not melt or disperse when subjected to the heat test. . (6) After each test, a leaching assessment shall be performed on the specimen by a method no less sensitive than the methods given in marginal 3642. 2. Test methods (1) Impact test: the specimen shall fall onto the target. from ·a height of 9 m. The target shall be as defined in marginal 3634. (2) Percussion test: the specimen shall be placed on a sheet of lead which is supported by a smooth solid surface and struck by the flat face of a steel billet so as to produce an impact equivalent to that resulting from a free fall of 1.4 kg through 1 m. The flat face of the billet shall be 25 mm in diameter with the edges rounded off to a radius of 3 mm ± 0.3 mm. The lead, of hardness number 3.5 to 4.5 on the Vickers scale and not more than 25 mm thick, shall cover an area greater than that covered by the specimen. A fresh surface of lead shall be used for each impact. The billet shall strike the specimen so as to cause maximum damage. (3) Bending test: the test is applicable only to long, slender sources with both a minimum length of 10 cm and a length to minimum width ratio of not less than 10. The specimen shall be rigidly clamped in a horizontal position so that one half of its length protrudes from the face of the clamp. The orientation of the specimen shall be such that the specimen will suffer maximum damage when its free end is struck by the flat face of a steel billet. The billet shall strike the specimen so as to produce an impact equivalent to that resulting from a free vertical fall of 1.4 kg through 1 m. The flat face of the billet shall be 25 mm in diameter with the edges rounded off to a radius of 3 mm to ± 0.3 mm. (4) Heat testi the specimen shall be heated in air to a temperature of 800°C and held at that temperature for a period of 10 min and shall then be allowed to cool. 3. Leaching assessment methods (1) For indispersible solid substances: (a) The specimen shall be immersed for seven days in water at ambient temperature. The water shall have a pH of 6 to 8 and a maximum conductivity of l0i,tS/cm at 20°c. (b) The water with specimen shall then be heated to a temperature of 50 ° ± 5 ° C and maintained at this temperature for four hours. 3639 3640 3641 36.42 EG>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) (c) The activity of the water shall then be determined. (cl) The specimen shall then be stored for at least seven days in still air of humidity not less than 9Q per cent at 30°c. (e) The specimen shall then be immersed in water of the same specification as in (a) above and the water with specimen heated to 50 ° C ± 5 ° C and maintained at this temperature for four hours. (J) The activity of the water shall then be determined, The actiYities determined in (c) and (J) above shall not exceed 0.05 f.l Ci. (2) For encapsulated substances: (a) The specimen shall be immersed in water at ambient temperature. The water shall have a pH of 6-8 with a maximum conductivity ,of 10 f.l S/cm. The water and specimen shall be heated to a temperature of 50 ° C ± and maintained at this temperature for four ·hours. (b) The activity of the water shall then be determined. (c) The specimen shall then be stored for at least seven days in still air at a temperature not less than 30°C. (cl) Repeat (a). (e) The activity of the water shall then be determined. The activities determined in (b) and (e) above shall not exceed 0.05 f.l Ci. D. INSPECTION REQUIREMENTS TO BE FULFILLED BEFORE FIRST USE • AND BEFORE EACH' SHIPMENT OF CERTAIN TYPES OF PACKAGES 1. Before first use Before first use of any package, the following requi~ements shall be complied with by the consignor: (a) For each Type B(U) and Type B(M) package, it shall be ensured that the effectiveness of its shielding and containment, and, where necessary, the heat transfer characteristics, are within the limits applicable to or specified for the approved design. • (b) If the design pressure of the containment system exceeds 0.35 kg/cm2 (gauge), it shall be ensured that the containment systeni of each package conforms with the approved design requirements relating to the capability of that system to maintain its integrity under pressure. (c) Where, in order to comply \vith the nuclear safety criteria, neutron poisons are specifically included as components of the packaging primarily for this purpose, tests shall be performed to confirm the presence and distribution of that poisoning. ·2. Before each shipment Before each shipment of any package, the following requirements shall be complied with be the consignor: (a) Type B(U) and Type B(M) packages shall be held until equilibrium conditions have been closely enough approached to demonstrate compliance with the shipment requirements for temperature and pressure unless an exemption from these requirements has received unilateral approval. (b) It shall be ensured that all the requirements specified in the approval certificates have been satisfied. (c) It shall be ensured by examination and/or, appropriate tests that all closures, valves and other openings of the containment system through which the radioactive contents might escape are properly closed and, where appropriate, sealed in the manner for which the demonstrations of marginals 3603 (1) and 3604 (2) were made. (cl) It shall be ensured that the provisions of marginal 3600 (5), with regard to lifting attachments have been complied with. 3643 3644 3645 3649 CHAPTER IV. - CONTROLS FOR TRANSPORT AND STORAGE IN TRANSIT A. MIXED PACKING A package containing radioactive substances shall not contain any other items except such articles and documents as are necessary for the use of the radioar.tive substances. Such items may be included, provided that there is no interaction between them and the packaging or contents that would reduce the safety of the package. B. NON-FIXED RADIOACTIVE CONTAMINATION The non-fixed radioactive contamination on any external surface of the package shall be kept as low as practicable and shall at no time during normal transport exceed the levels laid down in Table XIX. The level of non-fixed radioactive contamination may be determined by wiping an area of 300 cm2 of the surface concerned by hand with a filter paper, or a wad of cotton wool or any other. material of this nature. . Packages used for the transport of radioactive substances such as irradiated fuel, shall be assessed to determine whether activity is likely to be leached to the surface e.g. by rain. The frequency of such assessment shall be related to the likelihood of radioactive contamination having been absorbed into the surface coating, particularly paint. When activity is likely to be leached to the surface of the package, the continued use of such a package shall be conditional upon a radiation safety assessment by a qualified p~rson. TABLE XIX. MAXIMUM PERMISSIBLE LEVELS OF NON-FIXED RADIOACTIVE CONTAMINATION . Contaminant Maximum permissible level (see Note") ([!Ci/cm2) Natural and depleted uranium and natural thorium only 10·3 Beta and gamma emitters and the low-toxicity alpha emitters specified in Note" below 10·4 All other alpha emitters 10-5 Notes: "The above levels are permissible when averages over any area of 300 cm2 of any part of the surface. i. Low toxicity alpha emitters: Uranium-235 or uranium-238; thorium-232; thorium 228 and thorium-230 when diluted to a specific activity of the same order as that of natural uranium and natural thorium; radionuclides with a half-life of less than 10 days. C. CATEGORIES Packages and containers (both large and small) shall be. in one of the following three categories: • L Category I-WHITE (1) Packages: When the radiation level originating from the package at any time during normal transport does not exceed 0.5 rnrem/h at any location on the external surface of the package, and the package does not belong to Fissile Class II or III. (2) Containers: When the container contains packages of radioactive substances none of which is in a category higher than Category I-WHITE. 2. Category II-YELLOW (1) Packages: When the radiation level limit in marginal 3653(1) is exceeded, or the package belongs to Fissile Class II, provided that: 22Ti 3650 3651 3652 3653 3654 2278 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) (a) the radiation level originating from the package at any time during normal transport does not exceed 50 mrem/h at any location on the external surface of the package; and (b) the transport index at any time during normal transport does not exceed 1.0. (2) Containers: When the trasnport index of the container at any time during normal transport does not exceed'.'1.0, and when it contains no packages of Fissile Class III. • 3. Category III-YELLOW (1) Packages: When either of the two limits in marginal 3654(1) is exceeded, or when the package belongs to Fissile Class II or Class III, or when the package is being tranported under special arrangement, provided that: (a) the radiation level originating from the package at any iime during normal transport does not exceed 200 mrem/h at any location on the external surface of the package, except that, for full load shipments under the conditions specified in marginal 3659(7), the maximum allowable level shall be 1000 mrem/h; and (b) the transport index at any during nomarl transport does not exceed 10 unless the package is being transported as full load. (c) Containers: when the transport index of the container, at any time during normal transport, exceeds 1.0, or when the container carries packages belonging to Fissile Class III, or when it is being trasnported under special arrangement. D. LABELLING AND MARKING (see Appendix A.9) (1) Each package and container (both large and small) shall bear at least two labels which comform to the models 6A, 6B or 6C in Appendix A. 9 according to the category (see maginals 3652 to 3655) of that package or container. (2) The labels shall be affixed to two opposite sides of the outside of the package, or on the outside of all for sides of the container. (3) The labels shall be completed as follows in a clear and indelible manner: (a) next to the word «contents» shall be indicated the radionuclidY. or the substance whose presence constitutes the principai danger in the event of damage to the package (for example: strontium -90, irradiated uranium, radioac­ tive LSA); (b) next to the word «activity» shall be written the activity in curies; Note. This activity may also be expressed in micro, milli or kilocuries on condition th~t the prefixed micro, milli and kilo are written in full; (c) on the label to model Nos. 6B and 6C shall be written, in addition, the transport index in the largest possible figures in the frame intended for that purpose. (4) Each package of gross weight exceeding 50 kg shall have its gross weight plainly and durably marked on the outside of the package. (5) Each package which conforms to a Type A packaging design shall be plainly and durably marked on the outside of the package with «Type A». (6) Each package which conforms to a design approved under marginals 36 72 to 36 7 4 shall be plainly and durably marked on the outside of the package with the identification mark allocated to that design by the competent authority and, in the case of a Type B(U) or Type B(M) package design, with «Type B(U)» or «Type B(M)». (7) Each package which conforms to a Type B(U) or . Type B(M) package design shall have the outside of the outermost receptacle which is resistant to the effects of fire and water plainly -marked by embossing, stamping or other means resistant to the effects of fire and water with the trefoil symbol shown in the labels to models 6A to 6C. 3656 E. SEGREGATION OF RADIOACTIVE SUBSTANCES Packages of Category II-YELLOW or III-YELLOW shall be separated in carriage and in storage from packages which bear a label with the word «FOTO» by the safety distances given in the table in marginal 240 001 of Appendix B.4. F. STORAGE IN TRANSIT (1) Packages of radioactiv~ .substances shall not be stored near dangerous goods with which mixed loading is prohibited (see marginal 2700(3)). (2) The number of Category II-YELLOW and Category III-YELLOW packages and containers stored in any one storage area, such as a transit area, terminal building, store - romm or assembly yard, shall be so limited that the., total sum of the transport indices in any individual group of such packages or containers does not exceed 50. Groups of such packages and containers shall be stored so as to maintain a spacing of at least 6 metres from other groups of such packages or containers. (3) Where control of package accumulations is effected by reference to the red bands marked on the labels there shall not be more than 50 Category II-YELLOW or 5 Category III-YELLOW packages in any one group of packages. Where packages of both categories are present, one Category III-YELLOW package shall be taken as equivalent to ten Category II-YELLOW packages. ( 4) Except in the case of Fissile Class II or Class III packages, the limitations in marginal 3658(2) do not apply to packages marked «RADIOACTIVE LSA» and containing low specific activity substance or those marked «RADIOACTIVE LLS» and containing low level solid radioactive substance when they are maintained in a compact stack or in containers. (5) Mixing of different kinds of packages, including Fissile Class I packages with Fissile Class II packages, is permitted. G.TRANSPORT l. Packages (1) Packages shall be so l~aded in vehicles that they cannot shift dangerously, upset or fall. (2) Provided that its average surface heat flux does not exceed 15w/m2, and that the surrounding cargo is not in sacks or bags, a package may be carried among packaged general cargo without any special stowage provisions except as may be specially repuired by the competent authority in an appropriate certificate. If the heat flux exceeds 15W /m2 the package shall be carried as full load. (3) Categories I-WHITE, II- or III-YELLOW packages shall not be carried in compartments occupied by passengers, except those exclusively reserved for couriers specially authorized to accompany such packages. (4) Mixing of different kinds of packages, including Fissile Class I packages with Fissile Class II packages, is permitted. (5) Accumulation of packages and containers shall be controlled as follows: • (a) For both packages and containers, the number of packages and containers shall be so limited that the total sum of the transport indices in any vehicle does not exceed 50. Where this control of packages is effected by reference to the red bands marked on the packages see marginal 3658 (3). (b) In the case of full loads the limits under paragraph (5)(a) shall not apply, provided that the radiation level under normal conditions of transport does not exceed 200 mrem/h. al any point on, and 10 mrem/h at 2m from the outside surface of a freight container or vehicle. For Fissile Class II or III consignments, or mixtures thereof, the full load shall not include more than the allowable 3657 3658 3659 E<l>HMEPII: THr KYBEPNHrEQI (TEYXOr nPQTO) 2279 number of packages (see footnote to marginal 2700). (6) Vehicles and large containers carrying packages or containers labelled with any of the labels to Models 6A, 6B or 6C, or carrying full load consignments of any radioactive substances shall display the placard in marginal 240 010 of Appendix B.4 on the outside of each of the two lateral sides and the rear wall in the case of a vehicle. (7) In the case of full ioads the radiation level shall not exceed: (a) 1000 mrem/h at any point on the external surface of any package, provided that: (i) the vehicle is equipped with an enclosure which, during normal transport, prevents the access of unauthorized persons to the interior of the enclosure: (ii) prnvisions are made to secure the packages so that their position within the vehicle remains fixed during normal transport; (iii) there are no loading or unloading operations between the beginning and end of the transport. Under other contitions, the radiation level at any point on the external surface of the package shall not exceed 200 mrem/h. (b) 200 mrem/h at any point on the outer surface of the vehicle or large container, including the upper and lower surfaces, and, in the case of an open vehicle at any point on the vertical planes projected from the outer edges of the vehicle, on the upper surface of the load, and on the lower external of the vehicle and (c) l0mrem/h at any point 2m from the vertical planes represented by the outer lateral surfaces of the vehicle or large container, and, if the load is transported in an open vehicle at any point 2m from the vertical planes projected from the outer edges of the vehicle. (8) (a) The radiation level in any normally occupied position of a vehicle shall not exceed 2 mrem/h during transport. Under such circumstances the carrier shall ensure that the driver or any accompanying personnel, shall not receive more radiation than 0.5 rem. in any 12 month period. Maintaining the minimum distances listed in the table in marginal 240 000 of Appendix B.4, even in the absence of a protective shield, shall be considered as keeping within the 2 mrem/h 'limit. (b) As an alternative to (a) above, the carrier may operate to a scheme of work approved by the competent authority whereby records must be kept by him of the times spent by persons travelling in his vehicles and the radiation levels those persons and subjected to, in order that no person receives a greater dose than 3 7 5 mrem in any calendar quarter. 2. Tank Vehicles Low - specific - activity substances, LSA (I), of marginal 2703, schedule 5, other than uranium hexafluoride and substances liable to spontaneous ignition, may be carried in tank - vehicles in accordance with the requirements of Appendix B.la. 3. Tank - Containers Low specific - activity substances, LSA (I), of marginal 2703, schedule 5, including natural or depleted uranium hexafluoride, may be carried in tank - containers in accordance with the requirements of Appendix B.lb. CHAPTER V. - ADMINISTRATIVE REQUIREMENTS Approval by competent authorities is not required for package designs for substances consigned under Schedules l to 4 and, provided the contents are not fissile substances requiring approval under marginal 3674, for pack 0 age designs for substances consigned under schedules 5 to 8. 3660 3661 3662 3669 3670 A. . APPROVAL OF SPECIAL FORM RADIOACTIVE SUBSTANCES (l) Any design for special form radioactive substances, with the exception of the substances specified in Schedules 3 and 4, shall require unilateral approval. An application for approcal shall include: (a) a detailed description of the substances or, if a capsule, the contets; particular reference shall be made to both physical and chemical states; (b) a detailed statement of the design of any capsule to be used, including complete engineering drawings and schedules of materials and methods of construction to be used; . (c) a statement of the tests which have been done and their results, or evidence based on calculative methods to show that the substances are capable of meeting the tests, or other • evidence that the special form radioactive substances meet the requirements of this Appendix. (2) The competent authority shall establish a certificate stating that the approved design meets the definition. of special form radioactive substances as defined in marginal 2700 (2) and shall attribute to that design an identification mark. The certificate shall specify the details, of the radioactive substances. B. APPROVAL OF PACKAGE DESIGNS 1. Approval of Type B(U) pack~ge designs (including those for Fissile Class I, Class II and Class III packages which are also subject to marginal 367 4). (l)Any design of Type B(U) package originating in a country party to ADR shall be approved by the competent authority of this country; if the country where the package has been designed is not party to ADR, carriage is possible on condition that: • (a) a certificate has been supplied by this country, proving that the package satisfies the technical regulations of ADR, and that this certificate is counter - signed by the competent authority of the first ADR country reached by the consignment; {b) if no certificate has been supplied, the package design is approved by the competent authority of the first ADR country reached by the consignment; (2) An application for approval shall include: (a) a detailed description of the proposed contents with particular reference to their physical and chemical states and the nature of the radiation emitted; (b) a detailed statement of the design, including complete engineering drawings and schedules of materials and methods of construction to be used; (c) a statement of the tes!s which have been done and their results, or evidence based on calculative methods or other evidence that the package design is adecuate to meet the requirements of marginals 3602 and 3603; ( d) the proposed operating and maintenance instructions for the use of the package, in particular, in the case of packages likely to be immersed in contaminated ponds, the provisions incorporated to ensure that the surface of the package is not contaminated above the permitted levels; (e) if the package is designed -to have a maximum normal operating pressure in excess of 1.0 Kg/cm2 (gauge), the application for approval shall, in particular, state, in respect of the materials of construction of the containment system, the specifications, the samples to be taken and the tests to be made; (f) where the proposed contents are irradiated fuel, the applicant shall state and justify any assumption in the safety analysis relating to the characteristics of the fuel; (g) any special. stowage provisions necessary to ensure the safe dissipation of heat from the package; consideration shall be given to the type of ·vehicle or 3671 3672 3672 2280 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) container (see marginal 3681 (1) (a) ); (h) a reproducible illustration not larger than 21 cm X 30 cm, showing the make-up of the package. (3) the competent authority shall establish a certificate stating that the approved design meets the requirements for Type B(U) packages (see marginals 3677 and 3678). 2. Approval of Type B(M) package design (including those for Fissile Class I, Class II and Class III packages which are aslo subject to marginal 3674) (1) Each type B(M) package design shall require multilateral approval '. (2) An application for approval of a Type B(M) package • design shall include, in addition to the information required in marginal 3672 (2) for Type B(U) packages: (a) a list of those specific additional· requirements for Type B(U) packages specified in marginal 3603 with the package does not conform; . (b) any proposed supplementary operational controls5 to compensate for the deficiencies listed in (a) above; and (c) a statement relative to any special loading, carriage, unloading, or handling procedures; (d) the maximum and minimum ambient conditions (temperature, solar radiation) expected to be encountered during transport and which have been taken into account in the design. (3) The competent authority shall establish a certificate stating that the approved package design meets the requirements for Type B(M) packages (see marginals 3677 to 3679). 3. Approval of Fissile Class I, Class II and Class III package design (!)Package designs complying with the examples in marginal 3620, 3623 or 3624 shall require no further coriipeient authority approvals. (2) Package.1-designs complying with the examples in marginals 3616 and 3622 shall require unilateral approval. (3) All other package designs shall require multilateral approval. (4) An appli'cation for approval shall include all information necessary to satisfy the competent authority that the design meets the requirements of marginals 3610 to 3624. (5) The competent authority shall establish a certificate (see marginals 3677 to 3679) stating that the approved package design meets the requirements of marginals 3610 to 3624. C. APPROVAL OF SHIPMENTS (1) Multilateral shipment approvals shall be required for the following packages: (a) Type B(M) packages specially designed to ·allow continuous venting. (b) Type B(M) packages containing radioactive materials with an activity greater than 3 X 103 A1 or 3 X 103 A 2 , as appropriate, or 3 X 104 Ci, whichever iw the lower; c) Fissile Class II packages with marginal 3620. d) Fissile Class III packages. However, a competent authority can authorize transport into or through its country, without shipment approval, by a specific provision in its design approval. • . 2) An application for shipment approval shall include: a) the period of time, related to the shipment, for which the approval is sought; b) the actual contents, the type of vehicle and the pro­ bable or proposed route; and 5 That is, operational controls during transport not routinely provided for in this Appendix but which are considered necessary to ensure the safety of the package ci!'.rin l transport, such as human intervetion for temperature or pressure measurements or for periodical venting. These controls shall also take into account the possibility of unexpected delay. 3673 3674 3675 c) how the special precautions and special administra­ tive and operational controls referred to in the· package design certificates issued under marginals 36 73 and '36 7 4, are to be put into effect. 3) Upon approval of the shipment, the competent autho­ rity shall issue a certificate (see marginals 3677 to 3679). 4) The package and shipment certificates may be com­ bined into a single certificate. D.- APPROVAL OF TRANSPORT BY SPECIAL AR­ RANGEMENT 1) A consignment of radioactive substances which does not satisfy all the applicable requirements of this Appendix shall be transported only by special arrangement, which always requires multilateral approval. The special arran­ gements shall be adequate to ensure that the overall level of safety in transport is at least equivalent to that whic~ would be provided if all the applicable requirements of this Appendix had been met. 2) An application for appro~al shall include the infor­ mation required under marginals 3672 lo 3675 and also: a) a statement of the respects in which, and of the reasons why, the consignment cannot be made in full accordance with the applicable requirements of this Ap­ pendix;· and b) a statement of any special precautions or special administrative or operational controls which shall be taken during transport to compensate for the failure to meet the applicable requirements of this Appendix. 3) Upon approval of the special arrangement, the com­ petent authority shall issue a certificate (see marginals 3677 lo 3679). , E. COMPETENT AUTHORITY CERTIFICATES OF AP­ PROVAL 1. Competent authority identification marks 1) Each approval certificate issued by a competent au­ thority shall be identified by an identification mark. The mark shall be of the following generalized type: Symbol of nationality of country6 Number/Type Code a) The number shall be assigned by the competent authority, and shall be unique and specific with regard to the particular design or shipment. The shipment approval identification mark shall be clearly identified with the p"ac­ kage design approval identification mark. b) The following type codes shall be used in the order listed to indicate the types of approval certificates issued: A Type A package design (when also a fissile class pac kage) B(U) Type B(U) package desing B(M) Type B(M) package design F Fissile class package design S Special form material approval T Shipment X Special arrangement 2) These type codes shall be applied as follows: a) Each certificate and each package shall bear the appropriate identification mark composed of the symbols prescribed in paragraph (1) except that for packages, only the applicable package design type codes shall appear following the second stroke, i.e. the •S•, •T• and .x. shall not appear in the indentification marking on the package. Where the package design approval and shipment appro­ val are combined, the applicable Type Codes do not need to be repeated. For example: 6 The signs referred to are the national distinguishing signs for motor vehicles in international traffic. 3676 3677 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOr nPQTO) 2281 A/132/B(M)F: A/132/B(M)FT: A/137 /X: A Type B(M) Fissile Class pac­ kage approved by Austria for pac­ kage design number 132 (to be . marked on both the package itself and on the package design appro val certificate). The shipment approval certificate identification mark issued for that package design (to be marked on the certificate only). The shipment approval certificate identification . mark issued for Austrian design 137 under a spe­ cial arrangements shipment (to be m!J.rked on .the certificate only). b) Where multilateral approv·al is effected by validation, only the identificati9rl marks issued by the country of origin of the design or shipment would be used. Where multilateral approval is effected by issue of certificates by successive countries, each certificate would bear the ap­ propriate mark and the package whose design was so approved would bear all appropriate identification marks. For example, (A/132/B(M)F) (CH/28/B(M)F) would be the identification marks of a package which was origi nally approved by Austria and was subsequently ap­ proved, by separate certificate, by Switzerl and. Additional • identification marks would be tabulated in a similar man­ ner on the package .. c) The revision of certificate numbers shall be indicated • by a parenthetical expression following the identification mark on the certificate. For example, A/132/B(U)F. , (Rev.2) would indicate revision 2 of the Austrian-approved • package design certificate; or A/132/B(U)F. (Rev.0) would indicate the original issue of the Austrian-approved package design certificate. For original issue the parenthe­ tical expression is optional and other words such as •( origi­ nal issue)• may also be used in lieu of «(Rev.0)». Certifi­ cate revision numbers may only be issued by the country issuing the original certificate number. Revision by other than the issuing country shall require a new certificate • and identification number. d) Additional symbols (as may be necessitated by natio­ nal requirements) may be added in brackets to the end of the identification niark. For example, A/132/B(U)F (SP503). e) It is not necessary to alter the identification mark' on the package each time . that a revision to the package certificate is made. Such alteration shall be 'made only in those cases where the revision of the package design certi­ ficate involves a change in the letter type codes for the package design, following the second stroke. 2. Information required in certificates Each -approval certificate issued by a competent autho­ rity shall include the relevant information from the follo­ wing: a) The competent authority identification mark. b) A brief description of the packagjng, including mate­ rials of construction, gross weight, general outside dimen­ sions, and appoarance. This shall include a reproducible illustration not larger than 21 cm by 30 cm, showing the inake-up of the package. c) A brief specification of the permitted contents, incl­ uding any restrictions on contents which might not be obvious from the nature of the packaging. This should include the physical and chemical forms, the activities in c~ries (including those of the various isotopes:· if approp­ riate), ammints in grams for fissile substances, and whe ther in special form. • • d) Additionally, for fissile class packages: . i) Fissile Class I: a detailed description of the permis­ sible contents and any special features, on the basis of which the leakage of water in respect of certain void spaces has been assumed in the criticality assesment (see margi nal 3613(b)). ii) Fissile Class II: a detailed description of the permis­ sible contents, the corresponding allowable numbers (or transport index) ang any special features, on the basis of which the leakage of water in respect of certain void spaces • has been assumed in the criticality assessment (see margi­ nal 3618(b)). iii) Fissile Class III: a detailed description of the individ­ ual consignments including the permissible contents and the corresponding allowable numbers (or transport indi­ ces) together with any special precautions to· be taken during transport. e) A statement regarding the ambient conditions ass­ umed for purposes of design (see marginal 3602 (4)). I) For Type B(M) packages, a statement specifying those prescriptions of marginal 3603 with which the pac­ kage does not conform and any amplifying information which may be useful to other competent authorities. g) A reference to the following information provided by the applicant: i) instructions on the use and maintenance of the packa ging; • • ii) the actions to be taken by the consignor prior to the shipment, e.g. any special decontamination procedures. h) A detailed listing of any supplementary operational • requirements (see footnote 5) for package preparation, lo~ding, transport, storage, unloading, and handling, incl­ uding any special stowage provisions for the safe dissipa­ tion of heat from the package, or a statement that no such controls are required. j) A statement authorizing shipment where shipment approval is required under marginal 3675. k) Any restrictions on the types of vehicle containers, and any necessary routing instructions. I) Emergency arrangements specific to the approved de sign. • m) The following statement: «This certificate does not relieve the consignor from compliance with any require­ ment of the government of any country through or into which the package will be transported•. n) An issue date, and, if appropriate, an expiry date. o) Signature and identification of the certifying official. p) Appendices containing certificates for alternative package contents, other competent authority validations, or additional technical data or information. 3. Validation of certificates Multilateral approvals may be by validation of the origi­ nal certificate issued by the competent authority of the country of origin of the design or shipment. F. CONSIGNOR'S RESPONSIBILITIES 1. Particulars of ~onsignment The consignor shall include in the transport document for each consignment or radioactive substances, as well as the description given in the appropriate schedule, the 3678 following details: • a) The statement «The nature of the .goods and the packaging are in conformity with ·the provisions of ADR». b) The identification mark for each competent authority certificate (special form, package design, and shipment) applicable lo the consignment). c) The name of the radioactive substances, or nuclide. d) A description of the physical and chemical form of the substance, or whether it is in special form. e) The activity of the radioactive substances in approp­ riate curie units. I) The category of the package, i.e. I-WHITE, ll­ YELLOW, III-YELLOW. g) The transport index (Categories II-and III-YELLOW only). h) For a consignment of fissile substances: i) if exempted under marginal 3610, the words «FIS­ ' SILE EXEMPT»; or ii) if nots? exempted'. the fissile class of the package(s). 2. Information and notification for carriers • 1) The consignor shall provide in the transport doc 3681 2282 E<I>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) ument a statement regarding actions, if any, that must be taken by the carrier. The statement shall be in the langua­ ges deemed necessary by the carrier or the authorities concerned, and shall include at least the following points: a) supplementary operational requirements for loading, transport, storage, unloading, handling, and stowage for safe dissipation of heat, or a statement that no suppleme­ ntary operational requirements are necessary (see margi­ nal 3678 (h); b) any necessary routing instructions (see marginal 3678 (k)). c) emergency arrangemen~s specific to the approved design (see marginal 3678 (i). 2) In all cases where approval of the shipment or prior notification to the competent authority is required, all the carriers shall be informed of the requirements in advance, in order that they may take in good time any measures required for the transport. 3. Notification to competent authorities 1) Before the first shipment of a Type B(U) package containing radioactive substances with an activity greater than 3 X 103Al or 3 X 103A2, as appropriate, or 3 X 104Ci, whichever is the lower, the consignor shall ens­ ure that -copies of each applicable competent authority certificate applying to that package design have been submitted to the competent authority of each country in whose territory the consignment is to be transported. The consignor is not required to await an acknowledgement from the competent authority, nor is the competent autho­ rity required to make such acknowledgement of receipt of the certificate. 2) For each shipment listed in a) to d) below inclusive, the consignor shall notify the competent authorities of each country in whose territory the consignment is to be tran­ sported. This notification shall be in the hands of each competent authority prior to the commencement of the shipment, and preferably at least 15 days in advance. a) Type B(U) packages ,containing radioactive substan­ ces with an activity greater than 3 X 103 A1 or 3 X 103 A2, as appropriate, or 3 X 104Ci, whichever is the lower. b) Type B(M) packages. c) Fissile Class III packages under marginal 3674 (3). d) Transport by special arrangement. 3) The consignment notification shall include: a) sufficient information to enable the identification of the package, including all applicable certificate numbers and identification marks; and b) information on the date of shipment, the expected date of arrival and proposed routing. (4) The consignor is not required to send a separate notification if the required information has been included in the application for shipment approval (see marginal 3675 (2)). 4. Possession of certificates The consignor shall have in his possession a copy of each certificate required under this Appendix and a copy of the iristructions with regard to the proper closing of the package and other preparation for shipment before making any shipment under the terms of the certificates. G. QUALITY CONTROL IN FABRICATION AND MAINTENANCE OF PACKAGING The manufacturer, consignor, or user of an approved package design shall be prepared to demonstrate to any cognizant competent authority that: (a) the constructional methods and materials used for the construction of the packaging are in accordance with the approved design requirements; the competent authority may carry out inspection of the packaging during construction; (b) all packagings built to an approved design shall be maintained in good condition so that they continue to 3682 3683 3684 comply with all relevant regulatory criteria, even after repeated use. CHAPTER VI - ACTIVITY LIMITS DETERMINATION OF A1 AND A2 1. Single radionuclides (1) For single radionuclides of known· identity, the values of A and A 2 are given in Table XX. The values of A 1 and 1 A 2 are also applicable for radionuclides contained in (a, n) or (1, n) neutron sources. TABLE XX. A 1 and A.z VALUES RADIONUCLiuES Symbol of Element and A1(C,) A2(C,) radionuclide atomic number 227 Ac Actinium (89) 1.000 0.003 228Ac 10 4 l05Ag Silver (47) 40 40 IIOA6m 7 7 I II Ag 100 JOO 24I Am Americium (95) 8 0.008 243Am 8 0.008 3 7 Ar ( compressed or uncompressed) Argon (18) 1.000 JOOO 41 Ar (uncompressed) 20 20 41Ar (compressed) I I 73.o1s Arsenic (33) 1.000 400 74A, 20 20 76A, JO 10 77A, 300 300 211A, Astatine (85) 200 7 l93Au Gold (79) 200 200 l96Au 30 30 l98Au 40 40 !99Au 200 200 131 80 Barium (56) • 40 40 !33Bo 40 JO 14080 20 20 7Bc Beryllium (4) 300 300 206s; Bismuth (83) 5 5 FOR Specific activity (C,/g) 7.2x10 2.2x!06 3.lxl04 4.7x103 l.6xl05 3.2 l.9x!0·1 1.ox105 4.3Xl07 4.3xl07 2.4xl04 I.OxJ05 l.6x!06 l.lx!06 2.lx!06 9.3xJ05 l.2xJ05 2.5xJ05 2.JXJ05 8.7xJ04 4.0x!02 7.3xJ04 3.Sx!05 .9.9x!04 207m . 10 10 2.l6xl02 2!0s~RaE) 100 4 l.2xl05 2129; 6 6 I.Sxl07 2498k .Berkelium (97) 1.000 I l.8xl03 829, Bromine (35) 6 6 l.lxI06 14c Carbon (6) 1.00() 100 4.6 4Sc. Calcium (20) 1.000 40 l.9x!04 47c. 20 20 5.9xl05 109cd Cadmium (48) 1.000 70 2.6x!03 1l5cdm 30 30 2.6xl04 115Cd 80 80 S.lxl05 139c,, Cerium (58) 100 100 6.5xl03 14lce 300 200 2.8xl04 143ce 60 60 6.6xl05 144ce 10 z 3.2xl03 249cr Californium (98) 2 0.002 3.1 250cr 7 0.007 l.3xl02 252cr 2 0.009 6.Sxl02 36c1 Chlorine (17) 300 30 3.2xl0·2 38c1 10 10 l.3xl08 242cm Curium (96) 200 0.2 3.3xl03 243cm 9 0.009 4.2xl0 244cm 10 0.01 8.2Xl0 245cm 6 0.006 1.ox10-1 246cm 6 0.006 3.6xJ0·1 56co Cobalt (27) 5 5 3.0xl04 57co 90 90 8.5xl03 58c0 m 1.000 1.000 5.9xl06 58c0 20 20 3.lxl04 60co 7 7 L!x!03 Sic, Chromium (24) 600 ~00 9.2xl04 3685 3689 3690 !I!EK 225 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOr nPQTO) 228:} 131c, Caesium (55) 1.000 1.000 1.0xJOS 65Ni 10 JO l.9xl07 134esm 1.000 1.000 7.4xl06 237Np Neptunium (93) 5 0.005 6.9xl0-4 134c, 10 10 l.2xl03 239Np 200 200 2:3xlQS 135c, 1.000 100 8.8XlQ•4 1850, Osmium (76) 20 20 7.3xl03 136es 7 7 7.4Xl04 1910, 600 400 4.6xl04 137c, 30 20 9.8Xl0 1910,m 200 200 l.2xl06 64Cu Copper (29) 80 80 3.8xl06 1930, 100 100 5.3x1os 165Dy Dysprosium (66) 100 100 8.2xl06 32P Phosphorus (15) 30 30 2.9xl05 l660r 1.000 200 2.3xJOS 230p, Protoactinium (91) 20 0.8 3.2xl04 l69E, Erbium (68) 1.000 300 8.2Xl04 231p, 2 0.002 4.5xl0·2 17I~, 50 50 2.4xl06 233p, 100 100 2.lxl04 l52Eum Europium (63) 30 30 2.2xl06 210pb Lead (82) 100 0.2 8.8xl0 l52Eu 20 20 l.9xl02 . 212pb 6 l.4xl06 154Eu 10 5 1.5xl02 J03pd Palladium (46) 1.000 700 7.5xl04 155Eu 400 90 l.4xl03 l09pd - 100 100 2.lxl06 l8F Fluorine (9) 20 20 9.3xl07 l47pm Promethium (61) 1.000 80 9.4xl02 52,e Iron (26) 6 6 7.3xl06 l49Pm 100 100 4.2xl05 55Fe 1.000 1.000 2.2xl03 210p 0 Polonium (84) 200 0.2 4.5xl03 59,e 10 10 4.9Xl04 l42p, Praseodymium 72c, Gallium (31) 7 7 3.lxJ06 (59) JO 10 l.2xl06 l53Gd Gadolinium (64) 200 100 3.6xl03 l43p, 300 200 6.6xl04 159Gd 300 300 l.lxl06 l91p, Platinum (78) 100 l00 2.3xl05 71c, Gerll!4nium (32) 1.000 1.000 • J.6Xl05 l93Pt 200 200 3H Hydrogen (I) see 197Ptm 300 300 l.2xl07 T-Tritium l97p, 300 300 8.8xl05 181m Hafnium (72) 30 30 l.6xl04 238p" Plutonium (94) 3 0.003 l.7xl0 197 Hg"' Mercury (80) 200 200 6.6x)OS 239Pu 2 0.002 6'.2x10-2 197Hg 200 200 2.5xl()S 240p. 2 0.002 2.3xl0-1 20311g 80 80 l.4xl04 241p. 1.000 0.1 l.lxl02 l66Ho Holmium (67) 30 30 6.9x1os 242p. 3 0.003 3.9xl0·3 12s, Iodine (53) 1.000 70 l.7xl04 223R, Radium (88) 50 0.2 5.0xl04 126, 40 JO 7.8xl04 224Ra 6 0.5 l.6xl05 129, 1.000 2 l.62xl0-4 226R, 10 0.05 1.0 131, 40 10 l.2xlOS 228Ra 10 0.05 2.3xl02 132, 7 7 l.lxJ07 8611t, Rubidium (3 7) 30 30 8.lxJ04 1331 30 30 l.lxl06 87Rb Unlimited Unlimited 6.6xl0-8 1341 8 8 2.7x]07 Rb (natural) Unlimited Unlimited 1.8xJO-B 135, 10 10 3.5xJ06 l86Re Rhenium (75) 100 100 l.9xl05 11310m Indium (49) 60 60 l.6xl07 l87Re Unlimited Unlimited 3.8xl0·8 11410m 30 20 2.3xl04 188Re JO JO 1.0xl06 11510m 100 . 100 6.lxl06 Re (natural) Unlimited Unlimited 2.4xl0·8 1901, Iridium (77) 10 10 6.2xl04 103Rhm Rhodium ( 45) 1.000 1.000 3.2xl07 1921, 20 20 9.lxl03 105Rh 200 200 8.2xl05 1941, JO 10 8.5Xl05 222Rn Radon (86) 10 2 l.5xl05 42K Potassium (19) 10 JO 6.0xl06 97Ru Ruthenium (44) 80 80 5.5xl0S 85K,m (uncompressed) Krypton (36) 100 100 8.4Xl06 103Ru 30 30 3.2xl04 85K,m (compressed) 3 3 8.4xl06 • l05Ru 20 20 6.6xl06 85K,m (uncompressed) 1.000 1.000 4.0x102 106Ru JO 7 3.4xl03 85K, (compressed) 5 5 4.0x102 355 Sulphur (16) 1.000 300 4.3xl04 87 Kr (uncompressed) • 20 20 2.8xl07 122sb Antimony (51) 30 30 3.9xJ05 87 Kr (compressed) 0.6 0.6 2.8xl07 124sb 5 5 l.8xl04 1401.a Lanthanum (5 7) 30 30 5.6Xl05 l25sb 40 30 l.4Xl03 LLS Low-level solid 46s, Skandium (21) 8 8 3.4xl04 radioactive 47s, 200 200 8.2xl05 material See 48s, 5 5 I.5xl06 Marginal 2450 (2) 755e Selenium (34) 40 40 l.4xl04 LSA Low specific 31s; Silicon (14) 100 JOO 3.~xl07 activity material 147sm Samarium (62) Unlimited Unlimited 2.0xJ0·8 See Marginal l51sm 1.000 90 2.6XJ0 2450 (2) 153Sm 300 300 4.4xl05 I 77Lu Lutetium (71) 300 300 l.lxlOS 113sn Tin (50) 60 60 1.0xl04 MFP Mixed fission l2550 10 JO l.lxJOS products 10 0.4 855,m Strontium (38) 80 80 3.2xl07 28Mg Magnesium (12) 6 6 5.2XI06 855, 30 30 2.4xl04 52Mn Manganese (25) 5 5 4.4Xl05 875,m 50 50 l.2xl07 54Mn 20 20 • 8.3xl03 895, 100 40 2.9xJ04 56Mn 5 5 2.2x101 905, 10 0.4 l.5xJ02 99Mo Molybdenum (42) 100 100 4.7x1os 915, 10 JO 3.6xl06 22Na Sodium (II) 8 8 6.3xl03 925, 10 10 I.3xJ07 24N, 5 5 8.7xl06 T (uncompressed) Tritium (I) 1.000 1.000 9.7xl03 . 93Nbm Niobium (41) 1.000 200 I.Ixl03 T (compressed) 1.000 1.000 95Nb 20 20 3.9xl04 T (activated luminous 97Nb 20 20 2.6Xl07 paint) I 1.000 1.000 l47Nd Neodymium (60) 100 100 8.0xI04 T (absorbed on solid 149Nd 30 30 l.lxl07 carrier) 1.000 1.000 59Ni Nickel (28) 1.000 900 8.lxl0·2 • J' r (tritiated water) 1.000, 1.000 63Ni 1.000 100 4.6xlO T (other forms) 20 20 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 182Ta 160Tb 9~cm 9~c 97Tcm 97Tc 99Tcm 99Tc 125Tem 127Tem 127Te \29Tem 129Te 13\Tem 132Te 227Th 223n 230,,, 23\Th 232111 234-rh Th ( natural) Th (irradiated) 200TI 20\TI 202TI 204-ri 170Tm 17]Tm 2300 2320 233u 2340 235 0 2360 2380 u (natural) u (enriched) <20% or greater u ·(depleted) u (irradiated) 48v 181w 185w 187w 20% 131 x.m (compressed) I 31 x,m ( uncompressed) 133x, (uncompressed) l 33x, (compressed) l 35x, (uncompressed) l 35x, (compressed) 90y 9lym 9ly 92y 93y 175n, 65z,, 69z,,m 69z,, 93z, 95z, 97z, Tantalum (73) Terbium (65) Technetium (43) Tellurium (52) Thorium (90) Thallium (81) Thulium (69) Uranium (92) Vanadium (23) Tungsten (7 4) Xenon (54) Yttrium (39) Ytterbium (70) Zinc (30) Zirconium (40) 20 20 1.000 6 1.000 1.000 100 1.000 1.000 300 300 30 100 10 7 200 6 3 1.000 Unlimited 10 Unlimited a. 20 200 40 300 300 1.000 100 30 100 100 100 200 Unlimited Unlimited Unlimited 100 Unlimited b 6 200 1.000 40 10 100 1.000 5 70 2 10 30 30 10 10 400 30 40 300 1.000 20 20 20 6.2x103 20 l.lxl04 1.000 3.8xl07 6 3.2x!05 200 l.5Xl04 400 l.4xJ0-3 100 5.2x106 80 l.7xJ0-2 100 l.8xl04 40 4.0X\04 300 2.6xl06 30 2.5xl04 100 2.0x\07 10 8.0xl05 7 3.lx\05 0.2 3.2xl04 0.008 8.3xl02 0.003 l.9xJ0-2 1.000 5.3xl05 Unlimited l.lxl0-7 10 2.3xl04 Unlimited! (see Table ' I XXI) a 20 5.8xl05 200 2.2xlo5 40 5.4xl04 30 4.3xl02 40 6.0xl03 100 l.lxl03 0.1 2.7xl04 0.03 2.lxlO 0.1 9.5xlo·3 0.1 6.2xl0·3 0.2 2.lxl0-6 0.2 6.3xl0·5 Unlimited 3.3x!0·7 Unlimite<j .(see Table • XXI) Unlimite1 (see Table ',; µ1) 0.1 Unlimite, ~see Table Ii" ~'XXI(~ 6 l.7xl05 100 5.0xl03 100 9.7xl0·3 40 7.0x\05 10 l.Oxl05 100 l.Oxl05 1.000 l.9xl05 5 l.9xl05 70 2.5xl06 2 2.5xl06 10 5.3xl05 30 4.lx107 30 2.5xl04 10 9.5x!06 10 3.2xl06 400 l.8xl05 30 8.0x\03 40 3.3x!06 300 5.3x!07 200 3.5xl0·3 20 2.lxlO~ 20 2.0x\06 a. The values for A and A2 shall be calculated in. accordance "'.ith marginal 3691 (3) taking into account the act1V1ty of the fission products and uranium-233 in addition to that of thorium. b. The values for A and A2 shall be calculated i n accordance "'.ith marginal 3691 (3) taking into account the act1V1ty of the fission products and plutonium isotopes in addition to that of the uranium. TABLE XXI. ACTIVITY-MASS RELATIONSHIPS FOR URANIUM AND NATURAL THORIUM• (This table is referred to in Table XX). Radioactive material . Ci/g g/Ci Uranium (wt% 2350 present) 5.0x10·7 2.ox106 - 0.45 0. 72 (natural) 7.06xl0·7 l.42xl06 1.0 7.6xl0·7 l.3x106 • 1.5 l.Oxl0-6 l.Oxl06 5.0 2.7xl0-6 3.7xl05 10.0 4.8xl0·6 2.lxl05 20.0 1.ox10·5 1.ox105 35.0 2.ox10·5 5.0xl04 50.0 2.5x10·5 4.0xl04 90.0 5.8x10·5 l.7xl04 93.0 7.oxio-5 l.4Xl04 95.0 9.lxl0·5 l.lx104 Natural thorium 2.2x10·7 4.6xl06 (2)For any single radionuclide whose identity is known 1 but which is not' Iis~ed in Tabl~ XX, the val,,,ues of A 1 ana A2 shall be determined according to the procedure given below: (a) If the radionuclide emits only one type of radiation, A shall be determined according to the rules in (i), (ii), (ifi) and (iv). below. For radionuclides emitting different kinds of radiation, A 1 shall be the most restrictive value of those determinetl for each individual radiation. However, in both cases A 1 shall be restricted to a maximum of 1000 Ci. If a parent nuclide decays into a shorter lived daughter, of a half-life not greater than 10 days, A1 shall be calculated for both the parent and the daughter, and the more limiting of the two values should be assigned to the parent nuchile. (1) For gamma emitters, A 1 is determined by the expression: 9 -A = - cunes l f where r is the gamma-ray constant, corresponding to the dose in R/h at 1 m per Ci; the number 9 results from the choice of 1 rem/h at a distance of 3 m as the reference dose equivalent rate. (ii) For X-ray emitters, A 1 is determined by the atomic number of the nuclide: for Z ,,;;; 55; A 1 = 1.000 Ci for Z > 55; A = 200 Ci (iii) For beta emitters, A.1 is determined by the maximum beta energy (Em.J according to Table XXII. (iv) For alpha emitters A 1 is determined .by the expression: Al = 1.000 A3 • where A3 is the value listed in Table XXIII. · (b) A2 shall be the more restrictive of the following two values: (1) the corresponding A1 and (2) the value A 3 obtained from Table XXIII. TABLE XXII RELATIONSHIP BETWEEN ~-AND E FOR BETA • EMITTEtc; mu E ma,(MeV) Ai(Ci) <0.5 1.000 0.5 - < 1.0 300 1.0- < 1.5 100 1.5 - < 2.0 30 • > 2.0 10 a. The figures for uranium include the activity of ura­ nium -234 which is concentrated during the enrichment process. The activity for thorium includes the equilibrium concentration of thorium -228. ECJ>HMEPII THI KYBEPN~IEQI (TEYXOI nPQTO) TABLE XXIII RELATIONSHIP BETWEEN Aa.. AND THE ATOMIC NUMBER OF THE RADIONUCLIDE A3 1/\tomic numbe Half-life less l-Ialf-life 1000 days Half-life greater han 1000 days to 106 years than 106 years 1 to 81 3 Ci 50 mCi 3 Ci 82 and above 2 mCi 2 mCi 3 Ci (3) For any single radionuclide whose identity is unknown, the value of. A 1 shall be taken lo be 2 Ci and the value of A 2 shall be taken to be 0.002 Ci. However, if the atomic number of the radionuclide is known to be less than 82, the value of A 1 shall be taken to be 10 Ci and the value of A 2 shall be taken to be 0.4 Ci. 2. Mixtures of radionuclides, including radioactive decay chains (1) For mixed fission products the following activity limits may be assumed, if a detailed analysis of the mixture is not carried out: Al= 10 Ci A 2 = 0.4 Ci (2) A single radioactive decay chain in which the radionuclides are present in their naturally occurring proportions and in which no daughter nuclide has a half­ life either longer than 10 days or longer than that of the parent nuclide shall be considered as a single radionuclide. The activity to be taken into account and the A 1 or A 2 value to be applied shall be those corresponding to the parent nuclide of that chain. However, in the case of radioactive decay chains in which any daughter nuclide has· a half-life either longer than 10 days or greater than that of the parent nuclide, the parent and such daughter nuclides shall be considered as mixtures of different nuclides. (3) In the case of a mixture of different radionuclides, where the identity and activity of each radionuclide are known, the permissible activity of each radionuclide R 1 , R 2 .. : Rn shall be such that F 1 + F 2 + ... F n is not greater than unity, where F = Total activity of R1 l Ai(Rl) F = Total activity of J\ 2 Ai(R2) F = Total activity of R n A,(Rn) Ai (Rt), Ai (R2), ... ~ (Rn), is the value of A1 or A2 as appropriate for the nuclide R1, R1 ... Rn. ( 4) When the identity of each radionuclide is known but the individual activities of some of the radionuclides are not known, the formula given in paragraph (3) shall be applied to establish the values of A1 or A2 as appropriate. All the radionuclides whose individual activities are not known (their total activity will, however, be known) shall be classed in a single group and the most restrictive value of A1 and ~ applicable to any one of them shall be used as the value of A1 or A2 in the denominator of the fraction. (5) Where the identity of each radionuclide is known but the individual activity of none of the radionuclides is known, the most restrictive value of A1 or ~ applicable to any one of the radionuclides present shall be adopted as the applicable value. (6) When the identity of none or only some of the nuclides is known, the value of A 1 shall be taken to be 2 Ci and the value of A 2 shall be taken to be 0.002 Ci. However, if alpha emitters are known to be absent, the value of A2 shall be taken to be 0.4 Ci. CHAPTER VII. DECONTAMINATION, LE.t\.KING PACKAGES AND ACCIDENTS (1) If a package containing radioactive substances is broken or is visibly leaking or is involved in an accident during carriage, the vehicle or affected area shall be isolated so • as to prevent all contact of persons with radioactive substances and, when possible, shall be duly marked off or surrounded by barriers. No-one shall be authorised to stay within the isolated area until qualified persons arrive to supervise the handling and salvage work. The sender and authorities concerned shall be notified immediately. Notwithstanding these provisions, the presence of radioactive substances shall not be considered as a bar to operations for the rescue of people or fire­ fighting. (2) If radioactive substances have leaked, have been spilled or have been scattered in ·any way whatever in a 3691 place, area or on to goods or equipment used in storage, qualified persons shall be called in as soon as possible to direct decontamination operations. The place, area or equipment thus contaminated shall only be put ba~k into service when its use has been declared free from danger by qualified persons. (3) Except as provided for in paragraph ( 4) any vehicles, equipment or part thereof, which have been contaminated in the course of carriage of radioactive substances shall be decontaminated as soon as possible by a qualified person and shall not be reused unless the • non-fixed radioactive contamination is below the levels specified in Table XIX and the vehicles, equipment or part thereof have been declared safe in respect of residual radiation levels by a qualified person. ( 4) Vehicles or compartments used for the bulk transport or tank transport of low specific activity substances, or for the transport of packages of low specific activity substances carried as a full load or for the transport of low level solid radioactive substances as a full load shall not be used for other goods until decontaminated as specified in paragraph (3). APPENDIX A. 7 Reserved APPENDIX A.8 Reserved APPENDIX A. 9 Provisions relating to danger labels (1) Labels Nos. 1, 2A, 2B, 2C, 2D, 3, 4, 4A, 5, 6A, 6B and 6C shall be in the form of a square of 10 cm side standing on a corner. They have a black line 5 mm in the edge and running parallel to it. Labels to be affixed to fixed tanks (tank-vehicles and tankatrailers) shall be of not less than 30 cm side. (2) Labels Nos. 7, 8 and 9 shall be rectangular, of standard format AS (148 X 210 mm). For packages, these dimensions may be redu.::ed to a format not less than A7 (74 X 105 mm). (3) An inscription, in figures or letters, concerning the nature of the danger may be placed on the lower part of the labels. (1) Danger labels, where they are required under the provisions of this Annex, must be stuck on packages and 3692 3694 3695 3696 3699 3700 3799 3800 3899 3900 3901 2286 E<l>HMEPII: THI: KYBEPNHI:EOI: (TEYXOI: nPOTO) fixed tanks or affixed in some other suitable manner. Only where the state of the outside of a package does not permit : this should labels be stuck on cards or tablets securely • attached to the package. On outer packagings and fixed tanks, indelible danger markings corresponding exactly to the prescribed models may be used instead of labels. (2) Where a package is required to bear two labels of the same model, the labels shall be affixed in the manner indicated hereafter: (3) It is the sender's duty to affix the labels to p~ckages, and, where appropriate, to fixed tanks and containers. 2. Explanation of symbols The danger labels prescribed for substances and articles of Classes 1 to 8 (see annexed plate) have the following meanings: No. 1 (black bomb on orange liable to explosion; ground): · prescribed in marginals 211 7 ( 1) and (2), 2145 and 2563; No. 2A (black flame on red ground): danger of fire (inflammable prescribed in marginals 2224 (3), liquids); 2316 (3), 2478 (2), 2307 (1) and 2632 (l); No. 2B (black flame on ground of danger of fire (inflammable solids); equidistant alternate red and white vertical stripes): prescribed in marginal 2414 (l); No. 2C (black flame on white substance liable lo spontaneous ground, lower triangle oflabel red): ignition; prescribed in marginal 2443 ( 1 ); No. 2D (black flame on . blue danger of emission of inflammable ground): gases on contact with water; prescribed in marginal 2478 (l); No. 3 (flame over a circle, black on oxidizing substance or organic yellow ground): peroxide; prescribed in marginals 2511 (1) and 2563 (l); No. 4 (death's head on cross-bones, black on white ground): prescribed in marginals 2307 (1), 2316 (3), 2632 (1) and 2643 (3); toxic substance: to be kept apart in vehicles and al loading, unloading or transloading· points from foodstuffs and other articles for consumption; 3902 No. 4A (St. Andrew's Cross on ear harmful substance: to be kept apart of corn, black on white from foodstuffs in vehicles and at background): loading, unloading or transloading prescribed in marginals 2632 (1) and 2643 (3); No. 5 (liquid dripping from a test­ tube on to a plate and from another test-tube on to a hand; black on white ground, lower triangle oflabel black with a white border): prescribed in marginals 2511 (1), 2824 (1) and 2835 (3); points; corrosive substance; No. 6A (stylized trefoil, inscription • radioactive substance in packages of RADIOACTIVE, a vertical stripe in Category I - WHITE; in the event the lower half, with following text: of damage to the packages, danger Contents .. . to health by ingestion or inhalation Activity ... of, or contact with, spilled Symbol and inscriptions black on contents; white ground, vertical stripe red): prescribed in schedules 5 to 12 as appropriate and in marginal 3656 (1), (2) and (3); No. 6B (like the foregoing, but with two vertical stripes in the lower half and ihe following text: Contents .. . Activity .. . Transport index. Symbol and inscriptions black; upper half of ground yellow; lower half of ground white; vertical stripes red): prescribed in schedules 5 to 12 as appropriate and in marginal 3656 (1), (2) and (3); No. 6C (like the foregoing, but with three vertical stripes in the low~r half): . prescribed in schedules 5 to 12 as appropriate and in marginal 3656 • ( 1 ), (2) and (3); No. 7 (open black umbrella on white ground): prescribed in marginal 24 78 (l ); No. 8 (two black arrows on white ground): prescribed in marginals 2117 (2), 2224 (2), 2307 (3), 2414 (2), 2443 (2) and (3), 2478 (3), 2511 (2), 2563 (2), 2632 (2), 2664, 2709 (3), 2824 (2) and (3); No. 9 (red wineglass on white ground): prescribed in marginals 2117 (2), 2182, 2224 (1), (2) and (3), 2307 (3), 2414 (2), 2443 (3), 2478 (3), 2511 (2), 2562 (2), 2632 (2), 2664, 2709 (3) and 2824 (2); • radioactive substance in packages of Category II - YELLOW; packages to be kept away from packages containing undeveloped radiographic or photographic plates or films; in the event of damage to packages, ,danger to health by ingestion or inhalation of, or contact with, spilled contents, and risk of external irradiation at a distance; radioactive substance in packages of Category III - YELLOW; packages to be kept away from packages containing undeveloped radiographic or photographic plates or films; in the event of damage to packages, danger to health by ingestion or inhalation of, or contact with, spilled contents, and risk of external irradiation at a distance; keep dry this side up: label to . be affixed, with arrows pointing upwards, on two opposite sides of the package; handle with care, or: !do not drop, 3903 3999 E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPQTO) ""1C "' ·. , . . . ,· .... ' ' ' ' Afi, ,i'-~, , - ' NOSA ~ , ., , ' , ' l < > .. ·, V N07 APP£ •,DICE A 9 DANGER LABELS •SN- -.,q,"•· .;9021 Fln,,oOucl•r>ft ,.,,, '-0.K.eO It.Ill' N"'lA " ,,, ' , ' , ' , , ,,, . ,,, // i' < • >· V ~ IIOJ "' , ... ,,, ' . ,,, ' <. . . . .. ~~~ . :· .. • .. ~· ..;.~ "--~ ~ ~ 228i 2288 Ect>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) ECONOMIC COMMISSION FOR EUROPE ·• INLAND TRANSPORT COMMITTEE European Agreement concerning the international carriage of dangerous goods by road (ADR) and protocol of signature done at Geneva on 30 September 195 7 VOLUME III (Annex B) UNITED NA TI ONS NATIONS UNIES 1978 United Nations publications may be obtained from bookstores and distributors throughout the world. Consult your bookstore or write to: United Nations, Sales Section, New York or Geneva. FOREWORD The text below comprises, in addition to the Agreement itself and the Protocol of signature, the annexes in the form in which they entered into force on 29 July 1968 as well as the amendments thereto up to 1 October 1978. EUROPEAN AGREEMENT CONCERNING THE INTERNATIONAL CARRIAGE OF DANGEROUS GOODS BY ROAD (ADR) ANNEX B PROVISIONS CONCERNING TRANSPORT EQUIPMENT AND TRANSPORT OPERATIONS CONTENTS Marginals PLAN OF THE ANNEX 10 000 APPLICABILITY OF OTHER REGULATIONS, NATIONAL OR INTERNATIONAL 10 001 APPLICABILITY OF THE PROVISIONS OF CHAPTER I OF THIS ANNEX 10 002 CHAPTER I GENERAL PROVISIONS APPLICABLE TO THE CARRIAGE OF DANGEROUS SUBSTANCES OF ALL CLASSES Section I Section 2 Section 3 General Scope of this Annex Definitions Types of vehicles Full load Carriage in bulk Carriage in containers Carriage in tanks Tanks Crews of vehicles; Supervision Carriage of Passengers Transport documents Ai)proval of vehicles 10 OOOet seq. 10 100 10 102 10 104 10 108 10 111 10 118 10 121 10 127 10 171 10 172 10 181 10 182 Instructions in writing 10 185 Special requirements to the fulfilled by ve hicles and their equipment 10 200et seq. Fire-fighting appliances 10 240 Electrical equipment 10 251 Miscellaneous equipment 10 260 General service provisons 10 300et seq. Fire-fighting appliances 10 340 Portable lighting apparatus 10 353 Prohibition of smoking 10 ·374 Section 4 Special provisions concerning loading, unloading and handling 10 400et seq. Limitation of the quantities carried 10 401 Prohibition of mixed loading on one vehicle 10 403 Prohibition of mixed loading in one contai ner 10 404 Prohibition of mixed loading with goods contained in a container Cleaning before loading Handling and stowage Cleaning after unloading Loading and unloading of substances in containers Running the engine during loading or unloading 10 405 10 4i3 10 414 10 415 10 419 10 431 Section 5 Special provisions concerning the opera­ tion of vehicles 10 500et seq. 10 500 Vehicle signs • Parking in general 10 503 Parking at night or when visibility is poor Parking of a vehicle constituting a special danger. 10 505 10 507 10 599 Other provisions Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries 10 600et. seq. Rapid procedure for authorizing deroga­ tions for the purpose of trials 10602 CHAPTER II Classes la, lb and le Class Id Class le Class II Class Hla Class Illb Class Ille Class [Va Class IVb Class V Class VI Class VII APPENDICES SPECIAL PROVISIONS APPLICABLE TO THE CARRIAGE OF DANGE­ ROUS SUBSTANCES OF CLASSES I TO VII· Explosive substances and articles; Articles filled with explosive substances; lgniters, fireworks and si­ milar goods Gases: compressed, Liq­ uefied or dissolved under pressure Substances which give off inflammable gases on co­ ntact with water Substances liable to spo­ ntaneous combustion Inflammable liquids Inflammable solids Oxidizing substances Toxic substances Radioactive substances Corrosive substances Repugnant substances and substances liable to cause infection Organic peroxide Provisions common to the B.l Appendices Appendix B.la Appendix B.lb Appendix B.lc Provisions concerning fi­ xed tanks (tank - vehic­ les), demountable tanks and batteries of receptacles Provisions concerning tank - containers Provisions concerning fi­ xed tanks and demou­ ntable tanks in reinforced plastics Marginals 11000 et sec. 14000 ,. 15000 • 21000 • 31000 • 32000 • 33000 • 41000 • 42000 • 51000 • 61000 ,. 71000 • 200000-211099 211100-212099 212100-213099 213100-213999 E<l>HMEPII: THI: KYBEPNHI:EOI: (TEYXOI: nPOTO) 2289 Appendix B.ld Requirements concerning the materials and constru­ ction of fixed tanks, of demountable tanks, and of shells of tank-containers, Appendix B.2 Appendix B.3 • intended for the carriage of deeply - refrigerated liquefied gases of Class 2 Electrical equipment ·certificate of approval for vehicles carrying certain. dargerous ioods 214000-219999 220000-229999 230000-239999 Appendix B.4 Tables concerning the carriage of dangerous substances of Class 7; La­ bel to be placed on vehic­ les carrying these substan­ ces 240000-249999 Appendix B.5 List of substances mentio- ned under marginal 10 500 (2) 250000-250999 ANNEX B PR QVISIONS CONCERNING TRANSPORT EQUIP­ MENT AND TRANSPORT OPERATIONS Plan of the Annex This Annex comprises: (a) general provisions applicable to the carriage of dan gerous substances of all Classes (Chapter I); . (b) special provisions applicable to the carriage of dan­ gerous ·substances of Classes 1 to 8 (Chapter II); (c) Appendices as follows: . Appendix B.la concerning fixed tanks (tank - vehicles), demountable tanks and batteries of receptacles; Appendix B. lb concernfog tank-containers; Appendix B. lc concerning fixed tanks and demountable tanks in reinforced plastics; " Appendix B.ld relating to requirements concerning the materials and construction of fixed tanks, of demountable tanks, and of shells of tank - containers, intended for the carriage of deeply- refrigerated liquefied gases of Class 2; • Appendix B.2 concerning electrical equipment; Appendix B.3 containing a model certificate of approval for vehicles; Appendix B.4 containing tables concerning the carriage of substances of Class 7 and a model label to be affixed to vehicles carrying these substances; Appendix B.5 containing the list of substances mentio­ ned under marginal 10 500 (2) (2) The general provisions of Chapter I and the special provisions of Chapter II are divided into sections with the following headings: Section 1. General (this section contains, inter alia, the provisions concerning authorizations for the carriage of goods in bulk, in containers or in tanks); Section 2. Special requirements to be fulfilled by vehic­ les and their equipment; Section 3. General service provisions; 4000 9999 10 000 10000 Section 4. Special provisions concerning loading, unloa- (contd.) ding and haudling (this section contains the provisions concerning methods of despatch, restrictions on forwar ding and prohibitions on mixed loading); Section 5. Special provisions concerning the operations of vehicles; Section 6. Transitional provisions, derogations, and • provisions peculiar to certain countries. Applicability of other regulations, national or internatio- 10001 nal (1) If the vehicle carrying out a transport operation subject to the pr<:ivisions of ADR is conveyed over a section of the journey otherwise than by road haulage, then any national or. international regulations which govern the car riage of dangerous goods on that section by the mode of transport used for conveying the road vehicle shall alone be applicable to that section of the journey. (2) In cases where a transport operation subject to the provisions of ADR is likewise subject over the whole or a part of the road journey to the provisions of an. internatio­ nal convention which regulates the carriage of dangerous goods by a mode of transport other than road carriage by virtue of clauses extending the applicability of that conve­ ntion to certain motor - vehic: l~ services, then the provi­ sions of that international convention. shall apply, over the journey in question, concurrently with those of ADR which are not incompatible therewith; the other clauses of ADR shall not apply over the journey in question. Applicability of the provisions of Chapter 1 of this Annex 10002 Where provisions of Chapter II or of the Appendices to this Annex conflict with provisions of Chapter I, those provisions of Chapter I shall not apply. Nevertheless (a) the provisions of marginal 10 100 shall take prece­ dence over those of Chapter II; (b) the provisions of marginal 10 403 shall take prece­ dence over the prohibitions on mixed loading prescribed in the Sections 4 of Chapter II. Chapter I GENERAL PROVISIONS APPLICABLE TO THE CAR­ RIAGE OF DANGEROUS SUBSTANCES OF ALL CLASSES '.(see, however, marginal 10002) S!)ction 1 . General 10 003 1-0 099 Scope of. thi; Annex , ~~ ,. . 1 o l 00 (1) Annex A exempts from the provisions of the present Annex carriage performed under the conditions (of packa­ ging, weight, etc.) laid down in marginals 2201a, 2301a, 2401a, 2431a, 2471a, 2501a and 2801a. (2) (a) Limited quantities of dangerous substances in packages may be carried without application of the. provi­ sions of this Annex relating: to the types of vehicles (marginals « ... 104» of Chapt~rs , I and II, and marginals 11 105 and 11 106 of Chapter II concerning Classes 1 a, 1 b and le); ~ to the crews of vehicles and to supervision (Marginals « ... 1 7 l» of Chapters I and II); to the carriage of passengers (Marginal 10 1 72); to instructions in writing (Marginals 10 181 (1) (b), 10 185 and 61 185); to the special certificate of approval for vehicles (margi­ nals 10 182 and 11 182); to the special requirements to be fulfilled by vehicles and their equipment (all Sections 2 of Chapters I and II), subject, however, to compliance with the provisions of marginal 21 212; to places of loading and unloading (marginals 11 407, 21 407 and 61 407); and to the operation of vehicles (all Sectipns 5 of Chapters I and II), subject, however, to compliance with the provi sions of marginal 61 515. • Section 1 10 100 (b) The exemptions under (a) above shall apply to the (contd.) loading on one transport unit of: 1. One or more of the following dangerous substances, whatever the weight on condition that there are no other dangerous substances of ADR in the transport unit Class la Class le Class 3 Class 4.1 Class 4.2 empty packagings of 15 ° safety matches of 1 ° (a); empty receptacles of 6 °; substances of 9° and 10°; empty packagings of 14 ° and 15 °; Ea>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Class 4.3 Class 5.1 Class 5.2 Class 6.1 Class 6.2 Class 8 empty receptacles ·of 5 °; empty packagings of 11 °; empty packagings of 99°; empty packagings of 91 ° and 92 °; articles of 12°; and sodium sulphide of 36 ° and empty receptacles of 51 °; 2. One only of the dange~ous substances listed below, on condition that the gross weight of all the packages containing the dangerous substance does not exceed the weight shown and that there are no other dangerous substances of ADR in the transport unit Class lb Class le Class 2 Class 3 Class 4.1 Class 4.3 Class 5.2 Class 5.2 (contd.) Class 6.1 Class 8 articles of 2 ° (b) or 4 °: 100 kg; slow - combustion fuses of 3 ° : 100 kg; cyanogen chloride of 3° (et): 5 kg; phosgene (carbonyl chloride) of 3 ° (at): 25 kg; fluorine of 1 ° (at): 50 kg; diethyl ether, carbon disulphide of 1 ° (a) or mixtures of 1 ° (b) such as collodions and semi - collodions contai­ ning diethyl ether: 3 kg; acetaldehyde, acetone "or acetone mixtures of 5°: 75 kg sulphur of 2 ° (a), napthalene of 11 ° (b): 250 kg; calcium carbide of 2 ° (a), calcium silicide of 2 ° (d) or manganese calcium silicide of 2° (d): 1,000 kg; substances of 45 °, 46 ° (a), 4 7 ° (a) and (b) packed in conformity with the provisions of marginal 2559: 2 kg*; (not including the weight of the refrige­ rating system, if any) Section 1 substances of l O to 22 °, 30 ° and 31 ° packed in conformity with the pro­ visions of marginal 2561: 5kg; and substances of 1 ° to 22 °, 30 °, 31 ° and 40 ° packed in conformity with the provisions of marginals 2553 to 2556 and 2558: 10 kg; substances of 41°, 61 ° and 62°, 71 ° to 75°, ~3° and 84°: 100 kg; substances of 6 ° (a), 7 °, ·9°, 11 °, 12°, 14°, 15°, 22° 23° 34° and 35°: 10 kg; 3. One or more dangerous substances listed below of the same Class, on condition that the total gross weight of all the packages containing each dangerous substance does not exceed the weight indicated: Class la Class lb Class le Class 2 Class 3 Class 4.1 Class 4.2 any. dangerous substance of the Class other than those listed in l above: 5 kg; any article of the Class other than those listed in 2 above: 10 kg; any dangerous substance of the Class other than those listed in 1 and Z • above: 15 kg; any dangerous substance of the Class other than those listed in 2 above: 300 kg; any substance of the Class other than those listed in 1 and 2 above: 250 kg; any substance of the Class other than those listed in 1 and 2 above: 50 kg; substances of the Class other than those of 1 °, 2 °, 3 ° and 4 ° and the 10 100 (contd) • • ·Not including the weight of the refrigerating system, if any. Class 4.3 Class 6.1 Class 6.2 Class 8 empty packagings listed in 1 above: 250 kg; any substance of the Class other than those listed in l and 2 above: 10 kg; any substance of the Class other than those listed in 1 and 2 above: 5 kg; any substance of the Class other than those listed in 1 above: 300 kg; and any substance of the Class other than those listed in 1 and 2 above: 250 kg; Section 1 (3) For the purposes of paragraph (2) above, the weights of liquids or gases carried in the ordinary fixed tanks of vehicles for propelling tlie vehicles or operating their spe­ cial - purpose equipment (e.g. refrigerating equipment) and for ensuring their safety shall not be taken into ac­ count. ( 4) The only provisions of Chapter I of this Annex which are applicable to the carriage of dangerous substances of Class 6.2 shall be those of Chapter II which relate to this Class and those of the marginals of this Chapter I which are expressly rendered applicable by the aforesaid provi­ sions of Chapter II. (5) Derogatins from the provisions of this Annex may be made in the case of emergency transport to save human life. 10100 Definitions 10101 10102 (1) For the purposes of this Annex: the term «competent authority» means the authority designated as such in each country and in each specific case by the Government; the term •fragile package» means a package containing a fragile receptacle (i.e. a receptacle made of glass, porce­ lain, stoneware or similar materials) which is not enclosed in a packaging with complete sides protecting it effectively against shock (see also Aneex I>.., marginal 2001(5)]; the term •gas• means a gas or vapour; the term «dangerous substances•, when used alone, means the substances and articles designated as being substances and articles of ADR; • the term «RID• means the International Regulations concerning the Carriage of Dangerous Goods by Rail [An­ nex ~ to the International Convention concerning the Car­ riage of Goods by Rail (CIM)]; the term •carriage in bulk» means the carriage of a solid substance without packaging; tlie term «carriage in bulk» means the carriage of a solid substance without packaging; the term «container• means an article of transport equipment (lift van, demountable tank or other similar structure) of a permanent character and accordingly strong enough to be suitable for repeated use; specially designed to facilitate the carriage of goods, by one or more means of transport, without breakage of load; fitted with devices permitting its ready handling, par­ ticular when being transloaded from one means of tran­ sport to another; so designed as to be easy to fill and empty, and having an internal volume of not less than one cubic metre· the term •container» does not cover conventional 'pac­ kagings, or vehicles, or tank containers; . the term «large container» means a container having an l!lternal volume of more than 3 cubic metres; • the term •small container• means a container having an internal volume of not less than 1 cubic metre and not more than 3 cubic metres; cl>EK 225 EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO~ 2291 the term •tank-co~tainer» mearis an article of transport equipment conforming to the definition of the term «contai­ ner• given above and built to contain liquid, gaseous, powdery or granular substances but having a capacity of more than 0.45 cubic metres; the term •battery of receptacles» means an assembly comprising a number of receptacles (called «elements») whose individual or average capacity is over 150 litres and which are interconnected by a manifold and permane­ ntly mounted on a frame [for frames of gas cylinders, see Annex A, marginal 2212(d)]; • the term «demountable tank• means a tank, other than a fixed tank, a tank- container or a battery of receptacles, which has a capacity of over J .000 litres, is not designed for the carriage of goods without breakage of load, and normally cannot be handled except when it is empty; the term •fixed tank• means a tank which is structurally attached to a vehicle (which then becomes a tank-vehicle) or is an integral part of the frame of such vehicle; the term •tank-, when used alone, means a tank­ container or a tank of a capacity exceeding 1 m3 which may be a fixed tank, a demountable tank or a battery or receptacles. (See, however, a limitation of the meaning of the word •lank» in the provisions common to the B. l Appendices, marginal 200.000(2)); the term «transport unit• means a motor vehicle wi­ thout an attached trailer, or a combination consisting of a motor vehicle and an attached trailer; the term «closed vehicle» means a vehicle having a body capable of being closed; the term «open vehicle» means a vehicle the platform of which has no superstructure or is merely provided with side boards and a tailboard; the term •sheeted vehicle• means an open yehicle provided with a sheet to protect the load; the term •tank-vehicle» means a vehicle built to carry liquids, gases, or powdery or granular substances and comprising one or more fixed tanks; • the term «battery-vehicle» means a ~ank-vehicle com­ prising a number of fixed tanks (called •elements») inter­ connected by a manifold. (2) For the purposes of this Annex, tanks [see definition ( 1) above] are not placed on the same footing as receptac­ les, the term «receptacle» being used in a restrictive sense. Provisions concerning receptacles apply to fixed tanks, batteries of receptacles, demountable tanks and tank -co­ ntainers only if this is expressly stipulated. (3) The term «full load» means any load originating from one sender, for which the use of a vehicle or a large container is exclusively reserved and all operations for loading and unloading which are carried out in conformity with the instructions of the sender or consignee [see margi­ nal 10 108). (4) Unless expressly stated otherwise, the sign «%» or the expression «per cent• in this Annex represents: (a) in the case of mixtures of solids or of l iquids, and also in the case of solutions and of solids wetted by a liquid: a percentage by weight based on the total weight of the mixture, the solution or the wetted solid; (b) in the case of gaseous mixtures: a percentage by volume based on the total volume of the gaseous mixture. (5) All weights mentioned for packages in this Annex are, unless otherwise specified, gross weights. The weight of ccmtainers or tanks used for the carriage of goods is not included in the gross weight. (6) Pressures of all kinds relating to receptacles (such as test pressure, internal pressure, safety-value opening pressure) are always indicated in kg/cm2 gauge pressure (pressure in excess of atmospheric pressure); however, the vapour pressure of substances is always expressed in kg/cm2 absolute pressure. (7) Where this Annex specifies a degree of filling· for receptacles or tanks, that degree of filling is always refer­ red to a temperature of thw substances of 15 ° C unless some other temperature is indicated. 10103 10104 Types of vehicles (1) A transport unit loaded with dangerous substances may in no case include more than one trailer or semi-traler. (2) Special provisions concerning the types of vehicles to be used for the carriage of certain dangerous substances will, where appropriate, be found in Chapter II of this Annex (see also the marginals dealing with carriage in containers, the carriage of solid substances in bulk, car­ ·riage in tanks, and tanks). (3) Packages comprising packagings made of materials sensitive to moisture shall be loaded on to closed or on to sheeted vehicles. Full Load Where the provisions relating to carriage as a «full load» are applied, the competent authorities may require the vehicle or large container used for such carriage to b~ loaded at only one point and unloaded at only one point. Carriage in bulk (1) Solid dangerous substances may not be carried in bulk unless this mode of carriage is expressly authorized for the said substances by the provisions of Chapter II of this Annex, and then only under the conditions stipulated by those provisions. Nevertheless, empty packagings, uncleaned, may be carried in bulk if this mode of carriage is not explicitly prohibited by the requirements of Annex A, Part II. (2) For carriage in bulk in containers, see marginal 10118 (2) and (5). Carriage in containers Note: The provisions concerning carriage in tank­ containers will be found in the marginals headed «Carriage in tanks». (1) The carriage of packages in containers is authorized. (2) Substances may not be carried.in bulk in containers unless their carriage in bulk is expressly authorized (see marginal 1011 1 ); small containers must be of. the closed type and have complete walls. (3) Large containers must meet the requirements con­ cerning the body of the vehicle· which are laid down in this Annex for the load in question; the body of the vehicle need not then satisfy those provisions. (4) Subject to the provisions of the last phrase in (3) above, the fact that dangerous substances are enclosed in one or more containers shall not affect the conditions required to be met by the vehicle by reason of the nature and quantities of the dangerous substances carried. (5) If the ,fangerous substances carried in a container are such that, under Annex A, one or more danger labels are req1•ired to be affixed to the packages containing them, the sam.c label or labels shall be affixed to the outside of the container containing those substances in packages or in t. ilk. However, label No. 8 need not be affixed if the container comprises a device or inscription clearly showing which way up it should be kept. Carriage in tanks (1) Dangerous substances may be carried in tanks only if this mode of carriage is expressly authorized for those substances by the provis10n of Chapter II of this Annex; carriage must then comply with the provision of this Annex. Reinforced-plastics tanks may be used only if their use is expressly authorized in Chapter II. The temperature of the substance carried shall not exceed 50°C at the time of tilling. See marginal 10500 for the marking and label 1 ing of.vehicles. (2) If the substances carried in a demountable tank, a battery of receptacles or a tank-container are such that, under Annex A, one or more danger labels are required to be affixed to the packae:es containing them, the same 10103 10104 . ... 10105 10107 10108 10109 10110 10111 10112 10117 10118 10119 10120 10121 2292 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) label or labels shall be affixed to the outside of the demou­ ntabe tank, battery of receptacles or tank-container. Ho­ wever, label No. 8 need not be affixed if the tank comprises a device or inscription clearly showing which way up it should be kept. Tanks (1) The provisions concerning the design, inspection, filling and use of fixed tanks, demountable tanks and batteries of receptacles, and various provisions concerning tank-vehicles and their use, will be found in Appendix B.la and, so far as the design of fixed tanks, demountable tanks and batteries of receptacles intended for the carriage of refrigerated liquefied gases of Class 2 is concerned, in Appendix B. Id (for the approval of tank-vehicles, see marginal 10182). (2) The provisions concerning the construction, items of equipment, type approval, tests, marking, etc, of tank­ containers are to be found in Appendix B.lb and, so far as the construction of tank-containers intended for the carriage of deeply-refrigerated liquefied gases of Class 2 is concerned, in Appendix B.ld. {3) The provisions concerning the construction of fixed tanks and demountable tanks in reinforced plastics are to be found in Appendix B. le. ( 4) The provisions common to the B. l Appendices are to be found in marginal 200000. (5) For receptacles, see Annex A. Crews of vehicles: Supervision (1) Where the provisions of this Annex concerning spe­ cific goods require the driver to be accompanied by an assistant, the assistant must be able to take over from the driver. Section 1 {2) The requirements of this marginal relating to super­ vision during the time when a vehicle is parked shall apply only to dangerous substances carried in quantities in ex­ cess of the exemption limits. Transport units carrying dangerous goods for which the exemption limit is less than 1,000 kg shall be supervised at all times in arder to prevent any malicious act and to alert the driver and the competent authorities in the event of loss or fire. Transport units carrying dangerous goods for which the exemption limit is 1,000 kg or more shall either be super­ vised or alternatively may be parked, unsupervised in an isolated position in the open in a secure depot or secure factory. premises. If such facilities are not available, the transport unit, after having been properly secured, may be parked in an i~olated position meeting the requirements of paragraphs (i), (ii) or (iii) below. The parking facilities permitted in paragraph (ii) shall be . used only if those described in paragraph (i) are not available, and those described in paragraph (iii) may be used only if facilities described in paragraphs (i) and (ii) are not available. (i) A vehicle park supervised by an attendant who has been notified of the nature of the load and the whereabouts of the driver. (ii) A public or private vehicle park where the transport unit is not likely to suffer damage from other vehides, or {iii) A suitable open separated from the public highway and human habitation, where the public do not normally pass or assemble. Carriage of passengers No passengers not .members of the vehicle's crew may be carried in transport units conveying dangerous substan­ ces. Transport documents ( 1) In addition to the documents required under other 10122 10126 10127 101:28 10170 10171 10171 10172 10173 10180 10181 • regulations, the following documents shall be carried oii the transport unit: • (a) the transport documents prescribed in Annex A, marginal 2002(3) and (4), covering all the dangerous goods carried; and (b) instructions, as prescribed in marginal 10185, rela­ ting to all the dangerous substances carried. (2) Where the provisions of this Annex require the following documents to be drawn up, the said documents shall likewise be carried on the transport unit: (a) the special certificate of approval referred to in marginal 10182, for each vehicle: and {b) the permit authorizing the transport operation. Approval of vehicles (1) Tank-vehicles and, where so required undei;. the provisions of Chapter II of this Annex, other vehicles shall be subject to technical inspection in their country of regis­ tration to make sure that they conform to. the provisions of this Annex, including those of its Appendices, and the general safety regulations {concerning brakes, lighting etc.) in force in their country of origin; if these vehicles are. trailers or semi-trailers coupled behind a drawing vehicle, the drawing vehicle shall be subject to technical inspection for the same purposes. (2) A special certificate of approval shall be issued by the competent authority of the country of registration for each vehicle whose inspection yields satisfactory results. It shall be drawn up in the language or one of the languages of the country issuing it, and also, if that language is not English, or French, or German, in English, French or German, unless agreements concluded between the coun­ tries concerned in the transport operation provide other­ wise. It shall conform to the model shown in Appendix B.3. (3) A special certificate of approval issued by the com­ petent authorities of one Contracting Party for a vehicle registered in the territory of that Contracting Party shall be accepted, so long as its validity continues, by the com­ petent authorities of the other Contracting Parties. ( 4) The validity of special approval certificates shall expire not later than one year after the date of the technical inspection of the vehicle preceding the issue of the certifi­ cate. However, in the case of tanks subject to compulsory periodic inspection this provision shall not have the result of requiring tightness (leakproofness) tests, hydraulic pressure tests or internal inspections of tanks to be carried out at intervals shorter than those laid down in Appendix B.la and B.lc. lnstrunctions in writing (1) As a precaution against any accident or emergency that may occur or arise during carriage, the driver shall be given instructions in writing specifying concisely: (a) the nature of the danger inherent in the dangerous substances being carried, and the safety measures that need to be taken to avert it; {b) the action to be taken and treatment to be given in the event of persons coming into contact with the goods being carried or with any substances which might escape therefrom; (c) the measures to be taken in case of fire and, in particular, the fire-fighting equipment or. equipment not to be used; (d) the measures to be taken in case of breakage or deterioration of packagings or of the dangerous substances being carried, particularly where such dangerous substan­ ces have spilled over the road. (2) These instructions shall be prepared for each dange­ rous substance or Class of dangerous substances by the manufacturer or the sender, in a language of the country of origin; where that language is not the same as those of the countries of transit or destination, the instructions shall also he drawn up in the language of those countries. A set of these instructions shall be kept in the driver's cab. (3) These instructions shall be supplied to the carrier at the latest when the transport order is given, so as to 10182 10183 10184 10185 E<l>HMEPII THI KYBEPNHIEQI {TEYXOI nPQTO) 229:J enable him to take all necessary steps lo ensure that the employees concerned are aware of these instructions and are capable of carrying them out efficiently. Section 2 Special requirements to be fulfilled by· vehicles and their equipment Rear protection for vehicles carrying fixed tanks, demou­ ntable tanks or batteries of receptacles A bumper sufficiently resistant lo rear impacts shall be fitted over the full width of the tank at the rear of the vehicle. There shall be a clearance of at least 1 00 mm between the rear wall of the tank and the rear of the bumper, this clearance being measured from the rearmost point of the tank w~ or from projectirig fittings or accesso­ ries in contact with the substance being carried. Fire-fighting appliances (1) Every transport unit carrying dangerous substances shall be equipped with (a) at least one portable fire extinguisher of adequate total capacity, suitable for fighting a fire in the engine or in any other part of the transport unit, and such that, if it is used to fight a fire in the load, it does not aggravate the fire and, if possible, controls it; however, if the vehicle is equipped with a fixed fire extinguisher, automatic or easily brought into action, for fighting a fire in the engine, the portable extinguisher need not be suitable for fighting a fire in the engine; (b) in addition lo the equipment prescribed under (a) above, at least one portable fire extinguisher of adequate total capacity, suitable for fighting a fire in the load, and such that, if it is used to fight a fire in the engine or in any other part of the transport unit, it does not aggravate the fire and, if possible, controls it; (2) The fire-extinguishing agents contained in the fire extinguisher with which a transport unit is equipped shall be such that they are not liable to release toxic gases into the driver's cab or under the influence of the heat of the fire. • (3) Where a transport unit comprises a trailer and the laden trailer is uncoupled and left on the public highway, at a distance from the drawing vehicle, the trailer shall be equipped with at least one fire extinguisher conforming to the provisions of sub-paragraph ( 1) (b) of this marginal. Section 2 Electrical equipment The provisions concerning the electrical equipment of vehicles carrying various dangerous substances will be found in Appendix 8.2. Miscellaneous equipment (1) Every transport unit carrying dangerous goods shall be equipped with: (a) a tool kit for emergency repairs to the vehicle; (b) for each vehicle, at least one scotch of a size suited to the weight of the vehicle and to the diameter of the wheels; (c) two amber lights. These lights shall be independent of the electrical equipment of the vehicle and be so desig­ ned that their use cannot cause the goods being carried to ignite; they shall be steady or flashing. (2) The provisions of sub-paragraph ( 1) ( c) of this margi­ nal shall not apply in the territory of the United Kingdom. Section 3 General service provisions Fire-fighting appliances 10186 10199 10200 10215 10216 10217 10239 10240 10241 10250 10251 10252 10259 10260 10261 10299 10300 10339 10340 The crew o( the vehicle must know how to use the fire-fighting appliances. Portable lighting apparatus A vehicle may not be entered by persons carrying ligh­ ting apparatus comprising a flame. In addition, the lighting apparatus used shall not exhibit any metal surface liable to produce sparks. Prohibition of smoking Smoking shall be prohibited during handling operations, in the vicinity of packages awaiting handling, near halted . vehicles, and inside the vehicles. Section 4 Special provisions concerning loading, unloading and handling • Limitation of the quantities carried The fact that dangerous substances are enclosed in one or more containers shall not affect the weiglit limitations laid down by this Annex regarding carriage in a single vehicle or in a single transport unit. Prohibition of mixed loading on one vehicle Unless the contrary is explicitly prescribed by the pro­ visions of the Sections 4 of Chapter II of this Annex, the prohibitions of mixed loading on one vehicle shall not apply to • consignments of goods packed together. in the manner permitt ed by the provisions on mixed packing contained in Annex A. Compliance with the prohibitions on mixed loading shall be based on the danger labels of Appendix A.9, which shall be affixed to packages in accordance with the require­ ments laid down for th e various Classes in Annex A. Prohibition of mixed loading in one container The prohibitions of mixed loading on one vehicle shall also be observed within each container. Prohibition of mixed loading with goo.ds contained in a container For the purpose of the application of the prohibitions of mixed loading on one vehicle, no account shall be taken of substances contained in closed containers with complete sides. Cleaning l:iefore loading All the provisions in this Annex which relate to the cleaning of vehicles before loading shall also apply to the cleaning of containers. Handling and stowage. ( 1) The various components of a load comprising dange­ rous substances shall be suitably stowed on the vehicle and wedged by appropriate means lo prevent them from being displaced in any way in relation to eaph other and to the walls of the vehicle. (2) If the load comprises goods of different categories the packages of dangerous substances shall be separated from the other packages. (3) All the provisions in this Annex which relate to the loading and unloading of vehicles and to the stowage and handling of substances shall also apply to the loading,· stowage and unloading of containers on to and from vehi­ cles. (4) Nothing whatsoever may be loaded on top of a fragile package. • (5) A driver or a driver's assistant may not open a package containing dangerous substances. Cleaning after unloading . (1) If, when a vehicle which hl!s been loaded with packed 10341 10352 10353 10354 10373 10374 10375 10399 10 400 l0 401 10 402 10 403 10 404 10 405 10 406 10 412 10 413 10 414 10 415 E<DHMEPII: THI: KYBEPNHI:EQI:·(TEVXOr nPQTO) dangerous substances is· unloaded, some of the contents are found to have escaped from the packagings, the vehicle shall be cleaned as soon as possible and in any case before reloading. (2) Vehicles which have been loaded with dangerous substances in bulk shall be suitably cleaned before re­ loading unless the new load consists of the same dangerous substance as did the preceding load. (3) All the provisions of this Annex which relate to the cleaning or decontamination of vehicles shall also apply to the cleaning or decontamination of containers. ½oading and unloading of dangerous substances in con­ tainers. 10 416 10 418 10 419 The provisions of this Annex which relate to the loading and unloading of vehicles and the stowage and handling of dangerous substances shall also apply to the loading and unloading of dangerous substances in containers. Running the engine during loading or unloading Exi ept where the engine has to be used to drive the pumps or other appliances for loading or unloading the vehicle and the laws of the country in which the vehicle is operating permit such use, the engine shall be shut off during loading and unloading operations. 10420 10 430 10 431 Section 5 10 432 10 499 Special provisions concerning the operation of vehicle Vehicle signs (1) Transport units carrying dangerous substances spe­ cified in the ... 500 marginals shall display two rectangular reflectorized orange-coloured plates of 40 cm base and not less than 30 cm high, set in a vertical plane. The plates shall have a black border not more than 15 mm wide. They shall be affixed one at the front and the other at the rear of the transport unit, both perpendicular to the longitudinal axis of the transport unit. They shall be clearly visible.· Note. The colour of the orange plates in conditions of normal use should have chromaticity co-ordinates lying within the area on the chromaticity diagram formed by joining the following co-ordinates: Chromaticity co-ordinates of points at thP, corners of the area on the chromaticity diagram. X 0.52 0.52 0.578 0.618 y 0.38 0.40 0.422 0.38 Luminance factor. of reflectorized colour: B.> 0.12. Reference centre E, Standard Illuminant C, normal incidence 45° and viewed at 0°. Co-efficient of reflex luminous intensity at an angle of illumination of 5°, viewed at 0.2°: not less than 20 candelas per lux per m2 • (2) Transport units fixed tanks carrying only one of the substances listed in Appendix B.5 shall display orange­ coloured plates as prescribed above, on which the indenti­ fication numbers shown in that Appendix shall apear. (3) However, where two different substances are carried in an transport unit consisting of a tank-vehicle drawing • a tank-trailer, the vehicle and the trailer shall each display at both front and rear an orange-coloured plate bearing the respective identification numbers of the substances being carried. ( 4) Where a number of different substances are carried on a tank-vehicle in separate tanks or tank-compartments, orange-coloured plates identically similar to those pre­ scribed in paragraph ( 1 ), set parallel to the longitudinal axis of the vehicle and bearing the appropriate identifica 10 500 tion numbers, shall be so displayed on the sides of each tank or tank-compartment as to be clearly visible. In this case the plates prescribed in paragraph (1) above shall display no number. • (5) The identification numbers shall be made up of black digits 100 mm high and of 15 mm stroke thickness. The hazard~identification number shall be inscribed in the upper part of the plate and the substance-identification number in the lower part; they shall be separated by a horizontal black line, -15 mm in stroke width, extending from side to side of the plate at mid height (see Appendix B.5). The identification numbers shall be indelible and shall remain legible after 15 minutes' engulfment in fire. (6) The foregoing requirements are also applicable to empty tanks, uncleaned and not degassed. After the dan­ gerous substances have been unloaded and the tanks been cleaned and degassed, the orange-coloured plates shall no longer be visible. (7) Tank-vehicles shall also bear on both sides and at the rear the labels prescribed in Section 5 of each Class. Parking in general ,,-f No transport unit carrying dangerous subastances may be parked without the parking brake's being applied. Parking at night or when visibility is poor ( 1) If a vehicle is parked at night, or when visibility is poor, and its lights are not working, the amber lights referred to in marginal 10 260 (l)(c) shall be placed on the road, one about 10 m ahead of the vehicle, and the other about 10 m to the rear of the vehicle. (2) The provisions of this marginal shall not apply in the territory of the United Kingdom. Parking of a vehicle constituting a special danger Without prejudice to the measures prescribed in margi­ nal 10 505 above, if the nature of the dangerous substan­ ces carried in the parked vehicle constitutes a source of special danger to road-users (e.g. in the event of substan­ ces dangerous to pedestrians, animals or vehicles spilling over the road) and the crew of the vehicle is unable to eliminate the danger quickly, the driver shall alert the nearest competent authorities, or cause them to be alerted, immediately. He shall also, where necessary, take the measures prescribed in the instructions provided for in marginal 10 185. • Other provisions As to provisions not included in this Chapter or in Chapter II of this Annex which concern the operation of vehicles carrying dangerous goods, the relevant measures adopted in this· sphere by each Contracting Party on the basis of its domestic legislation and relating to domestic carriage shall be appliable to international carriage using its territory. Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries Rapid procedure for authorizing derogations for the purpose of trials For the purpose of carrying out the trials necessary with a view to amending the provisions of this Annex in order to adapt them to technological and industrial deve­ lopments, the competent authorities of the Contracting Parties may agree directly among themselves to authorize certain transport operations in their territories by tempo-· rary derogation from the provisions of this Annex. The authority which has taken the initiative with respect to the temporary derogation ·so granted shall notify the .competent· service of the United Nations Secretariat of the derogation, 10 501 10 502 10 503 10 504 10505 10 506 10 507 10 508 10 598 10 599 10600 10 601 10602 ECJ>HMEPII: TH:[ KYBEPNHI:EQI: (TEYXOI: nPQTO} which service shall bring it to the attention of the Contract­ ing Parties. Chapter II SPECIAL PROVISIONS APPLICABLE TO THE CARRIAGE OF DANGEROUS SUBSTANCES OF CLASSES 1 to 8 Classes la Explosive substances and articles 1 b Articles filled with explosive substances le Limiters, fireworks and similar goods Section 1 General 10 603 10999 11 000 11 103 Types of vehicles 11104 (See also marginals 11 105 and 11 106) Dangerous substances of Classes la, lb and le may be carried only in closed vehicles or in sheeted vehicles fitted with side boards and a tailboard. The sheet of a sheeted vehicle must be of impermeable material not roa­ dily inflammable. It must be tautened so as to cover the vehicle on all sides, with an overlap of not less than 20 cm down the sides of the vehicle, and be kept in position by lockable metal bars of chains. Categories of vehicles 11105 For the purposes of this Annex, transport units authori zed to carry dangerous substances of Classe1> la, lb and 1 c are classified as follows: (1) «A» transport units: Transport units whose engines use a liquid fuel with a flash-point below 55° C. (2) •B• transport units: Transport units whose engines use a liquid fuel with a flash-point of 55° C or more; this category B comprises the following sub-categories: Classes la, lb and le (a) «B.l.» transport units: These have either no trailer or a trailer meeting the following conditions: its coupling device is quickly detachable and is robust: and it is fitted with an effective braking device acting on all the wheels, actuated by the drawing vehicle's service-brake control, and automatically stopping the trailer in the event of breakage of the coupling .. (b) •B.lf. transport units: These have the following characteristics in addition to those of sub-category B.I.: 1. Engine and exhaust system The engine and the exhaust system are placed forward of the front wall of the body. The exhaust~pipe outlet is directed outwards from the vehicle. 2. Fuel tank The fuel tank is placed well away from the engine, the electric wiring and the exhaust-gas piping, and in such a· manner that in the event of leakage from the tank the fuel drains directly on to the ground and cannot reach the load of explosives. The fuel tank is well away from the storage battery, or is at least separated from it by a leak-proof partition. It is so placed as to be so far as possible protected in a collision. The engine is not gravity-fed. 3. Driver's cab No inflammable material has been used in the constru­ ction of the driver's cab, except in the seating equipment. Classes la, 1 b and le (c) «B.III» transport units These have all the characteristics of sub-category 8.11 and, in addition, their body exhibits the following features: 1. It is closed and has a continuous surface; it is separa­ ted from the driver's cab by a space of not less than 15 cm; it is robustly constructed in such a manner and of such materials that it adequately protects the goods car­ ried; the materials used for the lining are incapable of producing sparks; the insulating and heat-resisting proper­ ties of the body are at all points at least equivalent to those of a partition consisting· of a layer of asbestos board 5 mm thick between two metal walls or to those of a partition consisting of an outer metal wall lined with a layer of fire-proofed wood 10 mm thick. 2. The door or doors are provided with a lock and key; all joints and closures are of overlapping type. The door or doors must be so constructed as to reduce the strength of the body as little as possible. • Restrictions on the use of vehicles of certain categories 11106 (1) «A» transport units may carry only articles of Class lb, 2° (b), 4° (a), (b) and (e), and of Class le, 1 ° (a) and 30 No special limitation of weight is pre~crib~d for ·such carriage. (2) •B.I.» transport units may carry (a) without special weight limitations, articles of Class lb, 2° (b) and 4°, and of Class le, 1 ° (a) and 3°;. ·. ,. (b) subject to the weight limitations prescribed in margi­ nal 11 401, the dangerous substances referred to in that marginal. (3) The provisions relating to restrictions, in the light of the weight and nature of the load, on the use of «B.11» and «B.III» transport units will be found in marginal 11 401. Carriage in containers Small containers shall satisfy the requirements prescri­ bed in respect of the body of the vehicle for the transport operation concerned; it will then not be necessary for the body of. the vehicle to satisfy those requirements. Crews of vehicles: Supervision (1) A driver's assistant shall be carried on every tran­ sport unit. If the .national regulations so provide, the com­ petent authority of a cotjtracting country may require an· approved.official to.he carried in the vehicle at the carrier's expense. . (2) The provisions of marginal 10 1 71 (2) shall apply only to ~he dangerous goods listed below in quantities exceeding those specified below: Class ia: Sudstances and articles of 1 ° - 14 °: 5 Kg; Class lb: Articles of 1 ° (b), (c) and (d), 5° - 7° and 9? - 11 °: 50 Kg; and Class le: Articles of 21 ° - 23 °: 50 Kg. Approval of vehicles The requirements of marginal 10 182 shall be appli­ cable to «B.III» transport units. 11107 11117 11118 11119 11170 11171 11172 11181 11182 11183 11199 2W6 E<t>HMEPII THI KYBEPNHIEQI (TEVXOl: nPQTO) Section 2 Special requirements to be fulfilled by vehicles and their equipment Materials to be used in the construction of vehicle bodies 11200 In the construction of the body, no materials shall be used which are likely to form dangerous compounds with the explosives carried (e.g. lead in the case of the carriage of hexyl, picric acid, picrates, explosive organic nitro­ compounds soluble in water, or explosives of an acid nature [see also marginal 11 105 (2) (c)]. 11201 11215 Driver's cab 11216 (See marginal 11 105 (2) (b) 3.) 11217 11224 Combination of drawing vehicle and trailer 11225 [See marginal 11 105 (2) (a)] Engine and exhaust system [See marginal 11 105 (2) (b) 1.) Fire-fighting appliances The provisions of marginal 10 240 (1) (b) and (3) shall not apply to the carriage of dangerous substances of Class le, 1° to 3°, 5° to 20°, 24°, 25° and 27°. Electrical equipment (1) The rated voltage of the electric lighting system shall not exceed 24 V. (2) No circuit shall be installed inside the bodies of «B.11» and «B.IIJ. transport units. (3) The provisions of Appendix B.2, marginal 220 000(2), shall not apply to the electrical equipment of vehicles carrying articles of Class le, I O (a) and 3 °, or carrying articles of Class le, I O (b) in a quantity not exceeding 500 kg. (4) The provisions of Appendix B.2, marginal 220 000 (2) (a) and (c), shall not apply to the electrical equipment of vehicles parrying dangerous substances of Class le, 2°, 5 ° to 20°, 24 °, 25 ° and 27°, or carrying articles of Class le, lo (b) in a quantity exceeding 500 kg. Section 3 General service provisions (No special provisions) Classes la, lb and le Section 4 Special provisions concerning loading unloading and handling Method of despatch and restrictions on forwarding Substances oc Class la, 13° and 14° (a) and (b), may 11226 11230 11231 11232 11239 11240 11241, 11250 11251 11252 11299 11300 11399 11 400 be carried only as· a complete load. However, packages weighing not more than I 0 kg and handed over for carriage in a quantity not exceeding 100 Kg may be carried other­ wise than as a complete load. Limitation of the quantities carried. 11 40 l The quantity of dangerous substances of Classes la, lb and le which may be carried on one transport unit shall be limited as follows (see also Marginals 11 402 and 11 403 as regards the prohibition of mixed loading). (1) A •B.I» transport unit may carry only (a) one of the loads authorized ~y marginals 11 106 (l) and (2) (a); or (b) not more than 500 Kg of articles of Class l c, l O (b ); or ( c) not more than 300 Kg of substances of Class I a, 12°; or (d) not more than 100 Kg of substances of Class la 11 °, 13° and 14°. (2) A «B.11» transport unit may carry only (a) one of the loads authorized in (1) above for «B.I• transport units; or (b) not more than 500 Kg of substances of Class la, I 0 to 10° and 12°; of articles of Class lb, 1 ° to 4° and 6° to 11 °; or of dangerous substances of Class le. However, substances of Class la, 3° , 4° and 5° must be packed in accordance with what is· prescribed for consignments car­ ried otherwise than as a complete load. (3) A. «B.III» transport unit may carry only (a) one of the loads authorized in (2) above for «B.11» transport units; or, (b) provided that the weight of the load, of dargerous substances does not exceed 90 per cent of the weight of the load of ordinary goods declared ·permissible for the vehicle by the competent authority of the country of regis tration of the vehicle, not more than 9,000 kg of the dangerous substances of Classes la, lb or le per articula­ ted vehicle or vehicle without trailer, or than 15,000 kg of those dangerous substances per transport unit, of ano­ ther kind. However, if the load includes one or more substances of Class la, 11°, 13° or 14° or one or More substances of Class lb, 5°, 6° and 11 °, these limits shall be reduced to 6,000 kg and 10,000 kg respectively. Prohibition of mixed loading on one vehicle (1) Substances and articles of Class la shall not be loaded together on one vehicle with: (a) articles of Class lb enclosed in packages bearing two labels conforming to model No l; with (b) packages bearing a label of any of the models Nos 2D, 4, 4A, 6A, 6B and 6C; or with ( c) packages bearing a label or two labels or any of the models Nos. 2A, 2B, 2C and 5. (2) Articles of Class lb enclosed in packages bearing a label conforming to model No 1 shall not be loaded together on one vehicle with: (a) articles of Class lb enclosed in packages bearing two labels conforming to model No l; with (b) packages bearing a label of any of the models Nos 2D, 4, 4A, 6A, 6B and 6C; or with ' (c) packages bearing a label or two labels of any of the models Nos 2A, 2B, 2C, 3 and 5. (3) Articles of Class lb enclosed in packages bearing two fabels conforming to model No 1 shall not be loaded together on one vehicle with: (a)substances or articles of Classes la, lb or le enclosed in packages bearing a label conforming to model No l; or with (b) the substances indicated under (2) (b) and (2) (c) above, (4) Articles of Class le enclosed in packages bearing a label conforming to model No 1 shall not be loaded together in one vehicle with: (a) articles of Class lb enclosed in packages bearing two labels conforming to model No l; with . .. (b) packages bearing a label of any of the models Nos. 2D, 4, 4A, 6A, 6B and 6C; or with . (c) packages bearing a iabel or two labels of any ofthe' models Nos. 2A, 2B, 2C,3 and 5. 11402 11 403 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2297 • Prohidition of mixed loading with goods contained in a 11 405 container ( 1) The prohibitions of mixed loading of goods laid down in marginal 11 403 shall apply within each contai­ ner. (2) The provisions of marginal 11 403 shall apply as between the dangerous substances contained in a container and the other dangerous substances loaded on the same vehicle, whether or not the latter substances are enclosed in one or more other containers. Places of loading and unloading . (1) The following operations are prohibited: (a) loading or unloading dangerous substances of Classes la, lb and le in a public place in a built - up area without special permission from the competent authorities; (b) loading or unloading dangerous substances of the said Classes in a public elsewhere than in a built - up area without prior notice there of having been given to the competent autorities, unless the said operations are justi­ fied for serious reasons of safety. (2) If, for any reason, handling operations have to be carried out in a pyblic place, then: substances and. articles of different kinds shall be sepa­ rated according to the labels; and packages fitted with handles or supports shall be kept· flat. Cleaning before loading Before dangerous substances of Classes la, lb, or le are ·loaded, all remnants of straw, rags, paper and similar materials, and all iron objects (nails, screws, etc) not being an integral part of the body of the vehicle, shall be remo­ ved. Handling and stowage ( 1) The use of readily inflammable materials for stowing packages in vehicles is prohibited. (2) Packages containing dangerous substances of Clas­ ses la, lb and le shall be loaded in such a manner that they can be unloaded one by one at the point of destination without its being necessary to rearrange the load. (3) Packages shall be so stowed in the vehicle that they cannot be displaced therein. They shall be protected against any friction or impact. If casks are carried lying on their sides. they shall be so arranged that their longitudinal axis lies parallel to that of the vehicle, and wooden wedges shall be applied to prevent any lateral movement. Section 5 Spesial provisions .concerning the operation of vehicles Vehicle signs, . The provisions of marginal 10 500, paragraphs ( 1) and (6), shall apply to the carriage of dangerous substances of Classes la, lb and le. • Halts for passage through Customs When a transport unit or convoy of vehicles carrying dangerous substances of Classes la, lb, and le is to pass a frontier Customs .post, the transport unit (or convoy) shall stop at least 50 m from the Customs port. The driver's assistant shall proceed to the Customs port to inform the authorities of the arrival of the transport unit (or convoy) carrying dangerous substances. Halts of limited duration for service requirements So far as is possible, halts, for service requirements shall not be made near inhabited places or places of resort. A halt near such a place may not be prolonged . except with the agreement of the competent authorities. Convoys ( l) When vehicles carrying dangerous substances of • Classes la, 1 b and 1 c travel in convoy, a distance of not less than 80 m shall be maintained between each transport unit and the next: 11 406 11 407 11408 11412 11 413 11 414 11 415 11 499 11 500 11 501 11 507 11 508 11 509 11 510 11 519 11 520 (2) If, for any reason, the convoy is obliged to halt and if, in particular, loading or unloading operations have to be carried out in a public place, a distance of not less, than 50 m shall be maintained between the halted vehicles. (3) The competent authorities may lay down rules for the order or composition of convoys. Section Transitional provisions, derogations, arid provisions peculiar to certain countries Transitional provisions By derogation from article 4, paragraph 2, of the Agree­ ment, vehicles which were in service in the territory of a Contracting Party at the time of the entry into force of this Annex or were put into service there within two months after its entry into force may be used for the international carriage of dangerous substances of Classes'la, lb and le only during a period of one year from such entry into force if their design and equipment do not fully satisfy the requirements laid down in this Annex for sush carriage. Provisions peculiar to certain countries. The carriage of dangerous substances of Classes la, lb and le shall be subject in the territory of the United Kingdom to the regulations in force in that country at the time of carriage. Class 2 11 521 11599 11 600 11 604 11605 11 606 11 609 11 610 11 611 20 999 Gases: compressed, liquefied or dissolved under pressure Section 1 • General Carriage in containers The carriage i.n small containers of packages containing gases of 7°(a) and 8°(a) is prohibited. Carriage in tanks (1) Gases of Class 2 other than those listed below may be carried in fixed tanks, in demountable tanks, or in batteries of receptacles: fluorine and silicon tetrafluoride [l "(a t)]; nitric oxide [l 0 (c t)]; mixtures of hydrogen with not more than 10 per cent hydrogen selenide or phos~hine or·silane or germane by volume or with not more than 15 per cent arsine by volume; mixtures of nitrogen or rare gases (containing not more lhan 10 per cent xenon by volume) with not more than 10 per cent hydrogen selenide or phosphine or silane or germane by volume or with not more than 15 ·per cent arsine by volume [2°(b t)]; mixtures of hydrogen with not more than 10 per cent diborane by volume; mixtures of nitrogen or ·rare gases (containing not more than 10 per cent xenon by volume) with not more than 10 per cent diborane by volume [2°(c t)]; boron chloride, chlorine trifluoride, nitrosyl chloride, sulphuryl · fluoride and tungsten hexafluoride [3°(a t)]; methylsilane [3°(b)]; arsine, dichlorosilane, dimethylsilane, hydrogen selenide and trimethylsilane [(3°(b t)]; cyanogen, cyanogen chloride and ethylene oxide [3°(c t)]; mixtures of methylsi­ lanes [ 4"(b t)]; ethylene oxide containing not more than 50 per cent methyl formate by weight [4°(c t)]; silane [5°(b)]; substances of 5°(b t) and (c t); dissolved acetylene [9°(c)]; and gases of 12° and 13°. Class 2 21000 21117 21118 21119 21120 · 21121 (2) Cases of Class 2 other than those listed below may be 21121 .carried in tank-containers:· fluorine and silicon tetrafluo 2298 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) ride [l "(a t)]; nitric ·oxide [l 0 (c t)); mixtures of hydrogen with not more than: 10 per cent hydrogen selenide or phosphine or silane or germane by volume or with not more than 15 per cent arsine by volume; mixtures of nitrogen or rare gases (containing not more than 10 per cent xenon by volume) with not more than 10 per cent hydrogen selenide or phosphine or silane or germane by'­ volume or with not more than 15 per cent arsine by volume [2°(b t)]; mixtures of hydrogen with not more than 10 per cent diborane by volume;mixtures of nitrogen or rare gases (containing not more than 10 per cent xenon by volume) with not more than 10 per cent diborane by volume [2°(c t)]; boron chloride, chlorine trifluoride, nitro­ syl chloride, sulphuryl fluoride and tungsten hexafluoride [3 ° (at)]; methylsilane [3 ° (b )]; arsine, dichlorosilane, dimethylsilane, hydrogen selenide and trimethylsilane [3 ° (b t)); cyanogen, cyanogen chloride and ethylene oxide [3 ° (c t)]; mixtures of methylsilanes [4 °(b t); ethylene oxide containing not more than 50 per cent methyl formate by weight .[4°(c t)); silane [5°(b)]! and the gases of 12 ° and,;;13 °. However, chlorine and phos­ gene [3°(a t)] shall not be carried in tank-containers of a cubic capacity exceeding 1 m3• (3) Tank-containers containing substances of 1 °(b); 2°(b); 3°(b); chloroeth;me (ethyl chloride) or dimethyl ether of 3°(b t); substances of 3°(c); vinyl bromide or methyl vinyl ether of 3°(c t); or substances of 4°(b), 4°(c), 5°(b), 5° (c), 6°(c), 7°(b) or 8°(b) shall bear on both their sides a label conforming to model No. 2A. Tank-containers containing oxygen of 1 ° (a); boron trif­ luoride of 1 °(a t); mixtures containing more than 20 per cent oxygen by volume, of 2°(a); nitrous oxide of 5°(a); nitrous oxide or oxygen of 7°(a); or liquid air or mixtures containing more than 20 per cent oxygen by weight of 8°(a), shall bear on both their sides a label conforming to model No. Tank-containers containing ammonia, bromomethane, chlorine or sulphurdioxide, of 3°(a t), or ethylene oxide containing not more than .10 per cent by weight carbon dioxide, of 4°(c t), shall bear on both their sides a label conforming to model No. 4. Tank-containers containing gases of 1 °(b t) or 2°(b t), or dimethylamine, ethylamine, hydrogen sulphide, methy­ lamine, methyl chloride, methyl mercaptan, or trimethyla­ mine, of 3°(b t), shall bear on both their sides labels conforming to models Nos. 2A and 4. Tank-containers containing nitrous dioxide or phosgene of 3° (a t) shall bear on both their sides labels conforming to models Nos. 3 and 4. Tank-containers containing hydrogen bromide of 3°(a t) or hydrogen chloride of 5°(a t) shall bear on both their sides labels conforming to models Nos. 4 and 5. Class 2 Empty tanks (1) For empty fixed tanks, empty batteries of receptac­ les and empty demountable tanks, see Annex A, marginal 2201, 14°, Note 1. (2) For tank-containers, see marginal 212 177. Crews of vehicles: Supervision The provisions of marginal 10 1 71 (2) shall apply only to the dangerous goods listed below in quantities excee­ ding the weights indicated: boron trifluoride and fluorine [l 0 (a· t)); the substances of 3°(a t)]; of 3°(b t) other than dimethyl ether and ethyl chloride; and of 3°(c t); hydrogen chloride of 5°(a t); and the deeply-refrigerated liquefied gases of 7°(a) and 8°(a): 1,000 kg • the substances of 3°(b); dimethyl ether and ethyl chlo­ ride of 3°(b t); vinyl chloride of 3°(c); the substances of 21122 21127 21128 21129 21170 21171 4°(b); and the inflammable liquefied gases of 7°(b) and 8°(b): 10,000 kg Class 2 Section 2 Special requirements to be fulfilled by vehicles and their equipment Ventilation If packages containing gases of 1 ° to 6° and 9°(c) are carried in a closed vehicle, the vehicle shall be provided with adequate ventilation. Engine and exhaust system The engine of a vehicle carrying a gas of Class 2 in a fixed tank, in a demountalbe tank or in a battery of recep­ tacles, and where appropriate the engine driving the deca­ nting pump, shall be so equipped and placed, and the exhaust pipes so directed or protected, as to avoid any danger to the load through heating or igr1ition. Fire-fighting appliances The provisions of marginal 10 240 (I) (b) and (3) shall not apply to carriage other than that of inflammable gases or articles listed in marginal 220 002, or of empty packa­ gings of 14° which have contained ~uch gases. Electrical equipment The provisions of appendix B.2 shall not apply to car­ riage other than that of inflammable gases or articles listed in marginal 220002, or of empty packagings of 10° which have contained such gases. Special equipment When compressed gases or liquefied gases harmful to the respiratory organs of entailing a poison risk and identi­ fied by the letter •I» in the list of substances are being carried, the crew of the vehicle shall be provided with gas masks (respirators) of a type appropriate to the gases b~ing carried. Class 2 Section 3 General service provisions Portable lighting apparatus When inflammable gases or articles listed in marginal 220002 are being carried, a closed vehicle may not be entered by persons carrying lighting apparatus other than portable lamps so designed and constructed that they can­ not iginte any gases which may have penetrated into the interior of the vehicle. • 21172 21199 21200 21211 21212 . 21213 21230 21231 21232: 21239 21240 21241 21250 21251 21252 21259 21260 21261 21299 21300 21352 21353 21354 21399 <l>EK 225 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) 229!) Class 2 Section 4 Special provisions concerning loading, unloading, and handling Method ofdispatch and restrictions on forwarding Carbon dioxide and nitrous oxide of 7°(a), mixtures containing carbon dioxide and nitrous oxide of 8°(a), and the gases of 7°(b) and 8°(b) may be carried only in fixed tanks, in demountable tanks, in batteries of receptacles or in tank-containers. Prohibition of mixed loading on one vehicle Articles of Class 2 enclosed in packages bearing a label conforming to model No.2A shall not be loaded together on one vehicle with substances or articles of Classes la, • I b or 1 c enclosed in packages bearing a label or two labels conforming to model No. 1. Places of loading and unloading (1) The following operations are prohibited: (a) loading or unloading the following substances in a public place in a built-up area without special permission from the competent authorities: hydrogen bromide, chlo­ rine, nitrogen dioxide, sulphur dioxide or phosgene [3°(a t); hydrogen sulphide [3°(b t)]; and hydrogen chloride [5°(a t)J; . (b) loading or unloading the substances listed under (a) above in a public place elsewhere than in a built-up area . without prior notice there of having been given to the competent authorities, unless the said operations are justi­ fied for serious reasons of safety. (2) If for any reason handling operations have to be carried out in a public place, then: substances and articles of different kinds sh,i.11 be sepa­ rated according to the labels; and packages fitted with means of handling shall be kept. flat while being handled. Class 2 • 21400 ·21401 21402 21403 21404 21406 21407 21408 21413 Handling and stowage 21414 (1) Packages shall not be thrown or subjected to impact. (2) Receptacles shall be so stowed in the vehicle that they cannot overturn or fall and that the following requirements are met: (a) the cylinders referred to in marginal 2212 (1) (a) shall be laid parallel to or at right angles to the longitudinal axis of the vehicle; however, those situated near the for­ ward transverse wall shall be laid at right angles· to the said axis. • Short cylinders of large diameter (about 30 cm and over) may be stowed longitudinally with their valve­ protecting devices directed towards the middle of the veh­ icle. Cylinders which are sufficiently stable or are carried in suitable devices effectively preventing them from overtu­ rning may be placed upright. Cylinders which are laid flat shall be so welged or attached that they cannot shift; (b) receptacles containing gases of 7°(a) or 8°(a) shall always be placed in the position for which they were designed and be protected against any possibility of being damaged by other packages. 21415 21499 Class 2 Section 5 Special provisions concerning the operation of vehicles Vehicle signs 21500 (1) The provisions of marginal 10 500, paragraphs (1) and. (6) shall apply to the carriage of dangerous substan­ ces of Class 2. The provisions of paragraphs (2) to (5) shall additionally apply to the carriage of substances listed in Appendix. B.5. (2) Fixed tanks containing or (empty tanks, uncleaned) • having contained substances listed in Appendix B.5 shall in addition bear the following labels on both sides and at the rear: ..: Air, liquefied Ammonia, anhydrous Butadiene Butane Butylene Chlorine Cyclopropane Dimethyl ether Ethyl chloride • Ethylene Ethylene, liquid (refrigerated) Hydrocarbons, mixtures of (Mixtures A, AO, Al, Band C) Hydrogen bromide Hydrogen chloride Isobutane Isobutylene Methane, liquid ·(refrigerated) Methylamine, anhydrous. Methyl bromide Methyl chloride Methyl vinyl ether Natural gas, liquid (refrigerated) Nitrogen dioxide N02 Nitrous oxide N20 Oxygen (refrigerated) Phosgene Propylene Trimethylamine, anhydrous Vinyl chloride 3 4 2A 2A 2A 4 2A 2A 2A 2A 2A 2A 4:+5 4+5 2A 2A 2A 4 4 2A+4 • 2A 2A 3+4 3 3 3+4 2A 2A+4 '2A 21501 21508 Class 2 Halts of Limited duration for service requirements In the carriage of dangerous substances of Class 2 other than those of 1 °, (a) and (at); 7 ° (a); 8 ° (a); and 10 °, halts for service requirements shall so far as possible not be made near inhabited places or places of resort. A halt near such a place may not be prolonged except with the agreement of the competent authorities. Class 2 Section 6 Transitional provisions, derogations and provisions peculiar to certain countries Provisions peculiar to certain countries The carriage of dangerous substances of Class 2 shall be subject in the territory of the United Kingdom to the regulations in force tn that country at the time of carriage. 21509 21510 21599 21600 21609 21610 21611 3Q999 2300 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Class 3 Inflammable Liquids Section 1 General Carriage in containers Fragile packages within the meaning of marginal 10 102 (1) may not be carried in small containers. Carriage in tanks (1) All the 'liquids of Class 3 except nitromethane (3 °) may be carried in fixed tanks and in demountable tanks. (2) All substances of Class 3 except nitromethane (mo­ nonitromethane) (3 °) may de carried in tank-containers, (3) The following substances may be carried in reinfor­ ced-plastics tanks conforming to the provisions of Appen­ dix B.lc: . Crude petroleum and other crude oils; volatile products from the distillation of crude petroleum.and of other crude oils (1 °(a)). Semi-heavy products from the distillation of petroleum andf of ther crude oils (3 ° ). • Heating oils and diesel '!ils ( 4 ° ). Empty tanks (1) To be accepted for- carriage, empty fixed tanks and empty demountable tanks which have contained inflam­ mable liquids of Class 3 shall be closed in the same manner and leak-proof in the same degree as though they were full. • (2) For tank-containers, see marginal 212177. Crews of vehicles; Supervision The provisions of marginal 101 71 (2) shall apply only to the dangerous goods listed below in quantities excee­ ding those specified below: Class 3 The substances of 1 ° other than carbon disulfbide, acrylaldehyde (acrolein) and chloroprene (chlorobuta­ diene), and the substances of 5 °: 10,000 kg Carbon disulphide, acrylaldehyde (acrolein) and chlorop­ rene (chlorobutadiene) of 1 °: 1,000 kg Cab Class 3 Section 2 Special requirements to be fulfilled by vehicles and their equipment No readily-inflammable material shall be used in the construction of the cabs of vehicles carrying, liquids of 1 ° in fixed tanks or in demountable tanks. Engine and exhaust·system The engine of a vehicle carrying a liquid of 1 ° in a fixed tank or a demountable tank shall be so constructed and placed, and the exhaust pipe so directed or protected, as to avoid any danger to the load through heating or igni­ tion. Air-intake piping , In the case of vehicles carrying liquids of 1 ° in fixed tanks or in demountable tanks, the intake pipe of every 31000 31117 31118 31119 31120 31121 31122 31127 31128 31129 31170 31171 31172 31199 31200 31215 31216 31217 31230 31231 31232 petrol engine shall be fitted with a filter capable of serving as a flame-trap. Fud tank The fuel tank supplying the engine of a vehicle carrying a liquid of 1 ° in a fixed tank or in a demoyntable tank shall be so placed that it is protected ,so far as possible against forceful impact and that in the event of leakage of• fuel the latter can drain directly to the ground. The fuel tank shall in no circumstances be placed directly above the exhaus·t pipe. If the tank contains petrol; it shall • be equipped with an efficient flametrap fitting the filler hole or with a device by which the filler hole can be kept· hermetically closed. Electrical equipment The provisions of Appendix B.2, marginal 220000, shall not apply to the carriage of. dangerous substances of Class 3 other than inflammable liquids of 1 °, 2 ° and 3 ° and acetaldehyde, acetone and acetone mixtures of 5 °. Class 3 Section 3 General service provisions Use of portable lighting apparatus A closed vehicle may not be entered by persons car­ rying lighting apparatus other than portable lamps so de­ signed and constructed that they cannot ignite any gas which may have penetrated into the interior of the vehicle. Clase 3 Section 4 Special provisions concerning loading, unloading and handling Prohibition of mixed loading on one vehicle (1) Liquids of Class 3 enclosed in packages bearing a label or two labels conforming to model No. 2A shall not be loaded together on one vehicle with substances or articles of Classes la, lb or le enclosed in packages bearing a label or two labels conforming to model No. 1. (2) Substances of Class 3 enclosed in packages bearing two labels conforming to model No. 2A shall not be loaded together on one vehicle with: (a) substances of Classes 5.1 or 5.2 enclosed in packa­ ges bearing two labels conforming to model No. 3; or with (b) liquids of Class 8 enclosed in packages bearing two labels conforming to model No. 5. • Handling and stowage The use of readily inflammable materials for stowing packages in vehicles is prohibited. Precautions against electrostatic charges Before filling or emptying reinforced-plastics tanks with substances with a flash point of 55 ° C or lower, measures shall be taken in order to establish a good electrical conne­ xion from the vehicle chassis to earth. The filling rate for substances with a flash point of 55 ° C or lower shall be limited so as to avoid the generation of unsafe electrostatic charges. 31233 31234 31235 31236 31250 31251. 31252 31299 31300 31352 31353 31354 31399 31400 31402 31403 31404 31413 31414 31415 31416 31417 31418 31499 E<l>HMEPII: THI: KYBEPNHI:EQr (TEYXOr nPQTO) 2.301 Class 3 Section 5 Special provisions concerning the operation of vehicles Vehicle signs (l) The provisions of marginal 10500, paragraphs (1) and (6), shall apply to the carriage of substances of 1 °, 3°, 4° and 5°. The provisions of paragraphs (2) to (5) shall also apply to the carriage of substances listed in Appendix· B.5. (2) Fixed tanks containing substances listed in Appen­ dix B.5 shall in addition bear on both sides and at the rear a label conforming to model No. 2A; those containing or (empty tanks, uncleaned) having contained acrylalde­ hyde (acrolein) or chloroprene (chlorobutadiene [l O (a)] or methanol (methyl alcohol) (5°) shall in addition bear labels conforming to model No. 4. Class 3 Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries Transitional provisions Tanks which were in service in the territory of a Contrac­ ting Party at the time of the entry into force of the Agree­ ment under article 7, paragraph 1, or were put into service there within two months after its entry into force, may be used for the international carriage of dangerous substances during a period of three years from such entry into force even if their design and equipment do not fully satisfy the requirements laid down in Appendix B. I. Provisions peculiar to certain countries The carriage of liquids ~f Class 3 whose flash-poirit i; below 23 ° C shall be subject in the territory of the United Kingdom to the regulations in force in that country at the time of carriage. Class 4.1 Inflammable solids Section 1 General Types of vehicles . Packages containing substances of 4° to 8° shall be loaded on to closed vehicles or on to sheeted vehicles. Carriage in bulk (1) Sulphur of 2° (a) may be carried in bulk. (2) Naphthalene of 11 ° (a) and (b) may be carried in bulk; it must in that case be carried in closed vehicles with a metal body or in sheeted vehicles with a non­ inflammable sheet and either having a metal body or ha­ ving a sheet of closely-woven.material spread on the floor. For the carriage of naphthalene of 11 °(a), the floors of vehicles shall be protected by an oil-proof lining. Carriage in containers For the carriage of naphthalene of.I 1 °(a) and (b), small wooden containers shall be fitted with an oil-prooflining. Carriage in tanks (1) Sulphur (2°), phosphorus sesquisulphide, ph~s­ phorus pentasulphide (8°) and naphthalene (11 °) may be carried in fixed tanks or in demountable tanks. 31500 31501 31599 31600 31604 31605 31606 31609 31610 31611 40999 41000 41103 41104 41105 41110 41111 41112 41117 41118 41119 41120 41121 (2) These same substances may also be carried in tank­ containers. Class 4.1 Empty tanks For tank-containers, see marginal 212177. Crews of vehicles; Supervision (1) A driver's assistant shall be carried on every tran­ sport unit carrying more than 300 kg of substances of 6°. (2) The provisions of marginal 10171 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: The substances of 7°(a), (b) and (c): 1,000 kg. Class 4.1 Section 2 Special requirements to be fulfilled by vehicles and their equipment Electrical equipment The provisions of Appendix B.2, marginal 220000, shall not apply to carriage other than that of substances of 3° to 7°. Class 4.1 Section 3 General service provisions (No special provisions) Class 4.1 Section 4 Special provisions concerning loading; unloading and hanbling Method of despatch and restrictions on forwarding Sulphur in the melted state [2°(b)] and naphthalene in the melted state [11 °(c)] may be carried only in tank­ vehicles and tank-containers. Prohibition of mixed loading on one vehicle (l) Substances-of Class 4.1 enclosed in packages bea­ ring a label or two labels conforming to model No. 2B shall not be loaded together on one vehicle with substances or articles of Classes la, lb or le enclosed in packages bearing a label or two labels conforming to model No. I. (2) Substances of Class 4.1 enclosed in packages bea­ ring two labels conforming to model No. 2B shall not be loaded together on one vehicle with: (a) substances of Classes 5.1 or 5.2 enclosed in packa­ ges bearing two labels conforming to model No. 3; or with (b) liquids of Class 8 enclosed in packages bearing two labels conforming to model No. 5. Class 4.1 Section 5 Special provisions concerning the operation of vehicles Vehicle signs (1) The provisions of marginal 10500, paragraphs (1) and (6), shall apply to the carriage of substances of 2°(b), 4° to 8° and 11 °(c). The provisions of paragraphs (2) to (5) shall also apply to the carriage of substances listed in Appendix B.5. 41122 41127 41128 41129 41170 41171 41172 41199 41200 41250 41251 41252 41299 41300 41399 41400 41401 41402 41403 41404 41499 41500 (2) Fixed tanks containing or (empty tanks, uncleaned) . having contained substances listed in Appendix B.5 shall • in addition bear on both sides and at the rear a label conforming to model No. 2B. Section 6 Transitional provisions, derogallons, and provisions peculiar to certain countries (No special provisions) 41501 41599 41600 41999 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Class 4.2 Substances liable to spontaneous combustion Section 1 General Types of vehicles Packages containing substances of 4° and 10° shall be loaded on to closed vehicles or on to sheeted vehicles. Carriage in bulk Substances of 5°, dust from blast-furnace filters [6°(a)] and substances of 10° may be carried in bulk. Substances of 5 ° and 10° shall in that case be carried in closed vehicles with a metal body, and dust from blast-furnace filters in closed vehicles with a metal body or in sheeted vehicles with a metal body. • Carriage in tanks (1) White or yello~ phosphorus (1 °) and newly­ quenched charcoal, powdered or granulated, (8°) may be carried in fixed tanks or in demountable tanks. (2) White or yellow phosphorus (1 °), aluminium alkyls, halides and hydrides of aluminium alkyls (3°) and newly­ quenched charcoal, powdered or granulated, (8°) may be carried in tank-containers. Empty tanks (1) To be accepted for carriage, empty fixed tanks and empty demountable tanks which have contained phos­ phorus of 1 ° shall either be filled with nitrogen, in which case the transport document shall be required to certify that the tank, after closure, is gas-tight; or b~ filled to not less than 96 per cent of their capacity with water; between I October and 31 March this water shall contain, in a concentration making it impossible for the water to freeze during carriage, one or more non­ corrosive anti-freezing agents not liable to react with phos­ phorus. (2) For tank-containers, see 212177 and 212474. Crews of vehicles; Supervision (1) A driver's assistant shall be carried on every tran­ sport unit carrying substances of 1 °, 2°, 3° and 4°. (2) The provisions of marginal 10171 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: The substances of 1 ° - 3°, powder of zirconium of 6°(a) and metals in a pyrophoric form of 6 °(d): 10,000kg Section 2 Special requirements to be fulfilled by vehicles and their ecuipment Electrical equipment The provisions of Appendix B.2, marginal 220000, shall not apply to the carriage of dangerous substances of Class 4.2. Section 3 General service provisions (No spedal provisions) 42000 42103 42104 42105 42110 42111 42112 42120 42121 42122 42127 42128 42129 42170 42171 42172 42199 42200 42250 42251 42252 42299 42300 42399 Section 4 Special provisions concerning loading, unloading and handling Prohibition of mixed loading on one vehicle (1) Substances of Class 4.2 enclosed in packages bea­ ring a label or two labels conforming to model No.2 C shall not be loaded together on one vehicle with substances or articles of Classes la, lb or le enclosed in packages bearing a label or two labels conforming to Model No. 1. (2) Substances of 4° enclosed iri pa~kages bearing two labels conforming to model No. 2 C shall not be loaded together on one vehicle with: (a) substances of Classes 5.1 or 5.2 enclosed in packa­ ges bearing two labels conforming to model No. 3; or with (b) liquids of Class 8 enclosed in packages bearing two labels conforming to model No. 5. Handling and stowage (1) Receptacles and packages containing substances of 1 ° and 3° must not be subjected to impact. They shall be so placed in the vehicle that they cannot overturn or fall or be displaced in any way. (2) The use of readily inflammable materials for stowing packages in vehicles is prohibited. Section 5 Special provisions concerning the operation of vehicles Vehicle signs • • (1) The provisions of marginal 10500, paragraphs (1) and (6), shall apply to the carriage of substanoes of 1 ° to 4° and 6°. The provisions of paragraphs (2) to (5) shall also apply to the carriage of substances listed in Appendix B.5. (2) Fixed tanks containing or (empty tanks, uncleaned) having contained substances listed in Appendix B.5 shall in addition bear on both sides and at the rear a label conforming to model No. 2C. Section 6 Transitional provisions, derogations, and provisions pec­ uliar to certain countries (No special provisions) Class 4.3 42400 42402 42403" 42404 42413 42414 42415 42499 42500 42501 42599 42600 42999 Substances which give off inflammable gases on contact with water Section 1 General Types of vehicles Dangerous substances of Class 4.3. in packages shall be loaded on to closed or sheeted• vehicles. However, receptacles containing calcium carbide [2 ° (a)] may also be loaded on to open vehicles. Carriage in bulk ~alcium carbide ~2 ° ~a)] and calcium silicide in lumps [2 (d)] may be earned m bulk m vehicles equipped with movable or fixed receptacles which must conform to the general conditions of packing set forth in marginal 24 72 (1), (2) and (3). Such receptacles must be so designed that the openmgs used for loading or unloading can be closed hermetically. 43000 43103 43104 43105 43110 43111 43112 43117 43118 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 230:J Carriage in containers Small containers used for the carriage in bulk of the substances referred to in marginal 43111 shall conform to the provisions of that marginal concerning vehicles and the receptacles of vehicles. Carriage in tanks (1) Sodium, potassium, and alloys of sodium or potas­ sium [l 0 (a)], and trichlorosilane (silicochloroform) (4°), . may be carried in fixed tanks or in demountable tanks. (2) Th~se same substances may also be carried in tank­ containers. Class 4.3 Empty tanks • (1) To be accepted for carriage, empty tanks and empty demountable tanks which have contained sodium, potas­ sium or alloys of sodium and potassium [l 0 (a)] shall be closed in the same manner and leak-proof in the same degree as though they were full. (2) For tank-containers, see marginal 212177. Crews of vehicles; Supervision (1) A driver's assistant shall be carried on every tran­ sport unit carrying substances of Class 4.3 other than calcium carbide [2°(a)] and calcium sillcide [2°(d)]. (2) The provisions of marginal 10171 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: The alkali metals and substances containing alkali me­ tals of 1 °, alkali metal hydrides of 2 ° (b) and trichlorosi­ lane (silicochloroform) of 4 °: 10,000 kg 43119 43120 43121 43122 43127 43123 43129 43170 43171 I 4,1172 43199 Class 4.3 Section 2 Special requirements to be. fulfilled by vehicles and their • equipment (No special requirements) Class 4.3 Section 3 General service provisions (No special provisions) Class 4.3 Section 4 Special provisions concerning loading, unloading and han­ dling Prohibition of mixed loading on one vehicle Substances of Class 4.3 shall not be loaded together on one vehicle with substances or articles of Classes 1 a; 1 b or le enclosed in packages bearing a label or two labels conforming to model No. 1. • 43200 43299 43300 43399 43400 43402 43403 Handling and stowage Packages shall be so stowed in the vehicle that they cannot be displaced therein. T~ey shall be protected against any friction or impact. While packages are being • handled, special measures shall be taken to prevent them from coming into contact with water. • Class 4.3 Section 5 Special provisions concerning the operation of vehicles Vehicle signs (1) The provisions of marginal. 10500, paragraphs (1) and (6), shall apply to the carriage of dangerous substan­ ces of Class 4.3. The provisions of paragraphs (2) to (5) shall alsci apply to the carriage of substances listed in Appendix B.5. (2) Fixed tanks containing or (empt}'. tanks, uncleaned) having contained substances listed in Appendix B.5 shall in addition bear on both sides and at the rear a label conforming to model No. 2D. Class 4.3 Section 6 .. Transitional provisions, derogations, and provisions pec­ uliar to certain countries (No special provisions) Class 5.1 Oxidizing substances Section 1 General 43404 43413 43414 43415 43499 43500 43501 43599 43600 50999 51000 51110 Carriage in bulk 51111 (1) Sudstances of .4° to 6° and 7° (a) may carried in bulk as a complete load. (2) Substances. of 4 ° and 5 ° shall be carried in open metal «vat vehicles» (vehicules cuves) covered with an impermeable non-inflammable sheet,or in metal contai­ ners [see marginal 51118 (2)]. (3) Substances of 6° and 7° (a) aHd (b) shall be carried in closed vehicles or in vehicles covered wiih an imperme­ able non-inflammable sheet, the vehicles being so constru­ cted either. that the ~ubstance .cannot come into contact with wood or any other combustible material or that the entire surface of the floor and walls, if combustible, has been provided with an impermeable and incombustible surfacing or treated with substances rendering the wood in­ combustible. 51112 51117 Carriage in containers 51118 (1) Fragile packages within the meaning of marginal 10102 (1) and those containinl!; hydrogen peroxide or 2304 E<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) solutions of hydrogen peroxide (I 0 f or tetranitromethane (2 °) may not be carried in small containers. (2) Containers intended for the carriage of substances of 4 ° and 5 ° shall be made of metal, be leak-proof, be covered with a lid· or an impermeable sheet resistant to combustion, and be so constructed that the substances held in the containers cannot come into contact with wood or any other combustible material. (3) Containers intended for the carriage of substance!> of 6° and 7° (a) and (b) shall be covered with a lid or an impermeable sheet resistant to combustion and be so constructed either that the substances held in the contai­ ners cannot come into contact with wood or any other combustible material or that the entire surface of the floor and walls, if made of wood, has been provided with an impermeable surfacing resistant to combustion or has been coated with sodium silicate or a similar substance. 51119 51120 Carriage in tanks 51121 (1) Substances of 1 ° to 3 °; solutions of 4 ° (also powdery sodium chlorate in the moist or the dry state); and hot aqueous solutions of. ammonium nitrate of 6 ° (a) in· a concentration of more than 80 per cent but not more than 93 per cent on condition that: (a) the pH value, measured in a 10 per cent aqueous solution of the substance carried, is between 5 and 7, and that (b) the solutions not containing any combustible substance in a quantity greater than 0.2 per cent or any chlorine compound in such quantity that the chlorine co­ ntent exceeds 0.02 per cent may be carried in fixed tanks and in demountable tanks. (2) The substances of 1 ° to 3 °, the solutions of 4 ° and moist sodium chlorate of class 5.1 may be carried in tank­ containers. (3) Solutions of 4 ° (a), may be carried in reinforced­ plastics tanks conforming to the provisions of Appendix B.lc. 51122 51127 Empty tanks 51128 (1) To be accepted for carriage, empty fixed tanks and empty demountable tanks which have contained substan ces of Class 5.1 shall be closed in the same manner and leak-proof in the same degree as though they were full. (2) For tank-containers, see marginal 212177. (3) Empty fixed tanks and empty demountable tanks which have contained a chlorate, a perchlorate, a chlorite ( 4 ° and 5 ° ), an inorganic nitrate (8 °) or substances of 9 ° and 10° and have residues from their previous contents adhering to the outside are not to be accepted for carriage. 51129 51170 Crews of vehicles: Supervision . 511 71 (1) A driver's assistant shall be carried on every tran sport unit carrying sudstances of Class 5.1, 1 °, 2 ° and 3 ° (2) The provisions of marginal 10171 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: The substances of 1 ° to 3 ° and 9° (a): 10.000 kg 51172 51199 Class 5.1 Section 2 Special requirements to be fulfilled by vehicles and their equipment (No special requirements) Cab The following provisions shall apply to the carriage of liquids of 1 ° in fixed tanks or in demountable tanks: (1) unless the driver's cab is made of fire-proof mate­ rials, a metal shield of the same width as the sa~e tank shall be fitted at the back of the cab; \ (2) any windows in the back of the driver's cab or in the metal shield shall be hermetically closed. They shall be made of fire-resistant safety glass and have fire-proof frames; and (3) there shall be a clear space of not less than 15 cm between the tank and the driver's cab or the shield. Vehicle body For the carriage of liquids of 1 ° in fixed tanks or in demountable tanks, no wood (unless covered with metal or a suitable synthetic material) shall be used in the construction of ~ny part of the vehicle situated to the rear of the shield prescribed in marginal 51216 (1). Engine For the carriage of liquids of 1 ° in fixed tanks or in demountable tanks, the engine and (except where the vehicle is driven by a diesel engine) the fuel tank shall be placed forward of the rear wall of the driver's cab or of the shield, or shall if placed otherwise be specially protec • ted. Special equipment Vehicles carrying liquid,, of 1 ° in fixed tanks or in demountable tanks sh{lll carry on board a tank having a capacity of about 30 litres of water. The water tank shall be placed as securely as possible, and there shall be admixed to the water it contains an anti-freeze preparation which does not attack the skin or the mucous membranes and does not react chemically with the load. 51200 51215 51216 51217 51218 51230 51231 51232 51259 51260 51261 51299 Class 5.1 Section 3 General service provisions 51300 51302 Precautions with respect to articles of consumption 51305 In vehicles and at places ofloading, unloading or translo ading, tetranitromethane of 2o, barium chlorate of 4 ° (b), barium perchlorate of 4 ° (b ). barium nitrate and !earl nitrate of 7 ° ( c ), inorganic nitrites of 8 °, barium dioxide of 9 ° (b) and barium permanganate of 9 ° ( c) shall be kept away from foodstuffs and. other articles of consumption 51304 51399 E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Class 5.1 Section 4 Special provisions concerning loading, unloading and ha n­ dling .51400 51402 Prohibition of mixed loading on one vehicle 51403 (1) Substances of Class 5.1 enclosed in packages bea ring a label or two labels conformiQg to model No. 3 shall not be loaded together on one vehicle with ·substances of Classes 1 a, 1 b or 1 c enclosed in packages bearing a label or two labels conforming to model No. l. • (2) Substances of Class 5.1 enclosed in packages bea­ ring two labels conforming to model No.3 shall not be loaded together on one vehicle with: (a) substances of Classes 3, 4.1 or 4.2 enclosed in packages bearing two labels conforming to models Nos. 2A, 2B or 2C; or with (b) liquids of Class 8 enclosed in packages bearing two labels conforming to model No. 5. 51404 51413 Handling and stowage 51414 (1) Packages containing substances of Class 5.1 shall be placed flat on their bottoms. In addition, receptacles containing liquids of Class 5.1 shall be so wedged that they cannot overturn. • (2) The u se of r eadily inflammable ~aterials for stowing packages in vehicles is prohibited. . • "' •• ' Cleaning after unloading 51415 After unloading, vehicles which have been carrying substnces of 4° to 6° and 7° (a) and (b) in bulk shall be copiously swilled. Class 5.1 Section 5 Special provisions I concerning the operation of vehicles 51416 51499 Vehicle signs 51500 (1) The pro.visions of marginal 10500, paragraphs (1) and (6), shall :apply to the carriage of substances of 1 ° 2 °, 3 ° of chlorates and inorganic chlorate weedkillers of 4° (a), barh1m perchlorate of 4° (b), substances of 8° and g? (b), and barium permanganate of 9° (c). the pro~1s1ons of paragraphs (2) to (5) shall also apply to the carnage of substances listed in Appendix B.5. (~) fixed t~nks containing or (empty tanks, uncleaned) ~avmg -~ontamed su~stances listed in Appendix B.5 shall m add111on bear on both sides and at the rear a label conforming to model No. 3. Class 5.1 Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries (No special provisions) 51501 51999 51600 51999 Types of vehicles Class 5.2 Organic peroxides Section 1 General (1) Substances of 1 ° to 22 °, 30 ° and 31 ° shall be loaded on to closed or sheeted vehicles. Substances of 45 ° t o 55 ° enclosed in protective packagings filled with a refrigerant shall be loaded on to closed or sheeted vehic­ les. ~f the vehicles used are closed they shall be adequately ventilated. Sheeted vehicles shall be fitted with side boards and a tailboard. The sheets of these vehicles shall be of a impermeable material not readily inflammable. (2) Where, by reason of the provisions of marginal 52400, substances are required to be carried in insulated refr igerated or mechanically-refrigerated vehicles, thos; vehicles shall satisfy the requirements of m·argina:l 52248. Carriage in containers Fragile packages within the meaning of marginal 10102 ( 1) shall not be carried in small containers.· Carriage in tanks (~) Substances of 1 °, 10°, 14°, 15° and 18° may be earned in fixed tanks and in demountable tanks. (2) These substances may also be carried in tank contai­ ners .. Class 5.2 Empty tanks (1) To be accepted for carriage, empty fixed tanks and empty demountable tanks of 99° shall be closed in the same manner and leak-proof in the same degree as though they were full. • (2) F9r tank-containers, see marginal 212177. , Crews of vehicles: Supervision (1) A driver's assistant shall be carried on every trans spo[1 unit loaded with substances of 46 6 (a), 4 7 ° (a) and 49 (a) and on every transport unit loaded with more than 2,000kgofsubstancesof45°,46°(b)and(c) 50° 51° to 53 ° and 55 °. .. ' ' (2) The provisions ~f margin al 101 71 (2) shall apply . only t~ the dangerous goods hsted below in quantities exceedmg those specified below: Group A. Substances of 4°, 8°(a), 9°(a), : 1,000 13 °(a) and l 7°(a) kg Group C. Substances of 35 ° 1,000 kg Group E. Substances of 46°(a), 47°(a) and 49°(a) 100 kg Substances of 45 °, 46 ° (b) and (c), 47°(b), 48°, 49°(b), 50° , 2,000 55° 'kg 52000 52103 52104 52105 52117 52118 52119 52120 52121 52122 52127 52128 52129 52170 ' 52171 52172 52199 2306 ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Class 5.2 Section 2 Special requirements to be fulfilled by vehicles and their equipment Insulated, refrigerated and mechanically • refrigerated ve­ hicles Insulated, refrigerated and mechanically • refrigerated vehicles used by reason of the requirements of marginal 52400 shall conform to the following provisions: (a) the vehicle used shall be such and be so equipped as regards its insulation and source of cold that the ma­ ximum temperature prescribed in marginal 52400 is not exceeded whatever the atmospheric conditions may be; (b) the vehicle shall be so equipped that vapours from the substances carried cannot penetrate into the cab; c) a suitable device shall be provided enabling the tem­ perature prevailing in the loading space· to be determined at any time from the driver's cab; (d) the loading space shall be provided with vents or ventilating valves if there is any risk of a dangerous excess pressure arising therein. Care shall be taken where neces­ sary to ensure that refrigeration is not impaired by the vents or ventilating valves; (e) the refrigerant used shall not be inflammable; (f) the refrigerating appliance of a mechanically • refri­ gerated vehicle shall be capable of operating independe­ ntly of the engine used to propel the vehicle. Class 5.2 Section 3 General service provisions (No special provisions) Class 5.2 Section 4 Special provisions concerning loading, unloading and handling Method of despatch and restrictions on forwarding (1) Substances of Group E shall be forwarded in such manner that the ambient temperatures indicated below are not exceeded: substances of 45° : ma- tempe- +10°c ximum rature • • 46°(a) : . -10°c • • 46°(b) and (c) : . • -10°c » • 47°(a) : . • -10°c • » 47°(b) :» • -10°c • • 48° : . • +· 2°c • » 49°(a) : . • -10°C • • 49°(b) • » with· phleg matizer . : » • + 2°c • • with solvent : . • 5°c • 50° : . • 0°c • • 51 ° : . • 0°C • • 52° : . • +20°C » • 53° : . • -10°C • » 54° :» » +20°c » 55° : . • +10°C (2) Where substances of Group E are not carried in me chanically • refrigerated vehicles, the quantity of refrige rant in the protective packaging shall be so proportioned • that the temperatures specified in paragraph (1) above are not exceeded at any time during carriage, which term here includes loading and unloading. 52200-. 52247 52248 52249 52299. 52300 52399 52400 Class 5.2 (3) The use ofliquid air liquid oxygen as a refrigerant is prohibited. ( 4) The temperature of refrigeration shall be so selected as to avoid any danger which might arise from the separa­ tion of phases. Limitation of the quantities carried A transport unit shall not carry more than 750 kg of substances of 46° (a), 47° (a) and 49° (a), no more than 5,000 kg of substances of 45 °, 46° (b) and (c), 4 7 ° (b), 48°, 49°(b), 50° to 53° and 55°, no more than 10,000 kg of substances of 54 °. Prohibition of mixed loading on one vehicle Substances of Class 5.2 shall not be loaded together on one vehicle with: (a) substances or articles of Classes la, lb or le en­ closed in packages bearing a label or two labels confor- • ming to model No. l; with (b) substances of Classes 3, 4.1 or 4.2 enclosed in pac­ kages bearing two labels conforming to models Nos. 2A, 28 or 2C: or with (c) liquids of Class 8 enclosed in packages bearing two labels conforming to model No. 5. Cleaning before loading . Vehicles for the carriage of packages contammg substances of Class 5.2 shall be carefully cleaned. Handling and stowage (1) Packages containing substances of Class 5.2 shall be loaded in such a manner that they can be unloaded one by one at the point of destination without its being necessary to rearrange the load. (2) Packages containing substances of Class 5.2 shall be kept upright and be so secured and fixed that they cannot overturn or fall. They shall be protected against any da­ mage which might be caused by other packages. Class 5.2 (3) The use of readily inflammable mate.rials for stowing packages in vehicles is prohibited. (4) Packages containing substances of Group E shall not be placed on top of other goods; in addition,. they shall be so stowed as to be readily accessible. (5) Substances of Group E shall be' loaded and unloaded without intermediate storage, and shall in the event of tran­ sloading be transferred directly from one vehicle to ano­ ther. The prescribed maximum temperatures shall not be exceeded during such handling (see marginal 52400 ( 1) Vehicle signs Class 5.2 Section 5 Special provisions concerning the operation of vehicles (1) The provisions of marginal 10500, paragraphs (1) and (6), shall apply to the carriage of dangerous substances of Class 5.2. The provisions of paragraphs (2) to (5) shall apply to substances listed in Appendix 8.5 . (2) Fixed tanks containing or (empty tanks, uncleaned) having contained substances listed in Appendix 8.5 shall in addition bear on both sides and at the rear a. label con­ forming to model No. 3. Halts of limited duration for service requirements During the carriage of substances of 46 ° (a), 4 7 ° (a) and 49° (a), halts for service requirements shall so far as 52400 (contd) 52401 52402 52403 52404 52412 52413 52414 52414 (contd) 52415 52499 52500 52501 52508 . 52509 cl>EK 225 E<l>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) 2ao, possible not be made near inhabited places or places of re­ sort. A halt near such a place may not be prolonged except with the agreement of the competent authorities. The same rule shall apply where one transport unit is loaded with more than 2,000 kg of substances of 45 °, 46° (b) and (c), 48°, 49° (b) and 50° to 55°. Class 5.2 Section 6 Transitional provisions, derogations and provisions peculiar to certain countries (No special provisions) Carriage in bulk Class 6.1 Toxic substances Section 1 General (1) Substances of 41° and 73° may be carried in bulk as a complete load. (2) Substances of 41 ° shall be carried in closed or sheeted vehicles and those of 73° in open, sheeted or movable-roof vehicles Carriage in containers Fragile packages within the meaning of marginal 10 102 (1) may not be carried in small containers. Carriage in tanks ( 1) The following substances may be carried in fixed tanks or in demountable tanks: (a) the highly toxic substances listed by name in 1 ° (b) to 5°; (b) the toxic substances, carried ·in the liquid state, of 11 °(a); 12°, (b) to (e); l3°(b); 14°; 52°; 81 °(a); and 82°(a); and substances assimilable to them; (c) the other toxic and harmful substances carried in the liquid state, of 11° to 13°; 21° to 23°; 31°, (b) and (c); 32° (b); 61 °; 62°; 81 ° to 83°; and substances assimi­ lable to them; and (d) the powdery or granular toxic and harmful substan­ ces of 21° to 23°; 31° (a); 41°; 62°; 71° to 75°; 82° to 84°; and substances assimilable to them. (2) The following substances of marginal 2601 may be carried in tank-containers: Acrylonitrile (2°(a)), acetronitrile (methyl cyanide) (2°(b)), aqueous solutions of ethyleneimine (3°), ally! chlo­ ride (4°(a)), methyl chloroformate (4°(b)), ethyl chlorofor­ mate (4°(c)), 2-cyanopropane-2-ol (acetone cyanchydrin) (11 °(a)), aniline (11 ° (b)), l-chloro-2,3-epoxypropane ( epichlorohydrin) (l2°(a)), 2,2-dichlorodiethyl ether (chlo­ roethyl ether, 2-chloroethyl ether) (12°(f)), ally! alcohol (13 ° (a)), dimethyl sulphate ( 13 ° ( d) ), phenol ( 13 ° ( c) ), lead alkyls (14°), 2-bromophenylacetonitrile (bromobenzyl cya­ nide) (21 °(a)), phenylcarbylamine chloride (21 °(b)), 2,4 diisocyanatotoluene (21 °(c)), and its mixtures with 2,6 diisocyanatotoluene (which are assimilated to it), ally! iso­ thiocyanate (21 °(d)), chloroanilines (21 °(e)), mononitroa­ nilines and dinitroanilines (21 °(f)), naphthylamines (21 °(g)), 2,4-diaminotoluene (21 °(h)), dinitrobenzenes (21 °(i)), chloronitrobenzenes (21 °(k )), mononitrotoluenes (21 °(1)), dinitrotoluenes (21 °(m)), nitroxylenes (21 °(n)), toluidines (2l°(o)), xylidines (2l0(p)), cresols (22°(a)), xy­ lenols (22°(b)), xylyl bromide (23°(a)), phenacyl chloride (w-chloroacetophenone) (23°(b)), phenacyl bromide (w­ bromoacetophenone) (23°(c)), 4-chloroacetophenone (me­ thyl p-chlorophenylketone) (23°(d)), symmetrical dichloro­ acetone (23°(e)), solutions of inorganic cyanides (31 °(b)), ethylene dibromide (symmetrical dibromoethane) (61 °(a)), 52510 52599 52600 60999 61000 61 110 61111 61112 61 117 61 118 61119 61 120 61121 and carbon tetrachloride, chloroform and methylene chlo­ ride (which are assimilated to it), methyl chloroacetate (61 °(e)), ethyl chloroacetate (61 °(f)), benzyl chloride (61 °(k)), benzene trichloride which is assimilated to syb­ stances of 62°, and substances and preparations used as pesticides (81 °- 83°). Tanks The outside of the tanks must not be contaminated with toxic substances.· Empty tanks (1) To be accepted for carriage, empty-fixed tanks and empty demountable tanks must not be contaminated on the outside with toxic substances; they shall be closed in the same manner and leak-proof in the same degree as though they were full. (2) For tank containers, see marginal 212 177. (3) Empty demountable tanks and empty tank­ containers of 91 °, if forwarded otherwise than as a full load, shall bear labels conforming to model No 4 (see Annex A, Appendix A. 9). Crews of vehicles: Supe rvision (1) A driver's assistant shall be carried on every tran­ sport unit carrying more than one metric ton of substances of Class 6.1 1° to 5° and 14°, or more than 250 kg of fragile packages containing these substances. (2) The provisions of paragraph 10 1 71 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: The substances of 1 °- 5° 1,000 kg The substances of ll 0{a), 12°(a),, (b) and (d), 13° (a) and (b), 14° a:nd 81 ° 5,000 kg Instructions in writing Where substances of 14°, or receptacles which have contained them, are carried, the text of the written in­ structions shall specify, inter alia, the following: «(A) Precautions to be observed The substance being carried is highly toxic. In the event of leakage from one of the receptacles the following pre­ cautions should be taken: 1. avoid: (a) contact with the skin; (b) inhalation of vapours; (c) introduction of the liquid into the mouth; 2. when drums which are torn open or damaged or wetted with liquid are being handled, the use of 'the follo­ wing is compulsory: (a) respirators; (b) gloves made of rubber or some suitable plastics ma­ terial; ( c) boots made of rubber or some suitable plastics mate rial. , • • • In "the event of a serious accident involving obstruction of the public highway, it is essential that persons arriving to clear the site should be warned of the danger incurred. (B) Action to be taken All practicable steps, including the use of the notices .referred to in marginal 61 260, shall be taken to keep persons at a distance of not less than 15 metres from the site of the accident; the notices contained in the equipment box shall be set up round the enclosure and onlookers shall be kept away. The respirators, gloves and boots will enable one person to approach the load and verify its condition .. Should any of the· drums be tom op~n, the following should be done: (a) additional respirators, gloves and boots with which to equip the worker should be procured urgently; (b) drums still intact should be set aside; ( c) the liquid spilled on the vehicle or on the ground should be noutralized by copious swilling with an aqueous 61122 61 126 61127 61128 61129 61 170 61 171 61172 61 184 61185 2308 E<l>HMEPII: THI: KYBE.PNHI:EQI: (TEYXOI: nPQTO) solution of potassium permanganate (a neutralizing agent a bottle of which is kept in the equipment box); the solution is easily prepared by stirring 0.5 kj-1 ?f permanganate w ith 15 litres of water in a bucket; swillmg should be earned out several ·times, because it takes 2 kg of potassium permanganate to neutralize completely 1 kg of the substance being carried. . Where practicable, the best way to decontaminate the area is to pour petrol over the spilled fluid and ignite it. (C) Important notice In case of acciden·t, one of the first steps which must be taken is to notify by telegram or telephone . . . (insert here the addresses and telephone numbers of the establi • shments to be notified in each of the countries in whose • territory carriage is to take place). A vehicle which has been contaminated with the substance carried shall not be put back into service until it has been decontaminated under the supervision of a competent person. Any wooden parts of the yehicle which have been attacked by the substance carried shall be removed and burnt.» Section 2 . Special requirements to be fulfilled by vehicles and their equipment Fire-fighting appliances The provisions of marginal 10 240 (l)(b) and (3) shall not apply to the carriage of dangerous substances of Class 6.1. Electrical equipment (1) The provisions of Appendix B.2, marginal 220 000, shall not apply to the carriage of dangerous substances of Class 6.1. (2) However, vehicles carrying liquids of 1 4° in fi~ed tanks or in demountable tanks shall be fitted with a switch enabling the entire electric circuit to be opened (cut-out switch). The switch shall be situated near the storage batteries. The electrical equipment shall satisfy the pro • visions of marginal 220 000 (2)(c) 2. Special equipment Whenever substances of 14° or receptacles having co­ ntained them are carried, the driver shall, when he is given the transport document, at the same time be given a portable equipment box fitted with a handle and contai ning: three copies of the written instructions specifying the action to be taken in the event of an i:.ccident or incident occurring during carriage (see marginal 61 185); two pairs of gloves and two pairs of boots made of . rubber or some suitable plastics material; two respirators 'with an activated-charcoal cartridge of 500 cm3 capacity; a bottle (made of bakelite, for example) containing 2 kg of potassium permanganate and bearing the inscrip­ tion «dissolve in water before use»; Class 6.1 61186 61199 61200 61239 61 240 61 241 61 250 61 251 61 252 61 259 61260 six fibreboard notices bearing the inscription «DAN - 61260 GER - volatile poison spilled. Do not approach without respirator» in the language or languages of each of the countries in whose territory carriage takes place. This equipment box shall be kept in the driver's cab in a place where it can easily be found by the decontamina­ tion team. Section 3 General service provisions Action to be taken in the event of accident 61261 61299 61300 61301 61302 (See marginal 61 185) Precautions with respect to articles of consumption In vehicles and at places of loading, unloading or tran­ sloading, dangerous substances of Class 6.1 shall be kept from foodstuffs and other articles of consumption. Portable lighting apparatus The provisions of marginal 10353 shall not apply. Prohibition of smoking The provisions of marginal 103 7 4 shall not apply . Section 4 Special provisions concerning loading, unloading and handling Method of despatch and restrictions on forwarding The substances referred to under 2° (a) (acrylonitrile) and 61° (1) (l-chloro-1-nitropropane) may be carried in non-returnable metal drums [see marginal 2604(1) (b)2 • and 2623(2)(d)] only as a complete load on open vehicles. Prohibition of mixed loading on one vehicle Substances of Class 6.1 enclosed in packages bearing a label conforming to models Nos. 2A, 4 or 4A shall not be loaded together on one vehicle with substances or articles of Classes la, ib or le enclosed in packages bearing a lab~) or two labels conforming to model No. 1. Places of loading and unloading (1) The following operations are prohibited: (a) loading or unloading substances of 1 ° to 5 °, 13 ° (b) 14° and 81 ° in a public place in a built-up area without special permission from the competent authorities; (b) loading or unloading the said substances in a public place elsewhere than in a built-up area without prior notice thereof having been given to the competent authorities, unless the said operations are justified for serious reasons of safety. (2) If, for any reason, handling operations have to be carried out in a public place, then substances and articles of different kinds shall be separated according to the la­ bels. Cleaning after unloading (1) After unloading, vehicles which have been carrying substances of 41 ° and 73° in bulk shall be copiously swil­ led. (2) A vehicle which has been contaminated with substances of 14° or with a mixture thereof shall not be put back into service until it has been decontaminated under the supervision of a competent person. Any wooden parts of the vehicle which have been attacked by substan­ ces of 14° shall be removed and burnt. Section 5 Special provisions concerning the operation of vehicles Vehicle signs • (1) The provisions of marginal 10500, paragraphs (1) and (6), shall apply tci the carriage of substances of 1 ° to 5°, 11° to 14°, 21° to 23°, 31° to 33°, 41°, 51° to 54°, 61 °, 62°, 81 ° and 82°. The provisions of paragraphs (2) to (5) shall also apply to the carriage of substances listed in Appendix B.5. (2) Whenever substances of 14° are carried, the vehicle shall display on each side a warning notice to the effect that, if any liquid escapes, the grates! caution must be exercised and the vehicle must not be approached without gas-mask, gloves and boots of rubber or of some suitable plastics material. (3) Fixed tanks containing substances listed in Appen­ dix B.5 shall in addition bear on both sides and at the 6130 3 61304 61352 61353 61354 61373 61374 61375 61399 61400 61401 61402 61403 61404 61406 61407 61408 61414 61415 61416 61499 61500 E<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2.309 rear a label conforming to model No. 4. Those containing or (empty tanks, uncleaned) having contained acetonitrile, 2-cyanopropan-2-ol (acetone cyanohydrin), ally! chloride or acrylonitrile shall in addition bear labels conforming to model No. 2A. Halts of limited duration for service requirements Halts for service requirements shall so far as possible not be made near inhabited places or places of resort. A halt near such a place may not be prolonged except with the agreement of the competent authorities. Protection against action of sun During the period April to October inclusive, when a vehicle carrying hydrocyanic acid [l 0(a)] is stationary the packages shall, if the legislation of the country in which the vehicle is halted so requires, be effectively protected against the action of the sun, e.g. by means of sheets placed not less than 20 cm above the load. Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries Transitional provisions Pursuant to the last sentence of article 4, paragraph 2, of the Agreement, vehicles which were in service in the territory of a Contracting Party at the time of the entry into force of the Agreement under article 7, paragraph' 1, or were put into service there within two months after its entry into force, may be used for the international carriage of substances of 14° only during a period of two years from such entry into force if their design and equipment do not fully satisfy the requirements laid down in this Annex for such carriage. Class 6.2 . Repugnant substances and substances liable to cause infection Section 1 General Application of Chapter 1 of this Annex The only provisions of this Annex other than those of Sections 1 to 6 below which apply to the carriage of dangerous substances of Class 6.2.are those of marginals· 10001, 10100, 10102, 10111, 10118, 1018l(l)(a), 10404, 10405, 10413, 10414, 10415 and 10419. Carriage in bulk (1) Substances of 1 °, 2°, 3° and 5° may be carried in bulk. Substances of 9° may not be carried otherwise than in bulk. (2) When they are in bulk (a) substances of 1 °(a) and (c~ and 2 ° shall ~ loade~ on to specially fitted covered vehicles equipped with venti­ lating installations. During the months from November to February these substances may also be loaded on to.open vehicles on condition that they been sprayed with suitable disinfectants to remove their bad odour; (b) the following shall be loaded on t~ ope? vehic~e~; substances of 1 °(b ), after being sprayed with suitable dism­ fectants to remove their bad odour; substances of 3°; substances of 5°, after being sprayed with limewash so that no putrid odour is discernible; and substances of 9°. 61501 61508 61509 61510 61514 61515 61516 61599 61.600 61.604 61605 61606 61999 62000 62099 62100 62101 62110 62111 Class 6.2 . (3) In addition, when they are loaded on to open vehic­ les, they shall be covered with: (a) a sheet impregnated with suitable disinfectants and itself covered with a second sheet: substances of 1 °(a) and (c) and 2°; (b) a sheet or tarred or bituminized fibreboard (and sprayed with suitable disinfectants): fresh horns, cla·ws, hoofs or bones [ 1 °(b) ]; (c) a sheet: substances of 3°, unless they are sprayed with suitable disinfectants to prevent any bad odour; and (d) a sheet: substances of 9°. Carriage in containers The carriage of substances of 9° in small containers is prohibited. • Crews of Vehicles; Supervision The provisions of marginal 101 71 (2) shall not apply. Class 6.2 Section 2 Special requirements to be fulfilled by vehicles and their equipment (No special requirements) Class 6.2 Section 3 General service provisions Precautions with respect to articles of consumption ✓.,.. In vehicles and at places of loading, unloading and transloading, dangerous substances of Class 6.2 other than substances of 7° and than substances of 8 ° packed in conformity with the provisions of Annex A, marginal 2659 (2) (a) or (b), shall be kept away from foodstuffs and other articles of consumption. Class 6.2 Section 4 Special provisions concerning loading, unloading and handling Prohibition of mixed loading on one vehicle Substances of 9° and 10° shall not be loaded together on one vehicle with dangerous substances of Class 5.2. Cleaning after unloading After unloading, vehicles which have been carrying substances of Class 6.2 in bulk shall be copiously swilled and treated with suitable disinfectants. Class 6.2 Section 5 Special provisions concerning the operation of vehicles (No special provisions) Class 6.2 Section 6 Transitional provisions, derogations and provisions peculiar to certain countries (No special provisions) 62111 62112 62117 62118 62119 62170 62171 62172 62199 62200 62299 62300 62302 '62303 62304 62399 62400 62402 62403 62404 6241!1 62415 62416 62499 I 62500 62599 • 62600 70999 2:3LO E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Class 7 Radioactive Substances Section 1 General Carriage For details see the relevant schedule in marginal 2 7 03. Crews of vehicles: supervision The provisions of marginal 10171 (2) shall apply to a!l substance~, in whatever quantity. However, the provi­ sions of margmal 101 71 (2) need not be applied where: (a) the loaded compartment is locked and the packages carried are otherwise protected against any illicit unloa­ ding, and (b) the dose rate does not exceed 0.5 mR/h at any accessible point on the surface of the vehicle. Provisions Class 7 Section 2 Special requirements to be fulfilled by vehicles and their equipment For details see the relevant schedule in marginal 2703. Section 3 General Service Provisions Provisions For details see the relevant schedule in marginal 2703. Prohibition of smoking The provisions of marginal 103 7 4 shall not apply. Section 4 Special provisions concerning loading, unloading and handling Provisions For details see the relevant schedule in marginal 2703. Section 5 Special provisions concerning the operation of vehicles Vehicle signs (1) Marginal 10500 shall not apply. (2) Every road vehicle carrying radioactive substances shall bear on the outside of each side wall and of the rear wall a label conforming to the model shown in Appendix B.4, marginal 240010. If loading is done by the sender, it shall be his duty to affix these labels to the vehicles. Parking of a vehicle constituting a special danger (See, in addition to marginal 10507, marginal 3695 of Appendix A.6). Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries (No special provisions). Class 8 Corrosive substances Carriage in bulk Section 1 General (1) Lead sludge containing sulphuric acid [l O (e)] and 71000 71001 71170 71171 71172 71199 71200 71201 71299 71300 · 71301 71373 71374 71375 71399 71400 71401 71499 71500 71501 71506 71507 71508 71599 71600 80999 81000 81110 81111 bisulphates (13°) may be carried in bulk as a full load. (2) For such carriage, the body of the vehicle shall be lined with lead or with a sufficient thickness of paraffin­ waxed or tarred fibreboard, and if the vehicle is sheeted the sheet shall be so placed that it cannot touch the load. 81112 • -81117 Carriage in containers 81118 (1) Fragile packages within the meaning of marginal 10102 (1) and those containing dangerous substances of 1 ° to 7°, 9°, 14°, 33° and 41 • shall not be carried in small containers. (2) Small containers used for the carriage of bisulphates (13°) in bulk shall be lined with lead or with a sufficient thickness of paraffin waxed or tarred fibreboard. (3) The carriage in bulk in small containers of lead sludge containing sulphuric acid of 1 ° (e) is prohibited. 81119 81120 Carriage in tanks 81121 (1) All substances of marginal 2801 or covered by a collective heading may, if their physical state so permits, be carried in fixed tanks or in demountable tanks. (2) these same substances may also be carried in tank­ containers. However, hydrogen fluoride (anhydrous hyd­ rofluoric acid) [6° (a)] may not be carried in tank­ containers of a cubic capacity exceeding 1 m3. (3) The following may be carried in reinforced-plastics tanks comforming to the provisions of Appendix B. lc: substances of 1 ° (b), (c) and (d) and 2° (b) and (c), solutions of hydrochloric acid of 5°, and substances of 32°, 3 7• and 41°. Class 8 Empty tanks (1) Empty fixed tanks and empty demountable tanks of 51 ° shall be closed in the same manner and leak-proof in the same degree as though they were full. Fixed tanks which have contained bromine (14°) shall be hermetically closed. (2) For tank-containers, see marginal 212177. (3) Tank-containers and demountable tanks which have contained hrdrofluoric acid (6°) or dromine (14°) shall bear a label conforming to model No.5 (Appendix A. 9). They shall have no traces of acid or bromine on the outside. Crews of vehicles; Supervision (1) A driver's assistant shall be carried on every tran­ sport unit carrying more than 250 kg of dangerous substances of Class 8 in fragile packages, or more than three metric tons of substances of 6°, 7° 11 • 14° 22° 31°, 32° and 37°. ' ' ' ' (2) The provisions of marginal 10171 (2) shall apply only to the dangerous goods listed below in quantities exceeding those specified below: Chlorosulphonic acid, chlorides and oxychlorides of sulphur, and silicon tetrachloride, of 11 • (a), antimony pentafluoride of 15° (b), bromine trifluoride and bromine pentafluoride of 15° (d), acetyl chloride, acetyl bromide and benzoyl chloride of 22°, and hydrazine in aqueous solutions containing not more than 72% hydrazine, of 34°: 10.000 kg. Bromine of 14°: 1.00 kg. 81122 81127 81128 81129 81170 81171 81172 81199 E<l>HMEPlr THr KYBEPNHrEQr (TEYXOr nPQTO) 2;:11 Class 8 Section 2· Special requirements to be fulfilled by vehicles and their equipment 81200 81239 Fire-fighting appliances 81240 The provisions of marginal I 02 40 (I) (b) and (3) shall not apply to the carriage of dangerous substances of Class 8 other than those of 2° (a) and 3° (a) . 81241 81250 Electrical equipment 81251 The provisions of Appendix B.2,' marginal 220000, shall not apply to the carriage of dangerous substances of Class 8 other than those of 2° (a) and 3° (a). Class 8 Section 3 General service provisions Portable lighting apparatus The provision of marginal 10353 shall not apply. Prohibition of smoking The provisions of marginal 103 7 4 shall not apply. Class 8 Section 4 Special provisions concerning loading, unloading, and handling Prohibition of mixed loading on one vehicle (1) Substances of Class 8 enclosed in packages bearing a label or two labels conforming to model No.5 shall not be loaded together on one vehicle with subst~nces or articles of Classes la, lb or le enclosed in packages bearing a label or two labels conforming to model No. L (2) Liquids of Class 8 enclosed in packages bearing two labels conforming to model No.5 shall not be loaded together in one vehicle with: • (a) substances of Classes 3, 4.1 or 4.2 enclosed in packages bearing two labels conforming to models Nos. 2A, 2B or 2C; or with (b) substances of Classes 5.1 or 5.2 enclosed in packa­ ges bearing two labels conforming lo model No.3. 81252 81299 81300 81352 81353 81354 81373 81374 81375 81399 81400 81402 81043 81404 81412 81413 Cleaning before loading Vehicles for the carriage of packages contammg substances of 2° (a) and 3° (a) shall be carefully cleaned and, in particular, cleared of any combustible waste (straw, hay, paper, etc.). Handling and stowage 81414 (1) All packages containing substances of 2° (a) and 3° (a) shall rest on a stout floor, be placed with their openings at the top, and be so wedged that they cannot overturn. (2) The use of readily inflammable materials for stowing such packages in vehicles is prohibited. (3) Fragile packages shall be so wedged so as to prevent any displacement and any spilling of the contents. Class 8 Section 5 Special provisions concerning the operation of vehicles 81415 81499 Vehicle signs 81500 (1) The provisions of marginal 10500, paragraphs (1) • and (6), shall apply to the carriage of substances of 1 ° to 7°, 9°, 11°, 12°, 14°, 15°, 21° (b), (c) and (e), 22°, 31° to 35°, 37° and 41°. The provisions of paragraphs (2) to (5) shall also apply to substances listed in Appendix B.5. (i) Fixed tanks containing or (empty tanks, uncleaned) having contained substances listed in Appendix B.5 shall in addition bear on both sides and at the rear a label conforming to model No.5. Class8 Section 6 Transitional provisions, derogations, and provisions peculiar to certain countries (No special provisions) APPENDICES PROVISIONS COMMON TO THE B. I APPENDICES (I) The scope of application of the various B. l Appen­ dices is as follows: (a) Appendix B.la applies to tanks other than tank containers; \ (b) Appendix B. lb applies to tank-containers; • ( c) Appendix B. le applies to tanks, other than batteries of receptacles and tank-containers, made of reinforced plas­ tics; (d) for receptacles, see the relevant requirements of Annex A (Packages); and ( e) Appendix B. ld. is concerned with the materials and construction of fixed tanks, of demountable tanks, and of shells of tank-containers, intended for the carriage of deeply - refrigerated liquefied gases of Class 2. (2) By derogation from the definition given in marginal 10102 (1), the term «tank» when used alone in Appendix B.la and Appendix B.lc does not cover tank-containers. However, some of the requirements of Appendix B. la may be made applicable to tank-containers by the provisions of Annex B and Appendix B. lb. (3) It is recalled that marginal 10121 ( 1) prohibits the carriage of dangerous substances in tanks except where such carriage is expressly authorized. The B. l Appendices are therefore confined to provisions applicable to tanks or 81501 81599 81600 199999 200000 2312 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) lank-containers used for transport operations which -are expressly allowed. Appendix B.la PROVISIONS CONCERNING FIXED TANKS (TANK-VEHICLES), DEMOUNTABLE TANKS AND BATTERIES OF RECEPTACLES Note: Chapter I sets out the requirements applicable to fixed tanks (tank-vehicles), demountable tanks and batte­ ries of receptacles intended for the carriage of substances of any Class. Chapter II contains special requirements supplemeting of modifying the requirements of Chapter I. Chapter I REQUIREMENTS APPLICABLE TO ALL CLASSES Section 1 General; scope; definitions 200001 211099 These requirements shall apply to fixed tanks (tank- 211100 vehicles), demountable tanks and batteries of receptacles used for the carriage of liquid, gaseous, powdery or gran ular substances. • (1) In addition to the vehicle proper, or the units of 211101 running gear used in its stead, a tank-vehicle comprises one or more shells, their items of equipment and the fit tings for attaching them to the vehicle or to the running gear units. (2) When attached to the carrier vehicle, the demou­ ntable tank or battery of receptacles shall meet the require­ ments prescribed for tank-vehicles. In the following requirements. 211102 (1) (a) «shell» means the tank proper (including the ope­ nings and their closures); (b) «service equipment of the shell» means the filling, dis­ charge, venting, safety, heating and heat-insulating devices al'ld the measuring instruments; (c) «structural equipment» means the reinforcing, faste­ ning, protective and stabilizing members external or internal to the shell; (2) (a) «calculation pressure» means a notional pressure which is used to calculate the thickness of the walls of the shell. It is equal to the test pressure except in relati~n to certain dangerous goods for which a special, higher calc­ ulation pressure is laid down. External or internal reinfor­ cing devices shall not be taken into account in this calcula­ tion; Appendix B.la (b) «maximum working pressure» means the highest of the 211102 following three pressures: 1. the highest effective pressure allowed in the shell during filling (maximum filling pressure allowed); 2. the highest effective pressure allowed in the shell during discharge (maximum discharge pressure al­ lowed); 3. the effective pressure to which the shell is subjected by its contens (including such extraneous gases as it may contain) at the maximum working temperature; (c) «test pressure» means the highest effective pressure ap­ plied during the pressure test of the shell; (d) «filling pressure» means the highest pressure actually built up in the shell when it is being filled under pressure; (e) «discharge pressure» means the highest pressure ac­ tually built up in the shell when it is being discharged under pressure; (3) «Leakage test» or «leakproofness test» means the test which consists in subjecting the shell to an effective internal pressure equal to the maximum working pressure, but not less than 0:2 kg/cm2 (gauge pressure), by a pro­ cedure approved by the competent authority. Section 2 Construction 211103 211119 The materials used shall meet the following require- 211120 ments (1) Shells shall be made of suitable metallic materials . which, unless other temperature ranges are prescribed in the various Classes, shall be resistant to brittle fracture and to fissurizing corrosion under tensile stress between -20 ° C and +50°C. (2) For welded shells only materials of faultless weldabi­ lity and whose adequate impact strength at an ambient temperature of -20°C can be guaranteed, particularly in the welds and the zones adjacent thereto, shall be used. (3) Welds shall be skilfully made and shall afford the fullest safety. With regard to the execution and checking of weld beads, see also marginal 21112 7 (7). Appendix B.la Shells whose minimum wall thicknesses have been de­ . !ermined in accordance with marginal 211127 (3) to (6) shall be checked by the methods described in the definition of the weld coefficient 0.8. (4) The materials of shells, or of their protective linings in contact with the contents, shall not contain substances liable to react dangerously with the contents, to form dan­ gerous compounds, or substantially to weaken the mate­ rial. (5) The protective lining shall be so designed that its lea­ kproofness remains unimpaired whatever the deformation liable lo occur in normal carriage [211127 (l)]. (6) If contact between the substance carried and the ma­ terial used for the construction of theshell entails a prog­ ressive decrease in the thickness of the walls, this thickness shall be increased at manufacture by an appropriate amount. This additional thickness to allow for corrosion shall not be taken into consideration in calculating the thic­ kness of the shell walls. (1) Shells, their attachments and their service and struc.tural equipment shall be designed to withstand wi­ thout loss of contents (other than quantities of gas escaping through any degassing vents): static and dynamic stresses in normal carriage; prescribed minimum stresses as defined in marginals 2 11125 and 211127. (2) In the case of vehicles in which the shell constitutes a stressed self-supporting member, the shell shall be de­ signed to withstand the stresses thus imposed in addition to stresses from other sources. 211120 (contd) 211121 The pressure on which the wall thickness of the shell is 211122 based shall not be less than the calculation pressure, but the stresses referred to in marginal 211121 shall also be taken into account. Unless specially prescribed otherwise in the various 211123 Classes, the following particulars shall be taken into ac count in the design of shells: (1) gravity-discharge shells intended for the carriage of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of not more than 1.1 kg/cm2 (absolute) shall be designed to a calculation pressure of twice the static pressure of the substance to be carried, but not less than twice the static pressure of water; E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Appendix B.la (2) pressure - filled or pressure - discharge shells intended for .the carraige of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of not more than 1.1 kg/cm2 (absolute) shall be designed to a calculation pressure equal to 1.3 times the filling or discharge pressure; (3) shells - whatever their filling or discharge system intended for the carriage of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of not less than 1.1 and not more than 1. 75 kg/cm2 (absolute) shall be designed to a calculation pressure o.f at least 1.5 kg/cm2 (gauge pressure), or 1.3 times the filling or discharge pressure, whichever is the hi­ gher; ( 4) shells - whatever their filling or discharge system intended for the carriage of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of more than 1. 75 kg/cm2 (absolute) shall be designed to a calculation pressure equal to the hi­ gher of the following two pressures: 1.5 times the total pressure at 50°C, less 1 kg/cm2, subject to a minimum of 4 kg/cm2 (gauge); 1.3 times. the filling or discharge pressure. 211123 (contd) Tanks intended to contain certain dangerous substances 211124 shall be provided with special protection which shall be de termined for the various Classes. At the calculation pressure, the stress 6 (sigma) at the 211125 most severely stressed point of the shell shall no·t exceed the material - dependent limits prescribed below. Allo wance shall·be made for any weakening due to the welds. In addition, in choosing the material and determining wall thickness, the maximum and minimum filling and working temperatures should be taken into account. (1) For metals and alloys exhibiting a clearly-defined yield point or characterized by a guaranteed conventional yield stress (Re) (generally 0.2 per cent of residual elonga­ tion and, in the case of austenitic steels, 1 per cent of ma­ ximum elongation): (a) where the ratio Re/Rm is not more than 0.66: (Re = apparent yield stress, or 0.2 per cent proof stress or 1 per cent proof stress in the case of austenitic steels;) Appendix B. la Rm = guarante d minimum tensile strength: 211 125 a~0.75 Re • (b) Where the ratio Re/Rm exceeds 0.66: a~0.5 Rm (2). For Metals and alloys exhibiting no clearly - defined apparent yield stress and characterized by a guaranteed minimum tensile strength R. 6~0.43 Rm (3) For steel, the elongation at fracture shall be not less than 1,000 cletermimined tensile strength in Kg/mm2 but in any case it shall be not less than 16 per cent for fine - grained steels and not less than 20 per cent for other steels. For aluminium alloys the elongation at fract­ ure shall be not less than 12 per cent. 1 1 In the case of sheet metal the axis of the tensile testpiece shall be at right angles to the ditection of rolling. The permanent elonga­ tion at fracture (1 = Sd) shall be measured on a test - piece of circ­ ular cross - section in which the gauge length 1 is equal to five times the diameter d; if test - pieces of rectangular section are used: t~uge length shall be calculated by the formula 1 = S.6Syt· 0 , where F 0 is the initial cross - sectional area of the test piece. Tanks intended for the carriage ofliquids having a flash 211 126 point of or below 55 ° C and for the carriage of inflam­ mable gases shall be connected to all parts of the vehicle by equipotential connexion and shall be capable of being electrically earthed. Any metal contact capable of causing electrochemical corrosion shall be avoided. Shells and their fastenings shall withstand the stresses 211 127 specified in paragraph (1), and the wall thicknesses of shells shall be at least as determined in accordance with paragraphs (2) to (6) below. ( 1) The shelles and their fastenings shall be capable of absorbing, under the maximum permissible load, the follo­ wing stresses: in the direction of travel: twice the total weight; at right angles to the direction of travel: the total weight; vertically upwards: the total weight. vertically downwards: twice the weight. Under the stresses defined above, the stress at the most severely stressed point of the shell and its fastenings shall not exceed the value a defined in Marginal 211 125. (2) The thickness of the cylindrical wall of the shell shall be at least equal to that obtained by the following formula: e= RxD c,2-,.0..,.0 X a X--=A,-- mm, where P = calculation pressure in kg/mm2 ; D = internal diameter of shell in. mm; a = permissible stress, as defined in marginal 211 125 (1), (a) and (b), and (2), in Kg/mm2 ; and A= a coefficient, not exceeding 1, allo~ing for any weake ning due to welds. ,,. The thickness shall in no case be less than that defined in paragrarhs (3) .to (6) below. (3) The walls and ends of shells of circular cross 6 section not more than 1.80 m in diameter, 2 other than those referred to in paragraph (6), shall not be less than 5mm thick if of mild steel3, or of equivalent thickness if .of another metal. If the diameter exceeds 1.80m, this thic­ kness shall be increased to 6 mm if the shell is of mild stell, 3 or to an equivalent thickness if the shell is of another metal. «Equivalent thickness» means the thickness obtained by the following formula: lOxe 0 (4) Where protection of the shell against damage th­ rough lateral impact or overturning is provided, the compe­ tent authority may allow the aforesaid minimum thicknes­ ses to he reduced in proportion to the protection provided; however, the said thicknesses shall not be less than 3 mm in the case of mild steel, 3 or than an equivalent thickness in the case of other materials, for shells not more than 1.80 m in diameter 2 For shells with a diameter exceeding 1.80 m2 the aforesaid minimum thickness shall be incre­ ased to 4 mm in the case of mild steel 3 and to an equivalent thickness in the case of other metal. «Equivalent thickness» means the thickness obtained by the following formula: 2 For shells not of circular cross - section, for example box shaped or elliptical shells, the indicated diameters shall corres­ pond to those calculated on the basis of a circular cross - section of the same area. For such shapes of cross· - section the radius of convexity of the shell wall shall not exceed 2,000 mm at the sides or 3,000 mm at the top and bottom. 3 •Mild steel» means a steel having a minimum breaking strength between 37 and 44 kg/mm2. • 2314 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) lOXe 0 el= ------ 4f (Rm 1XAif'" Note: The following measures or equavalent measures may be adopted to protect the shell against damage: (a) The shell may be provided on both sides, at a height situated between its centreline and its lower half, with protection against lateral impact consisting of a rolled metal girder extending at least 25 mm beyond the extreme outer edge of the shell. This girder shall be of such cross section that if it is of mild steel3 or a stronger material it has a section modulus of at least 5 cm3, the force being directed horizontally and at right angles to the direction of travel. If weaker materials are used, the section modulus shall be increased proportionately to the limits of elonga­ tion. Protection against overturning may take the form of strengthening rings, protective canopies, or transverse or longitudinal members so shaped that in the event of overtu­ rning no damage is caused to the fittings and accessories mounted on the upper part of the shell. (b) There is also protection: 1. Where shells are made with double walls, the space between the latter being evacuated of air. The aggregate thickness of the outer metal wall and the shell wall shall correspond to the minimum wall thickness prescribed in paragraph (3), and the minimum thickness of the wall of the shell it self shall not be less than the minimum thic­ kness prescribed in paragraph (4); 2. where the shells are made with double walls with an intermediate layer of solid materials at least 50 mm thick, the outer wall having a thickness of at least 0.5 mm if it is made of mild steel3 and at least 2 mm if it is made of a plastics material reinforced with glass fibre. Solid foam (with an impact - absorption capacity like that, for examle, of polyurethane foam of about 400 Kg/m3 den­ sity) may be used as the intermediate layer of solid mate­ rial. (5) The thickness of tank shells designed in accordance with marginal 211 123 (1) which either are of not more than 5,000 litres capacity or are divided into leak - proof compartments of not more than 5,000 litres unit capacity may be adjusted to a level which, unless prescribed other­ wise in the various Classes, shall however not be less than the appropriate value shown in the following table: ~ aximum radius capacity of shell Minimum , f carvature of or shell compar- thick'ness (mm) tment shell (m) (ma) . Mild steel ~ ~5.0 3 2 - 3 ~3.5 3 >3.5 but~5.0 4 Where a metal other than mild steel is used, the thic­ kness shall be determined by the equivalence formula given in paragraph (3 ). The thickness of the partitions and surge - plates shall in no case be less than that of the shell. (6) Surge - plates and partitions shall be dished, with a depth of dish of not less than 10 cm, or shall be corruga­ ted, profiled or otherwise reinforced to give equivalent strength. The area of the surge - plate shall be at least 4 This formula is derived from the general formula e =e l o where Rm = 37; A 0 .'.:a 27 for the mild steel of reference; Rm 1 = minimum tensile strength of the metal chosen, in kg/mm2; and A 1 = minimum elongation of the metal chosen on fracture under tensile stress, in per cent. • 70 per cent of the cross - sectional area of the tank in which the surge - plate is fitted. (7) The manifacturer's qualificasion fo~ performing wel­ ding operations shall be one recognized by the· competent authority. Welding shall be performed by skilled welders using a welding process whose effectiveness (including any heat treatments required) has been demonstrated by test. Non - destructive tests shall be carried out by radiog­ raphy or by ultrasound and must confirm that the quality of thewelding is appropriate to the stresses. In determining the thickness of the shell walls in accor­ dance with paragraph (2), the following values 01 the coeffi­ cient lambda ().) should be adopted for the welds: 0.8: where the weld beads are so far as possible inspec­ ted visually on both faces and are subjected· to an non destructive spot check with particular attention to conne­ xions; 0.9: where all longitudinal beads throughout their len­ gth, all connexions, 25 per cent of circular beads, and welds for the assembly o large - diameter items of equip­ ment are subjected to non - destructive shecks. Beads shall be checked visually on both sides as far as possible; 1.0: where all beads are subjected to non-destructive checks and are so far as possible inspected visually on both sides. A weld test-piece shall be removed. • where the competent authority has doubts regarding the quality of weld beads, it may require additional checks. (8) Measures shall be taken to protect shells against the risk of deformation as result of a negative internal pressure. (9) The thermal insulation shall be so designed as not to hinder access to, or the operation of, fi1ling and dis­ charge devices and safety valves. Stability The overall Width of the ground - level bearing surface (distance between the outer points of contact with the ground of the right - hand tyre and the left - hand tyre of same axle) shall be at least equal to 90 per of the height of the centre of gravity of the laden tank-vehicle. In an articulated vehicle the weight on the axles of the load - carrying unit of the laden semi - trailer shall not exceed 60 per cent f the nominaltotal laden weight of the complete articulated vehicle. Section 3 Items of equipment The items or equipment, wherever situated, shall be so arranged as to be protected against the risk of being wrenched off or damaged during carriage or handling. They shall possess a degree of safety adapted to and comparable to that of the shells themselves, and shall in particular: be compatible with the substances carried; and meet the requirements of marginal 211 121. As many operating parts as possible shall be served by the smallest possible number of apertures in the shell wall. The leakproofness of the items of equipment shall be ensured· even in the event of overturning of the vehicle. • Gaskets shall be made of material compatible with the substance carried and shall be replaced as somf as their effectiveness is impaired, for example as a result of ageing. Gaskets ensuring the leakproofness of operating parts needing to be manipulated during normal use of the vehicle shall be so designed and arranged that manipulation of the operating part in which they are incorporated does not damage them. Appendix B.la Every bottom-discharge shell, and in the case of corn- 211131 partmented bottom-discharge shells every compartment, shall be equipped with two mutually independent shut-off devices mounted in series, the first taking the 'form of an cl>EK 225 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) . inlemal stop-valve5 mounted, with its seating, inside the shell and the second that of a sluice-valve or other equiva­ lent device, al each end of the discharge pipe-socket. The internal slop-valve shall be operable from above or from below. If possible, the setting - oppen or closed - of the internal stop-valve shall be capable of being verified from the ground in both cases. The controls of the internal slop­ valve shall be so designed as to prevent any inadvertend opening through impact or unconsidered action. The internal shut-off device must continue to be effective in the event of damage to the external control. The position and/or direction of closure of the sluice­ valves must be clearly apparent. In order to avoid any loss of contents in the event of da­ mage to the external filling and discharge fittings (pipes, la­ teral shut-off devices), the internal slop-valve and its sea­ ting shall be protected against the danger of being wrenched off by external stresses or shall be so designed as to withstand them. The filling and discharge devices (incl­ uding flanges or threaded plugs) and protective caps (if any) shall be capable of .being secured against any inadver tent opening. • The shell or each of its compartments shall be provided with an opening large enough to permit inspection. Shells intended for the carriage of substances all the openings for which are above the surface level of the liquid may be equipped, in the lower part of the body, with a clea­ ning aperture (first-hole). This aperture must be capable of being sealed by a flange so closed as to be leakproof and whose design must be approved by the competef!t authority or by a body designated by that authority. Shells intended for the carriage of liquids having a va­ pour pressure of not more than 1.1 kg/cm2 (absolute) at 50° C shall have a venting system and a safety device to prevent the contents from spilling out if the shell overturns; otherwise they must conform to the requirements of margi nals 211134 or 211135. • Shells intended for the q1rriage of liquids having a va­ pour pressure of not less than 1. 1 and not more than 1. 7 5 kg/cm2 (absolute) al 50° C shall have a safety valve set at not less than l .5 kg/cm3 gauge pressure and which must be fully open al a pressure not exceeding the test pressure; otherwise they must conform to the requirements of mar­ ginal 211135. Appendix B. la • Shells intended for the carriage of liquids having a va­ pour pre,ssure of not less than 1. 75 and not more than 3 • kg/cm2 (absolute) at 50° C shall have a safety valve set al not less than 3 kg/cm2 gauge pressure and which must be fully open at a pressure not exceeding the test pressure; otherwise they must be hermetically closed. 6 No movable parts such as covers, closures, etc., which are liable to come into frictional or percussive contact with aluminium shells intended for the carriage of inflammable liquids having a flash-point of or below 55 ° C or for the carriage of inflammable gases may be made of unprotected corrodible steel. • Section 4 Type approval 211132 211133 211134 ?11135 211136 211137 211139 The competent authority or a body. designated by that 211140 :; Save as may be otherwise provided in the case of shells intended for the carriage of certain crystallizable or highly viscous substances, of deeply refrigerated liquefied gases, or of powdery or granular substances. authority shall issue in respect of each new type of tank a certificate attesting that the prototype tank, including the shell fastenings which it has surveyed, is suitable for the purpose for which it is intended and meets the construction requirements of Section 2, the equipment requirements of Seclion 3 and the conditions peculiar to the Classes of substances carried. The test results, the substances for the carriage of which the tank is approved, and its approval number as a proto­ type shall be recorded in a test report. This approval shall be valid for tanks manufactured ac­ cording to this prototype without modification. Section 5 Tests Tanks and their equipment shall, either together or se­ parately, undergo an initial inspection before being put into service. This inspection shall include a check that the tank conforms to the approved prototype, a check of the design characteristics, an external and internal examination, a hydraulic pressure test at the test pressure indicated on the data plate. and a check of satisfactory operation of the eq­ uipment. Appendix. B.la 211141 211149 211150 The hydraulic pressure test shall be carried out before 211150 the installation of such thermal insulation as may be neces sary. If the shells and their equipment are tested separa tely, they shall be jointly subjected to a leakproofness test after assembly. , Tanks shall undergo periodic inspections at fixed inter- 211151 vals. The periodic inspections shall include an external and internal examination and, as a general rule, a hydraulic pressure test. 7 Sheathing for thermal insulation ;111d the like shall be removed only to the extent required for re­ liable appraisal of the shell's characteristics. The maximum intervals between • periodic inspections shall be six years. In addition, a leakproofness test and a check of the satis­ factory oper•.;ion of all the equipment shall be carried 941 every three years. The tests, inspections and checks in accordance with 211152 marginals 211150 and 211151 shall be carried out by the expert approved by the competent authority. Certificates shall be issued showing the results of these operations. When the safety of the shell or of its equipment may be 211153 impaired as a result of repairs, alterations or accident, an exceptional check shall be carried out by the competent authori ty or by the expert approved by that authority. Section 6 Marking 211154 211159 Every shell shall be fitted with a corrosion-resistant 211160 metal plate permanently attached to the shell in a place re adily accessible for inspection. The following particulars at least shall be marked on the plate by stamping or by any other similar method. These particulars may be engraved directly on the walls of the shell itself, if the walls are so reinforced that the strength of the shell is not impaired: 6 •Hermetically closed shells» means shells whose openings are • hermetically closed and which are not equipped with safety valves, frangible disc or other similar safety devices. Shells ha­ ving safety valves perceded by a frangible disc shall be deemed to be hermetically closed. 7 In special cases, and with 1he agreement of the expert approved by the competent authority, the hydraulic pressure test may be replaced by a pressure test using another liquid or a gas, where such an operation does not entail any danger. E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) Appendix B.la approval number; manufacturer's name or mark; manufacturer's serial number; year of manufacture; test pressure in kg/cm2 cm (gauge pressure); capacity in litres - in the case of multiple-element shells, the capacity of each element; design temperature (only if above +50° C) or below -20° C); date (month and year) of initial test and most recent pe­ riodic test; and stamp of the expert who carried out the tests. In addition, the maximum working pressure allowed shall be inscribed on pressure-filled or pressure-discharge shells. 211160 The following particulars shall be inscribed on the tank- 211161 vehicle itself or on a plate: name of operator; unladen weight; and permissible maximum weight. In addition, tank-vehicles shall bear the prescribed , danger labels. Section 7 Operation 211162 211169 The thickness of the walls of the shell shall not, throu- 2111 70 ghoul its use, fall below the minimum figure prescribed in marginal 211127 (2). Shells shall not be loaded with any dangerous 2111 71 substances· other than those for whose carriage they have been approved. Foodstuffs may not be carried in these shells unless the necessary measures have been taken to prevent any danger to public health. . The following degrees of filling shall not be exceeded m 2111 72 shells intended for the carriage of liquids at ambient tem peratures: . • ( 1) (a) where inflammable substances not presentmg ad­ ditional risks (e.g. toxic or corrosive properties) are loaded in shells with a venting system, with or without safety valves: 100 100 degree of filling-. or ------%of 1 + 0t(50-tF) 1 + 350t capacity; Appendix B.la (b) ~here toxic or corrosive substances, whether or not 2111 72 presenting a fire risk1 are loaded in shells with" a venting system, with or without safety valves: 98 98 degree of filling or ------%of 1 + 350t capa~ity; (c) where low-concentration inflammable substances and low-concentration acids and !yes are loaded in closed .. shells: 97 degree of filling = . . . . . . . . . . . . . . or 1 + 0t{50-tF) 97 ............ % of l + 350t .rapacity; (d) where high-concentration toxic s~bstances and high­ concentration acids and !yes are loaded m closed shells: 95 degree of filling-. or 95 %of 1 + 0t{50-tF) 1 + 350t capacity. (2) In these formulae, 0t represents the mean coeffici~nt of cubic expansion of the liquid between 15° and 50° C, 1.e. for a maximum variation in temperature of 35° C. a is calculated by the formula: a where di and d are the densities of the liquid at 15 ° C and 50° 1t respe~tively and tF is the mean temperature of the liquid at the time of filling. (3) The provisions of paragraph (1) above shall not apply to shells whose contents are, by means of a hea~ng device, maintained at a temperature above 50° C durmg carriage. In such a case the degree of filling at the outset shall be such, and the temperature so regulated, that the shell is not full to more than 95 per cent of its capacity at any tim'e during carriage, and that the filling temperature is not exceeded. ( 4) Where hot substances are loaded, the temperature of the outer surface of the shell or of the thermal insulation shall not exceed 70° ~ during carriage. Appendix B.la Where shells intended for the carriage ofliquids8 are not divided by partitions or surge-plates into sections of not more than 7 .500'litres' capacity, they shall be filled to not less than 80 per cent of their capacity unless they are prac­ tically empty. Shells shall be closed in such a way that the contents cannot run out uncontrolled. The leakproofness of the shell closures, particularly in the upper part of the dip-tube, shall be verified by the sender after the shell has been fil­ led. Where several closure systems are fitted in series, that nearest to the substance being carried shall be closed first. No dangerous residue shall adhere to the outside of shells during carriage, whether they are full or empty. To be accepted for carriage, empty shells must be closed in the same manner and leakproof in the same degree as though they were full. The connecting pipes between independent but inter­ connected shells of a transport unit shall be empty during carriage. • Flexible filling and discharge pipes which are not per­ manently connected to the shell shall be empty during car riage. • Section 8 Transitional measures 211173 211174 211175 21117.6 211177 211178 211179 Transitional measures 211180 Fixed tanks (tan~vehicles), demountable tanks and bat teries of receptacles built before 1 October 1978 and not 8 For the purposes of this provision, substances whose efflux time at 20° C from a DIN cup with a 4-mm orifice does not exceed 10 minutes (corresponding to an efflux time of less than 96 sec. at 20° C from a No. 4 Ford cup, or to less than 2,680 centistokes) shall be deemed to be liquids. E <D H M E P II T H I K~BEPNHIEQI (TEYXOI nPQTO) conforming lo the requirements of this Appendix may, if they were built in conformity with the requirements of • ADR, be used during a period of six years from 1 Octo­ ber 1978. Fixed tanks (tank-vehicles), demountable tanks and batteries of receptacles intended for the carriage of gases of Class 2 may however be used for 12 years from the same date if the periodic-test requirement is complied with. • On the expiry of this period the aforesaid units may be 211181 kept in service if the equipment of the shell meets the pre sent requirements. The thickness of the shell wall, except in the case of shells intended for. the carriage of gases of Class 2, 7° and 8°, shall be appropriate to a calculation pressure of not less than 4 kg/cm2 (gauge pressure) in the case of mild steel and of not less than 2 kg/ cm2 (gauge pressure) in the case of aluminium and aluminium alloys. For other than circular cross-sections of tanks, the dia meter to be used as a basis for calculation shall be that of a circle wliose area is equal to that of the real cross-section of the tank. Appendix B.la The periodic tests. for fixed tanks (tank-vehicles), de­ mountable tanks and batteries of receptacles kept in ser­ vice under these transitional provisions shall be conducted in accordance with the provisions o(Section 5 and with the pertinent special provisions for the various Classes. Unless the earlier provisions prescribed a higher test pressure, a test pressure of 2 kg/cm2 (gauge pressure) shall suffice for aluminium shells and aluminium-alloy shells. ~11182 211183 Fixed tanks (tank-vehicles), demountable tanks and bat­ teries of receptacles which meet these transitional provi­ sions may be used during a period of 15 years from 1 Oc­ tober 1978 for the carriage of the dangerous goods for which they have been approved. This transitinal period shall not apply to fix'ed tanks (tank-vehicles), demountable tanks and batteries of receptacles intended for the carriage of substances of Class 2, or to fixed tanks (tank-vehicles), demountable tanks and batteries of receptacles whose wall thickness and items of equipment meet the requirements of this Appendix. 211184 211199 Appendix B.la Chapter II SPECIAL REQUIREMENTS SUPPLEMENTING OR MODIFYING THE REQUIREMENTS OF CHAPTER I Class 2 Gases: compressed, liquefied or dessolved· under pressure Section 1 General: scope: definitions Section 2 Construction Shells intended for the carriage of substances of lo to 6° and 9° shall be made of steel. By derogation from marginal 211125(3), a minimum elongation at fracture of 14 per cent may be accepted in the case of weldless shells. The requirements of Appendix B. l d, marginals 214250 to 214285, shall apply to the materials and· construction of shells intended for the carriage of gases of 7o and 80. Shells intended for the carriage of chlorine or phosgene [3°(at)] shall be designed for a pressure of at least 22 Kg/cm (gauge pressure). Section 3 Items of equipment The discharge pipes of shells shall be capable of being closed not only by the devices prescribed in marginal 211131 but in addition by means of a blank flange or some other equally reliable device.· 211200 2112 l <J '2.H'HO 211221 211222 211223 211229 211230 Shells intended for the carriage of liquefied gases may 211231 be provided with, in addition to the openings prescribed • in marginal 211131, openings for the fitting of gauges, including pressure gauges, and thermometers and with bleed holes, as required for their operation and safety. Safety devices shall meet the following requirements: 211232 (1) Filling and discharge openings of shells intended for the carriage of liquefied inflammable and/ or toxic gases shall be equipped with an instant-closing internal safety device which closes automatically in the event of an inadvertent movement of the tank. It must also be possible to close the device by remote control. (2) All openings, other than those accommodating safety valves and than closed bleed holes, of shells intended for the carriage of liquefied inflammable and/or toxic gases shall, if their nominal diameter is more than 1.5 mm, be equipped with an internal shut-off device. (3) By derogation from the provisions of paragraphs ( 1) • and (2), shells intended for the· carriage of deeply­ . refrigerated inflammable and/or toxic liquefied gases may be equipped with external devices in place of internal devices if the external devices afford protection at least equivalent to that afforded by the wall of the shell. ( 4) If the shells are equipped with gauges, the latter shall not be made of a transparent material in direct contact with the substance carried. If there are thermome­ ters, they shall not project directly into the gas or liquid through the shell wall. (5) Shells intended for the carriage of chlorine or sulphur dioxide [3° (at)] or methyl mercaptan or hydrogen sulphide [3° (bt)] shall not have any opening below the surface level of the liquid. In addition, cleaning apertures ( fist-.holes) as referred to in marginal 21113 2 shall not be permitted. (6) Filling and discharge openings situated in the upper. part of shells shall be. equipped not only with what is. prescribed in paragraph (1), but in addition with a second, external, closing device. This device shall be capable of being dossed by a blank flange or some other equally reliable device. Safety valves shall meet the following requirements: 211233 ( 1) Shells intended for the carriage of gases of 1 ° to 6° and 9° may be provided with not more than two safety valves whose aggregate clear cross-sectional area of pas­ sage at the seating or seatings shall be not less than 20 cm2 per 30 m3 or part there of of the receptacle's capacity. These valves shall be capable of opening automatically at a pressure of between 0. 9 and 0.1 times the test pressure of the shell to which they are fitted. They shall be of such a type as to resist dynamic stresses, including liquid surge. The use of dead-weight or counter-weight valves is prohibi­ ted. Shells intended for the carriage of gases of 1 o to 9o harmful to the respiratory organs or entailing a poison risk'' shall not have safety valves unless the safety valves are preceded by a frangible disc. In the latter case the arrangement of the frangible disc and the safety valve shall be required to be satisfactory to the competent autho­ rity, Where tank-vehicles are intended for carriage by sea, the provisions of this paragraph shall not prohibit the fitting of safety valves conforming to the regulations gover­ . ning that mode of transport. (2) Shells intended for the carriage of gases of 7 o and 80 shall be equipped with two independent safety valves, each so designed as to allow the gases formed by evapora­ tion during normal operation to escape from the shell in such a way that the pressure does not at any time exceed by more than 10 per cent the working pressure indicated on the shell. One of the two safety valves may be replaced by a frangible disc which shall be such as to burst at the test pressure. I.n the event of loss of the vacuum in a 9 Gases identified by the letter «t» in the list of substances are deemed to be gases harrriful to the respiratory organs or entailing a poison risk. 2318 ECl>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) double-walled shell, or of destruction of 20 per cent of the insulation of a single-walled shell, the safety valve and the frangible disc shall permit an outflow such that the pressure in the shell cannot exceed the test pressure. (3) The safety valves of shells intended for the carriage of gases of 7° and 8° shall be capable of opening at the working pressure indicated on the shell. They shall be so designed as to function faultlessly even at their lowest working temperature. The reliability of their operation at · that temperature shall be established and checked either by testing each valve or by testing a specimen valve of each design-type. Thermal insulation 211234 ( 1) If shells intended for the carriage of liquefied gases of 3° and 4° are equipped with thermal insulation, such insulation shall consist of either: a sun shield covering not less than the upper third but not more than the upper half of the shell surface and separated from the shell by an air space at least 4 cm across; or a complete cladding, of adequate thickness, of insula­ ting materials. (2) Shells intended for the carriage of gases of 7° and 8° shall be thermally insulated. Thermal insulation shall be ensured by means of a continuous sheathing. If the space between the shell and the sheathing is exhausted of air (vacuum insulation), the protective sheathing shall be so designed as to withstand without deformation an external pressure of at least 1 kg/cm2 (gauge pressure). By derogation from marginal 211102(2), external and internal reinforcing devices may be taken into account in the calculations. If the sheathing is so closed as to be gas-tight, a device shall be provided to prevent any dange­ rous pressure from developing in the insulating layer in the event of inadequate gas-tightness of the shell or of its items of equipment. The device shall prevent the infiltra­ tion of-moisture into the heat-insulating sheath. (3) Shells intended for the carriage of liquefied gases having a boiling point below -182 ° C at atmospheric press­ ure shall not include any combustible material either in the thermal insulation or in the means of attachment to the frame. The means of attachment of shells intended for the carriage of argon, nitrogen, helium or neon of 7°(a) or hydeogen of 7°(b) may, with the consent of the competent authority, contain plastics substances between the inner and the outer sheath. • For batteries of receptacles (see marginal 2212(1) (c1° 211235 the following conditions shall be complied with: (1) If one of the elements of a multiple-element shell is equipped with a safety valve and shut-off devices arf' provided between the elements, every element shall be so equipped. • (2) The filling and discharge devices may be affixed to a manifold. 10. The provisions of this Appendix are not applicable to frames of cylinders. (3) Each element of a multiple-element shell intended for the carriage of compressed gases of 1 ° and 2° which are harmful to the respiratory organs or entail a poison risk 9 or are inflammable, shall be capable of being isolated by a valve (cock). (4) The elements of a multiple-element shell intenden for the carriage of liquefied gases of 3o to 60 shall be so designed that they can be filled separately and can be kept isolated by a valve capable of being sealed. (5) The following requirements shall apply to demou­ ntable tanks: (a) they shall not be interconnected by a manifold; and (b) if the demountable tanks can be rolled, the valves shall be provided with protective caps. By derogation from the provisions of marginal 211131, 211236 shells intended for the carriage of deeply-refrigerated liq uefied gases need not have an inspection aperture. Section 4 Type approval (No special requirements) Section 5 Tests The materials of shells intended for the carriage of gases of 7 o and 80 shall be tested by the method described in Appendix V.ld, marginals 214275 to 214285. The test-pressure levels shall be as follows: (1) For shells intended for the carriage of gases of lo and 2o: the levels indicated in marginal 2219 (1) and (3). (2) For shells intended for the carriage of gases of 3o and 4o: • (a) if the shells are not more than 1.5 m in diameter, the levels indicated in marginal 2220(2); (b) if the shells are more than 1.5 rri in diameter, the levels 11 indicated below: 11. 1. The prescribed test pressures are: (a) if the shell is equipped with thermal insulation, at least equal to the vapour pressure, reduced by 1 kg/cm2 of the !quid at 60°C, and not less than 10 kg/cm2; (b) 1f the shell is not equipped with thermal insulation at least equal to the vapour pressure, reduced by 1 kg/~m2 of the liqu(d at 65°C, and not less than 10 kg/cm2• (2) !n. view of the high toxicity of phosgene [3o (::it)], the mm1mum test pressure for this gas is fixed at l 5&g/ cm2 if the shell is equipped with thermal insulation and at l 7Kg/cm2 if it is not so equipped. (3) The ~aximum values in Kg/litre prescribed for the degree of fill mg a~e calculated ~s follows: maximum weight of contents per lttre of capac1ty=0.95x specific gravity of the liquid phase at 50°C. 211237 211239 211240 211249 211250 211251 E(J)HMEPI:[ TH:[ KYBEPNH:[EQ:[ (TEYXOr nPOTO) Minimum test Maximum weight pressure for of contents shells per litre Item with without of capacity Description of substance number thermal insulation kg/cm2 kg/cm2 kg Bromochlorodifluoromethane (R 12 Bl) 3 ° (a) 10 10. 1.61 Chlorodifluoromethane (R 22) 3 ° (a) 24 26 1.03 Chloropentafluoroethane (R 115) 3° (a) 20 23 1.08 l-Chloro-2,2,2-trifluoroethane (R 133 a) 3° (a) 10 10 1.18 Dichlorodifluoromethane (R 12) 3° (a) 15 16 1.15 Dichlorofluoromethane (R 21) 3 ° (a) 10 10 1.23 l,2-Dichloro-1,2,2-tetrafluoroethane (R 114) 3 ° (a) 10 10 1.30 Octofluorocyclobutane (RC 318) 3° (a) 10 10 1.34 Ammonia 3 ° (a t) 26 29 0.53. Methyl bromide 3 ° (a t) 10 10 1.51 Chlori ne 3 ° (a t) 17 19 1.25 Hexafluoropropylene (R 216) .3° (at) 17 19 l.ll Hydrogen bromide 3 ° (a t) 50 55 1.20 Nitrogen dioxide NO 2 3°· (at) 10 10 1.30 Phosgene 3 ° (a t) 15 17 1.23 Sulphur dioxide 3 ° (a t) 10 12 1.23 Butane 3 ° (b) 10 10 0.51 I-Butene 3 ° (b) 10 10 0.53 l-Chloro-1.1-difluoroethane (R 142b) 30 (b) 10 . 10 0.99 Cis-2-butene 3 ° (b) 10 , 10 0.55 Cyclopropane 3 ° (b) 16 18 0.53 1,1-Difluoroethane (R 152a) 3 ° (b) 14 16 0.79 lsobutane 3 ° (b) 10 lo 0.49 Isobutene 3 ° (b) 10 10 0.52 . Propane 3° 3b) 21 23 0.42 Propylene 3 ° (b) 25 27 0.43 Trans-2-butene • 3 ° (b) 10 10 0.54 1, 1, 1-Trifluoroethane 3 ° (b) 28 32 0.79. Dime thylamine 3 ° (b t) 10 10 0.59 Dimethyl ether 3 ° (b t) 14 16 0.58 Ethylamine 3 ° (b t) 10 10 0.61 Ethyl Chloride ., 3 ° (b t) 10 10 0.80 Hydrogen sulphide -, 3 ° (b t) 45 50 0.67 Methylamine 3 ° (b t) 10 ll 0.53 Methyl chloride 3 ° (b t) 13 15 0.81 Methyl mercaptan 3 ° (b t) 10 10 0.78 Trimethylamine 3 ° (b t) 10 10 0.56 1,3-Butadiene 3 ° (c) 10 10 0.55 Vinyl chloride 3 ° (c) 10 ll 0.81 Methyl vinyl ether 3 ° (c t) 10 10 0.67 Trifluorochlorethylene (R 1113) 3 ° (c t) 15 17 1.13 Vinyl bromide 3 ° (c t) 10 10 1.37 Mixture F 1 4° (a) 10 11 1.23 Mixture F 2 4° (a) 15 16 1.15 Mixture F 3 4° (a) 24 27 1.03 Mixture of gases R 500 4 °· (a) 18 20 1.01 Mixture of gases R 502 4° (a) ?5 28 1.05 . Mixtures of 19 to 21 per cent by weight dichlorodifluoro- 'I methane (R 12) and 79 to ~l per cent by weight bromo chlorodifluoromethane (R 12 Bl) 4° (a) 10 ll 1.50 Mixtures of methyl bromide and chloropicrin 4 ° (a t) 10 10 1.51 Mixture A (trade name: butane) 4° (b) 10 10 0.50 Mixture AO (trade name: butane) 4° (b) 12 14 0.47 Mixture A 1 4 0 (b) 16 18 0.46 Mixture B 4° (b) 20 23 0.43 Mixture C (trade name: propane) 4° (b) 25 27 0.42 Mixtures of hydrocarbons 4° (b) - 225 0.187 • containing methane - 300 0.244 Mixtures of methyl chloride and methylene chloride 4 ° (b t) 13 15 0.81 Mixtures of methyl chloride and chloropicrin 40 (b t) 13 15 0.81 Mixtures of methyl bromide and ethylene bromide 4 ° (b t) 10 10 1.51 Methylacetylene/propadiene and hydrocarbon mixtures Mixture P 1 4° (c) 25 28 0.49 Mixture P 2 4° (c) 22 23 0.47 Ethylene oxide containing not more than 10 per cent carbon dioxide by weight 4 ° (c t) 24 26 0.73 Ethylene oxide with nitrogen up to a total pressure of 10 kg/cm2 at 50° C · 4° (c t) 15 15 0.78 Dichlorodifluoromethane containing 12 per cent ethylene oxide by weight 4 ° (c t) 15 16 1.09 2320 E<DHMEPII THI KYBEPNHIEQI (TEVXOI nPOTOI Appendix B.la (3) For shells intended for the carriage of gases of 5° and 6°: 211251 (~ontd) (a) if the shells are not sheathed in thermal insulation: the levels indicated in marginal 2220 (3) and (4); (b) if the shells are sheathed in thermal insulation: the levels indicated below: Minimum Maximum weight - test of contents Description of substance item 'pres~ure per litre number of capacity . Kg/cm2 Kg Bromotrifluoromethane (R 13 B 1) 5° (a) 120 1.50 Carbon dioxide 5 ° (a) 190 0.73 225 0.78 Chlcrotrifluoromethane (R 13) 5° (a) 120 0.96 225 1.12 Hexafluorethane (R 116) 5° (a) 160 1.28 200 1.34 Nitrous oxide N 2 O 5° (a) 225 0.78 Sulphur hexafluoride 5° (a) 120 1.34 Trifluoromethane (R 23) 5° (a) 190 0.92 250 0.99 Xenon 5° (a) 120 1.30 Hydrogen chlorid e 5 ° (a t) 120 0.69 Ethane 5° (b) 120 0.32 Ethylene 5° (b) 120 0.25 225 0.36 1, 1-Difluoroethylene 5° (c) 120 0.66 225 0.78 Vinyl fluoride ' 5° (c) 120 0.58 225 0.65 Mixture of gases R 503 6° (a) 31 0.11 42 0.21 100 0.76 Carbon dioxi de containing not more than 35 per cent ethy 6 (c) lene oxide by weight 190 • 0.73 225 0.78 Ethylene oxide containing more than 10 per cent but not more than 50 per cent carbon dioxide by weight 6° (c t) 190 0.66 250 0.75 Appendix B.la ' Where shells sheathed in termal insulation are used 211251 (5) For shells intended for the carriage of gases of 7o and 80: not less than 1.3 times the maximum permitted working pressure, as indicated on the shell, but not less than 3 kg/cm2 (gauge pressure); for shells with vacuum insulation the test pressure shall be not less than 1.3 times the maximum permitted working pressure increased by 1 kg/cm2 • which have been subjected to a test pressure lower than that shown in the table, the maximum weight of the co ntents per litre of capacity shall be su:h that t~e pressut reached in the shell by the substance m questmn at 55 C does not exceed the test pressure stamped on the shel!, In such a case the maximum load allowed shall he prescn bed by the expert approved by the competent authorit~. . (4) For shells intended for the carriage of ammoma dissolved under pressure [9o (at)]: Minimum test Maximum weight pressure of contents Description of substance Item number per litre of capacity ke:/cm2 kg Ammonia dissolved .. under pressure in water with more than 35 per cent but not more than 40 per cent ammonia by 0.80 weight 9o (a t) 10 with more than 40 per cent but not more than 50 per cent ammonai by 9o (a t) 0.77 weight 10 The first hydraulic pressure test shall be carried out 211252 before the thermal imsulation is placed in position. the capacity of each shell intended for the carriage of 211253 gases of 3o to 60 and 9o shall he determined, under the supervision of an expert approved by the competent autho rity, by weighing of volumetric measurement of the qua ntity of water which fills the shell; any error in the measure ment of shell capacity shall be of less than one per cent. Determination by a calculation based on the dimensions of the shell is not permitted. The maximum filling weights allowed in accordance with marginals 2220 (4) and 211251 (3) shall be prescribed by an approved expert. Checking of the welds shall be c;mied out in accordance 211254 with the lambda-coefficient 1.0 requirements of marginal 211127 (7). By derogation from the requiremnts cif marginal 211255 211151, the periodic tests shall take place: (1) every three years in the case of shells intended for the carriage of boron trifluoride [lo (at)], town gas [2o (b t)], hydrogen bromide, chlorine, nitrogen dioxide, sulphur dioxide or phosgene . [3o (at)], hydrogen sulphide [3o (b t)], or hydrogen chlo­ ride [So (at)]; ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2321 (2) every six years in the case of shells. intended for the carriage of other compressed and liquefied gases or of ammonia dissolved under pressure [9o (a t)]; and (3) after six ·years' service and thereafter every twelve years in the case of shells intended for the carriage of gases of 7 o or 80. A leakproofness check shall be performed by an approved expert six years after each periodic test. Leakproofness tests of shells intended for the carriage of gases of lo to 60 and 9o shall be performed at a pressure of not less than 4 kg/cm2 (gauge'pressure). In the case of shells heat-insulated by vacuum, the hydraulic-pressure test and the check of the internal condi­ tion may, with the consent of the approved expert, be replaced by a leakproofness test and measurement of the vacuum. If apertures have been made, on the occasion of periodic inspections, in shells intended for the carriage of gases of 7 o or So, the method by which they are hermetically closed ~fore the shells are replaced in service shall be approved by the approved expert and shall ensure the integrity of the shell. 211256 211257 211258 211259 Section 6 Marking The following additional particulars shall be marked by 211260 stamping or by any other similar method on the plate prescribed in marginal '211160, or directly on the walls of the shell itself if the walls are so reinforced that the strenght of the shell is not impaired: (1) on shells intended for the carriage of only one substance: the name of the gas in full. This indication shall be supplemented in the case of shells intended foi;. the carriage of compressed gases of 1 o and 2o by an indication of the maximum filling pressure at 15°C allowed for the shell, and in the case of shells intended for the carriage of liquefied gases of 3o to 80 or of ammonia dissolved under pressure of 9o (a t) by an indication of the permissible maximum loan in kg and of the filling temperature if below -20°C; (2) on multi-purpose shells: the names, in full, of the gases for whose carriage the shell is approved. . • These particulars shall be supplemented by an indica­ tion of the permissible maximum load in kg for ~ach gas; (3) on shells intended for the carriage of gases of 7o or 80: the working pressure; and (4) on shells equipped with thermal insulation: the inscription «thermally' insulated• or «thermally ins­ ulated by vacuum•. The frame of a multiple-element shell shall bear near 211261 the filling point a plate spycifying: the test pressure of the, elements; . the maximum filling pressure at 15°C allowed for ele ments intended for compressed gases; the number of elements; the aggregate capacity , of the elements in litres • the name of the gas in full; and, in the case of liquefied gases: the permissible maximum load per element, in kg. In addition to the particulars prescribed in marginal 211262 211161, the following 'shall be inscribed either on the tank-vehicle itself or on a plate: (a) either: «minimum filling temperature allowed: 20°C» or «minimum filling temperature allowed: .... •; (b) where the !!,hell is intended for the carriage of one substance the name of the gas in full; for liquefied gase of 3o to 80 and for ammonia dissolved under pressure in water [9o (a t)], the permissible ma­ ximum load in kg (c) where the shell is a multi-purpose shell: the name in full of alf the gases to whose carriage the shell is assigned, with an indication of the permissible maximum load in kg, for each gas; (d) where the shell is equipped with ther~al insulation: the inscription «thermally insulated• or «thermally ins­ ulated by vacuum», in an official language of the forwar­ ding country and also in English, Fr ench or German, unless international road transport tariffs, if any, or agree­ ments concluded between the countries concerned in the transport operation, provide otherwise. The plates on vehicies carrying demountable tanks as referred to in marginal 211235 (5) shall not bear the particulars prescribed in marginals 211161 and 211262. 211262 211263 211264 211269 • Section 7 Operation A shell assigned at different times to the carriage of 211270 different liquefied gases of 3o to 80 (multi-purpose shell) may not carry substances other than those listed in one, and one only, of the following groups: Group 1: halogenated hydrocarbons of3o (a) and 4o (a); Group 2: hydrocarbons of 3o and 4o (b); Groupe 3: ammonia [3o (at)]; dimethyl ether, dimethy­ lamine, ethylamine, methylamine and tpmethylamine [3 (b t)]»; and vinyl chloride [3o (c)]; • Groupe 4: methyl bromide [3o (a t); ethyl chloride and methyl chloride [3o (b t)]; Groupe 5: mixtures of ethylene oxide with carbon dio­ xide and of ethylene oxide with nit rogen [4o (c t)]; Groupe 6: nitrogen, carbon dioxide, rare gases, nitrous oxide N 0; and oxygen [7o (a)]; air, mixtures of nitrogen with rar~ gases, and mixtures of oxygen with nitrogen, alsowhen they con tain rare gases [80 (a)]; Groupe 7: ethane, ethylene, and methane [7o (b)]; and mixtures of methane with ethane, also when they contain propane or butane [80 (b)]. • • Shells which have been filled with a substance of group 211271 1 or group 2 shall be emptied of liquefied gas before being loaded with another substance belonging to the same group. Shells which have been filled with a substance of groups 3 to 7 shall be completely emptied of liquefied gas and then blown down before being loaded with another substance belonging to the same group. The multiple use of shells for the carriage of liquefied 211272 gases of the same group shall be allowed if all the require ments prescribed for the gases to be carried in one and the same shell are observed. Such multiple use shall be subject to approval by an approved expert. The multiple use of shells for the carriage of gases of 211273 different groups shall be allowed if permitted by the appro ved expert. . . When shells are reassigned to gases of adifferent group, the shells shall be completely emptied of liquefied gases, then blown down and, lastly, degassed. The degassing of shells shall be verified and certified by the approved expert. When loaded tanks or empty but uncleaned tanks are 211274 handed over for carriage, only the particulars specified in marginal 211262 applicable to the gas loaded of iuct 2322 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) discharged shall be visible; all particulars concerning other gases shall be covered up. All the element of a multiple 211275 element shell shall contain only one and the same gas. In the case of a multiple-element shell intended for the carriage of liquefied gases, the elements shall be filled separately and be kept isolated by a sealed valve. The maximum filling pressure for compressed gases of 211276 I o and 2o other than boron fluoride shall not exceed the values prescribed in marginal 2219 (2). For boron fluoride [lo (a t)]the maximum filling weight per litre of capacity shall not exceed 0.86 kg. The maximum filling weight per litre of capacity accor­ ding to marginals 2220, (2), (3) and (4), and 211251, (2), (3) and (4), shall be abided by. The degree of filling of shells intended for the carriage 211277 of gases of 7o (b) and 80 (b) shall remain below the level at which, if the contents were .raised to the temperature at which the vapour pressure equalled the valve-opening pressure, the volume of the .liquid would reach 95 per cent of the shell's capacity at that temperature. Shells intended for the carriage of gases of 7o (a) and 80 (a) may be filled to 98 per cent at the loading temperature and the loading pressure. On shells intended for the carriage of nitrous oxide and 211278 oxygen [7o (a)], air, or mixtures containing oxygen [80 (a)], substances containing grease or oil shall not not be used to ensure leakproofness of the joints or for the mai ntenance of the closures. The requirement in marginal 211175 shall not apply 211279 to gases of 7 o and 80. Appendix B.la Class 3 Inflammable liquids Section 1 General! scope; definitions Section 2 Construction 211280 211299 211300 211319 Shells intended for the carriage of carbon disulphide 211320 [l 0(a)] shall designed for a pressure of 10 kg/cm2 (gauge pressure). Section 3 Items of equipment Shells which are fitted with a venting device not capable of being closed and which are intended for the carriage of inflammable liquids having a flash-point not exceeding 55 ° C shall have a flame-trap in the venting device. All openings of shells intended for the carriage of acry­ laldehyde (acrolein), chloroprene (chlorobutadiene) and carbon disulphide [l 0 (a)] shall be above the surface level of the liquid. No piping or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. The openings, other than those equipped with valves, shall be capable of being closed by leakproof dos­ , ures, and the latter shall be capable of being protected 211321 211329 211330 211331 by a locable cap .. If the shells are equipped with safety valves, the latter shall be preceded by a frangible disc. In such a case the arrangement of the frangible disc and the safety valve shall be required to be satisfactory to the competent authority. Section 4. Type approval (No special requirements) Appendix B.la Section 5 • Tests The minimum test pressure to which shells intended for the carriage of carbon disulphide [l 0 (a)] shall be subjected shall be 4 kg/cm2 (gauge pressure). The mi­ nimum test pressure to which shells intended for the car­ riage of the other substances of the Class shall be subjec­ ted shall be equal to that, as defined in marginal 211123, used for their design. Section 6 Marking (No special requirements) Section 7 Operation The following degrees of filling shall not be exceeded when shells filled with liquids having a vapour pressure of more than 1. 75 kg/cm2 (absolute) ~t 50°C are hermeti­ cally-closed shells: in the case of methyl formate [l 0(a)] and other liquids having a coefficient of cubical expansion of more than 150 X 10·5 but not more thant 180 X IO·S: .................. 91 per c«rn.t of capacity; in the case of acetaldehyde [5°] and other liquids having a coefficient of cubical expansion of more than 180 X 10·5 but not more thant.230 X 10·5: ................. 90 per cent of capacity; An aluminium-alloy shell shall not be used for the car­ riage of acetaldehyde [5 °] unless the shell is assigned solely to such carriage and the acetaldehyde is free from acid. • • In the cold season (October to March), light distillates for cracking and other liquid hydrocarbons having a va­ pour pressure not exceeding 1.5 kg/cm2 (absolute) at S0°C may be carried in shells of the type prescribed in marginal 211133. Appendix B.la Class 4.1 Inflammable solids Class 4.2 Substances liable to spontaneous combustion Class 4.3 Substances which give off inflammable gases on contact with water Section 1 General; scope; definitions 211332 211339 211340 211349 211350 211351 211359 211360 211369 211370 211373 211399 211371 211372 211400 211419 <1'€1: '2.'2..S ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2323 Section 2 Construction Shells intended for the carriage of white or yellow phos- 211420 phorus of marginal 2431 1 °, or trichlorosilane (silicochlo roform) of marginal 2471, 4°, shall be designed for a pressure of at least 10 kg/cm2 (gauge pressure). 211421 211429 Section 3 Items of equipment Shells intended for the carriage of sulphur [2°(b)] or 211430 naphthalene [ 11 °( c)] of marginal 2401 shall be equipped with thermal insulation made of materials which are not readily inflammable. They may be equipped with valves opening automatically inwards or outwards under the ef fect of a difference of pressure of 0.2 to 0.3 kg/cm2 • The discharge devices shall be capable of being protected by a lockable metal cap. Shells intended for the carriage of white or yellow phos- 211431 phorus of marginal 2 431, 1 °, shall meet the following req­ uirements: (1) The heating device shall not penetrate into, but shall be exterior to, the body of the shell. However, a pipe used for extracting the phosphorus may be equipped with a heating jacket. The device heating the jacket shall be so regulated as to prevent the temperature of the phosphorus from exceeding the filling temperature of the shell. Other piping shall enter the shell in its upper part; openings shall be situated above the highest permissible level of the phosphorus and be capable of being completely enclo­ sed under lockable caps. In addition, the cleaning apert­ ures (first-holes) referred to in marginal 211132 shall not be permitted. Appendix B.la (2) The shell shall be equipped with a gauging system 211431 for verifying the level of the phosphorus and, if water is used as the protective agent, with 11 fixed gauge mark showing the highest permissible level of the water. The openings and orifices (valves, sleeves, manholes, 211432 etc.) of shells intended for the carriage of substances of marginal 2471, 1° (a), shall be protected by leakproof locable caps, and such shells shall be equipped with ther mal insulation made of materials which are not readily in­ flammable. Section 4 • Type approval (No special requirements) Section 5 Tests· 211433 211439 211440 211449 Shells intended for the carriage of sulphur [2° (b)] or 211450 naphthalene [11 ° (c)] of marginal 2401 or wh!te or yellow phosphorus of marginal 2431, 1 °, and those intended f~r the carriage of trichlorosilane (silicochloroform) of margi nal 2471, 4°, shall be tested at a pressure of 4 kg/cm 2 (gauge pressure). 211451 211459 Section 6 Marking (No special requirements) Section 7 Operation 211460 211469 Shells intended for the carriage of sulphur [2°(b) or 211470 naphthalene [11 ° (c)] of marginal 2401 shall be filled to not more than 98 per cent of their capacity. White or yellow phosphorus of marginal 2431, 1°, 211471 shall, if water is used as the protective agent, be covered with a depth of not less than 12 cm of water at the time of filling; the degree of filling at a temperature of 60°C shall not exceed 98 per cent. If nitrogen is used as the protective agent, the degree of filling at a temperature of 60 ° C shall not exceed 96 per cent. Appendix B.la The remaining space shall be filled with nitrogen in such a way that, even after cooling, the pressure at no time falls below atmospheric pressure. The shell shall be hermetically closed so that no leakage of gas ·pccurs. For the carriage of substances of marginal 24 71, 1-" 211471 (a), caps ·shall be locked in conformity with. marginal 211432. In the case of trichlorosilane (silico~hloroform) of mar- 21] 473 ginal 2471, 4°, the degree offilling shall not exceed 1.14 kg per litre of capacity if filling is by weight or 85 per cent if filling is by volume. . ,.,;. Shells which have contained phosphorus of marginal 2114 7-'f 2431,' l 0 , shall when handed over for carriage either: be filled with nitrogen; the sender shall certify in the transport document that the shell, after closure, is gas­ light; or be filled with water to not less than 96 per cent and not more than 98 per cent of their capacity; between 1 October and 31 March this water shall contain one or more anti-freeze agents free from corrosive action, not liable to react with phosphorus; and in such concentration as to make it impossible for the water to freeze during car­ riage. Class 5.1 Oxidizing substances • Class 5.2 Organic peroxides Section 1 General; scope; definitions Section 2 Construction Shells intended for the carriage in the liquid state of substances referred to in marginal 51121 ( 1) shall be designed for a pressure of at least 4 kg/cm2 (gauge press ure). . . 211475 211499 211500 211519 Shells, and their items of equipment, intended for the 211521 carriage of hydrogen peroxide or of aqueous solutions of hydrogen peroxide of marginal 2501, 1 °, or of liquid organic peroxides of marginal 2551, 1°, 10°, 14°, 15° and 18°, shall be made of aluminium not less than 99.5 per cent pure or of suitable steel not liable to cause the hydrogen peroxide or the organic peroxides to decompose .. • 2324 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Appendix 8.1 a Shells intended for the carriage of concentrated and hot aqueous solutions of ammonium nitrate du marginal 250~, 6° (a), shall be made of austenitic steel. Section 3 Items of equipment Shells intended for the carriage of hydrogen peroxide and of aqueous solutions of hydrogen peroxide containing more than 70 per cent hydrogen peroxide, of marginal 2501, 1 °, shall have their openings above the surface level of the liquid. In addition, cleaning apertures (fist holes) as referred to in marginal 211132 shall not be permitted. In the case of solutions containing more than 60 per cent but not more than 70 per cent hydrogen peroxide, openings below the surface level of the liquid shall be permissible. In this case the shell - discharge system shall be equipped with two mutually independent shut - off devices mounted in series, the first taking the form of a quick - closing internal stop - valve of an approved type and the second that of a sluice - valve, at each end of the discharge pipe socket. A blank flange, or another device providing the same measure of security, shall also be fitted at the outlet of each external sluice - valve. The internal stop - valve shall be such that if the pipe is wrenched off the stop - valve will remain integral with the shell and in the closed posi­ tion. The connexions to the external pipe - sockets of shells shall be made of materials not liable to cause decomposition of hydrogen peroxide. Shells intended for the carriage of hydrogen peroxide or of aqueous solutions of hydrogen peroxide of 1 °, or of conce­ ntrated and hot aqueous solutions of ammonium nitrate of 6° (a), of marginal 2501 shall be fitted in their uppe.r part with a shut - off device preventing any build - up of excess pressure inside the receptacle, any leakage of liquid, and any entry of foreign matter into the receptacle. The shut off devices of shells intended for the carriage of conce­ ntrated and hot aqueous solutions of ammonium nitrate shall be so designed as to preclude obstruction of the de­ vices by solidified ammonium nitrate during carriage. Where shells intended for the carriage of concentrated and hot solutions of ammonium nitrate of marginal 2501, 6° (a), are sheathed in thermally - insulating material, the material shall be of an inorganic nature and entirely free from combustible matter. Shells intended for the carriage of liquid organic peroxides of marginal 2551, 1 °, 10°, 14°, 15° and 18°, shall be equipped with a venting device fitted with a flame - trap and fc:Jlowed in series by a safety' valve opening at a gauge pressure of 1.8 to 2.2 kg/cm2 . Appendix B.la Shells intended for the carriage of liquid oranic pero­ xides of marginal 2551, 1 °, 10°, 14°, 15° and 18°, shall be equipped with thermal insulation complying with the requirements of marginal 211234 (1). The covering and any uncovered part of the shell, or the outer sheathing of a complete lagging, shall be painted white and the paint shall be cleaned before each transport journey and renewed in case of yellowing or deterioration. The thermal insulation shall be free from combustible matter. Section 4 Type approval Section 5 (No special requirements) Tests Shells intended for the carriage of hydrogen peroxide or of aqueous solutions of hydrogen peroxide of 1 °, or of con­ centrated and hot solutions of ammonium nitrate of 6° (a), of marginal 2501, or of liquid organic peroxides of mar­ ginal 2551, 1 °, 10°, 14°, 15 ° and 18°, shall be tested at 211522 211523 211529 211530 211531 211532 211533 211534 211536 211539 211549 211540 211550 a pressure of 4 kg/cm2 (gauge pressure), Section 6 Marking (No special requirements) Section 7 Operation The inside of the shell, and all parts liable to come into contact with substances referred to in marginal 51121, shall be kept clean. No lubricant capable of combining dangerously with the substance carried shall be used for pumps, valves or other devices. Shells intended for the carriage of liquids of marginal 2501, 1 ° to 3 °, shall be filled to not more than 95 per cent of their capacity at a reference temperature of 15 °C. Shells intended for the carriage of hot aqueous solutions of ammonium nitrate of marginal 25Ql, 6° (a), shall be filled to not more than 97 per cent of their capacity, and the maximum temperature after filling shall not exceed 140°c. Appendix B.la Tanks used for the carriage of hot aqueous solutions of ammonium nitrate of marginal 2501, 6° (a), shall not be used for the carriage of other substances without being first carefully cleansed of any residues. Class 6.1 Toxic substances Section 1 General: scope: definitions Section 2 Construction Shells intended for the carriage of hydrocyanic acid sol­ utions of 1 ° (b), or queous solutions of ethyleneimine and propyleneimine of 3 °, or nickel carbonyl of 5 ° (a), shall be designed. for a pressure of at least 15 kg/ cm2 (gauge press­ ure). Shells intended for the carriage of other substances re­ ferred to in marginal 61121 (1), (a) and (b), shall be de­ signed for a pressure of at least 10 kg/cm2 (gauge press­ ure). Shells intended for the carriage of substances referred to in marginal 61121 (1), (c), shall be designed for a pressure of at least 4 kg/cm2 (gange pressure). Shells intended for the carriage of powdery or granular substances shall be designed in accordance with the requi­ rements of the general section of this Appendix. Section 3 Items of equipment All openings of shells intended for the carriage of substances referred to in marginal 61121 (1), (a) and (b), shall be above the surface level of the liquid. No pipirg or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. The openings shall be capable of being hermetically closed, and the closure shall be capable of being protected by a lockable cap. In addi­ tion, cleaning apertures (fist - holes) as referred to in mar­ ginal 211132 shall not be permitted for shells intended for the carriage of aqueous solutions of hydrocyanic acid [l 0 (b)]. Appendix B. la (1) Shells intended for the carriage of substances r~­ ferred to in marginal 61121 ( 1 ), ( c) and ( d), may be of the bottom - discharge type. (2) The bottom - discharge fittings of shells intended for the carriage of the substances referred to in marginal 61121 (1 ), ( c ), shall conform to the requirements of mar 211551 211559 211560 211569 211570 211571 211572 211573 211599 211600 211619 211620 211621 211622 211623 211624 211629 211630 211631 EQ>HMEPII THI KYBEPNHIEOI (TEVXOI nPOTO) 2325 ginal 211131, and in addition the discharge pipes of the shells shall be capable of being closed by a blank flange, a plug, or some other equally effective device. (3) All openings of the shells referred to in paragraph (1) shall be capable of being hermetically closed. If the shells are fitted with safety valves, the latter shall be preceded by a frangible disc. The arrangements of the frangible disc and the safety valve shall be required to be satisfactory to the competent authority. Tanks fitted with safety valves and frangible discs and intended for carriage by sea shall conform to the regula­ tions governing that mode of transport. Protection of equipment . ( 1) Fittings and accessories mounted in the upper part of . the shell Such fittings and accessories shall be either inserted in a recessed housing; or equipped with an internal safety valve; or shielded by a cap, or by transverse and/or longitudinal members, or by. other equally effective devices, so profiled that in the event of overturning the fittings and accessories will not be damaged. (2) Fittings and accessories mounted in the lower part of the shell Pipe - sockets, lateral shut - off devices, and all dis­ charge devices shall either be recessed by at least 200 mm from the extreme outer edge of the shell or be protected by a rail having a coefficient of inertia of not less than 20 cm3 transversally to the direction of travel; their ground clea­ rance shall be not less than 300 mm with the shell full. (3) Fittings and accessories mounted on the rear face of the shell All fittings and accessories mounted on the rear face shall be protected by the bumper prescribed in marginal 10216. Their height above the ground shall be such that they are adequately protected by the bumper. Appendix B. la Section 4 Type approval ~ Tanks approved for the carriage of toxic substances shall not be approved for the carriage of foodstuffs, articles of consumption or animal feeding stuffs. Section 5 Tests Shells intended for the carriage of the substances re­ ferred to in marginal 61121 (1), (a} to (c), shall be tested initially and periodically at a pressure of 4 kg/cm2 (gauge pressure). The periodic tests shall be carried out at intervals of not more than three years in the case of shells intended for the carriage of substances of 14 °. Section 6 Marking (No special requirements) Section 7 • Operation The degree of filling of shells intended for the carriage of substances referred to in marginal 61121 (1), (a) to (d), shall conform to marginal 211172 (1) (d). Shells intended for the carriage of substances of 5 ° (a) and 5 ° (b) shall be filled only to the extent of 1 kg ofliquid per litre of capacity. The openings of the shells shall be hermetically closed during carriage. Tanks used for the carriage of toxic substances shall not be used for the carriage of foodstuffs, articles of consum­ ption or animal feeding stuffs. 211632 211633 211634 211639 211640 211641 211649 211650 211651 211659 211660 2.11669, 211670 211671 211672 211673 211674 211699 Class 7 Radioactive substances Section 1 General; scope; definitions Section 2 Construction Shells intended for the carriage of the substances refer­ red to in marginal 2703, Schedule 5, paragraph 11, shall be designed for a pressure of at le~t 4 kg/ cm2 (gauge presssure). Where the radioactive substances are in solution or suspension in substances of other Classes and the calcula­ tion pressures prescribed for the shells of tanks intended for the carriage of the latter substances are greater, the latter pressures shall be applied. Section 3 Items of eq~ipment Shells intended for the carriage of liquid radioactive substances8 shall have their openings above the surface level of the liquid. No piping or pipe connexion shall pass through the walls of the shell below the surface level of the liquid. Section 4 Type approval Tanks approved for the carriage of radioactive substan­ ces shall not be approved for the carriage of £~stuffs, articles of consumption, animal feeding stuffs, cosmetics or medicaments, or of substances used in the manufactire of these products. Section 5 Tests Shells intended for the carriage of the substances refer­ red to in marginal 2703, Schedule 5, paragraph 11, shall be tested initially and periodically at a pressure of 4 kg/cm2 (gauge pressure). By derogation from the requirements of marginal 211151, the periodic internal inspection may be replaced by a check of the wall thickness by ultrasound, performed every three years. Section 6 Marking (No special requirements) Section 7 Operatio n The degree of filling at the reference temperature of 15 ° C shall not exceed 93 per cent of the total capacity of the shell. Tanks which have been used for the carriage of radioac­ tive substances shall not be used for the carriage of fo­ odstuffs, articles of consumption, animal feeding stuffs, cosmetics or medicaments, or of substances used in the manufactire of these products. Class8 Corrosive ~ubstances Section 1. General; scope; definitions Section 2 Construction Shells intended for the carriage of hydrogen fluoride (anhydrous hydrofluoric acid) (6°(a)], of aqueous solutions of hydrofluoric acid (6° (b)], or of bromine (14°) shall be designed for a pressure of at least 21 kg/ cm2 (gauge pressure). Shells intended for the carriage of bromine shall. be equipped with a lead lining not less than 5 mm thick, or with an equivalent lining. 211700 211719 211720 211721 211722 211729 211730 211731 211739 211740 211741 211749 211750 211751 211752 211759 211760 211769 211770 211771 211772 211799 211800 211819 211820 (8.2.1) 2326 EG>HMEPII: THI: KYBEPNHIEQI: (TEYXOI: nPQTO) Shells intended for the carriage of substances of 1 ° (a), 2° (a), 6° (c), 7° to 9°, 21° (a) and 230 shall be designed for a pressure of at least 10 kg/cm2 (guage pressure). Where the use of aluminium is necessary for shells intended for the carriage of substances of 2° (a), such shells shall be made of aluminium not less than 99.5 per cent pure, in which case, by derogation from the subparag­ raph above, the wall thickness need not exceed 15 mm. Shells intended for the carriage of monochloroacetic acid [21 ° (a)] shall be equipped with an enamel or equiva­ lent lining if the material of the shell is attacked by that acid. Shells intended for the carriage of the substances refer­ red to in marginal 81121 other than those listed in margi­ nals 211820 and 211821 shall be designed for a pressure of not less than 4 kg/cm2 (guage pressure). Shells intended for the carriage of aqueous solutions of hydrogen peroxide (410) shall meet the requirements of marginal 211520. Section 3 Items of equipment All openings in shells intended for the carriage of substances of 6° and of bromine (14°) shall be above the surface level of the liquid; no piping or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. In addition, cleaning apertures (fist­ holes) as referred to in marginal 211132 shall not be permitted. The closures shall be capable of being effecti­ vely protected by a metal cap. The following requirements shall apply to demountable tanks intended for the carriage of hydrogen fluoride (anhydrous hydrofluoric acid) [6° (a)] and of aqueous sol­ utions of hydrofluoric acid [6° (b)]: 1. they shall not be interconnected by a manifold; and 2. if the demountable tanks can be rolled, the valves shall be fitted with protective caps. Shells intended for the carriage of stabilized sulphur trioxide (9o) shall be thermally insulated and be ·fitted with a heating device on the outside. Shells may be of the bottom-discharge type. In this case the shell-discharge system shall be equipped with two mutually independent shut-off devices mounted in series, the first taking the form of a quick-closil}g internal stop-valve of an approved type and the second that of a sluice-valve fitted at the end of the discharge pipe-socket. A blank flange or some other . equally reliable device shall also be fitted to the outlet of each external sluice-valve. Shells and their service equipment intended for the carriage of hypochlorite solutions (3 7°) and of aqueous solutions of hydrogen peroxice (41 °) shall be so designed as to prevent the entry of foreign matter, the leakage of liquid, and any build-up of dangerous excess pressure inside the shell. Section 4 Type approval (No special requirements) Section 5 Tests 211821 211822 211823 211824 211829 211830 211831 211832 211833 211840 211849 Shells intended for the carriage of hydrogen fluoride 211850 . (anhydrous hydrofluoric acid) (6° (a)] and of aqueous sol utions of hydrofluoric acid [6° (b)] shall undergo the initial pressure test and the periodic tests at a pressure of 10 kg/cm2 (gauge pressure), and those intended for the car riage of the other substances referred to in marginal 81121, if those substances are carried in the liquid phase, at a pressure of 4 kg/cm2 (ga1:1ge pressure). The pressure test of shells intended for the carriage of 211851 hydrogen fluoride (anhydrous hydrofluoric acid) [6°(a)] and of aqueous solutions of hydrofluoric acid [6° (b)] shall be repeated every six years and shall be accompanied by an internal inspection of the shells and a check of their items of equipment. In addition, every two years the resis tance of the shells to corrosion shall be checked by means of suitable instruments (e.g. by ultrasound) and the condi­ tion of the equipment verified. The pressure test of shells intended for the carriage of stabilized sulphur trioxide (9°) shall be repeated every three years. The condition of the lining of shells intended for the carriage of bromine (14°) shall be checked every year by an approved expert, who shall inspect the inside of the shell. Section 6 "Marking Shells intended for the carraige of hydrogen fluoride (anhydrous hydrofluoric acid) (6° (a)], of aqueous solutions of hydrofluoric acid [6° (b)], or of bromine (14°), shall bear, in addition to the particulars already prescribed in marginals 211160 and 211161, an indication of the per­ missible maximum net load in kilogrammes and the date (month, year) of the most recent internal inspection of the shell .. Section 7 Operation Shells intended for the carriage of sulphuric acid [lo (c)]-shall be filled to not more than 95 per cent of their capacity, those intended for the carraige of stabilized sulphur trioxide (9°) to not more than 88 per cent, and those intended for the carriage of bromine (14°) to not less than 88 per cent and not more than 92 per cent or to the extent of 2.86 kg per litre of capacity. Shells inten­ ded for the carriage of hydrogen fluoride (anhydrous hyd­ rofluoric acid) [6° (a)] or of aqueous solutions of hydrofluo­ ric acid [60 (b)] shall not be filled to the extent of more than 0.84 kg per litre of capacity. Appendix B.lb . PROVISIONS CONCERNING TANK CONTAINERS (DESIGN AND TESTING) NOTE: Chapter I sets out the requiremenis applicable to tank­ containers intended for the carriage of substances of all Classes. Chapter II contains particular requirements suppleme­ nting or modifying the requirements of Chapter I. Chapter I REQUIREMENTS APPLICABLE TO ALL CLASSES Section 1 General; scope; definitions These requirements shall apply to tank-containers of a capacity of more than 0.45 cubic metre which are used for the carriage of liquid, gaseous, powdery or granular substances, and to their fittings and accessories. 211852 211853 211854 211859 211860 211861 211869 211870 211871 212099 212100 A tank-container shall comprise a shell and items of 212101 equipment, including equipment to facilitate movement withou t change of attitude . In the following requirements: 212102 (1) (a) «Shell» means the tank proper (including the ope nings and their closures); (b) «Service equipment» of the shell means filling and emptying, venting, safety, heating and heat-insulating de­ vices, and measuring instruments; and (c) «Structural equipment» means the reinforcing, faste­ ning, protective or stabilizing members external to the shell. (2) (a) «Calculated pressure» means a theoretical press­ ure at least equal to the test pressure which according to the degree of danger exhibited by the substance being E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2327 carried may exceed the working pressure more or less substantially. It is used solely to determine the thickness of the walls of the shell, to the exclusion of any external or internal reinforcing device; (b) «Maximum working pressure» means the highest of the following three pressures: Appendix 8.1 b 1. The highest effective pressure allowed in the shell 212102 during filling («maximum filling pressure allowed»); 2. The highest effective pressure allowed in the shell during discharge ( «maximum discharge pressure allo­ wed»); and 3. The effective pressure to which the shell is subjected by its contents (including such extraneous gases as it may contain) when the temperature reaches 50°C («total press­ ure»); (c) «Test pressure» means the highest effective pressure which arises in the shell during the pressure test; ( d) «Filling pressure» means the maximum pressur~ ac­ tually built up in the shell when it is being filled by press­ ure. (e) «Discharge pressure» means the maximum pressure actually built up in the shell when it is being filled by pressure. (3) «Leakage test» means the test which consists of subjecting the shell to an effective internal pressure equal· to the maximum working pressure, but not less than 0.2 kg/cm2 (gauge pressure), by a procedure approved by the competent authority. Section 2 Construction 212103 212119 Shells shall be made of ductile metallic materials. For 212120 welded shells only a material whose weldability has been fully demonstrated shall be used. Welds shall be skilfully made and afford complete safety. The materials of shells and of their protective linings which are in contact with the contents carried shall not contain substances liable to react dangerously with the latter to form dangerous com pounds, or substantially to weaken the material. Shells, their attachments and their service and 212121 structural equipment shall be designed to withstand at least the static and dynamic stresses in normal carriage without loss of contents. 1 Appendix B.lb The pressure on which the dimensioning of the tank- 212122 container shell is based shall be not less than the calcula ted pressure, but the stresses referred to in marginal 212121 shall also be taken into account. Except where special conditions laid down for the va- 212123 rious classes provide otherwise, the following minimum requirements shall be taken into account in the design of shells: (1) The shell of a gravity-discharge tank-container intended for the carriage of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) or not more than 1.1. kg/ cm2 (absolute) shall be designed for a test pressure of twice the static pressure of the liquid to be carried, but not less than twice the statice pressure of water; (2) The shell of a pressure-filled or pressure-dicharge tank-container intended for the carriage of substances having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of not more than 1.1. kg/cm2 (absolute) shall be designed for a test press 1. If there are degassing vent;, this shall not apply to quantities of gas escaping through them. ure equal to 1.3 times the filling or· discharge pressure; (3) The shell of a tank-container - whatever its filling or discharge system - intended for the carriage of substan­ ces having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of not less than 1.1. and not more than 1. 75 kg/cm2 (absolute) shall be designed for a test pressure of at least 1.5 kg/cm2 (gauge pressure), or of 1.3 times the filling or discharge pressure if the filling or discharge pressure is higher; (4) The shell of a tank-container - whatever its f,llfng or discharge system - intended for the carriage of substan­ ces having at 50°C a total pressure (i.e. vapour pressure plus partial pressure of inert gases, if any) of more. than 1. 75 kg/cm2 (absolute) shall be designed for a test press­ ure equal to the higher of the following two pressures; 1.5 times the total pressure at 50oC, less 1 kh/cm2, subject to a minimum of 4 kg/cm2 (gauge pressure); and 1.3 times the filling or discharge pressure. Tank-containers intended to contain certain dangerous 212124 substances shall be provided with additional protection, which may take the form of additional thickness of the shell (such additional thickness being determined in the light of the dangers inherent in the substances concerned; see the relevant classes) or of a protective device. At the calculated pressure or the test pressure whiche- 212125 ver is the higher, the stress o (sigma) at the most severely stressed point of the shell shall conform to the material­ dependent limits prescribed below. In addition, in choo sing the material and determining wall thickness the ma ximum and minhnum filling and working temperatures should be taken into account, with particular reference to the risk of brittle fracture. (1) For metals and alloys exhibiting a clearly-defined yield point or characterized by a guaranteed conventional yield stress Re (generally 0.2 per cent of residual elonga­ tion): (a) Where the ratio Re/Rm is not more than 0.66 (Re = apparent yield stress or 0.2 per cent proof stressrifrii = guaranteed minimum tensile strenght) o ~ 0.75 Re (b) Where the ration Re/Rm exceeds 0.66 I o ~ 0.5 Rm j (2) For metals and alloys exhibiting no apparent yield stress and characterized by a guaranteed minimum tensile strength Rm: o ~ 0.43 R~ ) ~ (3) The elongation at fractur~, 2 in per cent, shall be not less than 1,000/Rm; but shall be not less than 20 per cent in the case of steel and not less than 12 per cent in the case of aluminium alloys. Tank-containers intended for the carriage of inflammable 212126 liquids having a flashpoint of not more than 55 °C and for the carriage of inflammable gases shall be capable of being electrically earthed. Tank-containers shall be capable of absorbing the for- 212127 ces specified in paragraph (1) and the wall thickness of the shells shall be as prescribed in paragraphs (2) - (4) be low. , Appendix B. lb (1) Tank-containers and their fastenings shall under 212127 2 • The specimens used to dermine the elongation at fracture shall be taken transversely to the direction of rolling and be so secured that: Lo= 5d where Lo = length of the specimen before the test; and d = diameter. • 2328 E<DHMEPII THI KYBEPNHIEQI (TEVXOI nPQTO) the maximum permissible load be capable of absorbing the following forces; in the direction of travel: twice the total weight; horizontally at right angles to the direction of travel: the total weight; (where the direction of travel is not clearly determined, the maximum permissible load shall be twice the total weight); verically upwards: the total weight! and vertically downwards: twice the total weight. Under each of these forces the safety factors to be observed shall be the following: for metals having a clearly-defined yield point: a safety factor of 1.5 in relation to the apparent yield stress! or for metals with no clearly - defined yield point: a safety factor of 1.5 in relation to the guaranteed 0.2 per cent proof stress. (2) The minimum wall thickness of the shell barrel shall be calculated by the following formula: p >< D e= 200 xamm where P = calculated pressure or test pressure, whichever is the higher in kg/cm2 ; D = internal diameter of shell in mm; and o = permissible stress as defined in marginal 212205, paragraphs l(a), l(b) and 2, in kg/mm2. The thickness shall in no case be less than that prescri­ bed in paragraphs (3) and (4) below. (3) The barrels and ends of shells not more than 1.80 111 in diameter shall be not less than 5 mm thick if of mild st<'~I 3 (as specified in marginal 212125) or of equivalent thick1wss if of another metal. Where the diameter exceeds 1.80 111 this thickness shall • are increased to 6 mm if the tank is of mild steel 3/ (as specified in marginal 212 205) or to an equivalent thic­ kness if the tank is of another metal. Whatever the metal used, the thickness of the shell wall shall in no case be less than 3 mm. ( 4) Where additional protection of the shell against damage is provided, the competent authority may allow the aforesaid minimum thicknesses to be reduced in pro­ portion to the protection provided; however, the said thic­ knesses shall be not less than 3 mm in the case of mild . steel 3/, or than an equivalent thickness in the case of other materials, for shells not more than 1.80 m in diame­ ter. For shells with a diameter exceeding 1.80 m the aforesaid minimum thickness shall be increased to 4 mm in the case of mild steel 3 / and to an equivalent thickness in the case of another metal. Tank-containers shall be carried only on vehicles whose 212 128 fastenings are capable, under the maximum permissible load on the tank-containers, of absorbing the forces speci fied in marginal 212 127 (1) above. 212 129 Section 3 Items of equipment The items of equipment shall be so arranged as to be 212 130 protected against the risk of being wrenched off or dama ged during carriage and handling. If the connexion bet ween the frame and the shell allows relative movement as between these sub-assemblies, the items of equipment shall be so fastened as to permit such movement without risk of damage to working parts. The items of equipment shall exhibit a suitable degree of safety comparable to that of the shell. In addition, particular conditions applicable to bottom­ discharge tank-containers are prescribed, in marginal 212 131 below. 3. «Mild steel» means a steel having a breaking strenght between 37 and 44 kg/mm2• Every bottom-discharge tank-container, and in the case 212 131 of compartmented bottom-discharge tank-containers every compartment, shall be equipped with two mutually inde pendent shut-off devices, the first being an internal stop valve 4 fixed directly to the shell and the second being a sluice-valve or other equivalent device 5 , mounted in series, one at each end of the discharge pipe. The internal stop-valve shall be operable from above or from below. If possible, the setting -open or closed- of the internal stop-valve shall be capable of being verified from the ground in both cases. Internalsstop-valve control devices shall be so designed as to prevent any unintended opening through impact or an inadvertent act. • The internal shut-off device shall continue "to be effec­ tive in the event of damage to the external control device. In order to avoid any loss of contents in the event of damage to the external discharge fittings (pipes, lateral shut-off devices), the internal stop-valve and its seating shall be protected against the danger of being wrenched off by external stresses or shall be so designed as to resist them. The filling and discharge devices (including flanges or threaded plugs) and protective caps (if any) shall be capable of being secured against any unintended opening. A tank-container or each of its compartments shall, 212 132 save where· it is intended for the carriage of deeply refrige • rated gases, be provided with an opening large enough to enable the tank-container or compartment to be inspected. A tank-container intended for the carriage of liquids 212 133 having a vapour pressure of not more than 1.1 kg/ cm2 (absolute) at 50°C shall have a venting system and a safety device to prevent the contents from spilling out of the shell if the tank-container overturns, or shall conform to the requirements of marginal 212 134 or 212 135 below. A tank-container intended for the carriage of liquids 212 134 having a vapour pressure of not less than 1. 1 and not more than 1. 75 kg/cm2 (absolute) at 50°C shall have a safety valve set at not less than 1.5 kg/cm2 (gauge pres sure) and such that it is fully open at a pressure not exceeding the test pressure; or shall conform to the requi rements of marginal 212 135. A tank-container intended for the carriage of liquids 212 135 having a vapour pressure of not less than 1. 7 5 and not more than 3 kg/cm2 (absolute) at 50°C shall be equipped with a safety valve set at a gauge pressure of not less than 3 kg/cm2 and such that it is fully open at a pressure not exceeding the test pressure; or shall be hermetically sea led. • Moving parts such as covers, closures, etc., which are liable to come into frictional or percussive contact with aluminium tank-containers intended for the carriage of inflammable liquids having a flashpoint of not more than 55°C or for the carriage of inflammable gases shall not be made of unprotected corrodable steel. 212 137 212 139 Section 4 Type approval The competent authority or a body designated by that 212 140 authority shall issue in respect of each new type of tank container a certificate attesting that the prototype tank container, including fastenings, which it has surveyed is suitable for the purpose for which it is intended and meets the construction requirements of section 2 and the equip ment requirements of section 3. If the tank-containers are serially manufactured without modification, this approval shall be valid for the entire series. The test results, the substances for the carriage of which the tank-container is 4, Save as may be otherwise provided in the case of shells intended for the carriage of certain crystallizable or highly viscous substances. 5. I? the case of tank-containers or°Iess than 1 m3 capacity, the sluice-valve or other equivalent device may be replaced by a blank flange. E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2329 approved, and an approval number shall be specified in a test report. The approval number shall consist of the distinguishing sign 6, of the State in whose territory the approval was granted, and a registration number. •• Section 5 Tests 212 141 212 149 Shells and their items of equipment shall either together 212 150 or separately undergo an initial inspection before being put into service and shall thereafter undergo periodic in-· spections. The initial inspection shall include a check of the design characteristics, an internal and external exami nation and a hydraulic pressure test. If the shells and their items of equipment are tested separately they shall after assembly be jointly subjected to a leakage test. The perio dic inspections shall include an external and internal exa mination and, as a general rule, a hydraulic pressure test. Sheathing for thermal insulation and the like shall be removed only to the extent required for reliable appraisal of the tank-container's characteristics. The initial and pe riodic pressure tests shall be carried out. by an expert approved by the competent authority, at the lest pressure indicated on the data plate of the tank-conlairer, except in cases where lower tes~pressures are authorized for the periodic tests. In speciar cases, and with the agreement of the competent authority, the hydraulic pressure test may be replaced by a pressure test using another liquid or a gas. Tank-containers shall, before being pul into service and 212 151 thereafter at intervals not exceeding five years, be tested in conformity with the provisions of marginal 212 150 above. Before tank-containers are put into service, and thereafter at intervals not exceeding two and one - half years, all the equipment shall be checked. for leakproof ness and satisfactory operation. Certificates showing the results of these tests· shall be 212 152 issued by the expert approved by the competent authority. Section 6 Marking 212 153 212 159 Each tank-container shall be fitted with a corrotion- 212 160 resistant metal plate permanently attached to the shell in a place readily accessible for inspection. The following particulars al least shall be marked on the plate by stam ping or by any other similar method. The particulars may be engraved directly on the walls. of the shell itself if the walls are so reinforced that the strength of the shell is not impaired. Approval number; Manufacturer's name or mark; Manufacturer's serial number; Year of manufacture; Test pressure in kg/cm2 (gauge pressure); Capacity in litres; in the case of multiple-element tank-containers: the capacity of each element; Design temperature (only if above 50°C or below 20°C); Month and year of initial test and of most recent periodic test; . Stamp of the expert who carried out the tests. On pressure-filled or pressure-discharge tank­ containers the maximum working pressure allowed shall be inscribed in addition. The following particulars shall be inscribed either on the lank-container itself or on a board: The names of the: owner and of the operator; The capacity of the shell; The unladen (tare) weight; The maximum permissible laden weight; and 6, Distinguishing sign for use in international traffic prescri­ bed by the Convention on Road Traffic (Vienna, 1968). The name of the substance being carried, 7. In addition, tank-container~ shall bear the prescribed danger labels. 212 162 212 169 Section 7 Operation During carriage, tank-containers shall be fixed on the 212 170 carrying vehicle in such a way as lo be adequately protec ted by the fillings of the carrying vehicle or of the tank container itself against lateral and longitudinal impact and against overturning. 8 • If the shells and the service equip ment are so constructed as to withstand impact or over turning they need not be protected in this way. Tank-containers shall not be loaded with any dangerous 212 171 substances other than those for whose carriage they have been approved. The following degrees of filling shall not be exceeded 212 172 in tank-containers intended for the carriage of liquids at ambient temperatures: Appendix B.lb (1) - (a) Inflammable substances not exhibiting addi­ tional risks (e.g. not toxic or corrosive) in lank - containers with a venting system and with or without safely valves: 212172 (contd) degree of filling 100 or 100 %of capacity; 1+35a (b) Toxic or corrosive substances, whether or not exhibi­ ting an inflammability risk, in tank - containers with a ve­ nting system and with or without safety valves: degree of filling 98 or 98 %of capacity; 1+35a (c) Low - concentration inflammable substances and low concentrations acids and !yes in closed tank - containers: degree of filling 97 or 97 %of capacity; 1+35a (d) High - concentration toxic substances and high - cori­ centration acis and !yes in closed tank - containers: degree of filling 95 or 95 %of capacity; o 1+35a (2) In these formulae a is the mean coefficient of cubical expansion of the liquid between 15 ° and 50° C, i.e. for a maximum variation in temperature of 35 ° C. 7. A collective description or an index number may be given instead of the name. 8. Examples of protection of shells: 1. Protection against lateral impact may for example consist of longitudinal bars protecting the shell on both sides at the level of the median line. 2. Protection against overturing may for example consist of reinforcing rings or bars fixed transversally in relation to the frame. 3. Protection against rear impact may for example consist of a bumper or frame. 2330 E<DHMEPII THI KVBEPNHIEQI (TEVXOI nPQTO) a is calculated by the formula: in which d 15 and d 5 are the density of the liquid at 15 °C and 50°C respectivefy. tF is the mean temperature of the liquid during filling. (3) The provisions of marginal 212172 (1) above shall not apply to tank - containers whose contents are mai­ ntained 'by means of a heating device at a temperature above 50°C during carriage. In such a case the degree of filling at the outset shall be such and the temperature shall be so regulated that the tank - container is not full to more. than 95 per cent of its capacity al any time during carriage. Appendix B.lb If the shells of tank - containers in tented for the carriage of liquids 9* are not divided by partitions or surge plates into sections of not more than 5,000 litres capacity, the said shells shall be filled to not less than 80 per cent of their capacity unless they are practically empty. Tank-containers shall be closed so that the contents cannot run out uncontrolled. Where several closure systems are fitted in a series, that nearest to the substance being carried shall be closed first. No residue of the dangerous substance being carried shall adhere to the outside of a tank - container during car­ riage. To be accepted for carriage, empty tank - containers shall be closed in the same manner and leakproof in the same degree as though they were full. Sect.ion 8 Transitional measures (1) Tank - cont~iners of a capacity below 1,000 litres built before the entry into force of these requirements and not conforming to them may, if they were built in confor­ mity with the requirements of ADR and RID concerning receptacles, be used during a period of three years imme­ diately following the entry into force of these requirements for the carriage of liquid, gaseous, powdery or granular substances. (2) Tank - containers of a capacity of not less than 1,000 litres may with the approval of the competent authority of the countries in which they are to be carried, be used during a period of five years immediately following the entry into force of these requirements for the carriage of liquid, gaseous, powdery or granular substances. Appendix B. lb Chapter II PARTICULAR REQUIREMENTS SUPPLEMENTING . OR MODIFYING THE REQUIREMENTS OF CHAPTER I CLASS 2 Gases: compressed, liquefied or dissolved under pressure Section" 1 General; scope; definitions Section 2 Construction 212173 212174 212175 212176 212177 212178 212179 212180 212181 212199 212200 212219 , The shells of tank - containers intended for the carriage. 212220 of substances of 1 ° to 6° and 9° shall not be made of al uminium or aluminium alloy. The requirements of Appendix B.ld, marginals 212221 214250 to 214285 shall apply to the materials and construction of the shells of tank - containers intended for the carriage of gases of 7 ° and 8 °. 9* Substances whose efflux time at 20°C from a DIN cup with a 4 mm orifice is less than 10 minutes ( correspon­ ding to an efflux time of less than 96 sec. at 20°C from a No. 4 Ford cup, or less than 2,680 centistokes) shall be deemed to be liquids for the purposes of this provision. 212222 212229 Section 3 Items of equipment In addition to being equipped with the devices pres- 212230 cribed in marginal 213131, the discharge pipes of tank container shells shall be capable of being closed by blank flanges or some other equally reliable device. The shells of tank - containers intended for the carriage 212231 of liquefied gases may be quipped, in addition lo the filling, discharge and gas - pressure - equalizing orifices, with ope nings in which gauges, thermometers and manometers can be fitted. Appendix B. lb Safety valves shall meet the conditions prescribed in pa- 212232 ragraphs (1), (2) and (3) below. (1) The shells of tank-containers intended for the car­ riage of gases of 1 ° to 6 ° and 9 ° may be fitted with not more than two safety valves. The safety valves shall be capable of opening automati­ cally under a pressure of'from 0.9 to 1.0 times the test pressure of the shell to which they are fitted. They shall in addition be constructed in such a way that in the event of total fire engulfment the pressure inside the shell does not exceed the test pressure. They shall be of such a type as to resist dynamic stresses, including liquid surge. The use of deadweight or counterweight valves is prohibited. The shells of lank-containers intended for the carriage of gases of 1 ° to 9 ° harmful to the respiratory organs or entailing a poison risk (Gases identified by the letter "t" in the list of substances are dee~ed to be gases harmful to the respiratory organs or entailing a poison risk) shall not have safety valves unless the safety valves are preceded by a bursting disc. In the latter case the arrangement of the bursting disc and the safety valve shall be lo the satisfaction of the competent authority. (2) The shells of tank-containers intended for the car­ riage of gases of 7 ° (a) and 8 ° (a) which are not in constant communication with the outside air, and of those intended for the carriage of gases of 7 ° (b) and 8 ° (b) shall be fitted with two independent safety valves each so designed as to • permit evacuation of the gases from the the shell in such a way that the pressure does not at any time esceed the wor­ king pressure indicated on the tank - container by more than 10 per cent. . In addition, the shells of such tank ~ containers may be fitted with bursting discs in series with and preceding the . safety valves. In such a case the arrangement of the bursting disc and the safety valve shall be to the satisfaction of the competent authority. (3) The safety valves of the shells of tank-containers intended for the carriage of gases of 7 ° and 8 ° .shall be ca­ pable of opening at the working pressure indicated on the tank - container. They shall be so designed as to function faultlessly even at the lowest working temperature. The re­ liability of their operation at that temperature shall be es­ tablished and checked either by testing each valve or by testing a specimen valve of each type. An internal flow restricting valve or equivalent device shall be fitted to every orifice more than 1.5 mm in diame­ ter provided in the shell for the passage of gases or liquids, other than orifices carrying safety valves. 212233 Appendix B. lb • Thermal insulation. 212234 ( 1) If the shells of tank - containers intended for the car­ riage of. liquefied gases . of 3 ° to 4 ° are equipped with ther'!1al msu l~tion, such insulation shall be subject to the special prov1s1ons under (2) below either: . Consist of a sun shield covering not less than the upper third but not more than 'the upper half of the tank - contai­ ners's surface and separated from the shell by an air space about 4 cm across; or ~onsis~ of a complete cladding, of adequate thickness, of msulatmg materials. The thermal insulation shall be so designed as not to E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) 2331 hinder access to the filling and discharge devices. (2) The shells of tank - containers intended for the car­ riage of 1,3 - butadiene [3 ° (c)], or of methyl vinyl ether, trifluorochloroethylen~ or vinyl bromide [3 ° (et)], shall be protected by a sun - shield as defined above. (3) The shells of tank - containers intended for the car­ riage of gases of 7 ° and 8 ° shall be thermally insulated. The thermal insulation shall be protected against impact by means of continuous metal sheathing. If the space between· the shell and the metal sheathing is under vacuum (vacuum insulation), the protective sheathing shall be so designed as to withstand without deformation an external pressure of at least 1 kg/ cm2 (gauge .pressure). If the sheathning is so closed as to be gas - tight, a device shall be provided to pre­ vent any dangerous pressure from developing sin the ins­ ulating layer in the event of inadequate gas - tightness of the shell or of its items of equipment. The device shall pre­ vent the infiltration of moisture into the heat - insulating sheath. ( 4) The shells of tank - containers intended for.the car­ riage of oxygen [7 ° (a)], or of air or mixtures of oxygen with nitrogen [8° (a)], shall not incluiie any combustible mate­ rial either in the thermalinsulation or in the means of atta­ chment to the frame .. In the case of multiple - element tank - containers, the 212235 following conditions shall be met. (1) If one of the elements of a multiple - element tank container is fitted with a safety valve and shut - off devices are provided between the elements, every element shall be so fitted. (2) The filling and discharge devices may be fitted to a manifold. Appendix B. lb (3) Each element of a-multiple - element tank - container intended for the carriage of compressed gases of 1 ° and 2 ° harmful to the respiratory organs or entailing a poison risk 10* shall be capable of being isolated by a valve. (4) The elements of a multiple - element tank- container intended for the carriage of liquefied gases of 3 ° to 5 ° harmful to the respiratory organs or entailing a poison risk 10* shali be so designed that they can be filled separately and be kept isolated by a valve capable ofbeing,sealed. Section 4 Type approval 212235 (contd) · 212236 212239 212240 (No special requirements) 212249 Section 5 Tests The materials of the shells of tank - containers intended 212250 for the carriage of gases of 7 ° and 8 ° shall be tested by the method described in Appendix B.ld, marginals 214250 to 214285. The test pressure shall be as follows: 212251 (1) Tank - containers intended for the carriage of gases of 1 ° to 2 °, in conformity with marginal 2219 ( 1 ); 10* The following are deemed to be liquefied gases harmful to the respiratory organs or entailing a poison risk: hydrogen bromide (anhydrous hydrobromic acid), hyd­ rogen fluoride (anhydrous hydrofluoric acid), hydrogen sulphide (sulphuretted hydrogen), ammonia, chlorine, sulphur dioxide (anhydrous sulphurous acid), nitrogen dio­ xide (nitrogen peroxide; nitrogen tetroxide), T gas, methyl vinyl ether, chloromethane (methyl chloride), bromome­ thane (methyl -bromide), phosgene (carbonyl chloride), vinyl bromide, methylamine (monomethylamine), dime­ thylamine, trimethylamine, ethylamine (monoethylamine), ethylene oxide, methanethiol (methyl mercaptan), mixt­ ures of carbon dioxide with ethylene oxide and liquefied hydrogen chloride (anhydrous hydrochloric acid). (2) Tank-containers intended for the carriage of gases of 3o and 4o, in conformity with marginal 2220 (2) if the shells are not more thanl5mm diameter, and in conformity with marginal 211251 (2) (b) if the shells are more than 1.5 m in diameter; (3) Tank-containers intended· for the carriage of gases of 5° and 6°, in conformity with marginal 2220 (3) and (4), and in conformity with marginal 211 251 (3) (b) in the case of multiple-element tank-containers whose ele­ ments are interconnected and form a battery, are not isolated from one another, and are encased in a thermal insulation; (4) Tank-containers intended for the carriage of ammo­ nia dissolved under pressure [9o (at)], in conformity with marginal 211251 (4); (5) (a) Tank-containers fitted with safety valves and intended for the carraige of gases of 7° and 8°: 1.5 times the working pressure indicated on the shells, but not less than 3 kg/cm2 (gauge pressure); for tank-containers with vacuum insulation the test pressure shall be 1.5 times the working pressure increased by 1 kg/ cm2• (b) In the case of tank-containers without safety valves and intended for the carriage of gases of 7° (a) and 8°(a), the first test shall be performed at 2 kg/cm2 (gauge press­ ure) and the periodic tests at 1 kg/cm2 (gauge pressure). The first hydraulic pressure test shall be carried out before thermal insulation is applied. The capacity of the shell of each tank-container inten­ ded for the carriage of gases of 3°, 4° and 9° shall be determined, under the supervision of an expert approved by the competent authority, by weighing or volumetric measurement of the quantity of water required in order to fill the shell. The measurement of shell capacity shall be accurate to within 1 per cent. Determination by a calculation based on the dimensions of the shell is not permitted. The maximum permissible wei ghts of filling according to marginals 2220 (4) and 211251(3) shall be prescribed by an approved expert. All welds in the shell shall. be non-destructively tested radiographically or ultrasonically. Notwithstanding the requirements of marginals 212150 and 21215 I; the periodic tests shall take place: (1) Every two and. one-half years in the case of tank­ containers intended for the carriage of boron trifluoride [lo(at)], town gas [2o (bt)] chlorine, hydrogen bromide, nitrogen dioxide, phosgene or sulphur dioxide [3o (at)], hydrogen sulphide [3o (bt)] or hydrogen chloride [So (at)];. (2) After six years' service in the case of tank­ containers, without safety valves, intended for carriage of gases of 7° (a) and 8° (a); (3) After eight years' service and thereafter every 12 years in the case of tank-containers fitted with safety valves and intended for the carriage of gases of 7° (a) and 7° (b) and of tank-containers intended for the carriage of gases of 7o (b) and 80 (b). A leakproofness check may be performed, at the request of the competent authority, bet­ ween any two successive tests. At the periodic tests for tank-containers equipped with vacuum insulation and intended for the carriage of gases of 7° and 8°, the hydraulic test may be replaced by a leakage test performed either with the gases which the tank-containers are intended to contain or with an inert gas. If, at the time of periodic inspections, manholes are made in the shells of tank-containers intended for the carriage of gases 11 ° to 13°, the method by which they are hermetically closed before the tank-containers are returned to servise shall be one approved by the approved expert and shall ensure the integrity of the shell. Section 6 Marking , In addition, the following particulars shall be marked by stamping or by any other equivalent method on the plate described in marginal 212160. or directly on the 212251 212252 212253 212254 212255 212256 212257 212258 212259 212260 2332 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) walls of the shell itself if the walls are so reinforced that the strength of the shell is not impaired. (1) On tank -containers intended for the carriage of only one substance: The name .of the gas in full. This shall be accompanied, in the case of tank­ containers intended for the carriage of compressed gases of 1 ° and 2° by the tank-container's maximum permitted loading pressure and, in the case of tank-containers inten­ ded for the carriage of liquefied gases of 3° to 8° and of ammonia dissolved under pressure of 9° (at), by the per­ missible maximum load in kg. (2) On multi-purpose tank containers: The names, in full, of the gases for whose carriage the tank-container i~. approved followed by particulars of the permissible maximum load, in kg, for each of them. (3) On tank-containers equipped with safety valves and intended for the carriage of gases of 7° (a), and 8 1a) av-d on tank-containers intended for the carriage of gases of 7° (b) and 8° (b): . The working pressure. (4) On tank-containers equipped with thermal insulation the expression «thermally insulated» shall be inscribed in one of the official languages of ADR. • The frame of a multiple-element tank-container shall be fitted near the filling point with a plate specifying: The test pressure of the elements; The working pressure of elements intended for com pressed gases; The number of elements; The aggregate capacity of the elements, in litres; The name of the gas in full; and, in the case of liquefied gases. The permissible maximum load per element in kg. Section 7 Operation A tank-container assigned at different times to the car­ riage of different liquefied gases of 3° to 8° (multi-purpose tank-containers) may not carry substances other than listed in one, and one only, of the following groups: Group 1: halogenated hydrocarbons of 3° (a) and 4° (a); Group 2: hydrocarbons of 3° (b) and 4° (b); Group 3: ammonia (3° (at)]; dimethyl ether, dimethyla­ mine, ethylamine, methylamine and trimethylamine (3° (bt)]; and vinyl chloride (3° (c)]; Group 4: methyl bromide (3° (at)]; ethyl chloride and methyl chloride (3° (bt)]; • Groupe 5: mixtures of ethylene oxide with carbon dio­ xide and of ethylene oxide with nitrogen (4° (et)]; Groupe 6: gases of 7° (a) and mixtures of gases of 8° (a); Group 7: ethane, ethylene and methane [7° (b)]; and mixtures of ethane with methane, also when they contain propane or butane (8° (b)]. Tank-containers which have been filled with a substance of group 1 or group 2 shall be emptied of liquefied gas before being loaded with another substance belonging to the same group. Tank-containers which have been filled with a substance of one of the groups 3 to 5 shall be completely emptied of liquefied gas and blown down be­ fore being loaded with another substance belonging to the same group. The multiple use of tank-containers for the carriage of liquefied gases of the same group shall be allowed jf all the requirements prescribed for the gases to be carried in one and the same tank-container are observed. Such multiple use shall be subject to approval by an approved expert. The multiple use of tank-containers for the carriage of gases of different groups shall be allowed if permitted by the approved experts. When loaded tank-containers or empty but uncleaned tank-containers are handed over for carraige, only the particulats applicable under marginal 211161 to the gas loaded or just discharged shall be visible; all particulars 212261 212262 212269 212270 212271 212272 212273 212274 concerning other gases shall be covered up. All the elements of a multiple- element tank-container shall contain only one and the same gas. In the case of a multiple-element tank-container intended for the carriage of liquefied gases harmful to the respiratory organs or entailing a poison risk 1°, the elements shall be filled sepa­ rately and be kept isolated by a sealed valve. The maximum permissible degrees of filling in kg/litre prescribed in marginals 2219 (2), 2220, (3) and (4) 211251 (2), (3) and (4) shall be adhered to. The degree of filling of the shells of tank-containers fitted with safety valves and intended for the carriage of gases of l lo to 130 shall be such that at· the «alert» temperature, at which the vapo1,1r pressure is equal to the valve-opening pressure, the volume of the liquid does not exceed the permissible degree of filling of the shell at that temperature, i.e. 95 per cent in the case of inflammable gases and 98 per cent in the case of other gases. On the shells of tank-containers intended for the car­ riage of oxygen [7o (a)], or of air or mixtures of oxygen with nitrogen (80 (a)], substances containing grease or oil shall not be used to ensure leakproofness of the joints or fot the maintenance of the closures. Section 8 Transitional measures CLASS 3 lnflammabel liquids Section 1 General; scope; definitions Section 2 Construction The shells of tank-containers intended for the carriage of carbon disulphide [lo (a)] shall be designed for a calc­ ulated pressure of 10 kg/cm2 (gauge pressure). Appendix B. 1 b Section 3 Items of equipment Tank containers which are fitted with a venting system with no shut-off device, and which are intended for the carriage of inflammable liquids having a flashpoint not exceeding 55 ° C, and tank-containers fitted with a safety valve shall have a flame-trap in the venting system. All openings in the shells of tank-containers intended for the carriage of acrylaldehyde (acrolein), chloroprene (chlorobutadiene) and carbon disulphide (1 ° (a)) shall be above the surface level of the liquid. No piping or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. The openings shall be capable of being hermetically closed and the closure shall be capable of being protected by a lockable cap. Section 4 Type approval (No special requirements) Section 5 Tests (No special requirements) Section 6 Marking (No special requirements) Section 7 Operation In the case of liquids having a vapour pressure of more than 1. 75 kg/cm2 (absolute) at 50° C, the following deg­ rees of filling of hermetically closed shells shall not be. exceeded: for methyl formate (1 ° (a)) and other liquids having a coefficient of cubical expansion of more· than 150 X 10-5 but not more than 180 X 10-5 ............ 91 212275 212276 212277 212278 212279 212280 212299 212300 212319 212320 212321 212329 212330 212331 212332 212339 212340 212349 212350 212359 212360 212369 212370 ECl>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2333 per cent of capacity; for acetaldehyde ( 5 °). and other liquids having a coefficient of cubical expansion of more than 180 X 10·5 but not more than 230 X 10·5 ......... . 90 per cent of capacity. Appendix B.lb An aluminium shell shall not be used for the carriage of acetaldehyde (5°) unless the shell is reserved solely for such carriage and the acetaldehyde is free from acid. 212371 In the cold season (October to March), light distillates for cracking and other liquid hydrocarbons having a va­ pour pressure not exceeding 1.5 kg/cm2 (absolute)" at 50° C may be carried in shells of the type prescribed in margi­ nal 212133. 212372 Carbon disulphide (1 ° (a)) shall not be carried otherwise than in hermetically closed shells or in shells equipped with valves set at not less than 3 kg/cm2 (gauge pressure). Section 8 .Transitional measures CLASS 4.1 Inflammable solids CLASS 4.2 Substances liable to spontaneous combustion CLASS 4.3 Substances which give off inflammable gases on contact with water Section 1 C~neral; scope; definitions Section 2 Construction The shells of tank-containers intended for the carriage of white or yellow phosphorus of marginal 2431, 1 °, and of trichforosilane (silicochloroform) of marginal 24 71, 4 °, shaUbt; designed for a calculated pressure of 10 kg/cm2 (gauge pressure). The shells of tank-containers intended for the carriage of aluminium alkyls, and of h'alides and hydrides of alumi­ nium alkyls, of marginal 2431, 3°, shall be designed for a pressure of not less than 21 kg/cm2 (gauge pressure). Appendix 8.1 b Section 3 lteme of equipment The shells of tank-containers intended for the carriage of sulphur of marginal 2401, 2° (b), and of naphthalene of marginal 2401, 11 ° (c), shall be equipped with thermal insulation so made of materials which are not readily inflammable that the temperature on the outer surface cannot rise above 50° C during carriage. They may be ·equipped with valves opening automatically inwards or . outwards under the effect of a difference of pressure of 0.2 to 0.3 kg/cm2 . The discharge devices shall be capable of being protected.by a lockable metal cap. The shell!; of tank-containers intended for the carriage of white or yellow phosphorus of marginal 2431, 1 °, shall meet the following requirements: (1) The heating device shall not penetrate into the body of the shell but be fitted outsid it. Other piping shall enter the shell in its upper part; openings shall be above the hig hest permissible level of the phosphorus and be ca­ pable of being completely enclosed under lockable caps. (2) The shell shall be equipped with a gauging system for verifying the level of the phosphorus and, if water is used as the protective agent, with a fixed gauge mark showing the highest permissible level of water. The openings and orifices (valves, ducts, manholes, etc.) in the shells of tank-containers intended for the car­ riage of substances of marginal 2471, 1° (a), shall be equipped with leakproof lockable caps, and such shells • shall be equipped with thermal insulation so made of materials which are not readily inflammable that the tern 212373 212374 212379 212380 212399 212400 212419 212420 212421 212422 212429 212430 212431 212432 perature on the outer surface cannot rise above 50° C during carriage. The shells of tank-containers intended for the carriage of aluminium alkyls, and of halides and hydrides of alumi­ nium alkyls, of marginal 2431, 3°, shall not have openings or connexions, even if closable, below the surface level of the liquid. Openings, including their fittings and acces­ sories, in the upper part of the shell shall be capable of being protected by a protective cap. Section 4 Type approval (No special requirements) Appendix B.lb Section 5 Tests The shells of tank-containers intended for the car~iage of sulphur of marginal 2401, 2° (the filling temperl\ture must additionally be taken into account in the case of shells made of aluminium), naphthalene of marginal 2401, 11 °, white or yellow phosphorus of marginal 2431, 1 °, and trichlorosilane (silicochloroform) of marginal 24 71, 4 °, shall be tested al a pressure of 4 kg/ cm2 (gauge press­ ure). The shells of tank-containers intended for the carriage of aluminium alkyls, and of halides and hydrides of alumi­ nium alkyls, of marginal 2431, 3°, shall undergo an initial pressure test, and periodic tests every five years, perfor­ med at a pressure of 10 kg/cm2 (gauge pressure) with a:· liquid which does not react with the substance to be car­ ried. Section 6 Marking (No special requirements) Section 7 Operation . The shells of tank-containers intended for the carriage of sulphur of marginal 2401, 2°, shall be filled to not· more than 98 per cent of their capacity. White or yellow phosphorus of marginal 2 431, 1 °, shall if water is used as the protective agent be covered with a depth of not less than 12 cm of water at the time of filling; the degree of filling at a temperature of 60° C shall not exceed 98 per cent. If nitrogen is used as the protective agent, the degree of filling at a temperature of 60° C shall not exceed 96 per cent. The. remaining space shall be filled with nitrogen in such a way that, even after cooling, the pressure at no time falls below the.atmospheric pressure. The shell shall be hermetically closed so that no leakage of gas occurs. For the carriage of substances of marginal 2471, 1° (a), caps shall be locked in conformity with marginal 212432 and the temperature of the outside surface of the shell shall not exceed 50° C. • In the case of trichlorosilane (silicochloroform) of margi­ nal 2471, 4°, the degree of filling shall not exceed 1.14 kg per litre of capacity if filling is by weight, or 85 per cent if filling is by volume. The shells of tank-containers which have contained phosphorus of marginal 2431, 1 °, shall when handed over for carriage either: be filled with nitrogeni the sender must certify in the transport document that the tank, after closure, is gaslight; or be filled with water to not ltss than 96 per cent and not more than 98 per cent of their capacity; between 1 October and 31 March this water shall contain one or more anti-freeze ~gents free from corrosive action, not liable to react with phosphorus, and sufficiently concentra­ ted to prevent the water freezing during carriage. 212433 212434 212439 212440 212449 212450 212451 212452 212459 212460 212469 212470 212471 212472 212473 212474 212475 212479 2334 ECJ>HMEPlr THr KYBEPNHre,u: (TEYXOr nPQTO) Section 8 Transitional measures CLASS 5.1 Oxidizing substances CLASS 5.2 Organic peroxides Section 1 General; scope; definitions Section 2 Construction The shells of tank-containers, and their items of equip­ ment, intended for the carriage of hydrogen peroxide or of aqueous solutions of hydrogen peroxide of marginal 2501, 1 °, or for the carriage of liquid organic peroxides of marginal 2551, 10°, 14° and 15° shall be made of aluminium not less than 99.5 per cent pure or of suitable alloy steel not liable to cause the hydrogen peroxide or the organic peroxides to decompose. Appendix B. lb Section 3 Items of equipment The shells of tank-containers intended for the carriage of aqueous solutions of hydrogen peroxide containing more than 70 per cent hydrogen peroxide and of hydrogen peroxide of marginal 2501, 1 °, shall have their openings above the surface level of the liquid. In the case of solution containing more than 60 per cent but not more than 70 per cent hydrogen peroxide, openings below the surface level of the liquid shall be permissible. In this case the shell-discharge system shall include two mutual~ - inde­ pendent shut-off devices, the first being a quick-closing internal stop-valve of an approved type and the second a sluice-valve, mounted in series, one at each end of the discharge pipe. A blank flange or some other equally reliable device shall also be fitted to the outlet of each external sluice-valve. The internal stop-valve shall be such that it remains rigidly locked to the shell and in the closed position if the pipe is wrenched off. The connexion to the external pipe-outlets of tank­ containers shall be coated with a suitable plastics material. The shells of tank-containers intended for the carriage of liquid organic peroxides of marginal 25Sl, 10°, 14° and 15°, shall be equipped with a venting device fitted with a flame-trap and followed in series by a safety valve opening automatically at a pressure of 1.8 to 2.2 kg/cm2 (gauge pressure). The materials of which closures liable to come into contact with the liquid or its vapour are made shall not have a catalytic effect (spring-loaded safety valve made of aluminium-silicon alloy (silumin) or of V2A stain­ less steel or of a material of equivalent quality). The shells of tank-containers intended for the carriage of liquid organic peroxides of marginal 2551, 10°, 14° and 15°, shall be equipped with thermal insulation in accordance with the requirements of marginal 212234 (1 ). The covering and the uncovered part of the shell shall be painted white. • Section 4 Type approval (No special requirements) Appendix B.lb Section 5 Tests 212480 212499 212500 212519 212520 212521 212529 212530 212531 212532 212533 212534 212539 212540 212549 The shells of tank-containers intended for the carriage 212550 of hydrogen peroxide or of aqueous solutions of hydrogen peroxide, of marginal 2501, 1 ° or of liquid organic pero­ xide of marginal 2551, 10°, 14° and 15°, shall be tested at a perssure of 4 kg/cm2 (gauge pressure). Section 6 Marking (No special requirements) Section 7 Operation The inside of the shell of the tank container, and all metal parts liable to come into contact with hydrogen peroxide of marginal 2501, 1 °, shall be kept clean. No lubricant capable of combining dangerously with the substance carried shall be used for pumps, valves or other devices. The shells of tank-containers intended for the carriage of liquids of marginal 2501, 1 ° to 3°, shall be filled to not more than 95 per cent of their capacity at a reference temperature of 15 ° C. The shells of tank-containers inten­ ded for the carriage of liquid organic peroxides of margi­ nal 2551,10°, 14° and 15°, shall be filled to not more than 80 per cent of their capacity. Shells shall be free from impurities at the time of filling. Section 8 Transitional measures CLASS 6.1 Toxic substances Section 1 General; scope; definitions Appendix B.lb Section 2 Construction The shells of tank-containers intended for the carriage of substances of marginal 2601, 2°(a), 3°, 4°(a), 11 °(a), 13 °(b), 14 °, 23 °, 61 °(a), 61 °(e), 61 °(f), 81 ° and 82°, shall if these substances are liquid at +40°C ( except carbon tetrachloride, chloroform and methylene chloride) be designed for a calculated pressure of 10 kg/cm2 (gauge pressure). The shells of tank-containers intended for the carriage of substances referred to in marginal 61121 (3) other than those enumerated in marginal 212620 above shall be so constructed that they can be discharged at a pressure of not less than 3 kg/cm2 (gauge pressure). Section 3 Items of equipment 212551 212559 .212560 212569 212570 212571 212572 212579 212580 212599 212600 212619 212620 212621 212622 212629 (1) All openings in the shells of tank-containers inten- 212630 ded for the carriage of substances referred to in marginal 61121 (3) shall be above the surface level of the liquid. · (2) No piping or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) 2335 The openings shall be capable of being hermetically closed and the closure shall be· capable of being protected by a lockable cap. In addition the shells of such tank-containers· may be fitted with bursting discs mounted in series prece­ ding th~ safety valves. In such a case the arrangement of the bursting disc and the safety valve shall be to the satisfaction of the competent authority. Section 4 Type approval (No special requirements) Section 5 Tests· 212631 212639 212640 212649 Tank-containers intended for the carriage of substances 212650 of marginal 2601 2° (a), 3°, 4° (a), 11° (a), 13° (b), 14°, 23°, 61° (a), 61° (e), 61° (f), 81 ° and 82° shall if the~e substances are liquid at +40°C be tested initially and periodically at a pressure of 4 kg/cm2 (gauge pressure). Appendix B.lb Section 6 Marking (No special requirements) 212651 212659 212660 212669 Section 7 Operation The shells of tank-containers intended for the carriage 212670 of substances of marginal 2601, 2° (a), 2° (b), 4° (a), 11 ° (a), 12° (a),. 13~ (a), 13 ° (b) and 81 ° to 83 °,. shall be filled to not more than 93 per of·their capacity. The shells of tank-containers intended for the carriage 212671 of aqueous-solutions ofethyleneimine (3 °) and of substan ces of marginal 2601, 14°, shall be filled to not more than--95 per cent of their capacity. Section 8 Transitional measures CLASS 7 Radioactive substances Section 1 General; scope; definitions Section 2 Construction 212672 212679 212680 212699 212700 212719 Tank-containers intended for the transport of the 212720 substances referred to in Schedule 5, with the exception of uranium hexafluoride, shall be designed for a calcula tion pressure of at least 4 kg/cm2 • In the case of tank­ containers intended for the transport of uranium hexafluo ride, the calculation pressure shall be fixed at 10 kg/cm2• When the radioactive substance is in solution or suspen­ sion in hazardous substances of other Classes and when the calculation pressures required for the tank-containers intended for the transport of the latter substances are greater, these pressures shall be applied. Appendix B.lb Section 3 Equipment 212721- . 219729 The openings of tank-containers intended for the Iran- 212730 sport of liquid radioactive substances 9) shall be above the level of the liquid and no piping or pipe connexion shall pass through the walls of the shell below t~e surface level of the liquid. Section 4 Type approval 212731 212739 Tank-containers approved for the transport of radioac- 212740 live substances shall not be approved for the transport of any other substance, Section 5 Tests 212741 212749 • The tank-containers shall undergo, at least once every 212750 five years, a hydraulic pressure test at a pressure of 4 kg/cm2• Notwithstanding marginal 212150, the periodic internal inspection may be replaced by an ultrasonic test of the wall thickness conducted every two-and-a~half ye ars. Section 6 Marking (No special requirements) Section 7 Operation ~ 212751 212759 212760 212769 The degree of filling a,t. the reference temperature of 212770 15 ° C shall not exceed 93 per cent of the total· shell capacity. Tank-containers which have been used for the transport of radioactive substances shall not be used for the transport of other substances. Appendix B. lb Section 8 Transitional provisions CLASS 8 Corrosive substances Section 1 General; scope; definitions 212771 212779 212780 212799 2336 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Section 2 Construction 212800 212819 The shells of tank-containers intended for the carriage 212820 of hydrogen fluoride (anhydrous hydrofluoric acid) [6°(a)], of aqueous solutions of hydrofluoric acid [6°(b)], or of bromine ( 14°), shall be designed for a pressure of not less than 21 kg/ cm2 (gauge pressure). Appendix B. lb The shells of tank-containers intended for the carriage 212821 of substances of 1 °, (a) and (b); 2°, (a) and (b); 6° (c); 7° to 9°; 21 ° (a); and 23°, shall be designed for a pressure of not less than 10 kg/cm2 (gauge pressure). The shells of tank-containers intended for the carriage 212822 of substances referred to in marginal 81121 (2), other than those listed in marginals 218200 and 218201, shall be designed for a calculated pressure of 4 kg/cm2 (gauge pressure) and shall be so constructed that they can be discharged at a pressure of not less than 3 kg/ cm2 (gauge pressure). The shells of tank-containers intended for the carriage 21282 3 of aqueous solutions of hydrogen peroxide (41 °) shall meet the requirements of marginal 216200. . Section 3 Items of equipment 212824 212829 All openings in the shells of tank-containers intended 212830 for the carriage of substances of 6° or of bromine (14°) shall be above the surface level of the liquid. No piping or pipe connexions shall pass through the walls of the shell below the surface level of the liquid. The closures shall be capable of being effectively protected by a metal cap. The shells of tank-containers intended for the carriage 212831 of stabilized sulphur trioxide (9°) shall be thermally insula ted and be filled with a heating device on the outside. Shells may be of the bouom-discharge type. In this case the shell-discharge system shall include two mutually in­ dependent shut-off devices, the first being a quick-closing internal, stop-valve of an approved type and the second a sluice-valve, mounted in series, one at each end of the discharge pipe. A blank flange or some other equally reliable device shall also be fiued to the outlet of each external sluice-valve. The shells of tank-containers intended for the carriage· 212832 of hypochlorite solutions (37°) and of aqueous solutions of hydrogen peroxide (41 °) shall be so designed as to prevent the entry of foreign mailer, the leakage of liquid, and the development of any dangerous excess pressure in the shell. • Section 4 Type approval (No special requirements) Section 5 Test 212833 212839 212840 212849 T he shells of tank - containers intended for the carriage 212 850 of hydrogen fluoride (anhydous hydroflouric acid) [6 ° (a)], or of aqueous solutions of hydrofluoric acid of 6° (b), shall undergo the initial pressure test and the periodic tests at a pressure of 10 kg/cm2 (gauge pressure), and those intended for the carriage of the other substances referred to in marginal 81 121 (2), at a pressure of 4 kg/cm2 (gauge pressure). The pressure test of tank - containers intended for the 212 851 carriage of stabilized sulphur trioxide (9°) shall be repeated every two and one - half years. The condition of the lead lining of the shells of tank - 212 852 containers intended for the carriage of bromine (14°) shall de checked every year dy an approved expert, who shall inspect the inside of the shell. In addition to the tests prescribed in Section 5, the corro- 212853 sion resistance of tank 6 containeri, intended for the car riage of hydrogen fluoride (anhydrons hydrofluoric acid) (6° (a)], or of aqueous solutions of hydrofluoric acid of 6~ (b), shall be checked by means of suitable instruments (e.g. by ultrasound methods); and the condition of the items of equipment verified, every two and one - lalf ye ars. • Section 6 Marking In addition to the particulars prescribed in marginals 212 160 and 212 161, the following particulars shall be marked on tank - containers intended for the carriage of hydrogern fluoride (anhydrous hydrofluoric acid) [6° (a)], of aqueous solutions of hydrofluoric acid of 6° (b), or bromine (14°): the permissible maximum net load in kg, and the date (month and year) of the most recent internal inspection of the shell. Section 7 Operation 212 854 212 859 212860 212861 212869 The shells of tank - containers intended for the carriage 212 8 7 O of sulphuric acid [l O (c)] shall be filled to not more than 95 per cent of their capacity, those intended for the car-· riage of stabilized sulphur trioxide (9°) to not more than· 88 per cent, and those intended for the carriage of bromine (14°) to not less than 88 per cent and not more than 92 per cent or to the extent of 2.86 kg per litre of capacity., Shells intended for the carriage of hydrogen fluoride (anhydrous hydrofluoric acid) [6° (a)] and of aqueous sol- .. utions of hydrofluoric acid [6° (b)] shall not be filled to . the extent of more than 0.84 kg per litre of capacity • 212871 • 212879 Section 8 Transitional measures Appendix B. le PROVISIONS CONCEHNING FIXED TANKS AND DE­ MOUNTABLE TANKS IN REINFORCED PLASTICS Notes This ~ppendix applies to fixed tanks and demountable tanks; 11 does not apply to batteries of receptacles, to tank contamers, or to receptacles. :-For receptacles, see the requirements concerning them m Annex A (pagkages). It is recalled that marginal 10 121 ( 1) prohibits the carnage ~f da~gerous substances in tanks except where such carnage 1s expressly authorized. This Appendix is there fore confined to provisions applicable to fixed tanks and demountable tanks in reinforced plastics used for transport operations which are expressly authorized. Section 1 General provisions concerning the construction of fixed tanks and demountable tanks • 212 880 213 099 The !anks must satisfy the following requirements ~f 213 100 Appendix B. la: . • ( 1) General provisions applicable to tanks used for carriage of substances of all Classes: . • • • • • E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2337 Marginals 211 120, (4), (5) and (6); 211 121, (1) and (2); 211 122; 211 124; 211 126; 211 127, (5); 211 128; 211 130; 211 132; 211 137; 211 140; 211 150 to 211 153; 211 160 and 211 161; 211 171; 211 172, (1) and (2); and 211 173 to 211 178. (2) Provisions applicable to tanks for carriage of substan­ ces of Class 3: marginal 211 330. The leakprofness test and the internal inspection shall be performed ·every three years. (3) Special provisions applicable to tanks used for carriage of substances of Class 8: Marginal 211 833. The walls of the tank must present no material defect 213 101 causing a reduction in safery. The walls of the- ta~k must have a lasting resistance to 213 102 the mechanical, thermal and chemical stresses to which they are s ubject~d. • • Tank openings . . 213 103 (1) Where the tank has one Qr more discharge openings below the level of the liquid, any. pipe or valve fitted to such opening or openings shall be protected either by being recessed into the tank shell or by any other means approved by the competent autority and providing equiva lent protection. • (2) The use of screwed plugs is strictly prohibited. Valves shall be of a model approved by the competent au­ thority. (3) Filling apertures shall be closed by a hermetic de­ vice. If the device projects outwards from the tank shell it shall be protected by a cap capable of withstanding wrenching stresses occurring through accidental overtu­ rning of the tank. Section 2 Materials used for the walls of the tank 213 104 213 119 The walls of tanks may be made of the following materials: 213 120 ( 1) • Sythetic resin non - ·saturated polyester resins; epoxide resins; other resins with similar characteristics, provided that the safety ·of the wall is demonstrated. (2) Fibre reinforcements. Glass fibres (glass of types E and C) l/ with an approp­ riate coating, for example with a silane base or similar products. The glass fibres may be used in the form of cut or uncut rovings including prestressed continuous rovings or filaments, mats, surface mats or ·woven fabric. ·(3) Additives (a) Additives necessary for the treatment of resins, for example, catalysts, accceleratos, monomers, hardene.rs, thixotropic substances, in accordance with instrucions by the manufacturer of the resin. (b) Extenders, pigments, colorants and. other products enabling the required properties to be· obtained, for exam­ ple, the increase of fire-- restistant properties, provided that they cause no reduction in the safety of use of the walls of the tank. 213 121 213 129 Section 3 Structure of the walls of the tank The external surface layer of the walls of the tank must 213 130 be resista)it to atmosphe~ic effects and also to brief contact with the substance to be carried. • The walls of the tank and the sealed joints inust satisfy 213 131 the mechanical resistance requirements liste d in section 4. The internal surface layer of the walls must be resistant 213 132 to the lasting effects of the substance to be carried. This layer must be made of reinforced resin having a minimum thickness of 1 mm. The fibres used must not reduce the chemical resistance of the layer. The inner part of the layer must be rich in resins and must have a minimum thickness of 0.2, mm. l/ Glass of types E ancl C is defined in Table 1. The requirements detailed in marginals 213 140 (6) and 213 142 (2) of section 4 must be satisfied. The finished walls must satisfy the requirements detailed 213 133 in marginal 213 140 (3) of section 4. The minimum thickness of the wall shall be 213 134 3.5. mm if the capacity of tank does not exceed 3,000 litres 5.0 mm if the capacity of the tank is more than 3,000 litres. Section 4 213 135 213 139 Test methods and qualities required Tests and qualities required for materials 213 -140 for prototype tank (1) Taking of specimens The spesimens required for the test must wherever possible be taken from the walls of the tank. For this purpose cut - out parts resulting from the making of apertures etc. may be used. (2) Percentage of glass fibre The test must be conducted in accordance with the methods prescribed in ISO Recommendation Rl 172 1970. The glass content of tqe specimen must be higher than 25 per cent and lower than 75 per cent by weight. (3) Degree of polymerization (a) Wall in polyester resins The residual styrene content may not be higher than 2 per cent, calculated on the total quantity of resins. The test shall be conducted in accordance with a suitable me­ thod.21 (b) Wall in epoxide resins The acetone extract may not be higher than 2 per cent calculated on the total quantity of resins. The test shall be conducted ii:i accordance with a suitable method 3/ (4) Bending and tensile strength The mechanical properties must be determined: for the shell, in the axial and circumferential directions; for the ends and walls of compartments, in any direction. If-the principal directions of the reinforcement do not coincide with the axial and circumferential directions (for example in the case of biaxial winding), the strength must be determined in the principal directions of the reinforce­ ment and calculated for the axial arid circumferential di­ rections by applying the following formulae: Tensile aT,c = 2crT,H sin2 :oC aT,a = 2o-T,H cos2 o<; Bending aF,c = 2.-F,H sin2·o(; aF,a = 2crF,H cos2o(; T = tensile c = circumfere~tial a= axial H = helicoidal F = bending o(, = preferential winding angle The tensile strength must be tested in accordance with the methods prescribed in document ISO/ TC61/ WG2/ TG «Tests of glass reinforced plastics» No 4 of February 1971. The bending strength must be tested in accordance with the methods prescribed in Recommendation ISO /TC6 l No 1540 of April 1970. Requirements New tanks must meet the following safety factors against rupture: Safery factor for static loading: 7.5 Safery factor for dynamic loading: 5.5. The acceleration values to be applied in computing the dynamic load are as follows: 2/The method prescribed in standard DIN 16945 of June 1969, paragrafh 6.4.3 is regarded as suitable. 3/The method prescribed in star1dard DIN 16945 of June 1969, paragraph 6.4.2 is regarded as suitable. 2338 :E::..:<l>::....:H...:..::M==-E'-Pl=I'-T=---=-H=I=--..:....:;KY...c..=BE=P'---'N..CCH:...:.I=E=Q=I"---'-'(T'-"Ec....c.Y-'-XC...CO..CCI'-'n~P~Q~T O=),. 2 g in direction of travel; 1 g at right angles to direction of travel; 1 g vertically upwards; and 2 g vertically downwards. As the characteristics of a reinforced plastics laminate may vary ac~ording to its structure, minimum values are not prescribed for bending and tensile strength but for lo­ ads: A = ea where a is the tensile strength at break; B=e2 ~ where' a is the <lending strength at break; F F where is the thickness of the wall. The minimum values for forces A and B are: For bending Capacity of tank ~3,000 litres circumferential direction B = 600daN axial direction B= 300 daN Capasity of tank > 3,000 litres circumferential direction B = 600 daN axial direction B = 600 daN For tensile: circumferential direction A = lO0daN/mm axial direction A= 70 daN/mm Module E on bending is measured at - 40°C and at +60°C. The two values may not differ by more than 30 per cent from the value obtained at 20°C. Behaviour of wall material during a tensile test lasting more than 1,000 hours. The test tension is a T 7.5 During the test the factor K= E lOOO may, not be higher than 1.6. E = elongation of loaded speciment at beginning of test E 1000= elongation of loaded specimen at end of test (5) Impact behaviour (a) Nature of test Impact behaviour is determined on a sample of laminate corresponding to the structural material used for the construction of the tank. The test is carried out by dropping a 5 kg steel weight onto the surface of the laminate corres­ ponding to the external surface of the tank; (b) Apparatus The apparatus consists of a 5 kg steel weight, a guidance device for this weight and a specimen-bearing chassis. A general diagram of the apparatus is given in diagram 1. The weight is in the form of a steel cylinder provided with two guide channels, the lower extremity being spherically shaped, 90 mm diameter. The guidance device is fitted vertically to a wall. The specimen-bearer is composed of two angle-bars of 100xlO0X25 mm and 300 mm long, welded to a 400x400 mm metal support. The gap between the two bars is 175 mm. The specimen-bearer, fixed to the ground, is provided with a 50 mm deep cavity to allow fle­ xion of the specimen. (c) Preparation of specimens. From the sample, three specimens are taken, each me­ asuring 200X200 mmXthickness of the sample. ( d) Operating method The speciment is placed ·symmetrically on the speci­ men-bearer; if possible it rests on the support following two basic straight lines of the surface, in such a way that the weight strikes the centre of the face of the specimen corres­ ponding to the external surface of the tank. The weight is allowed to fall from a determined height, care being taken to ensure that it does not rebound and strike the specimen a second time. The test must be conducted at ambient temperature. the height to which the weight is raised in the guidance device is noted. The other two specimens are tested in the same way. ( e) Requirement The drop height for a 5 kg weight shall be 1 metre; the speciment must not allow leakage of more than 1- litre per 24 hours when subjected to a column of water of 1 -m. (6) Resistance to chemical agents. Flat reinforced plastics test plates, prepared in the labo­ ratory, are subjected to attack by the dangerous substance at a temperaure of"50°C for 30 days in accordance with the following procedure: (a) Description of the test apparatus (and -shown in dia~am 2). l he test apparatus comprises a glass cylinder, diameter 140xl50 mm, 150 mm high wiU) two nozzles positioned at 1350 one fitted with an NS 29 joint to take an interme­ diate pipe for a reflux condenser (1), the other nozzle fitted with an NS 14,5 joint to take a thermometer (2), an inter­ mediate pipe for a reflux condenser and a reflux condenser not shown in the diagram. The glass part of the apparatus shall be in glass resistant to changes of temperature. The specimens taken from the test plates form the base and the top of the glass cilinder. They .are sealed to the sides of the cylinder by a PTEE collar. The cylinder with the two specimens is clamped between two pressure plates in corrosion-resistant steel with six threaded bolts tigh­ tened by means of wing nuts. An asbestos washer must be placed between the pressure plates and the specimens. These washers are not shown in diagram 2. Heating is ef­ fected from outside by means of an automatically co­ ntrolled sleeve heater. The temperature is.measured in the chamber containing the liquid. • (b) Operation of the test apparatus. The test apparatus allows only flat plates of uniform th­ ickness to be tested. The test plates should, if possible, be 4 mm thick. Should these plates be covered with a gel coa­ ting, they must be tested in condition as for practical use. Six hexagonal specimens, each side measuring 100 mm are cut from the test plate. • For each test, three specimens are prepared per appa­ ratus. One of these samples is used .as a reference and the other two are used for checking in the liquid zone, and va­ pour zone of the device respectively. (c) Test procedure The specimens to be tested are placed on the apparatus with the surface which may be gel-coated facing inwards. 1,200 ml of test liquid is poured into the glass cylinder. The apparatus is then heated tothe test temperature. A constant temperature is maintained during the test. After the test the apparatus is cooled to the ambient temperature and the test liquid removed. The specimens tested are im­ mediately washed with distilled water. Liquids which are not soluble in water are removed with a solvent which does not attack the specimens. Mechanical cleaning of the plates cannot be ·performed because of the danger of damaging the surface of the specimens. (d) Evaluation A visual examination is made: if the visual examination reveals ·excessive .attack ( cracks, bubbles, pores, peeling off, swelling, or rough­ ness), the test is conclusive negatively; if the visual examination reveals no abnormality, ben­ ding tests are made by the methods specified in marginal 213140 (4) on the two specimens subjectd to c;hemical at­ tack and on the reference specimen. In this case the ben­ ding strength shall not be more than 20 per cent lower than the value ascertained for the test plate not subjes::ted to any stress. Test and quality required for the prototype unit 213141 The prototype tank shall be subjected to a hydraulic pressure test conducted by an expert approved by the com petent authorities of a Contracting Party. If the prototype tank is divided into compartments either by bulkheads of by baffle plates, the test shall be condu­ cted on a unit made for this purpose with the same external ends as the entire tank and which represents the part-of the tank subjected, under normal conditions of use, to the gre­ atest stresses. This test should not be conducted if there has already been a successful test on another prototype unit of the same section or a section with larger dimensions, geometri­ cally similar to that of the prototype unit in quesrion, even if <l>EK 225 EQ>HMEPI:[ THr KYBEPNH:[EQ:[ (TEYXOr nPQTO) that unit has a different internal surface layer. This test mus demonstrate that the prototype unit has, under normal conditions of use, a factor of not less than , 7 .5 so far as rupture is. concerned. • It must be proved, e.g. by calculation, that safety factors against fracture given in marginal 213140 (4) are com­ plied. with for each section of the tank. Rtipture occurs when the test liquid escapes from the tank in the form of jets. Consequently, before this rupture, the presence of delaminations and losses of liquid through these delaminations in the form of droplets is permitted. The prototype unit shall be submitted to a hydraulic press­ ure. H=7.5xdxh where H is the height of the column of water , • h is the height of the tank d is the density of the substance to be carried. If a rupture ocours with a water-column heght H 1 less than H, there must still be H 1 ;,.7 .5xdx(h-h 1 ) where h 1 is the height of the highest point where the first jet of liquid appears. Should the flow of liquid at point h 1 be too great, it is es­ sential to make a temporary repair and temporaty local strengthening to enable the test to continue to height H. Conformity check on tanks produced in series 213142 ( 1) The inspection of conformity on tanks produced in series shall be carried out by conducting one or more of the tests listed in marginal 213140. However, the measurement of the degree of polymeriza­ tion is replaced by Barco! hardness measurement. (2) Barco! hardness The test must be conducted in accordance with suitable procedures4. Barco! hardness measured on the internal surface of the finished tank shall not be less than 75 per cent of the value obtained in the laboratory on pure harde­ nedresin. (3) The percentage of glass fibre must be within the li­ mits prescribed in marginal 213140 (2) and, in addition, must not deviate by more than 10 per cent of the figure for the prototype tank. Tests and qualities required for all tanks before being put 213143 into service Leakproofness test The leakproofness test shall be conducted in accorqance with the provisions of Il¥lrginals 211150 and 211151 of ADR and the expert's stamp shall be applied to the tank. Section 5 213144 213149 Special provisions for tanks used for the carriage of substances with a flash point of 55 °C or lower The tank must be constructed so as to ensure the elimi- 213150 nation of static electricity from the various component parts so as to avoid the accumulation of dangerous electric charges. All metal parts of the tank and the transport unit and 213151 also wall layers conducting electricity must be interconnec • ted. The resistance between each conducting part and the 21315 2 chassis must not be higher than 106 ohms. Elimination of hazards due to charges generated by fric tion . The surface resistance and the discharge resistance to 213153 earth of the entire surface of the tank shall conform with the requirements of marginal 213154. 4. The procedures prescribed in standard ASTM-D 2583-67 are regarded as suitable. • ·The surface resistance and discharge resistance to eaith 213154 measured in accordance with marginal 213155 must sa tisfy the following requirements. i (1) Walls not equipped with electrically conducting ele­ ments: (a) Surfaces upon which one can walk: The discharge resistance to earth shall not be higher than 108 ohms. (b) Other surfaces: The surface resistance shall not be. higher than 109 ohms. (2) Walls equipped with electrically conducting ele­ ments: (a) Surfaces on which one can walk~ The discharge resistance to earth shall not be higher than 108 ohms. (b) Other surfaces: . 213 154 Conductance shall be considered as sufficient if the ma ximum thickness of non-conducting layers on conducting elements, for example conducting sheets, metal netting or other appropriate material, connected to the earthing con nexion, does not exceed 2 mm, and 'that in the case <if a metal netting, the surface area of the mesh does not exceed 64 cm2. (3) Any measurement of surface resistance or discharge resistance to earth required to be carried out on the tank itself shall be 'replaced at intervals of not more than one year to ensure that the specified resistances are not excee­ ded. Test Methods 213 155 1. Surface Resistance (RIOJ - (insulating resistance) in ohms, electrodes of conducting paint in accordance with figure 3 of Recommendation IEC 16 7 of 1964, measured in the standard 23/50 atmosphere according to Recom­ mendation ISO R291, paragraph 3.1, of 1963. , 2. The discharge resistance to earth in ohms is the'ratio between the direct voltage measured between an electrode described below in contact with the surface of the tank of the vehicle and the earthed chassis of the vehicle, and the total current. The conditioning of the specimens is the same as in pa­ ragraph 1. The electrode is a disc with a surface area of 20 cm2 and a diameter of 50 mm. Its close contacrwith the surface of the tank must be ensured, for example by using damp paper or a damp sponge or any other ~uitable substance. The earthed chassis of the vehicle is used as the other electrode. A direct voltage in the range of 100 volts 500 volts shall be applied. The measurement shall be car ried out after the test voltage has been applied for one min­ ute. The electrode may be placed on any point of the internal or external surface of the tank. If measuring is impossible on the tank, it may also be carried out, under the same conditions, in the laboratory, on a specimen of the material. . Elimination of hazards due to charges generated during M~g . Metallic components bonded to earth shall be provided 213 156 and so disposed that at any stage of the filling or emptying process there is an area of not less than 0.04 sq. metres of earthed metal in contact with the product per cubic meter of product ·contained in the tank at that instant, and that no part of the product shall be more than 2.0 metres from the nearest earthed metal component. Such metallic compo nents may take the form of: • • '(a) A metal foot valve, pipe outlet, or plate provided the total area of metal in contact with the liquid is not less than that specified, or , (b) A metallic grill with wire thickness not less than 1 mm diameter and hole area not greater than 4 sq. centi­ metres, provided that the total.area 9f the grill 'in contact with the liquid is not less than that specified. Marginal 213 156 shall not apply to reinforced-plastics 213 15 7 tanks equipped with any other system for eliminating the hazard from charges generated during filling, provided it has been demonstrated by a practical comparative test iri accordance with marginal 213 158 that the relaxation time 2340 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) of the charge generated within the tank during filling is eq­ uirnlent to that obtained for a metal tank of compar able dimensions. • Comparative test 213 158 ( 1) A comparative test of the electrostatic charge relaxa tion time in accordance with the conditions of test discribed in paragraph (2) shall be carried out on a prototype reinfor­ ced-plastics tank and steel tank in the following manner (see diagram 3). (a) The reinforced-plastics tank shall be mounted in \he same manner as it would be in use, for example, on a steel support simulating a vehicle's chassis, and shall be filled to not less than 75 per cent capacity with automotive dissel fuel, a proportion of which is passed through a suitable microfiher in such a manner that the charge density of the total flow is approximately 100~ c/m3. (b) The field strength in the tank vapour space shall be measured by a suitable continuous reading field meter mounted with its axis vertical and placed at least 20 cm from the vertical fill pipe. (c) A similar. test shall be carried out on a steel tank whose width, length, breadth, and volume are within 15 per cent of those of the reinforced-plastics tank, or on a reinforced-plastics tank of similar dimensions, coated internally with metal foil connected to earth. (2) The following conditions of test shall be met: (a) The test shall be carried out in a covered area in con­ ditions of relative humidity less than 80 per cent. (b) The automotive diesel fuel used in the test shall have a rest conductivity at the temperature of measurement bet­ ween 3 and 5 p5 /m. This shall be measured in a cell in which VT/d2 is less than or equal to 2.5xl06 where V = applied voltage d = spacing between electrodes in metres T = duration of measurement in seconds The rest conductivity measured on samples of the product taken from the test tank after'filling shall not differ in successive tests on plastics and metal tanks by more than 0.5 p5/m. ( c) Filling shall be at a constant rate within the range 1 to 2 m3 /min and shall be the same for the reinforced-plastics tank and for the steel tank. At the end of filling, the flow should be stopped in a time which is short compared with the relaxation time for the charge in the steel tank, (d) The charge density shall be measured by a suitable continuous reading meter (for example, a field mill type) immersed in the product and placed as close as possible to the filling pipe. (e) The supply pipes and the vertical filling pipe shall be of 10 cm internal diameter and shall terminate in a "T" type filling pipe outlet. (I) A suitable microfilter, • with an adjustable by-pass enabling the proportion of flow passing through it to be reg­ ulated, shall be fitted not more thim 5 m from the filling pipe outlet. (g) The liquid level shall not reach the bottom of the fil­ ling pipe or the field meter. Comparison of relaxation times (3) The initial value of the field strength shall be that re­ corded at the earliest point of time after the cessation of flow of the fuel when a smooth decay curve has been estab­ lished. The relaxation time in both tests shall be expressed as the time taken for the field strength to decay from the initial value to 0.37 of the initial value. (4) The relaxation time of the reinforced-plastics tank shall not exceed that of the steel tank. Table 1. COMPOSITION OF GLASS Glass E: Composition by weight: 213 159 213 999 Silica Alumina Lime Magnesia Boric Oxide Fluorine Ferric Oxice Titanium Oxide Alkaline Oxides Glass C: 52 to 55 per cent 14 to 15.5 per cent 16.5 to 18 per cent 4 to 5.5 per cent 6.5 to 21 per cent 0.2 to 0.6 per cent < 1 per cent Composition by weight: Silica Alumina Lime Magnesia Boric Oxide Iron Sodium Oxice Potassium Oxide < 1 per cent 63.5 to 65 per cent 4 to 4.5 per cent 14 to 14.5 per cent 2.5 to 3 per cent 5 to 6.5 per cent 0.3 per cent 7 to 9 per cent 7 to 9 per cent • A Rellumit 5 has been found to be suitable. E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) • Diagram 1. Device for measuring impact resistance by means of a spherically-ended falling weight . ---- ----r Section AX A A' · 0 8 n 1 1 8 8 ~ Angle-bar walded to chassis i - Concrete base I . ------------~ 400 .. 2:342 ECI>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Diagram 2. Device to test resistance to chemical agents. 125 --------, 190 =--= ·,.?": -- --i-~ ,'/ ,# ,,, I// ., ./ // '/ / I .. \ / \/ / 0 I ,.-\ I • I ' ......... ----L-----/ ...::r~ -:. / 0 • " ,~/ .0 Ill • Tightening (clamp) glass cylinder level of liquid Heating sheath Teflon joint Specimen plate (liquid phase) Tightening ring (clamp) Bolts threaded to wing nuts (M6 X 200) STORAGE TANK /. ~ ~ FLOW METER FLOW BY PASS ! MICROFILTER PUMP Diagram 3. Schematic layout of rig for comparative test. SUPPLY PIPES "' ..• of;.' CHARGE DENSITY METER / FILLING PIPE ~ FIELD METER ·-··. ·----- ~;.· f .. TANK UNDER TEST m a :::i: s: m "lJ M I :::i: M " -< a, m "lJ 2 :::i: M m :0 M =i m < >< 0 M :::J "lJ :0 I 0 a,,;, i ~ ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) Appendix B.ld REQUIREMENTS CONCERNING THE MATERIALS AND CONSTRUCTION OF FIXED TANKS, OF DEMOUNTABLE TANKS, AND OF SHELLS OF TANK-CONTAINERS, INTENDED FOR THE CAR­ RIAGE OF DEEPLY-REFRIGERATED LIQUEFIED GASES OF CLASS 2 214000 214249 ( 1) Receptacles, tanks and shells shall be made of steel, 2142 50 aluminium, aluminium alloy, copper or copper alloy, e.g. brass. However, receptacles, tanks and shells made of copper or copper alloy shall be allowed only for gases co ntaining no acetylene; ethylene may however contain not more than 0.005 per cent acetylene. (2) Only materials appropriate to the lowest working temperature of the receptacles, tanks and shells and of their fittings and accessories may be used. Impact strength 1, 2 of sheet metal and weld beads at lowest working tempe rature Material kgrn/cm2 , 3 kgrn/cm2, 4 Unalloyed killed steel 3.5. 2.8 Ferritic alloy steel Ni< 5% 3.5. 2.2 Ferritic alloy steel 5% ,,;;; Ni,,;;; 9% 4.5. 3.5 Austenitic Cr-Ni steel 4.0 3.2 1 Impact strengths determined with different test-pieces are not mutually comparable. 2 See marginals 214275 to 214277. 3 The values relate to test-pieces with a U-shaped notch as illustrated below. 4 The values relate to test-pieces with a V-shaped notch confor­ ming to ISO R 148. The following materials shall ~e allowed for the man- ,,2 1 4 2 5 1 -= ufacture of receptacles, tanks anil shells: • ,,1 (a) steels not subject to brittle fracture at the lowest wor- "\,Q 1 king temperature (see marginal 214265). 1/.'.' The following may be used: I 1. fine-grained unalloyed steels, down to a temprerature of -60°C; 2. nickel steels (with a nickel content of 0.5 to 9 per cent), down to a temperature of -196 ° C, depending on the nickel content; 3. austenitic chrome-nickel steels, down· to a tempe­ rature of -270°C; r. ..... - --t 7 + O,l (b) aluminium not less than 99.5 per cent pure, or al­ uminium alloys (see marginal 214266); - ,l- - . .1.---------------'~;... (c) deoxidized copper not less than 99.9 per cent pure, or copper alloys having a copper content of over 56 per cent (see marginal 214267). ·<--· 55 • ---,· I (1) Receptacles, tanks and shells shall be either seam- 214252 less or welded. (2) Receptacles under marginal 2207 miide of auste­ nitic steel, of copper or of copper alloy may alternatively be hard-soldered. The fittings and accessories may either be screwed to 214253 the receptacles, tanks and shells or be secured there to as follows: • (a) receptacles, tanks and shells made of steel, alumi­ nium or aluminium alloy: by welding; (b) receptacles, tanks and shells made of austenitic steel, of copper or of copper alloy: by welding or hard­ soldering. The construction of receptacles, tanks and shells and 214254 their attachment to the vehicle, to the underframe or in the container frame shall be such as to preclude with certainty any such reduction in the temperature of the ioad-bearing components as would be likely to render them brittle. The means of attachment of receptacles, tanks and shells shall themselves be so designed that even when the receptacle, tank or shell is at its lowest working temperature they still possess the necessary mechanical properties. 1 ; Materials, receptacles, tanks and shells (a) Steel receptacles, tanks and shells The materials used for the manufacture of receptacles, tanks and shells, and the weld beads, shall at their lowest working temperature meet at least the following require­ ments as to impel strength. The tests may be conducted with test-pieces having ei­ ther a U-shaped or a V-shaped notch. 214255 214264 214265 In the case of austenitic steels, only the weld bead need be subjected to an impact-strength test.· For working temperatures below -196 ° C the impact strength test is not performed at the lowest working tem­ perature, but at -196 °C. (b) Receptacles, tanks and shells made of aluminium or al­ uminium alloy The seams of receptacles, tanks and shells shall at am- 214266 bient temperature meet the following requirements as to bending coefficient: rrhickness of sheete in mm Bending coefficient k 1 for the seam ~oot in compres- Root m s10n zone tension zone .,;;;; 12 ;;;,, 15 ;;;,, 12 > 12 to 20 ;;;,, 12 ;;;,, 10 > 20 ;;;,, 9 ;;;,, 8 1 See marginal 214 285. (c) Receptacles, tanks and shells made of copper or copper alloy It is not necessary to carry out tests to determine whe­ ther the impact strength is adequate. 2. Tests (a) Impact-strength tests 214267 214268 214274 ECJ>HMEPll: THI: KYBEPNHl:EQl: (TEYXOl: nPQTO) 2345 The impact strengths indicated in marginal 2142 65 re- 2142 7 5 late lo lest-pieces measuring 10Xl0 mm and having a U-shaped or a V-shaped notch. • • Notes: 1. With regard to the shape of the test-piece, see mar­ ·ginal 214265 (table), footnoles3 and4. 2. For sheets less than 10 mm but not less than 5 mm thick, tesl0 pieces with a cross-section of 10 X e mm, wnere «e» represents the thickness of the sheet, shall be used. Such impact-strength tests generally yield higher values than do such tests on standard test-pieces. 3. No impact-strength test shall be carried out on sheets less than 5 mm thick, or on their seams. (1) For testing sheets the impact strength shall be deter- 214276 mined on three lest-pieces. Test-pieces with a U-shaped notch shall be taken al right angles to the direction of rol ling and test-pieces with a V-shaped notch in the.direction of rolling. Appendix B.ld (2) For testing seams the lest -pieces shall be taken as follows: e~lO three lest-pieces from the centre of the weld; • three lest-pieces from the zone of deformation created by the weld (the notch shall be completely outside the melted area but as near to it as possible); i.e. six test-pieces in all. Centre of weld Zone of deformation The test-pieces shall be so machined as to have the ma­ ximum possible thickness. l0<e~ 20 three lest-pieces from the centre of the weld; three test-pieces from the zone of deformation; Centre of weld l.i ( I I I Zone of deformation i.e. six test-pieces in all. e>20 Two sets of three test-pieces (one set on the upper face, one set on the lower face) al each of the points indicated below: Centre of weld Zone of deformation i.e. twelve test-pieces in all. (1) For sheets, the average of the three tests shall meet 214277 the minimum values indicated in marginal 214265; none of the values may be more than .30 per cent below the mi nimum shown. (2) For welds, the average values obtained from the test­ pieces taken al the different points, centre of weld and zone of deformation, shall correspond to the minimum values in­ dicated. None of the values may be more than 30 per cent below the minimum indicated. 214278 (b) Determination of bending coefficient 214284 (1) The bending coefficient k referred to in marginal 214285 214266 is defined asfollows: e k = 50 ----, r where e= thickness of the sheet in mm; and r=mean radius of curvature in mm of the test-piece when the first crack appears in the tension zone. (2) The bending coefficient k shall be determined for the jeam. The width of the lest piece shall be equal to 3 e. (3) Four tests shall be performed on the seam, two with the root in the compression zone (fig. 1) and two with the root in the tension zone (fig. 2) all individual values ob­ tained shall meet the minimum -value requirements of marginal 214266. fig. 2 214286 219999 2346 E<DHMEPII TH'I KYBEPNHIEQI (TEYXOI nPQTO) Appendix B.2 ELECTRICAL EQUIPMENT (1) The lighting of vehicles shall be electrical (2) The electrical equipment of vehicles shall meet the following requirements: Requirements applicable to the electrical equipment as a whole (a) Wiring: Conductors shall be generously dimensioned to prevent overheating. They shall be appropriately insula­ ted. Circuits shall be protected against excess current by fuses or automatic cut - outs. The wiring shall be fumly attached and so placed that the conductors are protected against impacts, projected stones and heat emitted by the exhaust system (b) Storage batteries: A switch for breaking all the elec­ tric circuits shall be placed as close to the battery as possible. A direct or remote control system shall be instal­ led in the driving cab and outside the vehicle. It shall be easily accessible and distinctively marked. The switch shall be openable while the engine is running without causing a dangerous surge. The electrical supply to the tachograph may, however, be provided by a circuit connected direct to the battery. This apparatus and its. installation shall be intrinsically safe in a mixt~re consisting of 2.0 per cent hydrogen and 80 per cent air. If the batteries are situated elsewhere than under the engine bonnet, they shall be secured in a vented case of metal or another material of equivalent strength, with insulating inner walls. Requirements applicable to the part of the electrical equipment situated behind the driver's cab (c) The whole of this equipment shall be so designed, installed and protected as not to be able to cause ignition or short circuiting in normal conditions of use of the vehicles and as to reduce to a minimum the risk of either occurrence in the event of impact or distortion. In particular: 1. Wiring Conductors [see 2 (a)] shall consist of cables protected by seamless and rust - proof casings. 2. Lighting Screw - cap bulbs shall not be used. If the lamps in the body of the vehicle are not fixed in parts of the walls or ceiling so strengthened as to protect them against any mechanical damage, they should be protected by a strong cage or grid. Appendix B.2 220000 220001 220002 The inflammable gases and articles of Class 2 whose carriage is not exempted by the provisions of marginal 21251 from the application of the requirements of marginal 220000 are the follo­ wing (a) Compressed gases Hydrogen [l O (b)] Methane [l O (b)] Carbon monoxide [l O (bt)] Mixtures of gases of 2° (b) Synthetic gases [2 ° (bt)] Town gas [2° (bt)] Water gas [2° (bt)] (b) Liquefied gases Butane [3° (b)] Butylene [3 ° (b)] Cyclopropane [3 ° (b)] Isobutane [3 ° (b)] Isobutylene [3 ° (b)] Propane [3 ° (b)] Propylene [3 ° (b)] Ethyl chloride [3 ° (bt)] Methyl chloride [3 ° (bt)] Dimethyl ether [3 ° (bt)] Ethylamine [3 ° (bt)] Hydrogen sulphide [3 ° (bt)] Methylamine [3 ° (bt)] • Methyl mercaptan [3 ° (bt)] .Trimethylamine [3 ° (bt)] Butadiene [3 ° (c)] Vinyl chloride [3 ° ( c)] Appendix B.2 Vinyl bromide [3 ° (et)] Cyanogen chloride [3 ° (et)] Ethylene oxide [3 ° (et)] Gaseous mixtures A. AO, Al, B or C [4° (b)] Ethane [5° (b}] Ethylene [5° (b)] (c) Deeply - refrigerated liquefied gases The gases of 7° (b) and 8° (b} (d) Gases dissolved under pressure Acetylene [9° (c)] (e) Articles containing gas Aerosol dispensers of 10°, (b) and (bt) Appendix B.3 20002 (contd) 220003 229999 (see marginal 10182) 230000 CERTIFICATE OF APPROVAL FOR VEHICLES CAR- 239999 RYING CERTAIN DANGEROUS GOODS 1. CERTIFICATE NO. 2. testifying that the vehicle specified below fulfils the conditions prescribed by the European Agreement concer­ ning the International Carriage of Dangerous Goods by Road (ADR) for its acceptance for the international car­ riage of dangerous goods by road. 3. Valid until ............................ • .. 4. This certificate must be returned to the issuing ser­ vice when the vehicle is taken out of service; if the vehicle is transferred to another owner; on expiry of the validity of the certificate; and if there is a material change in one or more essential characteristics of the vehicle. 5. Type of vehicle: closed vehicle, open vehicle, tank vehicle with / without closed / open trailer / semi trailer (strike out words which do not apply) ........ . 6. Name and business address of carrier (owner) .. . 7. Registration number (if' none: chassis number) .. . 8.' The vehicle described above has undergone at ......................... the inspection prescribed by ADR, An­ nex B, marginal 10182 and fulfils the conditions required for its acceptance for· the international carriage by road of dangerous goods of Classes ................... . item numbers .... .......................... . 9. Remarks ............................... . 10 ............................... 19 .......... . 11. Signature and stamp of issuing service at ...... . Appendix B.3 • 12. The validity of this certificate is extended until .. 13. Signature and stamp of issuing service at . 14. The validity of this certificate is extended until .. 15. Signature and stamp of issuing service at . 16. The validity of this certificate is extended until .. I 7. Signature and stamp of issuing service at . Notes: 1. • The dimensions of the certificate. shall be 210 X 297 mm (format A 4). Both front.and back shall be used. The colour shall be white, with a pink diagonal stripe. 2. Every trailer shall be the subject of a separate certifi­ cate unless it is covered by the certificate of the vehicle to which it is coupled. 3. Where a certificate is issued pursuant to article 4, paragraph 2, of the Agreement to a vehicle whose constru­ ction does not entirely conform to the requirements laid down in Annex B, the certificate's validity shall not extend beyond the duration of the derogation granted by the said article 4, subject where appropriate to the provisions of marginals 11605, 21605, 31605 and 61605; and the text of paragraph 8 of the certificate of approval shall be replaced by the following • The vehicle described above does no~ entirely• to the benefit of the provisions of article 4, paragraph 2, of the Agreement-. · Appendix 8.4 Tables concerning the carriage. of dangerous substances of CLASS 7; Label to be placed on vehicles carrying these substances. The minimum distances indicated in the table below bet- 240000 ween radioactive substances and areas on vehicles reser ved for the driving arid accompanying personnel are com patible with the provisions of marginal 3659(8) Total sum of transport index Minimum distances in metres, no sheilding mate rial intervening, from Ii ving accommodations or regularly occupied wor king space Applicable data in the case of exposure time not exceeding 250 hours per annum Less than 2 1.0 2 to 4 1.5 4 to 8 2.5 8 to 12 3.0 12 to 20 4.0 20 to 30 5.0 30 to 40 5.5 40 to 50 6.5 the minimum safetey distances referred to in marginal 365 7 for the loading and storage of packages which bear a label «FOTO» together with packages of Category II YELLOW or Category III - YELLOW are given in the following table. Separation distances for the loading and the storage of packages which bear a label with the word FOTO ~ogether with packages of Categories II - YELLOW or III - YEL­ LOW •Conform to the requirements laid down in Annex B, but is entitled. 240001 Appendix 8.4 Total sum of the Journey or storage duration, in ~o~·rs packages of the category lfotal sum YEL- YEL of the LOW LOW II transport 1 2 4 10 24 28 120 240 index III Mini111um .. 0.2 0.5 0.5 0.5 0.5 0.5 0.5 0.5 1 1 0.5 0.5 1 2 2 0.5 1 1 4 4 1 1 1.5 8 8 1 1.5 2 1 10 10 1 2 3 2 20 20 l.5 3 4 3 30 30 2 3. 5 4 40 40 3 4 5 5 50 50. 3 4 6 I Appendix 8.4 distances in 0.5 1 1 1 1. 2 1 2 3 1 1.5 3 3 4 6 4 6 8 4 7 9 6 9 13 7 11 16 8. 13 18 .9 14 • 20 metres 2 3' 3 5 5 7 4 9 '9 13 13 18 14 20 20: 30 25 35 30 40 32 45 240002 240009 . The label to be affixed tote walls of vehicles pursuant 240010 to the provisions of marginal 3659(6) shall conform to the model reproduced below: RADIOACTIVE , ' , .., , , ,· , , , , (Minimum lenght of side: 15 cm) Symbol and inscription black on white ground , , , , , , , , ., , 240011 249999 2:.-148 EG>HMEPII THI: KYBEPNHIEQI (TEYXOI nPQTO) Appendix B.5 LIST OF SUBSTANCES MENTIONED UNDER MARGINAL 10500 (2) NOTE The first figure in the hazard - identification number indicates the primary hazard as follows: 2. Gas 3. Inflammable liquid 4. Inflammable solid 5. Oxidizing substance or organic peroxide 6. Toxic substances 8. Corrosive The second and third figures indicated secodary ha­ zards: 0. no meaning 1. explosion risk 2. gas may be given off 3. inflammable risk 5. oxidizing risk 6. toxic risk 8. corrosive risk 9. risk of vi~lent reaction from spontaneous decomposition or self-polymerization Where the first and second figures are the same, an intensification of the primary hazard is indicated, viz. 33 means a highly inflammable liquid (falsh - point below 21 ° C); 66 indicates a very dangerous toxic substance; 88 means a very dangerous corrosive substance. Where the first two figures are 22, a refrigerated gas is indicated. The combination 42 indicates a solid which may give off a gas on contact with water. Where the hazard - identification number is preceded by the letter «X», this indicates an absolute prohibition of the application of water to the product. The substances mentioned under marginal 10500 (2) 250000 are listed below: ECJ>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) 2349 Appendix B.5 Hazard Substance Class and Identification Identification Name of Substance item number No No (upper part) (lower part) (a) (b) (c) (d) A Acetal (1, 1-diethoxyethane) 3, 1 °(a) 33 1088 Acetaldehyde 3, 5° 33 1089 Acetic acid, glacial (and its acqueous solutions containing more 8, 21°(c) 83 1842 than 80% pure acid) Acetic anhydride 8, 21°(e) 83 1715 • Acetic ester (see ethyl acetate) 3,.5° Acetone 33 1090 Acetone cyanohydrin (see 2-cyanopropan-2-01) Acetonitrile 6.1, 2°(b) 633 1648 Acetyl Chloride 8, 22° 83 1717. Acrylaldehyde 3, 1 °(a) 336 1092 Acrylonitrile 6.1, 2°(a) 633 1093 Air 2, 8°(a) 22 1003 Alcohol (see ethanol) Ally! alcohol 6.1, 13°(a) 63 1098 Allyl chloride 6.1, 4°(a) 633·· 1100 Ammonia 2, 3°(at) 268 1005 Ammonia, dissolved in water, with mor than 35% but not more 2, 268 2073 than 40% ammonia by weight Ammonia, dissolved in water, wit more than 40% but not more 2, 9°(at) 268 • 2073 than 50% ammonia by weight Amyl acetate (see pentyl acetate) Amyl alcohols (other than tertiary) 3, 3° 30 1105 Amyl alcohol, tertiary 3, 1 °(a) 33 1105 Appendix 8.5 (a) (b) (c) (d) Aniline 6.1, ll 0(b) 60 1547 Antimony pentachloride 8, 11 °(a) 80 1730 Argon (refrigerated) 2, 7°(a) 22 1951 B Benzaldehyde ~ 3, 4° 30 1990 Benzene 3, 1 °(a) 33 1114 Benzoyl chloride 8, 22° 83 1736 Bromine 8, 14°. 886 1744 1,3 Butadiene 2, 3°(c) 239 1010 Butane 2, 3°(b) 23 1011 Butan-1-01-(butyl alcohol, normal) 3, 3° 30 1120 Butan-2-01 (sec-butyl alcohol) 3, 3° 30 1121 Butanol, tertiary 3, 5° 33 1122 n-Butyl acetate 3, 3° 30 1123 sec-Butyl acetate 3, 1 °(a) 33 1124 n-Butyl alcohol (see butan-1-01) sec-Butyl alcohol (see butan-2-01) • Butylamine 3, 5° 338 1125 n-Butyl chloride (see 1-chlorobutane) 1-Butylene . 2, 3°(b) 23 1012 Butyraldehyde 3, 1 °(a) 33 1129 C Calcium chlorate solution 5.1, 4°(a) 50 2429 Carbon dioxide 2, 5°(a) 20 1013 Carbon dioxide, liquid (refrigerated) 2, 7°(a) 22 2187 Carbon disulphide 3, 1 °(a) 336 1131 Carbonyl chloride (see phosgene) Chlorine 2, 3°(at) 266 1017 Chlorobenzene 3, 3° 30 1134 2350 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO} Appendix B.5 ,, . (a) (b) (c) (d) 1-Chlorobutane (butyl chloride) 3, 1 °(a) 33 1127 Chlorodifluoromethane (R22) 2, 3°(a) 20 1018 l-Chloro-2, 3-epoxypropane 6.1, 12"(a) 663 2023 ( epichlorohydrin) , 2-Chloroethanol (see glyc,ol chlorohydrin) Chloroprene 3, 1 °(a) 336 1991 Chlorosulphonic acid 8, 11 "(a) 88 1754 Chlorotrifluoromethane (Rl3) 2, 5:(a) 20 1022 Cresols 6.1, 22°(a) 60 2076 Cumene 3, 3° 30 1918 Cyanides, inorganic, solutions of 6.1, 31 °(b) 66 1935 2-Cyanopropan-2-01 (acetone cyanohydrin) 6.1, ll"(a) 66 1541 Cyclohexane 3, 1 °(a) 33 1145 Cyclohexanole 3, 3° 30 1915 Cyclohexane 3, 1 °(a) 33 2256 Cyclopentane 3, 1 °(a) 33 1146 Cyclopropane 2, 3°(b) 23 1027 D Decahydronaphthalene 3, 3° 30 1147 Diacetone alcohol, technical 3, 5° 33 1148 1,2-Diaminoethane (ethylene diamine) 8, 35° 83 1604 1,6-Diaminohexane (hexamethylene diamine) 8, 35° 80 1783 Dichlorodifluoremethane (Rl2) 2, 3°(a) 20 1028 1,2-Dichloroethane 3, 1 °(a) 336 1184 Dichlorofluoromethane (R2 l ), 2, 3°(a) 20 1029 Dichloromonofluoromethane (see dichlorofluoromethane) Appendix 8.5 (a) (b) (c) (d) Dichloropropene 3, 3° 36 2047 1,2-Dichloro-1, 1,2 2, 3°(a) 20 1958 2-tetrafluoroethane (R.114) 1,1-Diethoxyethane (see acetal) ,, Diethylamine 3, 5° 338 1154 diethyl benzene 3, 4° 30 2049 Diethyl ether (sulphuric ether) 3, 1 "(a) 33 1155 Di-isopropyl ether 3, 1 °(a) 33 1159 2,2-Dimethyl benzyl hydroperoxide 5.2, 10° 539 2116 Dimethyl carbonate 3, 1 °(a) 33 1161 Dimethyl ether 2, 3°(bt) 23 1033 Dimethyl sulphate , 6.1, 13°(b) 663 1595 Dioxane 3, 5° 336 1165 Disulphur dichloride . 8, 11 °(a) 886 1828 .~ ~ E t,, Epichlorohydrin (see l-chloro-2,3-epoxypropane) Ethanethiol (ethyl mercaptan) 3, 1 °(a) 336 2363 Ethanol (ethyl alcohol, alcohol) 3, 5° 33 1170 Ethoxyethyl acetate 3, 3° 30 1172 Ethyl acetate (acetic ester) 3, 1 °(a) 33 1173 Ethyl acrylate 3, 1 °(a) 339 1917 Ethyl alcohol (see ethanol) Ethyl benzene 3, 1 °(a) 33 :1175 Ethyl chloride 2, 3"(bt) 23 1037 Ethylene 2, 5°(b) 23 1962 Ethylene, (refrigerated) 2, 7°(b) 223 1038 Ethylene diamine (see 1,2-diaminoethane) Ethyl formate 3, 1 °(a) 33 1190' Ethyl silicate (see tetraethyl silicate) Ethyl mercaptan (see ethanethiol) E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Appendix B.5 : (a) (b) (c) (d) F Fluoboric acid (aqueous solutions containing not more than 8, 7° 88 1775 78% pure acid) Formic acid (containing not less than 70% pure acid) 8, 21°(b) 80 1779 Furfural 3, 4° 36 1199 G Glycol chlorohydrin (2-chloroethanol) 6.1, 12°(b) 66 1135 H Hexamethylene diamine (see 1,6-diaminohexane) Hydrazine•in aqueous solutions contraining not more than 72% hydrazine: solutions containing more than 64% 8, 34° 86 2029 solutions containing not more than 64% 8, 34° 86 2030 Hydrobromic acid, anhydrous (see hydrogen bromide) Hydrobromic acid, solutions of 8, 5° 88 1788 Hydrocarbons, liquid, pure or in mixtures, not otherwise speci fied in this Appendix: with a flash point below 21 ° C 3, 1 °(a) 33 1203 . -with a flash poin.t between 21 ° C and 55° C 3, 3° 30 • 1223 with a flash point above 55 ° C 3, 4° 30 1202 Hydrocarbon gas mixtures, A, AO, Al, B and. C (liquefied) 2, 4°(b) 23 1965 Hydrochloric acid, anhydrous (see Hydrogen chloride, liquefied) • Hydrochloric acid, solutions of 8, 5° 88 1789 Hydrocyanic acid solutions (containing not more than 20% hyd- 6.1, 1 °(b) 66 1613 rocyanic acid) Hydrofluoric acid, aqueous solutions containing more than 85 per cent pure acid 8, 6°(b) Hydrofluoric acid, aqueous solutions containing more than 60 per cent but not more than 85 per cent pure acid 8, 6°(c) 886 1790 Hydrofluoric acid, aqueous solutions containing not more than 60 per cent pure acid ·, 8, 6°(d) Hydrofluoric acid, anhydrous (see hydrogen fluoride) . Hydrogen bromide 0 2, 3°(at) 286 1048 Hydrogen chloride 2, 5°(at) 286 1050 Hydrogen fluoride (anhydrous hydrofluoric acid) 8, 6°(a) 886 1052 Hydrogen peroxide solutions containing more than 40% but not more than 60% hydrogen peroxide 8, 41 °(a) 85 2014 containing more than 6% but not more than 40% hydrogen peroxide 8,41 °(b) 85 2014 Hydrogen peroxide and solutions of hydrogen peroxide contai ning more than 60% hydrogen peroxide 5.1, 1 ° 559 2015 Hypochl~rite solutions ;,: containing more than 50 gm available chlorine per litre 8,37°(a) 85 1791 containing not more than 50 gm available chlorine per litre 8, 37°(b) • 85 1791 I lsobutane 2, 3°(b) 23 1969 Isobutyl acetate 3, l 0 (a). 33 1213 lsobutvlene 2, 3°(b) 23 1055 isoprene cmethyl butadienes 3,1 °(a) 339 1218 lsopropanol (see propan-2-ol) Isopropyl acetate 3, 1 °(a) 33 1220 Isopropyl alcohol (see propan-2-ol) lsopropylamine 3, 5° 338 1221 L Laughing gas (see nitrous oxide) Lead alkyls, mixtures with halogenated organic compo.nuds e.g. 6.1, 14° 663 1649 ethyl fluid M p-Menthanyl hydroperoxide (with peroxide content not exceeding 5.2, 14° 539 2125 95% 2:i::,2 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) :\1 ethane ( refrigerated) 2, 7°(b) 223 1972 Methanol (methyl alcohol, wood spirit) 3, 5° 336 1230 MPthoxymethane (see dimethyl ether) Methyl acetate 3, 1 °(a) 33 1231 Methyl arcylate 3, 1 °(a) 339 1919 Methylal 3, 1 °(a) 33 1234 Methyl alcohol (see methanol) Methylamine 2, 3°(bt) 263 1061 Methylamyl alcohol 3, 3° 30 2053 Methyl bromide (bromotethane) 2, 3°(at) 263 1062 Methyl butadiene (see isoprene) Methyl chloride (chloromethane) 2, 3°(bt) 236 1063 Methyl ethyl ketone 3, 1 °(a) 33 1193 Methyl formate 3, 1 °(a) 33 1243 Methyl isobutyl ketone 3, 1 °(a) 33 1245 Methyl methacrylate 3, 1 °(a) 339 1247 Methyl propionate 3, 1 °(a) 33 1248 Methyl vinyl ether 2, 3°(ct) 239 1087 Methyl vinyl ketone 3, 1 °(a) 33 1251 Mixed nitrating acids (sulphuric. and nitric acids) containing more than 30% pure nitric acid 8, 3°(a) 856 1796 containing not more than 30% pure nitric acid 8, 3°(b) 886 1796 Mixtures A, AO, Al, Band C (see hydrocarbon gas mixtures, liquefied) Monochlorodifluoromethane (see chlorodifluoromethane Monomethylamine (see methylamine) Monomethylamine, aqueous solutions 3, 5° 336 1235 N Naphthalene in the melted state 4.1, l1°(c) 44 2304 Natural gas (refrigerated) 2, 8°(b) 223 2043 Nitric acid containing more than 70% pure acid 8, 2°(a) 856 2032 containing more than 55% but not more than 70% pure acid 8, 2°(b) 886 2031 / 1 "' Nitrobenzene 3, 4° 36 1662 Nitrogen (refrigerated) 2, 7°(a) 22 1977 Nitrogen dioxide No 2 (nitrogen peroxide, nitrogen tetroxide N20 4 2, 3°(at) 265 1067 Nitrogen peroxide (see nitrogen dioxide) Nitrogen tetroxide (see nitrogen dioxide) Nitrous oxide N20 2, 5°(a) 25 1070 0 Oleum 2,7°(a) 225 1073 Oxygen (refrigerated) p 3,1 °(a) 33 1264 Paraldehyde 8, 1 °(a) 886 1831 Pentyl acetate (amyl acetate) 3, 3° 30 1104 Perchloric acid, in aqueous solutions: containing more than 50% but not more than 72.5% perch loric acid 5.1, 3° 588 1873 containing not more than 50% pure acid 8, 4° 85 1802 Phenol 6.1, l3°(c) 68 1671 Phosgene 2, 3°(at) 266 1076 Phosphorus oxychloride (see) phosphoryl chloride) Phosphorus trichloride 8, 11 °(a) 88 1809 Phosphorus, white or yellow 4.2, 1° 436 1381 Phosphoryl chloride (phosphorus oxychloride) 8, 11 °(a) 88 1810 Potash lye 8, 32° 88 181.4 Potassium 4.3, 1 °(a) X423 2257 Potassium chlorate solution 5.1, 4°(a) 50 2427 Propane 2, 3<b) 23 1978 n-Propanol (propyl alcohol) 3, 5° 33 1274 Propan-2-ol (isopropyl alcohol) 3, 5° 33 1219 Propionaldehyde 3, 1 °(a) 33 1275 Propyl acetate Propyl alcohol (see n-propanol) 3, 1 °(a) 33 1276 P.ropylene 2, 3°(b) 23 1077 Propylene diamine 8, 35° 83 2258 Propylene oxide 3, 1 °(a) 336 1280 Pyridine 3, 5° 36 1282 E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPOTO} 23S3 R Rl2 (see dichlorodifluoromethane) Rl3 (see chlorotrifluoromethane) R2 l (see dichlorofluoro methane) R22 (see chlorodifluoro methane) Rl 14 (see dichlorotetrafluoroethahe) s Silicon tetrachloride 8, 11 °(a) 88 1818 Soda lye 8, 32° 88 1824 Sodium 4.3, 1 °(a) X423 1428 Sodium chlorate solution 5.1, 4°(a) 50 2428 Sodium chlorite solution 5.1, 4°(c) 50 1908 Styrene 3, 3° 30 2055 / ' / Sulphur dioxide 2, 3°(at) 26 1079 Sulphuric acid containing more than 85% pure acid 8, 1 °(a) 88 -1830 containing more than 75% but not more than 85% pure acid 8, 1 °(b) 88 1830 containing not more than 75% pure acid 8, 1 °(c) 88. 1830 waste, completely denitrated 8, 1 °(d) 88 1832 Sulphuric and nitric acids (see mixed nitrating acids) Sulphuric ether (see diethyl ether) Sulphur in the melted state 4.1, 2°(b) 44 2448 Sulphurous acid, anhydrous (see sulphur dioxide) Sulphur trioxide 8, 9° 885 1829 Sulphuryl chloride 8, 11 °(a) 88 1834 T Tetraethyl lead 6.1, 14° 663 1649. Tet~aethyl silicate (ethyl silicate) 3, 3° 30 1292 Tetrahydrofuran 3, 5° 33 2056 Tetramethyl lead 6.1, 14° 663 1649 Thionyl chloride 8, 11 °(a) 88 1836 Titanium tetrachloride 8, 11 °(a) 88 1838 Toluene 3, 1 °(a) 33 1294 Triethylamine 3, 5° 336 1296 Triethylene tetramine 8, 35° 80 2259 Trimethylamine 2, 3°(bt) 236 1083 Trimethylamine, solutions of 3, 5° 336 1297 266-trimethyl norpinanyl hydroperoxide with a peroxide content not exceeding 95% 5.2, 15° 539 2162 Tripropylamine 8, 35° 83 2260 Turpentine 3, 3° 30 1299 V Vinyl acetate 3, 1 °(a) 33 1301 Vinyl chloride 2, 3°(c) 239 1086 w Wood spirit (see methanol) X Xylenes 3, 3° 30 1307 Xylenols 6; 1, 22°(b) 60 2261 2354 E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) Appendix B.5 Identification numbers shall be shown on the plate as 250001 indicated below: . i I I ~i;~~ ., ·.a: . . . ..... :;;,~!'!~-c - ; . ,. •• ...;... ... .. . •· · - ~ . -~; . l I t ~- £': .• . . .. . .. .. ':-: . --- . Background orange. Border, horizontal line and figures black, 15 mm thic­ kness. 250002 250999 Identification number of danger (2 or 3 figures). Identification number of s~bstance (4 figures). '11EK 225 ECDHMEPII THI KYBEPNHIEOI (TEYXOI nPOTO) 0IK0N0iv:iIRH .ETIITP0flH rIA THN :B."YPQIIH EHI TPO[ili JiE'rAWPhJN i~QTEPIKOY EvpwnaIX:rj Eu µcpwvC a. r 1, a. 't'T) i'.l 1, e:.-& vrj 061. 11.rj M e:"to:cpopct Ere 1.- • }itvodvwv Eµnope:uµcfx.w.v (ADR). .. "Ka·1. ITpw"tox.oAAO Ynoypacpf/<; Ynoyp&cpnxe:· C't'T) re:vE~T) "t"T)V30 EETC't'Eµ~pCou I957 TO"MOE I . (:Zuµcpwv(cx, I1pw"t61-toAAO Ynoypa:cpt'j<; 'Ka1, IIo:pcfp,;T)µa ~) H lifQMENA Ee NH I978 .. n P. 0 AO r OE To napaxa,;w, rt.e:C µc: vo rce:p t.A!lf.J.~~ve: 1.,. e:rct. npoo{}ti:wc; 'tT)<; EuµcpwvCcx<; rt.at. ,;ou Ilpw,;ox6A.Aou Ynoypcxqn'jc;, 'ta: napap,;1j­ µa,;a µe: 't.T) µopcpfi µe: 't'T)V onoCa. ,;{&T)xcxv ae:. 1.ax-6 't'T)V 29T)v Iout..Cou 1968 ·}la-&w<; XQ:;l, 'tl.<; 'tp01t01tOt.~ae:1.c; 't'OU<; µ,l.xpt 't'T)<; IT)<; Ox,;w~pCou 1978. 235G 235G ECl>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) EYP~mAIKH iYlV@~Jj:fIA rIA TH llibEJNH 06IKH METAcl>OPA EIIIKIN 6YN~~l{ EMIIOPEYMAT.QN (ADR) TA EY.iVlBAAAOlVlENA MEPH , EHISYMOYNTA vex a;u~~crouv 'tT)V a;crcpaAe:t.a 'tT'J<; 01,e:-&vou<; o&t.xD<; µe;,;a;cpop~<;, tD;l<1>~2NHEAN ,;a; ncxpcx'Ka'tw: r 1, a 'tT) v e:cpa;p ~1.0 y,1 'tT) c; -r.:o:p 060:a <; .Eu µ<pwv Ca<;, (~l µe: ,;ov 6~o "~xuµo:" voouv,;a1, ,;a a:u,;oxCvT),;~, o:p3~w,;~ o­ xi1µa:,;a, puµou11.x'ouµe:va ox,1µa;,;a; (TRAILERS) xau, T)µ1,­ pu.µnu11. xou µe: va (SEMI-TRAILERS), 6nw.<; op C ½,e:,;a 1, cr,;o ap3po 4 ~T'J<; Euµl3aO"T)<; IIe:pC 061,x~<; Kux\ocpopCa:<; 'tT)§ I9T)<; Ee:n,;e:µ­ l3p.Cou I949, e:'K't6<; ,;wv oXT)~,;wv nau avDxouv i1 -re:11.ouv un6 rt.<; 61,a,;ayf~ ,;wv e:v6n11.wv 6uvdµe:wv ,;ou Euµ~a:11.11.6µe:vou Mtpou<;• (13), µe: ,;ov 6po "e:.1t1.xCv6uva E~nope:uµa-i;a.'1 voouv,;at, QI, UAE<; xat. ,;a; e:C6TJ ,;wv o~o~wv T) &1,e:3v~<; 061,K~ µe:,;a;cpop& ana:yo­ pe:de:,;a;1, an6, i1 e:n1,,;pfne:,;a1, µ6vov un6 wp1,o:µfvou<; 6pou<; an6 .· ,;a Ila:pa:p,;t;µa;,;.a A Ka:t. B• (y),, µe: ,;ov 6po 11 61, e:Sv~<; µe:,;a;cpop.&11 voe:C,;cx:1, on:01,a:011no,;t e:rtL­ xe:CpT)OT) µe:,;a;~op~<;, EX'tEAouµe:vT) O"'tT)V e:oa:cpLXD ne:p1,ox~ (e:1t1,xpa,;e:1,a;) 6uo 'tOUAdXt.O"'tOV ~vµ~CXAAOµe:vwv Me:pwv µe: ox,1µa-ra:~ TtO!J opC!';ov-ra:1, O"'tT) TI,td navw. na:p<fypacpo (a;.). 'A 3 o 2 ,e ,e Io- Yno 'tT)V e:nt.<pUACX:~T) 'tWV 61,0:,;d~e:wv ,;ou ~p3pou 4, no:pdypa­ cpo<; 3, e:n1,xCvovva. e:µnope:uµcx:,;a Tl µe:,;o:cpopa 'tWV onoCwv CXTIOKAe:Ce:,;a;t, an6 'tO Ila;pap,;T)µi A 6e:v 3a: yCv~v~a;I, 6e:x,;d LS£Z: .. n1,t a 50.1.r>ri~idr>dnu noi 513j~1n19 511. 3ri X>A(Y)cbripo no~919 . . C'J')'( o 1::01'\)3 1\39 Sno.1. S9ri.o 1\'.1L0j3 o 1:0'K y n3'K.OX>1.X)')1 u. 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Su.1. l.!3x,"{pcb,n3 I\U.1. 911n 1n.1.;i3.1.090,ono33 n-e- i\M1prin3d01Lri3 l\cYll\ ~<]l\;'><'ll!.3 I\M\'."{3) pdodiXl.1.3rl S~l\-8-3'1<] H -·z •~docbn.1.3ri Y."B-3'19 :x,1.t (OJ.OdU lOXA3.U l03lHNd38A>I lH.l lld311\1H<l>3 2358 ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO} 'tOU Tiapap-r~µa-ro<; B, µEI, uxh:.C •· ;, T) 1tEpC060<; a::u-rD µnopEC va:: vovCCou\l, µe: e:1,61,xfc; i°•µe:.pe:Cc; ~ 1t0Auµe:pe:Cc; cruµcpwvCe:c;, 6nw.c; mp1,aµfva a::n6 't(X £1tl,XCv6ova £µ1tope:uµcx-ra:: ,;ex; orcoCa cruµcpwva µ£ 'tT) napoda~ EuµcpwvC~ a1toK\£Cov,;a1, an6 6AEc; ,;1,c; ~1,E&vECc; µe:-racpopfc; µ1topo~v, un6 'tl)V e:n1,cpdAa~T) mp1,crµfvwv 6pwv, va ·yCvevi;cx;1, OEX't~ y1,a: 61,e:&VD µe:-rcxcpopa a,;1,c; e:1t1,xpd-re:1,€,; -rove;, D 6nwc;. e:n1,xCv6uva e:µnope:u~a,;a:: -ra onoCa crdµcpwva µe: -rn na­ po1aa Euµq,wvCa. yCvov'taL 6Ex-r<f. y1,a 61,e::&v~ µE-racpopcf µ6vov un6 e:1,61,aodc; 6pouc; µnopo~v va:: yCvov,;a~ 6e:x,;a y1,a:: 61,e:&v~ µE-r.acpop<f. 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( 31-Evo e:.CI; e:1.,<; e:1tC 't"WV &oxe:Cwv (.I) Tex. µe:'ta:AA 1, ){.(l o OX; e: C cc &a: c:p fp OU v 'ta: 1ta:pa:Ka't"W 2~8 O't'..01,Xd.CX µe: ypaµµa:u:cx xcx&cxpcti<; E:UiCIVayvwa't(l: K(XI, 61,cxpxe:Ccx<;: ( ,. C , , ..( , , .a/.~ µ a: ,;wv ovoµcxat.wv 'tou a:e:piou ., -rou µ1,yµa:'to<; cxe:pi.wv, 1tADPl1, 01tW~ 6Coe:i;o;1, O'tO 1te:p1.&wp1,o 220I, r 0 f~ 9°• 'tl)V e:1twvuµCcx D 'to ODµct· ,;ou xa:i:acrne:ucca,;~ D 1,61,ox.,;1j,;, ... t• }t.(XI, 'tOV a;p1,&µ6 'tQU; &oxe:Cou, (l3Ae1te: e:JtCO'T)c;; 1te:p1,&wp1,o 2:2(il2: (3)). 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T) µe:po µT} v Coo: ( µ1j vex, f,;o <;) 'tT) c.;; ye: vo µf vT) c.;; 'te:A e:u ,;a:C ac;; ECl>HMEPII: THI: KYBEPNHI:EOI: (TEYXOI: nPOTO) ( ) , s:. , e: 'tl) acppa:y1.ucx: -rou e:µ1te:1.poyvwµova,. rove; e:Alyxouc; xcx:1, • e:1t1.&e:wp~ae:1,~· xcx:1, e:n1,npoo&f-rw~: (a1t} npoKe:1.µfvou, 1te:pC 1te:1t1.e::.aµfvwv cx:e:pCwv ~ µ1.yµ<f'twv 1t~ 7tl, e:cr·µlvw;v. cx:e:pCw v (I 0 , 2~, 12° l1.CX:I, I3° ).: 't"T)V CX:VW'ta­ 'tl) 1tCe:OT1. 7tAT)pw.oe:wc; a-rouc; I5°C 'tT)V e:1t1..-rpe:1toµfvT) y1,a 't0 «-o,&fµcx:' •. 6oxe:Co (13A,6te:. 1te:p1,&wp1,o 2219)• 2218 ( m., v e:x c i:.e:­ ,; ex: I, ) (l;,,); npoKe:1.µf:vou ne:pC cp-&op.1.ouxou f3op-Cou.1 (I 0 (cx: '1')), uypo­ no 1, l)µ.!vw.v cx:e:pC w~· ( 3° fw:c; 6°). Kcx:1. cx:µµwvC cx:c; 61, cx:Auµf VT)<; o't"o ve:p6 (9°(cx: T:)1): -ro e:1t1.'tpe:1t6µe:vo cx:vw,;cx:,;o ye.-· µ1,aµoo., xcx:-& 'tl) xwpT)'&I.K6'tr)'tctc. IlpoKe:t.µfvou• y1,cx: f3cx&e:1.!X­ Kcx:-re:<j>uy µevcx cx:fpt;.a:. ((DEEPLY-REJ!'RIGERATED GASES) ,;wv 7° Kcx:1, 8°: 'tl) XWPl)-:t" 1,x6'il)'t,<Xl:• (l)) npoKe:t.µfvou ne:pC cx:xe:-ruAe:vCov 61.cx:Avµfvou oe: 61.cx:Au1:1,­ K6 µfc:10 ( 9°( y ),) : 't"l) v.. e:n ~ 1:pe:.1toµf VT) nC EO'Tl 1tAT)pw:oe:wc; (13Ae1tE 1te:p1,%1p1,o 2221(2)), KCX:L 't0 f3apoc; 't0U KEVOU 6oxe:loV- ouµ1te:p1.Acx:µf3cx:voµfvou 'tOU f3apouc;: 'tWV e:~cx:p'tl)µcf­ 'tW.W KCX:I, 1tcx:pcx:KOAOU&l)µ(l'UuV, ,;ov 1topw6ouc; UAI, xou., KCX:t, ,, ~ou 61.cx:Aui;1,xo6 µfoou• (&) 1tpoxe:1,µfvou ne:pC µ1,yµ&,;wv cx:e:pCwv ,;11c; 12° KCX:l. cx:e:pCwv 6 ox 1, µwv ( e:A l yxwv) i;TJ c; I 3 °, o 1, A fl; e: 1, c; "µC y µcx:,;cx: cxe:p C wv" D 11 a:fp1,a e:Alyxwv", a:va:Aoywc; 'tT)<; 1te:pl.1t'tWOe:wc; &ex: xcx:­ p<faoov'tcx:t. O'tO 6oxe:Co o<fv YEVI.XD fv6e:1.~T) 'tOU 1te:p1.e:xo­ µfvou. Axp1,~~c; 1te:p1.ypcx:cp~ ,;ov 1te:p1.e:xoµfvou &ex: e:1.xo vC t;e;,;cx:1, xcx:& 'OAT) 'tT) µe:-rcx:q>opcf • (1,,) npoxe:1,µfvou ne:pC µe:'tcx:AAl.}(,WV 6oxe:Cwv -rcx: onoCa, ouµcpw­ vwc; 1tpoc; ,;o 1te:p1,&wp1,o 2202(3), yC,voV'tCX:l. 0El1.'ta y1,cx: "(;T) µe:'tcx:~op<f e:voc; cx:p1,&µod 61,cx:cpope;,;1,}1.~V cx:epCwv (&oxe:Ccx: E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) ( O:VE~ C'tT)A.0£) noAAO:TIA~c; xpfiaEw~), o:xp1,~fjc;, 61,a:pxECo:c;/nEp1,ypa:cpfi r;ou ne:p1, EXoµevou -&a: e::1,xovC/;.E'to:1, 61,0:pxoVOT)<; 'tY)<; µE --ca:cpo pcf <; • (2); 01, e::voEC~e:L<; -0-o: xa:p<faaov-r;a:1, EC'te:: e:nC EVLoXU­ µevou -r;µfjµo:'t:o<; 'tOU ooxe:Cou, i::C--ce: e:nC ◊C(XTUA.LOU, i::C--ce:: e:nC I •· ' , C L C TTA.ct>ti<; a va: y pa:cp o 0 er~<; a--co 1, X e: a:.., -r;ono-0 E 'tT) µ c; VT)<; X wp <; va: r1. 1, 22I8 ve:C-n:a.t, O'tO ooxe:Co •. En1,npocr{}e-r;w,c;, Y) ovoµa:aCa: Tf)<; UA.T)<; µno..;. pe:C VO: OTJfl.E:.l,OU'tO:l, crir,o ooxe:Co 01, 'opa:--c,1'c; e:uxp1,vouc; e:n1,ypo:qn1c; 61,a: ~-a:cp,1°<; fj 01,a:ao,1°11:o-,;e: aA/\T)<; 1,aoouvc!µou µe:-&66ou. ( Y ) gf~.£!L~2:!:l!:~£.z. .@~~!:2£ ~~!1E~.£.§:~£1. ~~= 212~21 X~f2:!l.!i.!;.t~!l.'.E£4.iz. .!~1~~21.§:f ~~ ( ~/\en e: e:nCcrnc; rce:p1,-&w.p1,a: 2238, 2II ISO xa.L 212 ISO (.I) Ilpoxe:1,µfvou ne:pC 6oxe::Cwv rcpoop1,(oµlvwv y1,a: t°T) 22I9 µe::-ra:cpopd ne::u1,e:aµevwv o:e:pCwv --cwv I~, 2° xaL r2°, T) e:crw--ce: pt.x-fi nCEOT) (nCe::crT) oox1,µfjc;) T) e:cpa:pµocr-i;ta: y1,o: EAEYXO uopo:u /\.l,}Lfj<; 7tl,£0£W.<;, npE7t£l, va: e:Cva:1, 'tOUA.<fx.1.a't'oV µ1,d ... µ1,cru cpop& T) nCEOT) TCA.T)pWcrtw<; O''t'OtJ<; I5°c T) O'T)µEt,OUµEVT) O''tO ooxe:Co, 0:A./\~ 6X 1, µ1, }tp6't'e:pT) 't'WV, IO KG/ CM 2• (2) IT po xe: 1, µf vo u rce:p C 6 ox e:C w.v npo op 1, l:..o µtvwv y 1, a: 't'T) µE-,;o:cpo p&. UA. w'I, 't'T) <; I O (a:) TIA T) v ,;o u 't e::,;pcxrp{}o p 1, o µe:-Oa:-µ Co u • o e: u r e:p Co u xcn u6po16vou 'tT)<; I 0 (f3)• ,1' a:e:pCwv Tf)<; 2°(a.), T) nCe:O'T) TTA.l)p~cre:w.c;, oe:v -&a:. une:pf3a:Cve::L --co: 300 KG/CM2 'ta-a:va:cpe:p6µe::va: y1, a: {}e:pµoxp~.aCa:-. rs 0 c-. L'tT) ne:pCrt't'WO'T) 1:WW oe:,a:µe:vw,v, n rcCe:O'T) Tt/\T)'pw.ae:wc; oe:v {}o: une::p f3a:{VEl, 't(X, 250 KG/ CM 2 1:0: o:va:cpe:poµe:vo:. OE {}£pµoxpo:aCa: I 5° c. Tipoxe::1,µfvou rce::pC ooxe:Cwv xo:1,.oe:,a:µe::v~,v rcpoopL E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) Coµlvwv y1,cx. 'tT) µe:'tacpopa <XAA.WV ae:pCwv 'tWV r 0 l1,(XI, 2° T) 22I9 • 2 (Euve:xCl:.e:-nCe:OT) 1tAT)pctl:oe:wc;; 6e:v -&a une:p~cxCve:t. ,;a 200 KG/CM 'ta ava ~a1.). cpe:p6µe:va. oe: -&e:pµortpacrCoc I5°c. (3) n·p .. orte'.1.µtvou ne:pC 6oxe:Cwv 1tp:oop1, l:oµtvw·v yi;.a 't.T) µe-racp,op.<t cp-&opCou. (I0 (a, T·)} T) e:ow'te:pt.rt-fi nCe:aT) (nCe:011 e:>..eyxou). T) e:cpcxpµocr,;fo: y1,cx 't0V fAe:yxo 'tT)<; u6pocUA.l,l1.D<; 111,f­ cre:wc;; -&oc eCv<u. 2~'o KG/CM 2 rtat. T) 1tCe:011 1tAT)p~cre:wc;; &e:v -&ex une:p~aCve:u. 'tet. 28 KG/CM 2 oe: -&e:pµortpa:crCcu. I5°c• e:1tt.1tpocr-&f'tw<;; Kcxvfva: &oxe:lo 6e:v -&~ ne:p1,fxe:1. ne:p1,cro6'te:pi ,;wv 5 KG'cp,-&o­ pCou. TI po Kin µf vou ne:p C 6oxe:Cw.v np.oopt. Coµtvwv y 1,a 't'.T) µe:.,;acp,op~ ,;p.1,cp-&op.1,ouxou fJopCou (1°(~ T).) T) u6pa:uA.t.K1i nC e:01) T) e:cpa:pµocr't.la .. O'tT)VnCe:011 ooKt. µ-fie;; ( e:A €yxou) -&oc e:Cvo:1, • e::.C,;:e::. 300 KG/ CM 2 , on6,:e: 't'0 CXVW'tCX'tO ~apo<;. 't'0U 1te:p1, e:xoµtvou ava A~'t'.po XWPT)'tt,Y.61;:r)1;.a..c;; 6e:v -&oo: une:pfJa:..Cve:1,. ,:a O.7I5 KG. (4) Ilporte:1,µfvou ne:pC 6oxe:Cwv npoop1,1:oµfvwv yt.a:- .. i-ri µe:i:o::cpop~ uo"o~e:1,&Cou ,;au a,~.-i:ou NO (I° Cr T)), T) xwpT)'tt.­ K6't'.T)~-&o:: ne:pt.opC,;e:,;a:(l, O't'O:: ~o L. T) uopcxu;\.1,r1,-fi nCe:011 TJ e:cpo::p.;. µocr-rfo: xo::-ra 't'T)V 6oKLµr\ (nCe:cr-T) 6ox1,µ1jc;;) -&o:: e;Cvo:t. 200 KG/· Cl!JI 2 • xai T) nCe:01) 1tAT)pw:oe:w; 6e:v -&a. une:p~a.Cve:1, ,;a 50 KG/CM 2 oe: -& e:pµoxpo:crC oc I 5° c. 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A1.yw,;e:po ,;ou 20'1t~, e:x.a:,;6v o:6pa:vono1,17,;L.lt~<; oucr.Co:c; (PHLEGIVIATIZER),. ~!li:ff~.2!1: - y opol)ne:poije: C 6 l, 0 tp l,'i;Q)' e:vouc; '30U'tUA C OU ( TERTIARY BUTYL HYDR0PER0XIDE} µe: 6x,1, AL"(W'H;po ,;ou 20~0)(.c Elta:,;6v U1te:po~e:1,0Cou &1,,;p1,,;oye:vovc; pou'tu 2551 25!"17 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) · i\Cou ai\i\a xwpCc; a6pavonoL~tLX~ ouaCa un6· cr't'OLXECov 3I 0 • o:vaypacpE'tCXI, '2551 ( Euve:x et:e:­ ,; at, ). 3° I:!!f22~i2!:£~ !2i!2!~~£-f2!2.!Q~i2 (TERTIARY BUTYL PER.ACETATE), µe: 6x1, i\1,yw1:e:po -i;ou 30 (6r~ • Elta1:6v 50 a6pa~onoLn'tLKD<; ouaCac;. XZ!fE.@f~~2:f.2!:2 !.ei:E£!f~f£ Q£~!2t;l2 ( TEl{TI ARY BUTYL PERBENZOATE),. TERTIARY BUTYL PERivlALEATE µe: 6x1, i\1,yw1:e:po -i;ou 50 -----------------~ 6° ~1~~f.e?Q~~;2!:£~~€i!El!~!f~~£-~~~!~~i2 (DITERTIAR.Y BUTYL DIPERPHTALATE) µe: 6x 1, ;\.1, ywi;e:po 1:ou 50 G'ttX e:xa't'6v a6pivon?1,~~1,x~c; ouaCac;. 7° g, g=~f~-l!~~!!~!-~~'.£1~£!~~~1-~£'.£~!! µe: 6x1. 11.1. ywi;e:po 'li0U 50G't0G·: e:xcn:6v aopavono1.n't't..}t'l1<; ouaCcq;;. ,;-.,· (a.;), µe: 6x1. At..ywi;e:po 'L"OU I O G't.O\ e:Ha,;6v uowp• (.~). µe: , OXL AL)'W'tEpO 'tOU 30 Ci-i-o<. e:n.a,;6:v CCOpaVOOLT) Tt,l-f.~<; ouaCac;. I!ll::.fl~2.fi£t:- I.- ~I.10 une:p0Ge:Co1,o -i;ou ~e:vl;oOi\Cou ~~ l;T)pch· l1.ct~ao1:av'1 '11· µe: i\1,yw1:e:po 1:ou, IO &,;04: e:xa-i;6v u.owp, ,'j 11.1,ywi;e:po '"C"OU 30€ft'~ '• EH.a'"C"OV a:opa:vonoLT)'t'Ll-f.'11<;; ouaCac; e:CvaL 6i\T) '"C"T)<; KAacre:w<;; I~ (~Afne: ne:p1,&wp1,o 2I0I I0°( oc}i. 2.- Yne:pol;e:C61.o 1:ou ~e:v~oUACou ne:p1.fxo~ OXL ALywi;e:po 't0U 706,;od. Elta't'OV l;T)pcx X.0:1, a6pccv11 crpe: p ea o e: v un6ltE 1, 't"O:I, a-i-q; o 1, a1:al; e: 1, c; 'tT)<; ADR. 9 o !2!.f.e2~ff2l~-2!:~2:~2f~f!Y~6.!l£i ( I-HYDH.OXY-I '-HYDROPEROXY E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPOTO) ·nrcYCLOHEXYL PEROXIDE AND BIS (I-HYDROXYCYCLOHEXYL) . (a:,) µe:· 6xt. 11.1,yw-H:po 't'OU 5 b't'C>t e: 'KO: 't' 6 V 6&iup• (~) µe: 6xt. /I. I, yw-i;e:po 't.OU 30 ,'tot, £'1-tet:'t'6V ccopavono1,11 'Hlt~<; ouaC a<;. f!ll:fl.§~fi~: - I • - Yrce:pol; e: C 5 1, cc xu1tA. o e:l;av 611. T)<; xa 1, 't'CC µC y­ µaxa 't"OU<; ae: ~T)pa KO:'t<XO''t'O:<JT) 11 µe:: A I, yw,;e:po 'tOU 5 6't"Oll ·. e::K.a't"6V OOWp ~ Al,)'&J't'e:po 't'OU 30 (1!6d, Emn6v CXOp.CXVOTtO l,11 'Cl,lt~<; ovaCac; e:Cvcc1, ,Jic:\; ·n1c; K11.aae:wc; lEa. ( ~Aem: ne:p1,-&~ 0 .•· . p 1, o 2I O I , I O ( 13}),. 2~- Yrce:po~e:Co1,a xuKAoe:~ccv6AT)<; xa1, ,;a µCy­ µa-i;a 't"OU<; ncp 1, tX,OV't'CC• 6x 1,' A. 1, )'W'te:po 't"OU 70 b't"o4. EltCX'tOV ~T)p~ KC(l, a6pav~ 01Epta 6e:V un6KE1,V't'O:l, O''t"L<; 6La't'a~EO<; 'HJ<; ADR. I O O ~,.. $;..= £!~~'.!:~!~~~g~!~ !:!!~~2~~~£!E£~ ( u op oU re e: p oi; e: Co 1, o 61,µe:-&vAope:vCuACou) (CUMYL HYDROP1'1."lOXIDE): µe: ne:p1,e:x6 µe:vo cre: urccp.oi;e:C61,o µY) u1te:p~o:Cvov -i;o 95&,,;o4, :, om1:.6v. II 0 !1!f££~ff.2l£-~!!!~£~~!~• I2° li~L2i4-~~!~~~~2=l=li~~~!!~-~!~~Q~~~2!;~~ I3.0 2 4-DICHLOROBENZOYL PEHOXIDE (une:po,e:(61,0 61,xi\wpo~e:v- L <:oUl...Cou) (a.).. µe: ox1, i\1,yw-i;e:po 't'OU IO<c't'o4. E1t(X't0V oowp• ( p). µe: 6X.,L i\ l,)'W't'EpO 't'OU 30 ''t't.X. .EKet:'t'6V CXOpO:VO'JtO Vr)'t°L ,-t~<; ouaCac; (PHLEGivlATIZER):. I 4° P-MENTHANYL HYDRO PEROXIDE 81,0 µ11 une:p~aivov 't'o 95b't'CX e:xo:T6v (urc6;\01,nov: cx;\.11.06- • i\ai, xo:1, xe:'t'6va1,). 259!) 2600 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) J.5: fL2L§.=!~f~!~!~-~£~~! !~~! l !~!!~~~~!f£~ ( PINANYL 25 5I HYDROPEROXIDE• PINANE HYDROPEROXIDE}; µe: rce:p1,e:x6µe:-(~uve:xCl:e: . ,· icn ). , .. , VO e:u,c;; tJ)'Jte:po~e:.(61,0 µT) U1te:pl3cn vov 'li'.O 95. b'tiOCt EXO:'t.6V ( u1t6Ao i; nov: ~An.6Acu:. xa:1, x-e:,;.6va:1,). 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( l3A.E1te: 1te:p1,-&wp1,o 2IOI, ro 0 2.- To urce:po~e:Co1,o rca:pa:xA.W~o~e:v~oUA.Cou rce:­ p1,fxov 70 'tOLc;; e:x.a;'t6v 11 rce:p1,aa6,;e:pov ~TJP<X x.a:1, a:6pa:vi'j (J't'Epe:ct oe::v u1t6J1.e:L't-O:L O''t'l,c;; 01,a:,;&~e:1,c;; i-1,c;; ADR. I8o DI~ISOPROPllBENZENE HYDROPEROXIDE (ISOPROPYLCUMYL HYDROPEROXIDE) µe. 45 't'o 1, <; e:xa:,;6v µC yµa a;;\x.06;\ TJ<; xcx1, ~Xe::..~ VT)<;• I 9 ° 1=~~!!!!~~~!.!!~=g=Q~~~L~~!!~~!.~! ( !.~~~:!!!!!!~~~!!!~~!~~~ ~!~~!!.~~) µe: 6x1. 1'.1.yw,;e:po 't',OU 40 G't'°"· en,a;,:6v a;opavo 7t0LT)'t',1,X.'f)c;; ouaCa:c;. E<l>HMEPII: THI: KVBEPNHI:EQI: (TEVXOI: nPOTO) 2601. • • ·\ J ~~!!.~!-~!:!!!~ (!':z. ~=-!=~f~!~!~~~!!;!!!2 E~2!!~! 2551 µe: . .Sx1, 1te:p)t, 0'0'6·n:po a:1t6 95 "'tO(, s e:,.1.a:,;6v U1te:po~e:(- (~,U V·e:xC<:e:~a:1,, & I, o. ( ~ 1, o:>1.e:'tuA C oul 21° Xllfl22~ff.§12J2;~2!!!~/ µe: 6x1, Aliy~,;e:po i;ou 75,~ott ~ e:no:1:.6 v o:&po::vori:o 1, T)'t.1, rdj <; oua.C a:<; ( PHL!Gl'viA.TlZERJ. 2'2: o !?E§.e£iff.§l2-~l!-f!~~2=~f~~2~l2~ (ACETYL BENZOY~ PEROXIDE) µe: 6x1, )\1,yw~e:po 't'ou;,,60G'&'.o<.f; e:na:1:6v, o:&pa. vono1,T)1:1,n1jc; ouaCac;. f!1!:ff~£.!:.~=-!:!£gf r 0 ··lw:c; 22°. 'YAe:.:c; 11:ou e:Cva:1, a:&pwe:Cc; ae: opya,l11,~d, ~i~e::p~;:~c~td: }I.CCI, €xouv O'T}µe:Cov a:vo:cpAE~e:wc; 6x1, ,«.aµT}AJiit-po'·'iwv; roo0c 'Kett, OT)µe:Cov ~pa.aµou 6x1, xo:•µT)Aw.1;:e:po '&.WN I50°c -Oe:wpouv,:a,1, 6-,;1, e:Cva:1, cc&pa:vo 7t01,i)1:l,l!.h.; 6Ae:c; .. 01, 6Ae:<; 'tT}<; Oµa&oc; A µ1topo6v e:1tCO'T)<; va-: CCP<lLwSouv µe: &1,a:A61:a:c; 7t0U e:Cvcn o:opa:,:ve:Cc; O''tL,<; ·u AE~ a;,u-r.fc;. 3-0° !2:!E2~ff£.!:.2-~.g~!~~2~f2~ ( ~.!:.~~~2::!:f~~~2:!:f!2~=~2:fE2- ·. ~e:(61,0) (BUTANONE PEROXIDE (ETHYL METHYL KETONE PEROXIDE') ( o:J, µe:. 6x 1, A, 1, yw,: spo 't'OU. 5.o~,;o(.~ E:'KO:'t'OV o:&pcw 01to t. 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Ta: ~o.:p€A1.a: oe:v -&a: ye:µCCov-i;a:1, n{pav -i;ou 95(o-i;cx. e:wx­ i;6v 't"Y)<; XWPY)'t"t.Xo't"Y)'t"6<; 't"WVi. E&v, µa:CC µe: -i;o rce:p1.e:x6µe:v6 .. 't"ouc ;, ~uyCCouv rc&vw o.:rc6 275 KG, -&o.: e:cpoo1.&Cov-i;o.:1, µe: xu At. 6µe: ve:c; o-i;e:cpcxve:c; (ROLLING HOOPS) .• E<J>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) :~}01, UAEc; 'tT)c; 23° (!3) µnopouv enCaT)c; va au­ ~~~-i;a, t,: (a,) aE EpµT)'tt,rt.wc; rt.Ae:1,aµlva rt.&v1,a,;pw. rt.a-i-aart.e:uo:~eva an6 rt.a-i=aAAT)AO µe-i=o:AAo, µe: µo:Aax1111 crrt.AT)pfi auyrt.6AAT)OT), ~~ 60 AC-i-pa Ko:1, e~o­ xwpT)'tl, rt.o'tT)'toc; µT) une:p!3ai voua11c; 11.Brt..ijjrt.'lltBM.~rt.EKB'.'lltBll'li. 61,0:aµeva µE XE1,p0Aa!3€c;. To: K<XVl,O~po:: 6ev 3a yeµCtov­ ~0:.1., nepo:,v 'tOU 95 b't(D)\ ex.a,;6v 't.T)c; XWPT)'tl,KO'tT)'t6c; 't'WV. 'Eva: ~t~o1,o rt.6Aov 6e:~ npfnE1, vo: ,urC,e:1, n&vw o:n6 75 KG• fi 28I3 (EuvexCCe:­ i=cx.1;.) 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EpµT)'t'.,l,}tW<; KAe:1,aµlvo: 6oxeCo: rf.O:'t"CWKEUo:aµevo: an6 ucc­ AO, nopaEA<XVT), EC6T) Ke:pccµe:1,x11c; ~ no:pe:µ~e:pec; VAL}(.O, fi ccm:i }(.O:'t<XAAT)AT) 1tAcca,;.1,x17 VAT), rt.0:1, 6e:v -&o: ne:p1,€xouv n&~w an6 5 KG UAT)c; -i;o rt.o:&€vcc. Ta: 6oxe:Ca: o:u-i;& 3o: o:a~o:­ AC(ov-i;o:1, µe: o:noa!3e:o-i;1,rt.6 uA1,x6 ae: ~uA1,vo x1,!3w-i;1,o 11 .. E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) ~i'X~7t0.l,,C(, aAi\ T) e:~W'H:p I. XD ouoxe:ua:oC CX XO:'t'a:i\i\ DAOU J jiil.Jxfic;. 'Eva: 't'i't'o1. o x6i\o v· 6e:v 1tpe1te:1, va: Cuy C­ .·~~ 1t<ivw a1t6 75 KG• fi 28I 4i ~); OE e:pµT)'tl.XW<; xi\e:1,oµtva µe:'t'.a:i\i\1,xa 6oxe:Ca,. µe: xa~ ~i\T)i\O e:1tfv&u.0T) e:av xpe:1,ao-&e:C, 't'(X,. 01t0Ca &e:v 1tpl 1te:.1, vex. 1te:p1, txouw 1tavw a:1t6 15 KG Ui\T)c; 't'O xa:-&lvcx. T.'a: ooxe:Ca: O::U't'a -&a: a:ocpa:i\CCov1:-cx.1, µe: 0:7tOO~EO't'1,}t6 ui\1, K6 oe:, ~6i\ 1, vo xi. ~W't' 1, o D ae: xa1to 1, a: c£i\i\ t) e:~w't'e:p 1, K~ ou.ax~ua:o C ex,. xa'taAi\ fii\ou a:v't'OXD c;. 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KW<; MA e: I. aµf VOU <; O'evt Y..OU ~, XO:'t'CXO'l1.EUO:O:µf VOU<; an6 XCX't.aAAT)AT) ni\a:O'tl,}t~ UAT), 01, OTIOLOI, ~a 't07tO~E't'OUV'rCX:I, ae: ~67'.1.vo x1.~w-,;1,o D ere: xcino1.a: <XAAT) e:~w't'e:pt.H~ auax,e:ua:­ oCcx xa:'t'aAAD7'.ou a:v't'ox11c;. 'Eva: 't'E1:01.o x,6Aov 6e:v npene:1, Va: ,uyCCe:1. navw'an6 75 KG. D <l>EK 225 EG>HMEPII: THI: KYBEPNHI:EOI: (TEYXOI: nPOTO) '.!78i ·cp-<~ '1 &-:~rt.ltOU<; an6 y1,ou't'a. ,t.a;,&1,0't'a:µlvou<; uypoO't'Eya:vou<; 2814 •• •• • L • (Euve:xCi:e:'t'ocr.) I'-£ e:nf VOUO'T} 'KO:'t'O:O'KEU<X:Oµt:,; VT) a:1t6 rta:'t'aAA T)AO UA 1, rt6, - e:.1t1,xp,1,oµfyou<; µE ~l,'t'OUµ1,o\l', D OE Oa'KrtOU<; a:n6 y1,ou't'a: E..1tE.V0 diuµf vou.<; µE EpµT)Tl, KW<; 'KAE 1, oµEVOV ocx,rnov 'KO:'t'O:­ a.'Ke:ua:oµf vo\l an6 'Ka't'<XAAT)AT) 1tAaO't'l, rtfi 611.T). 'Eva 't'E't'O I, 0 rt.6AO\l' oe:v 1tpf1tEI, VO: r,uyCGEI, nav~ a:n6 55 KG. 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( 1tAT) \I 't'W'V uypono l, ouµf vwv ~ a:pa:1.ouµfvwv µe: 1t'tT)'t1.xf<; 6Ae:~, n.x. 6&wp) 61,a: 'ta: onoCa T)' op;1,cxxt1 61,aµ.e:-i-po<; oe:v e:Cvcu, µ1,xp.6'te:pT) ,::w,v 9 MM 1tpf1tEI, E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) \id·:· a:·e:w.p.ouvi;cxi.. w, e:xprp,1.,;1,xlc;; 6Ae:, 'tT)t;; KA&:-cre:w<; Iex (i3Alne: e1tCOll<; ariµe:Cwµex O't"O 1te:p1,-&wp1,o 2550). 6011.1,µfi e:u.a1..ct-&T)aCex<; oe: 1tp.60Kp.ouari ( ~AE1tE 1te:p1,-&wp1, a 3155 3103 f~ 3110 xa:1, 3.Il 2} (ex} 6ox.1, µl) p,C<J,e:w<;-e-cp6pex, (FALL-HAJ.iiiidER TEST) l (E1, x6 vec.; 7 KCXI, 8) 'K(X't.(X i3a:a1,xou - (u.,n 6 e1'.e:yxov) e:KpT)X'HKOU (I).. 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(2) H ouoxe:u~ 61,cx 'tT)V 01..e:l;a.ywy~v 'tT)<; oox1,µ~, a.no ,; E:Ad 't(XI, exn6 EV.a: i3apo '' 'tO 01t0 CO V, OA I, a-&a;C VO V µe:,;a;I; 6 660 pai3&w,v, e:Cva:1, oe: -8-EClT) V<X pu-8-µ1, o-&e:C vex 1t~e:-,i, a:n6 1tpoxa;-&o­ p1, oµfvo u<j,o<; xex1, vex excpe:-&e:{ e:uxe:pw, Va; nfoe:L. To i3apoc;; &e:v 1t E(P.'tE!. exn 'e:u-&e:C a:c;; a,;o E)i(.pl)X'tL x6, O:AACX nfcp,;e::1, navw oe: E:1tL­ xp:ouoTl)pCX D 7tOU; 'KCI-8-E:'t(XI, 7t<IVW oe:: axµova: (a:µ6v1,) E, ),(.O:t. QI, &uo ( e:n:vx.pouoi;~p.gSxa:1, a:µ6v1,) an6 not..lS- O'KAT)p6 -XaAui3a., xa:1,. 0/\.U,<J,&'cxCve:t. e:uxe:pwc;; O''t"OV o&rn6 0(XX't'.1JALO F (E1,xwv 7 ). To &e:Cyµa: ,;ou., e:HpT)X'tl..}1.0U ~01to-8-e:1:e:C1:a:1, µe:,;a.l;t i;ou e:n1,xpoua1:~­ p~ ><.exr,. 'tOU CXXµO V(I)( ■ 0 E:1tl, XpOUO''t~ ~) 0 aHµG)Vot,SK(XI, 0 Obl)y6c;; DX 5~dcbX>'{3 911x, 5M3tf,Jd 5]ri1l<Og t\CJ'}'{'lL )1L3 '5ld3D.0]..1. 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ECJ>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) f'¥bt,e:pov -6<1>0~ &1, e:;cfr,ov't"ac., xcx·c. 061:w xa:-&' e:~fj,. 3!55 <'1) To -xai111hc'-'te:pov '6<koc; pC<j>e:wc; -ro 1tp.oxa:houv a>p1.aµfv11v fxp11!,&,uve:xC­ C e:i;a;t,) a:u~ Aa:µj3cfve:i-a:1,., w~ 't.o 6pc.ov e:um,a&T)<i»Ca:~. (&:) H ooxc.µfj 1tpoa-xpov.ae:w.<; &1.~cfr,e:-m-11. xa:vovi;rtw, µe: pCq,111 • j3cfp.ou:<; Z KG• e:v 'tOV'tOC.-~, e:tXVl) e:ucu.a-&T)aCa: orrT) 1tfi)X5crxpou:­ OT). µe: -ro !3ap:o<; a:v.1t6 a:ncxi.-re:C -6(j>oc; pC(j)e:wc; µe:ya:k6-re:p.ov "tWW 60 ~- 70 CM, T) &ox1, µfj npooxpo6oe:w<; np,fne:1, vex cS.1,,~~a:x-&e( µe: j3cfpo" 5 KG • . ., (J} Lloxi.µT); p.C <j,e:<.i.l<;-acp,upa:~ (FALL-HAMMER TEST)✓ II (Ei. x6 ve:~ 9 fwc; 13} µe: a:pi.-&µT)-rc.xfjv &1.ai:unwoV)I 'tT)<; Eua:.to-&T)aCa:<; a'e: ri~a,xp.ouo11; (e:vfpye1,,a: npoaxpouae:w~ cre: KGM) (I)i H 6ox1.µT) ~ ne:pi.ypa:q>oµfvT) o't'o (ex-,), µnope:C va: av-r1,xa:­ ra:a-~-&e:C an6 'tT) napa:xa't'W &oxi.µfj. ( 2 ),. II e: p..1,.,: p ex <p,fi 't"T) <; au ox e: ufj <; : Ta: j3acr1,x<f e:,a:p,:fiµct't<X- 'tT)<; ouaxe:ufj<; e:Cva:1, o µT)Xa:-·., .. ~U't'-6 vi.o:µ6~ npoaxp:ouoEwc;; (j3Af1te: uno o,;01.xe:Cov (4)),, -i-o/XCXAVj3Gu, vo our.xpo't"T)µa: µE "tT) j3aOT), 0 axµ•v~S,T) 01:fiATJ, 01, OOT)yoC 'K(XI, T) aqµ1pa: µe: µT)xavi.o.µ6v a:cpfcre:w<; (Ec.l1.w·v. 9)... 'Eva~ Xa:Auj3&1,vo<; cf>1.µ&Vo<'s(&1,cxµf-rpou IQO MM, u(j>ou.c; 70 MM) !31,&wve:'t"a: 1, a-ro Xa\u j3&.1, vo auy,xp6-rT)µa: ( 230 X 250 X 200 MM) xu-i;:6 cre: lva. owµa: µe: TT) 13&cn:i, ( 450 X 450 X 6.0 MM). B1,,&wµe vo ai:o nC aw µfpo·, 't'ou xa:•Au 13& C vou, ouy;Kpo,;:.fjµa-r;o~ e:Cva:1. 't'o o-r'flpi.yµa a-ro onoCo cr't'e:pEwve:'tai. T) cr't'rjAT) a.mS xaauj3cS1,vo awA.fjva (SEAMLESS-DRAWN STEEL TUBE) (E~w1:e:p1,x'fl, &1,a.µe't'pou 90 MM, Eaw,e:pi.rtfjc; &1,aµf1:pou 75 MM). 01, c56o ocST)yoC cr't'e:pe:,vov't'ai. 0't'TJ 01:fjAT) µfa~ 't'pe,wv e:yxapcrCwv &oxwv xa.1, e:Cva:1. e:q>ocS1,a.aµlvo1, µe: o&ov,;w:i;tj pal360 61,cx \la; 1tEPL0 ECJ>HMEPlr THI KYBEPNHl:EQr (TEYXOr nPQTO) 3I55 ;- ;PJ/a&e:C T) ava:ntj6T)ovi 'tT)<; ocpupa:c; xa:1, µe: µLex Xl.VT)'tD l3a:-&µo­ rvoµT)µEVT) KACµa:Ka: y1,a: 'tT) pu-&µLOT) 'tau -6q,ouc; 'tT)<; p{q,e:wc; (ni.woe:wc;). O µT)xa:v1,aµ6c; ouy>t.pa;i;tjoe:wc; xa:1, a:cp€cie:wc; "t'T)<; {1:u ve:x Cl; e:­ nu) ,. , -r:' J:: , , ' a<pu.pa:c; pu-&µ1, l;e:'ta:1, µe:'ta: .... u. "t'W.V ouT)yw.v xa:1, oua<p1,yye:"t"cx1, a CXU"t"our;, &1, a 'tT) c; A.El, -mupyC cxc; ne:p I, XOXAL OU µe:"t'cx µoXAOU· (LEV.ER.­ NUT) mxvw oe: &uo OLQCy6ve:c;. H ouaxe:utj e:Cva:1, f,;01, O'te:pe:wµf­ VT) e:nC o:vµncqou~ ouyxpo't'.fj µa:-i-o i; EX µne:,;6 v ( 600 X 600 X 600 MM), &1,cx 'te:aaapwv xoxA1,wv rcpoo&foe:wc; crcppcxy1,oµtvwv cr"t'o µne:i;6v WO'tE n i3cxO"'J va: e:Cvm .. cre: e:rca:cpD µe: 't"O- µne:,;6v xcx-& '6 AOV. 'tOV XfilPOV O:U"t'OU }t(XI, 01, OOT)yoC vex e:Cvcxu, cxxp1, l3wc; x&-&e:,;01, • 36'A1,vo a:v't.f.X,ov o"t'a: -&pcx6crµa:"t'cxc x1,i3w1:"1,ov i;o orcoCov fxe:1, e:ntv 6uol\-'y lha: µ0Au,i3&ou mxxouc; 2 MM xa:1, a:voCye:1, E:UXOAW.~ rce:p:i­ i3aAA e:~ 'tT) ouaxe:ufj µfxp,t. 't.OU e:m .. 1tEOOlJI 'tT) c; e:yxapoC a:c; & OXQ\J; "t"ou nu-&µf.vo, .• 'Eva:,; e:E;a:ywye:6c; a:e:pCw.v naptxe:1, 'tT) ouva"t"6-i-rrta: O'ia, cxfj~U,.ct 'tT)<; E:Kptj,e:w.<; XO:l. 'tT)V OX6VT) CXVCX acpa:.1,pe:-8-0UV 0:1t6 "t'TJV (3) Ile:pt. Yi pacp,tj "t"w.v ocpupwv-p,C cjJe:wr;, (FALL-HAMMERS):­ Ka-&€- 0(9,UpCti: e:Cva1, e:cpw&1,aoµevT) µe: ouo O:'UAa:Ke:c; e:µcppa-­ f; e:w.r;, (POSITIONING GROOVES) TtOU "t'TJ V ouyxp~:"':ouv µe:,;a:,u "t'WV i:: ' Cl., ' ~ -r: C ,.,. C ouT)yuiv. xa:vwc; 1tt.1t't€-t. Kett.- µe: ~.va: a: .... ov oxo a:1,w.p"cre:wc;, µ ci: ouva:µfvri va a:cpat.pe::&e:C. xe:cpcxAtj rtpoox.pouoe:wr; '1.a;1, µCa apmxyl) ctV<XJtT)&fjoe:w~ (REBOUND CATCH). rcou !31.owvov"t"(X;.I;, O"t'TJ ocp6pa. (E1.­ XWi\l II),. H xe:cpctAll 1tpooxp;o6cre:w.c; e:Cvcn an6 OXAT)p6 XaAvi3a: (HRC 60 fw.r; 63}· T1 Kct"t'W~~T) 61.aµe:"t'p.6,; "t'l)<; e:Cva:1, 25 MM· fxe:1. fva w.µCo.1.0 'tO orcoCo- "t'TJV e:µnooC~e::.1, WJtO "t'OU Va; 1tl, e:cr-&e:C O'tT) ocpupoo:, 01,a; "t'l)<; 7tpooxp,ouoe:wc; • . Yncxp,xou" "t'pe:C c; ocpupq; 01, a:cpope:--ct. xou l3cxpouc;. 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I ' ' 1 ' U'tO:,);ll a:p KE'tO a:no ppocpT)'tl, XO Ut\l, KO I .,a:rcoppocpc~ 660 cpopec; 'tOV 6yxov 'tOU 1te::p1.e::xoµfvou 'tOU uypou e::upCaxe::-ra:1, e::v-roc; 'tOU , . . ouo-rfjµcx,;oc; urco6oxfuv (CONTAIN1vlENT SYSTEM) xa:1, : ECJ>HMEPII: THI: KYBEPNHI:EQI (TEYXOI nPQTO) (a::) 't'O anoppoq>T)'t't.K6 U/\.t.K6 EUp(O:~E't'0:1, EV't'6<; 't'OU n p.o o:,;a:,; e:.u't 1, xo u X<XA. u µµa::,; o <; a: x,; 1, ·v o f3o "-Ca:<;,• ,1 360I (tuve:xCCe:~ 't;(Xl,} (~) ,;o ~noppoq>T)'t'LX6 UAL.Ko EupCo:KE't'a:L. EK't'o<; ,;ou npoo:'t'.(X't'E:.UTl.'11,0U KaA.uµµa:,;.oc; a:x,;1, vof30At-'a:c;, un6 't'OV 6pov 6-,;.1,. -&a:. µrcopEC \)(X a:no◊EL.X-&e:C 6-,;1, EaV 6 , , , ,;o n&pLe:X µe:vov ,;ou uypou a:ne:ppoq>e:L'to uno ,;au artoppoq>T)"t.t.xou U/\.Lrf,OU ,;a npox6rc1:ov £.nCne:&ov CX:l-t'tl,VOf30ACac;, El.<; 't'T)V Ent.cpavua:v 'tOU x6Aou .. OEV &a: un EP t f3a: L ve:: ,;a: 200 MREM/H ( wp 1, a: C we;). (I7) H o:wo:xe:ua:o:Ca: T-6nou A ri o:xe:61,a:crµevri y1,a: ne:nLE­ o:µfva:: D µT). ne:n1,e:o:µlva: a:lp1,a:, -&a: e:µno6Cl;:e:1,, e:n1,npocr-&['t,Wc;~111. a:nWAEl.ctV D 61.;a:o:nopcfv 'tOU pa:61, EVEpyou TIEPl. Epxoµtvou tav 'tO xoi\ov u.nof3AT)-&e:.C El.<; 'tl.<; ◊OKLµE<; 'H<; opLl;:oµe:.v.e:<; cr1:o 1tEp.L-f}.wp1,o 3636. }:uo:Kt:uacrCa: oxe:5t.a:cr-&e:Ccra: yL.a: ,;pC-rt.o Ka:t. a:py6-37, u:n:6 a:e:pA,WOT) µopcprjv }ta:1, )'La: opa:01,v µtxp1, 200 01., &a: e:.,a:1,pe:C-ra::1, 'tOU napOV'tO<; opou. r .- BAEIKOI IIP0~6ETOI OPOI I'IA KO.AA TYflOY B(U) KAI TYilOY B(M) (I) Ew~6<; we; npof3Ac:ne:.i;a:1,, e:1,<; ne:p1,-&wp1,ov 3603(I)(a:) xa::1, 3604-(2) a:v-·n.a,;oCxwc;,·1:a: X0/\.0: Tu,nou B(U) xa:1, Tunoy B(M) -&a: OXEOL.cxC:9v1:a:L W.O:'tE. va: TIA.T)pOUV 't'OU<; npoo:-8-E'tOU<; o- · pou<;. 'tOU-<; OpL C:oµlvou.<; y1,a: x611.a: Tu:n:ou A El. c; 1tEp1,-&wp1.ov 360I(I) Ew<; (I5). cruµn&p1,11.a:µf3a:voµ€vwv. ( 2 )1 H o:ucrxEua:o:C a: -&a: EC va: 1, E'tcrt. crx EO 1, a:crµt vri wcr-i; e: Ecf v unof3AT)-&~C 01:1,c; 6ox1,µfc; 1:ou TIEpt.-&wpCou 3637 -&oc o:uyxpa:1:0~0:E a:pXE't~V a:X'tl.VOf3011.Ca:v EL<; 'tponov W.O''t'E va: E~a:cr~a:ACl;:E'tO:l. O~l. 'tO E1tCne:6ov a:x,;1,vof30A(a:c; El.<; IM a:no 1:T)<; E1tl.Cj)O:VE(a:<; 'tOU KOAOU. OEV -&a: U1tEpf3a:CVEL I REM/H (wpt.a:Cwc;) E<XV 1:0 XO/\.OV 3602 E<l>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) . n~e::Cxe:. a:p¾e:'t6 1,p,{01.o-I92 WO't'E va: na:pa:x-&e:C E1tC1tEOOV (I}t'tl.- 3602 , £ (EuvexCt~ vo~o/\C.a:c; IO MREM/H Et.<; I M crn6 'tT)<; e:n1,cpa:vE1.a:<; npo 'tw·v uo- •. . 'tCXL) ,1.1,µ<flN. Ooalfl..1,,<; l) XP~OI.<; 'tT)<; OUO¾EUa:oCa:c; .7tpOXEl,'t(XI, vane:. p.1,op1,a-&e:C e:1;.<; auyxExp1.µfva palhovou,1.Ae:1'01.0:, 'ta: pa:01,ovou XAe:.:t 01.a au-ucf µnopou v vcc :XPT)<H µono 1, ouv'ta:t we; 1tTJY~ nccpcmoµnD c; ( a; vcccpo p.a c;), a: V'tC 1:0 u I, p CO I, o-I 9 2. 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Qj;i): (a:t}° 0Epµ6,;ric; ·ncxpcxyoµfvT) e:v,;6c; ;n:ou x6.Aou u.n6 't'ou pcx&:1, e:ve:pyo~ 1tep1, E:Xoµf vou oe:.v -&a: E1tT)pe:cfte:1. OUOµEVW<;, U7tO X<XVOVt,K~<; OUV-8-~KCX<; µE't'O:q>Opa~ I (we; e:6e:.:Cx-&TJ 01.a: ,;wv ◊QH.1,µwv 'tOU ne:p1,-&wpC·ou 3635}, 't"O x6A.oV XCX't'a. 'tOI.OU'tOV ,;p6nov WO't~ , '\ , , 6 ,;ou't'o va: .. µT) n,'-TJPOt. 't'ouc; 1.axuov,;a:c; pou<; y1,a:. unoooxe:Cc; x.a:1, npoa1:a:0Ca:v e:&v a:q>E-&e:C a:na:pccxo­ Aou◊T)'tov 61.a: xpov1.x~v ne:pCo&ov µ1,~c; e:~&oµcf­ &oc; .• 1&1.a:C't.EpT) npoaoxD -&a: 6Coe:1cx1. O'tl,.<; e:n1.­ &p~ae:.:1,c; 'tT)<; -8-e:pµo'tT)'tO~ 7t0U µnopouv: <l>EK 225 E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) (1,) vex ·rpo1to1tul.DOouv 'tT)V 61,e:uB-E'tT)ot.v, 't"T)V ye:wµe:- 3602 ( I:u ve:x C Ce: pa:Ot.E..VEP)'OU ne:pt.EXOµEVOU 'fi,. E~V 't·O U/\t.X.6V X,/\,E.,1,.0'-&s.C OE µn1..'t"6v1, ti ooxc:Cov (n.x •• e:ne:voe:5u­ . µeva O''t"Ol.Xe:Ca: x.a:uoCµou), VC( fl:pox.a:AEO'OUV 't"O /\.UWOl.µO 'tOU µn1,'t,OVl,OU, ooxe:Cou D UAl,XOU:. XCX'tW 'tT)~ O:K't"l,VO~OACa~ UAl,KOu· (~1,1,) EV ouvouaoµw µ& 't"T)V uypa:oCav va E7tL'tax6vouv 't"T)V (\~) H ,&.e:pµoxpaaCa 'tWV npoa1,,;wv e:n1,cpav,e:1,wv x6AOU T6nou B(Ul ~ T6nou B(M} 6e:v -&a: une:p~a:Cve:1, ~ou~ 50°c un6 O'Kt,aV EX'tO~ e:av 'tO x.6/\0V µe:,;a:,cp,e:pB-e:C w<; ltAl)pe:<; cpop 't"Cov. (4) Ecpa:pµoCov'tE~ 't"T)V na:paypa:cpov (3)(a:J 3a npfne:~: <~) T) -Oe:pµox.pa:oCa: 'tOU ne:p1-aaA/\OV't"O£ va: e:Cva:1, 38°c (al T) El,£ 'tOV tiALOV f-&e:aL, va: e:tva:1. odµcpwvo~ Ecp,a:pµoC,ov'tE:<;. 't"T)V no:paypa:cpov (3}'(~;), npoU-rco1::C-&e:'tal, T) 6na:p~1,~ 't"OU xa:1;w,;fpw 6pou: ee:pµox.pa:crCa: ne:p1.~&A~ov't"o£ 3s0 c. llpoKELµEVOU ne:pC XOAWV T6nou B(Mt 't"~ onoCa: npoKEL'tO:L \ '6 , , J:: , , , L . 1\ax·nxo1, poi., µrcopouv va y1,vouv ue:x.1;01, ano ouµcpwvou µe:'tc.1, 'tWV a:p,µ.06 Cwv a:px.wv 'tW.V Xt.upwv 0:1J'tWV. 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P1 4° (y) MC y µa P 2 4 ° ( y ) A~-&u~vol;e:C61,o ne:p1.€xov 6x1, 11.vw ·,;.ou xo 0 /o &c..ol;e:Co1,ov 'WU a.v&paxo <; >1.a,;a l3apo <; 4 o ( y T ) At.-&u)e:vol;e.C&t.o. µe: a<;w1..ov oi\1. }t-fi<; n1.€ae:wc; µfxp1.. 10 KG/C1v1 2 e:.t.-<;50°C 4°(y T.) ll l, xi\wpoo t.q>&o po µe:S-aVl.O ne:p I, EXO V 12 -ro1, <; E:}tCX'roV a:1,-&u;>,.,e:vol;e:C 61,0 }tCX't.a l3apoc; 4°(y T) f X E , I3 I3 I0 25 22 24 15 15 t, a ) 225 300 IS IS I0 28 23 26 15 I6 O.I87 0.244 0.8I 0.8I I.5I 0.49 o. 47 0.73 0.78 I.09 ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) (3J 6.t:,J:I, ltf;A.UcpT) 1tpoopl,<:6µe:va: Ol,a; 'tT)V µe;,;a:cpopav a:e:pCwv 'tWV ·5'° )1.(X l, 6 0 : • (a) eav 'ta l1.EA6cpT) 6e:v fxouv e:nc:vou-&e:C µe: -&e:pµt,l1.1jV µ6 vwat.v: ,;~ e:nCne:oa ia opl,C6µe:va: e:t.~ ,;o 1tEpt.-&~p1,ov 2 2 20 ( 3 ) Ka:i ( 4) • 2II. 25I ( Eu VEX C ce:­ ua: I, ) (13) e:av ,;a l1.EA6cp11 txouv e:ne:v6u-&EC µe -&e:pµt.l1.1')V µ6vwcrt.v: ,;a,. Kai;w-i;fpw opt. <:6µc: vo; .e:nC 11it-i>a: ~-------------------~-~ n e:pt.y pacpfi 6AT) ~ ECoou~ Bpwµo,;p1,cp-&opoµe:-&av1,o (R I3 B I) 5° (a) 6.t.oi;e:C6t.o 'tau, av-&pa:Ko~ 5°(a) XA wpo-i;p 1,cp-Oopo µe:-&aVl,O (R I3) 5° (a) EC: a,cp-&o poa: 1,-&a Vl, 0 (n. II 6) 5°(a) »no~e:C~Lo ,;ou a:<:&-i;ou N20 5° (a) E~acp-&op1,ouxo -&e:Co 5° ( a) T pt. cp-&o poµ e:-&a V 1,0 (R 23) 5° (a) Zfvov ~o (a.) y 6 pox/\cnp.1,0 5°(a:'T). At.-&av1,o 5°(13) A t.-&UA E VI, 0 5°(13) ITC e:cr1, ~ 6.oKt.- ne:pt. e:xoµlvou av~ µfj ~ AC 'tpo v xwpr11; t. x6 'H) 'tO ~ KG I20 I.50 I90 0 •. 73 225 o. 78 I20 o. 96 225 r.r2 I60 I. 28 200 I.34 225 0.78 I20 I.34 I90 0.92 250 o. 99 I20 I. 30 I20 0.69 I20 o.. 32 I20 0. 25 225 0.36 . <l>EK 225 ECl>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) ::1 i'I - - - - - - -- - - ... EC oou c; TIC e:m. <;, ll.o'Kt.- ne:pt. e:xoµtvov cx:v& µ 1i c; r.. C,;: po v x wpr)i; 1, 'K6 ( t. \l \) f. X e: l, 0: ) I, I-lSl 1, cp,&o pocx: 1,-&u;\ f v1,o ! Bt. vu;\oq>&opC& t.o MC y µa,,;:,cx. ae:pC wv R 50 3 0 6 (a.) ll. 1, o l;, E: C 6 1, o -i; o u & v-& pa 'Ko c; 1t e: p 1, l x o v 6Xt. aVW 'tOU 35 't"Ot.<; E:K<X't6V (Xl, &ur..e:Vo,e:t.6Cou.Kcx'ta p&poc; 6°~y) At.-&ur..E:vo~e:C&t.o 1te:p1,fxov &vw 'tou 10 ti ot, e:xa,;b (XA.i\a 6x t. a vw 'tOU 50 e\:c,a... .· ~Ka:'tC, 6 t. 0~ e:t. 6C OU 'tOU 120 225 I20 225 31 42 IOO 1 90 225 ci v-&paxo c; x.a't.& ~6:po c; • 6 ° ( y T) .I 90 250 KG o.66. 0.78 0.58 o.65 O.II o. 21. 0.76 0.73 o.-1a 0.66 0.75 ~ 0aax.1, c; XPT)Ot.µono1,ou'v'tcit. x.e:AU<pT) e:ne:voe:ouµ[vcx µ.e: B-e:pµ1,­ m1 v µ6 vwcr 1, v, uno P AT)f t v-i;cx e: 1, c; 7t C e: cr 1, v· 6 o ;--. L µ fi c; xcx-i;w -i; t pa v 'tT) c; E:.1. ' x.ov1.,oµf.vric; e:1,c; 'tov nCvcxx.ex, -i;o cxvw-i;ex-i;ov ~apoc; ne:p1.e:xoµtvou cxv& A C-i; po V XWPT) 't I, x.6 't'T) 't.O c; -&ex e: C vex l, 't E't:O 1..0 wcr,; e: T) e: I, c; 't'O X. EA u cpo c; 1t C e: 01, c; uno 't'T)<; 7te:pC 11<; 1tp6HE:l,'t(Xl, 611.ric; e:1.c; 'tOU<; 55°0 vex µT)V U1te:p­ ~a:Cve:1, 'tT)V rr.Ce:at.v OOHl,µfic; 'tr)V acppa.y1,a-&e:Cacxv e:nC 'tOU xe:t..'ucpouc;. ::17'!. ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) I:v 't"OJ.al'.'>'TT) ne:pt.n't'wcre:t. 'to e:nt.'t"pe:n6µe:vov a:vw't"a.;,;ov cpop't"Cov 2II~25I &a: -~pof3.\. ETIE't',CX:-1, un6 't'0U e: µne:-.1, po y vwµo VO<; 't'0U e:y xp 1,,8-g v- ( Eu ve:x C Ce: 't0 c; un6 TY)<; a.:pµoo Ca<; a:pxrj <;. ( 4) (1,,a. xe:.\.vcpr, npoop 1, C6µe: vex: (t, a 't"T) v µe:,;a.:cpo pav a:µ­ µwvCac; 61.a:i\u-&e:C011c; un6 nCe:a1,v (.9°(ru T)): 't'O.: I,) . ~ EC6ouc; nCe:crt.c; f10-x.1,- ne:p1.e:x.oµtvou a:va µt'j c; AC 't"po v xwprrtt. x6 'tY)'t"0 «; KG/ CM 2 KG ( 'E u v t X E L a: ) . 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OAt.ycfne:pov 'tWV 4 KG/ClVI 2 (nCe:at.c; &A.1, (3oµf,;pou) f" a xe:Avcpn µe: µ6 vwcrvj xe:vo6 T) nC e:at. <; OoJ.tL µfi c; oe:v -&a: e:Cva:1, µ1.xp6,;fpa. ,;wv I.3 cpopcti.v '!T)<; a.:vw-i;a:'t'T)<; e:nt.'t'pe:no • µfVT)c; ·m,fcre:w.:c; au,T)-8-e:Canc; xa:'t'~ I KG/O1 2 • ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) ::i 7:: • li ¥~TT) 6ox.1,µ,1 u&pa:u.11.1,x.-fjc; nd:crewc; ,&o:; e:wt'e:11.e:cr-&e:C 2II. 25f 'ItP,'b'tou~iG.~e:C e:1,c; -&fcnv TJ -&e:pµ1,x1) µ6vwcr1.,. 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(a I e:1tt.'t.p.e:1toµfvou a;vw,;ai;wu cpop,;Cou e:.t.c;; KG. f'~U.«i)&,t.. ,rxep1,ov• .(3} e:nC 'KE:/\U(j)W~ npoopt, c:;oµf vwv Yt.cx 't'T) v JJ.E:'t'a;cpo'pav a;e:pCwv ~wv 7°. 1j 8°: T) nCe:at.c;; AE:t.'t'oupyCa:c;;• xa:1, (4) e:nC Ke:Aucpwv e:cpo61..a:crµfvwv µe: -&e:pµ1,r1.1jv µ6vwa1,v: T) si: 1, y pa:cpfj 11-& e:pµ.1, r1.Jc;; µo vwµt va" 1j 11 -&e:pµt, r1.<f>c;; µo vwµf vrx . & 1,.a; xe: vo6 11 • ::1 ;,; ECJ>HMEPII THI KYBEPNHIEQI (TEYXO.I nPQTO) . 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Erct.npocr-8-t'tw<; -i;wv cr'to1,xe:Cwv 'twv rcpopAErcoµtvwv vn6 'tOU rce:p1,-&wpCou 2II .I6I, 't'O: Y,a:'tw-&1, -Oa; o:va:ypa9wv-r.-o:1, sC't'E El-<; o:u-i;-6 't'o6'to 'to ~u,;1,ocp6pov e:C-i;e: ere rcA&tta:: (a:) e:C-i;e:: "e:nt.'tpe:rcoµlvf') ,ta;-i;wx&-r.-11 -8-e:pµortpo:crCa: TIAY)­ pw crEW<;: -20 ° Q11 : "e:rc~·-r.-pe:noµlvr1 Y.Q'.'t'W't'Cl't'T) -&e:pµox.po:crCo: TIAT) , • II • pwcre:wc;. • •••••• • • • • • • C~) §~g1 12 ~f~~l25-~£22Ef~~1zi E~-!~~-~£1~~2E~~ l:.:~£ !;~~2~-~~!1£: • T) TIAT)PYJ<; ovoµa;crCa: ,;ou a:e:pCou• y1.a; yyporcot.T)µfvo: a:fpt.o: ~wv 3° fw<; a0 x.a:1. y1,a a:µµwvCo:v 61,0:\u-8-e:Ccro:v vn6 nCe:01.v e:v-r.-6<; 66a.:'to<; (9° (a T )), 'to e:nt.-rpe:7t6µe:vov cxvw-rcx-r.-ov cpop-i;Cov e:t. <; KG•· (y) 2!g~ !£ ~i~~l£S Ef~g~ ~f~~l£5 ~£~~~~~~~-£~2~~~! YJ TIAl')PYJ<; ovoµa:crCa 6A.wv -r.-wv ae:pCwv fa 'TT)V µera 2II. 26 2 E<J>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPDTO) ::i -;, 2II. 262 µE 't"Y)V fvOEL~Y) 't"OU ETTL't"pEnoµlvou i;C OU u c; KG, f ,.,i! : ul9 t :~~a €,p Lo· . avwi;&i;ou cpop- (EuvexC­ 'E't"CXL) (o) ~!~~-l2-~~~~12~-Ef~~l-~?~l~£~E~2~-~f-~E2~l~~~ \ '() Envy pacp~ " -& EP µ L }tw c; µo vwµf vo v" fj 11 -& E p µL r1.w c; µo vwµf vov OLCI. }tEVOD 11 , ~~ c:nC011µ111 Y/\.WC;O"~'t"Y)<; U:TTOCT't"E/\.060T)c; XWPCI.<; we; xa·L EL<; 't"11V Ayy/\.LKtjv, faA­ /\.LKtjV fj f c:pµaVLltfjv, Ot't'6t; EaV, 't"UX6V, OLE-8-Vfj 6a­ aµoAO)'LCX QOLK~c; µEi;acpopcxc;, fj auµ~aac:Lc; auvacp-&EC­ OCI.L µEi;a~6 't"WV XWpWV i;wv EVbLacpEpoµfVWV bLa 't"T)V ETTLXECpY)aLV µE't"acpopac;, opC,ouv (X/\.AWc;. OL TTLVaK(6e, TTOU SptaKOVtaL navw Ota ox~µata ta onota µeta (l)&pouv r>e~aµevtc; nou µnopouv va anoauvapµoAOV L8ouv, 6nw, , 21141 6 3 avaq>tpovta L ato nep L8wp L.o 211 235 ( 5) , l>ev ea cpfpouv ta. 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(3° ( a T)) • . 61, µ,e:&uAa 1,-&epa:~, o-&µe:&u- • Aa:µCVT), a:1,-&u7'.a:µCvT}, µe:-9-u>-.aµCVT} xa1, 't'pt,µe:-&u­ AaµCVT) (3° (f:3 T)r tt.al, pl,VU/\OX/\WpC0.1,c) 2II. 270 (Euve:xC­ Ce:-ra: l,) (30 (y))· Oµ&s; 4: µe:-&uAof:3pt0µC61,o·:(3.0 (a T))· a:1,&u/\ox\wpC61,o • ! xoc1, µe:&U/\OXAwpC6io (3° (~ T))• Oµac; 5: µCyµa't"a in&u/\e:Vo,e:1,oCou µe: 61,o:e:Co1,ov 't'OU av­ &pa:rto~ Hat, a1,-S-uAe:vo,e:1,6Cou µe: a,W't'OV (4°(y T))· Oµ(f.<; 6: a,w't".oV, 61,o~e:C61,o v 'tOU 6:v-&pa:rto<;, crncfv1,a: a:fp1,a:, uno~e:C61,o 't"ou a,tfi,;ou N2o, xa1, o~uy6vov (7°(oc))• cxfip, µCyµa'ta: a,W't"OU µe: crnav1,a: cd:p1,a:, rta:1, µCy­ µa't"a o~uy6vou µe: a:Cw't"ov, e:nCcrT}c; 6-i;a:v rce:p1,exouv a:n~v1,a: a:fp1,a: (8°(oc))• Oµcfc; 7: a:1,-&a;v1,ov, a:1,-&U/\EVl,OV, xa1, µe:-&av1,ov (7° (f:3))· xa:1, µCyµa:'ta: µe:·Sa:vCou µe: a:1,-&a;v1,ov, e:rdcrT}<; 6-i;a:v ne:pt,EXOUV rcporcaVt,OV fj pOUCXVl,OV (SO (p)). 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H -ro1,a61:.T) 1tO/\./\.CX1tA~ Xp-ficrt.<; -&a U7tOH.E:1,'t(X.l, E:L<; 'tT)V {;y (Eu•ve:xC ce: 't'at,') • H 1tOAAai1tA1l XP'l'i~~ xe:Aucpwv ft.a 't'T)V µe:'t'.a:cpop&v cxe:plwv 61,acp6pwv oµ&6wv·.a-a e:yxpCve:,;0:1, e:&v e:n1,,;pane:C un6 ' . ~· 'tOU E~'KpL-8-fv,;o<; e:µne:1,poyvwµoVo<;~ ' . 'Oi;:a,v 'KEAUcpT) np9op,l;;ov'ta1, e:x vfou &1, 'o:fpt.ci 61,a cp6pou 0µ&60<; -&a exxe:vo6v-r;o,.1, 7tA'DPW£ ,;wv uyponot.T)µ{;v~v o:e:­ pCwv, ,a cruv~xe:to: -&a cpucro6v'tat. xa1., ,;fAo<;, -&a anapa1,ouv­ ,;a1,. ·H o:nafpwcrL<; Ke:Aucpwv -&a e:1taAT}-&e:6e:,;.a1, xa1, n1,crrnno1,e:C­ ,;a1, un6 ,;ou e:yxpt.-&fv,;oc; e:µne:t.poyv<f>µovoc;. 'O-,;a.v cpop,;wµfva:1, oe:,aµe:vaC 1) ~6e:1,a1, a:AA<X a:xa-&cf­ p1,cr,;01, 6e:C:cxµe:va:C napa6C6wv't.cXL 61,a µe:'ta:cpop&v, µ6vov ,;a O't.ot.xe:Ca. 't'O: opt.l;6µe:va: EL<; 1te:p1,-&wp1,ov 2II.262 't'CX 1,·crx6ov 2II. 273 2II. 27 4 'tCX.. 61,a 'to cpop'tw-&fv, l'i µ6/\.t.<; EiHpop,;w-&{;v a{;p1,ov -&a: e:Cvo:1, ,o­ pa,;d.• 61\.o: -i:a: cr,;01,xe:Ca: 'tee cxcpopwv,;a /\.01,rca afp1,a -&a: ttcxA.urc,;wv ,; a " • '011.a 't'.O: crt.01,xe:Ca H.EA.Ucpouc; 1t0/\.I\.CX1t/\.WV crto1.xe:Cwv &ex 1te:p1,exouv µ6vov fvcx }{.(XI, 'tO ccu,;6 a:fpt.o. E't'T) 1te:pC1t'tWO'T) tte:1'.ucpou, 7tOAA0:7tAWV crtot.xe:Cwv. npoopt. l;oµevou CL.a 'tT)V µe:'ta­ cpop&v, uypono~T)µfvwv ae:pCwv, ,;a; cr,;01,xe:Ca -&a: TIAT)po6v~cc1, xw­ P l, O"li& xa: I, -&a: 'tT) pou V't cc I, µo vwµf va 6 L. a: cr,; e:y a: V01to l, T) µ f VT)<; t3aA""". 2II. 275 • H ex vwi:&1:n 1t C ccri-1 1t ~ n pWO tit' f • ex 1t rn, eaµ E vex ex l- 2II. 27 6 pt.a: ,;wv· r° Ka:t. 2° nAT)v ~op1,01.fxou ~opCou 6e:v -0-a: une:p~a:Cve:1, 't~<; 'tt.µ(~ 't~S npo~11.e:-r/oµtv£c; un6 ,;ou 1te:p1,-&wpCou 2219(2). Li1.-a: cp-&opt.o6xov ~6p1;ov (I0 (a T.)) 'to ·a:vw,;a,;ov ~a E<DHMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) To a:v~.a:'t'OV j3apo, 'JtAT)p<f>m:w, a:va t..C't'pov XWPT)'t'l. 2II. 276 O:~ ve:x C l;:e:­ ,;:a:.1. ) xon}1;:o, O"Uµc;ewvw~ npo, 't"a: 1te:p1.-&cf>p1.a:. 2220, (2)~ (3) xa:1. (4),. xa:t. 2II.25I, (2), (3) xcn (4), -&a: 't'T)pe:C't'a:1.. 0 j3a:-&µ6~ 1tA"()pwae:w, xe:Aucpw.v npoopt. 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EnC xe:l\.Ucpwv npop·t, Coµfvwv &1,a; 't'T)V µe:-ra:cpop~v uno- 2II.278 ~ o· l;e:t.&Cou 't'ou a:l;:w't'ou xa:1, ol;uy6vou (7 (a.}), a:fpo~, 1) µt.yµ& 't'WV 1te:p1,e:xov,;wv ol;uy6vov (8°(a.)), UA~V 1te:p1.e:x6v-rwv ACno, fj. ft..CXl,OV OE:V -&a; XPTJO'Lµono1,06v't'a:1, 1tpo, e:l;a;acpaAt,Q'l,V 't'T)<; O''t'E­ ya;v6,;T)'t'O' 't'WV e:vwoe:wv fi &1,a; 't'T)V O'UV't',1pT)C11,V 't'WV XAe:1,cr1,µa;,;wv. H &1,a;-i;a:l;1,c; '&'.OU 1te:p1,-&wpCou 2II.I75 oe:v -&a; 1.axoe:1, 2II.279 O l,.(X 't'a; 0:Ept. a; 't'W.V 70 XCU BO• ECl>HMEPII THI KYBEPNHIEQI (TEYXOI nPOTO) • !~~£!:~-1 E~cpAe:x·rn: Yypa . '!e~.e2 ! £~~~.:::~.:-~~.:El.:::ffl::f121.: 2.el.2'l::2f , !-.e~.e2 ,g !~1~~f~1 KEA u q>T). n~o o-p 1,, C~ µ e: va I\ a: 't"T) v &paxo<; (I0 (a:.)) -&a: axe:61, ai:wv,;o:1, 61,a: (nCe:a1,<; -&A1,~oµf,;pou). 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E(l)HMEPII THI· KYBEPNHIEQI (TEYXOI nPOTO) ~2!!-.!:1:!i~!!.!:-~.2.!:.~~.!.f.S ~!!~.!:.!.2~1:.f~!! l.!:~-2~.§:.S .!±.S 2f~~!:!:= 213 • I 43 ·:1!S-~2:E-2~-l.f~.2~~-~~;..~~!lE£~f !!··· ~ o Kt.. µ.di a,;e: ycxv6,;,ri,;4J H 6oKt.µfj a,;,e:.ycxv6,;rp;.Q.c; -&a 6t.e:1;cfye:u-at. ~icpwv61C.,. npoc; ,;.,c.§ 6t.cx,;.a1;e:.t.c;, ,;wv 1ttp;c.-&wpCwv 2II.I50 Kcr:i. 2.II.I5I ,;.TJc; ADR Kcx t. T) acppcx y C 6 a ,;.o u e: µ1t e.t. R-O y vwµ~\o c; -&a ,;.C -& e:,; a 1, a,;ri 6 e:~ a µe: v:t'j. 2I3.I44 2I3.I49 'Ap.&po 5 ' !.!:~.!:~.!f-~.!:~~~E.!:..S l.!:.~-~Ef!i!!:~E~-l!.2~~E~E.!:1:£~~.!:.~~~.!~.!:-l.!:.~ !!J;..!:fJgJ.2.E~-~·~§2 !:.f E!l!:if .21 g1~.9??~!~E~5-2.2~.9 !1 1g1::!J~§.:E.f £2~ H oe:,cxµe:.v:t'j 1tpoie:.1, vex KCX'tCXOKe:ua,e:iat. Kcx-t& Tp6- 2I3.I50 no v e:,cxacpaAC t;o v,;,a: ,;.,ri v cxnaAo 1, cpfj ( µrice: vt. oµ6 v) ,;ou cncx,;,1, xo6 ~AEXTpt.aµo6 an6 m Ot.acpopa oua'ta't'.t.Xcf µlpT) wo,;e: vex cinocpe:6 . y e:.-r;.a.a. T) aua owp e:uat. c; e:n 1, xt. vo 6~vw.v T) 11. e:x,;p 1, }(.WV cpo p-rC wv. µe:~cp,opcfc;, x.a-&wc; }t.(Xl, ,;a O'tpwµam 'tWV 't'OI, xwµcf,;wv· 7tOU e:C Val. cxyw.yo C T)Ae:>1:tp1, aµo6 nplne.1. vex a~A T)Aoauvo fw~o: 1.. H avc-.Ca-r;amvr µe:1:a,u e:xcfcr-i;ou aywyCµou ,;µfjµa,;.,oc; 2I3.I52 ){.(Xl, 'tOU aa.aaC 6e:v rcpbte:t. vex e: Cva1, µe:ya.Au,;fpcx 't'WV ro 6 OHMS. ~~~~~.!:.!~ !!-.!:.~~~!~1-2!.§:.!:~21:i1~~~~s~!2E!f~-~E2.§:£l21:.§:~~-g~2 .!£>.!:~:11 H e:.n l. ~a. ve: 1.a:K7i IX vt C a-&.a;cr,n • xa I, T) CX V't C' O't'CX0'\1 • e:x.­ xe: vwoe:wc;, e: I, c; 't'T) V yfj V 'tT) c; 0 At. itfi c; e:rc I, cpa ve:C a: c; 'tT) c; 6 e:, a. µe: vfj c; &ex auµµopcpo6vt.cx1. rcp.oc; ,;ouc; 6pouc; -r;ou ne:pt.-&wpCou 2I3.I54. 2I3. I5i3 H e:1tt.cpave:1.cxKfj a:v,;Ca-ra:a"Y) xa:1, T) av,;:Ca,;cxa,r· e:x.- 2I3.I54 X.E:VWOEW<;, El.<; 'tO f6a:cpoc; (yfj) µe:,;pouµe:v-6J auµcpwvwc; 7tpoc; 't'O E<l>HMEPII THI KYBEPNHIEOI (TEYXOI nPOTO) ne:p.1,-&w.p.1,o • 2!3.155 npf.ne:1, vex 1,xexvono1.06v ,;ov,c; nexpex>1.~'tw 6p.ou ~ 2I}.I54 ( .E\JJVEX C ,e­ 't:~1,) (I} To1.xwµex,;,a:. µl) e:cpo&1,exaµfvex µe: a,;c01.xe:Ccx nou e:C ( 2.) , ,. , vex.1,. exywyo 1, l)/\ e:x,;,p1, aµou: (ex) Em.qicfve:1,~ e:nC ,;w.v onoCw.v µnope:C >1.~no1,oc; va. •• 130:0 C cre:,1, : H a: V't,ttO":-&,a;Q"I, c;. E:K>te~wae:w<; a'tl) yfi O £ V np fn e: I, va: e:.Cvex1, ·µe:yo:Auifpa ,;.wv .10 8 OHMS (QM} •. (~}'AAA~; e:n1, cpa.ve:1,a~: H e:n1.~ve:1,a:l1.1j a:v,;.Ccr,;a:cr1,c; 6e:v npfne:i; vex e:Cva:1, µe:.ycxAV't.Epa: 't-WV IO g OHMS (QM). T 01, xwµa,;a e:<po61,acrµf va: µe: a,;01.xe:Ca nou. e:C va: 1, a:yw yoC (a} l) A e:x,; p 1, aµo u.: Em, cp<f ve:i, i) e:nC . ,;wv onoCwv >1.ano1.oc; µnope:C va: r:,a:oCcre: 1,: H a:v,;{ O'ta:cr~ E:XltE: VWOEW<; a'tT) V yT) 6 e: V np fn e: I, vex e:Cvcn µe:ya:Au'tepa: 1:.wv 10 8 OHMS (QM). (~)'AAA~ e:n1.qxfve:1."~: H a:ywy1,µo'tT)<; -&a: -&e:wpe:C,;~1, e:.rca;pxfic; e:<fv 'to a:vw­ TO v n<fxo c; -i-wv µl)-a:ywy C µwv cr,;pwµcf-i-wv e:nC ay<.v, y Cµw.v ITT.01.xe:Cwv, n.x. a:ywy1.µa: cpuAAa: (e:Acfcrµa: ... t m.}, µ e:'ta:AA 1, Kfj 61, x -r;u,wcr1, c; 1j a.AA o xax<f AA T)Ao uA1. x6 ,. auv6e:6e:µfva: µe: "t'T)V npocrye:Cwcr1,v, 6e:v une:p­ r:,a:Cve:1, ,;a 2 MlVI, ·xa:1, a'tT) rce:pCrc"t'WcrT) µe:"t'.a:AA1.x11c; (i".o e:µl3a:66.v e:rct.cpa:ve:Ca:c;) 01,X"t'UWO"E:W~., 0 e:nt.cpa:ve:1,a:><.6<; XWpog'tT)<; onfic; "t'OU 6 1, x,;uou. (lViESH) 6 e: v • vn e:p l3a:{ va 1. :~a 64 CM 2• (3) 01.a:6-fjno,;e:. µe-i-pT)°"'\ e:n1,cpa:ve:1.a:x-~c; av-i-1,cr,;a.aE:w<; ·fi a:v,;1,­ cr'tcfcre:w,c; e:,rne:vwcre:wc; O"'tT) y-fj a:Jt0:1,"t'OUµEVT) va: 61.e:~a:x-&e:C e:n'a:v,;fic; E<DHMEPll: THI: KYBEPNHl:EQl: (TEYXOl: nPQTO) 'Ht6't"t)C -i-Jl-t &e:l;a:µe:vfic; -&a: avT1,xa:-&Ca,;a,;.a1, oe: xpov1,x(f &1,a:- 213.154 cri::~µO:'t".CX 6xt. .µ.e:yail.6,;e:pa 't"0U e:v6c; E.'t"OU<; yt.a va d;a:acpail.C- (Euve:xC ce:­ 't".a.t, ) l;e:,;.a:1, 6'&-1, &e:v u.ne:p~aCvov,;a:1, at. xaSop1,o-&e:Coa:1, O:V't"t.crtacre:t.c;. Ml-&0&01, ~0>1.1.µwv (EA EYXWV) l .- En 1, cpa.ve.1..a.xfj A v-c,C a,;aat. c; ,Rroo L- ( µo vw,;.t,xfi a;v,;,Cari;ac.~c;) ae: OHMS (4J.), T)Ae:wr; . .po&1,a. (ELECTRODES "OF CONDUO]ING PAINT) auµcpwvwc; npoc; ,;ov a:p.1,-&µ6v (crxfiµa) 3 'tT)c; REOOMMENDATION lEC I67 'tOU, 1964, µe;,;pouµe:va,, µe: 't"O np.6,;unov 23/r;JJ a--r;.µoacpa1,.'pfil.:v ·:au µcpwvw~ np.oc; 't"T)V RECOMMENDA­ TION ISO R29I, napaypa;q>,o'c; .3~I ,;.ou 196-3. 2.- H a Wt;,~O'ta<H, > e:x x e: vwo e:wc; O't"T) y fi en: OHMS ( wµ) e:Cva:t. o il.6y,oc; µe.~a:1;6, iric; auve:xo-6.c; uae:wc; µe::1;pouµfvT)c; µe:~6, T)AEX't".po&C.ou ne.p1,ypa:cpoµf vou Ka:,;w,; .. fpw oe: e:nacpfi µe: 213. l 55 • 't"T) \l- 61t t, <pcf \l·El.<X 't"T) c; & e:~ a:µ e: ~ c; 't" OU OX fiµct.'t" O c; • KO: 1, 't" o U 'Y e: t, wµf VO U aa:ooC 't"OV O xfiµa,;,0 c;, Ka: I, 't" OU OAI, }(.O\J p e:6µa'k-O c;. H -Ka:'.mcn:a:ollf (CONDITIONING) ,;wv &e:t.yµcf,;wv e:Cva.t. T} <XU't".fj 't"T} c; na:pcx:y p<fcpou I. T.o T) AE:.>1.'t" p6& 1.0 'e:c va: l, & C O'K0 c; µe e:µ~cx66v E1tt.cpa:ve:Ca:c; 20 CM 2 xa:1, &1,cfµe:,;pov 50 MM. H a,;e;vfi ,;ou e:ncx.cpfi µe: 't"T)V e:1t1.cpa.ve:1.a: TT)c; &e:l;aµe:VJ1c; npfne:t. vex e:f;cxocpcx­ AC,e::-w:a-, n.x. &1,a: 't"T)c; xpfiae;w,c; uyp,ou xcfpimu fi uypou an6y­ you fi 01.aa&fino,;.e. aAl\T)c; Ka:WAAfjAov 67'.T)c;. To ye:1.wµf vo aa:aaC 't.OU oxfiµa:'&Oc; XPTJOl.µ01to1.e:C,;a;1, we; 't"O al\1'.o T)AEWtp6&1,o. ~t.a:p )(. fi c; i;cfa~ c;, 't"T) c; K1'.C µa:Ko c;, IOO ~6 A 't" - 500 ~ 6il.-c, -&a: e:cpcx p;µ6 Ce:,; ex 1, • H µfT.pT)OI..~ -&a: &1.e;cfie't",,(ll,, µe:Ta 't"T)V e:nC fva: AE:Tt't".6 e:cpa:pµo y 'ii v 't"T} ~ ,;,cf oe:w,c; & o"K 1, µ,1 c;, To T) A e: x,;p6 b 1, o µnope: C vex ,; o no-& e:'t"T) ,& e.C e:n C o 1, ou &fjno,; e: OT)µ e:C o u 't".T) c; e:ow't .. e:p 1, x fi c; fj £~ W't" e:p 1, xfi c; e:n 1,­ cpa: ve.Ca c;, ;uric; & e:l;a:µe: ~ c;. EG>HMEPII THI KYBEPNHIEQI (TEYXOI nPDTO) 'Ecfv T) µf,;.pfl0'-1 e:Cva1, a66va-c,oc; e:nC ,;TJc; oe:,ci­ µe.v'fi~, µnope:C e:nCOT)c; va 61,e:,ax&eC, Uno ,;due; cxu,;ouc; 6 pou.•c;, e:~c; ,;o e:pycxo,;ljp.1,ov, e:.nC 6e:.Cyµcx,; .. oc; ,;ou vl\.1,x.06. 2I3.I55 (>::uve:xC­ Ce:,;cx I, ) ~~~~~i~-~~~~~~~~-~!E~~~~!~~1-~E-!2Elf!:~~e2~e!2~~~!: ~.!:!:.G!!-.2~.22JS !1JS !!~!lEfE£~S ' Me:,;ai\i\1,xc£ au.a:r.oc,;.1,Kcf µfpT) auv&e:oe:µfvcx o,;11 yfj • 2I3.I56 . I . r:.t:1~ 1 /J ,;p6no·:, wa'te: ae:· ono1,06fjno,;.e o,;cf61,o '~n~ ni\T)pwae:wc; fi 'tT)c; 61,cx61,xa0Cac; e:xxe:vlf>ae:wc; va unapxe:1. e:µ~a66v 6x1. µ1,xp6,;e:pov ,;w v 0.04 ,;.e:'tpay. µf,;pwv ye:1,wµfvou µe:-y;cfi\A.ou ~g. e:nacp'4f µe: 'to npo"C6v avcf xu'31.K6v µf-i:pov npot 6v,;oc; ne:p1, txoµfvou e:1, c; ,;T)v oe:l;a­ µe:vfjv 'J;T)V o,;.1,yµfjv e:xe:CvT)v, }1.(XI, xavfva ,;µfjµa ');QU npo·iov,;oc; vex a-1tfxe:1, ne:p1,006,;e:pov cxno 2.0 µf,;pcx ano -ro ni\r,01,fo,;e:po ye:.1,wµf.vo µe:'to;AAt.xo aua,;a,;.1,x6 µfpoc;. Ta. µe:,;aAALxcf au,;cf OUO'ta't1,xa µfpT) µrtopouv va e:Cvcx1, 'tT)c; µopqrfjc;: (a) Me:,;.cxAA1.xfjc; no6oi3aAi3C&oc;, o-i-.oµCou crwA11voc;, fj nX'al-1.6<; (e:Acfoµa:-i-.oc;) e:q:;'6aov ,;o 0/\.1,,1.ov e:µi3a:66v i-.ou oe:. e:na:cpfj µe: ,;o uyp6 µe:,;cfAi\ou 6e:v e:Cvcx1, µ1,­ xp6-i-e:pov TOU OPLCoµfvou, fj (13-) 1{e:-ra:AA.l,Kfjc; axapac; µe: cr6pµcx ncfxouc; 6x1, µ1,x.po-rf­ pac; 'tOU I M.Vl (Xt.A.) 61,aµf,;pou }1.(Xl, e:µi3a:60~ onric; 6xt. µe:yaAu,;e:po V ,;wv 4 -re:,;pa:y. e:xc.no a,;wv, e:cp '6 oo v ,;o 0A1,x6v e:µ!3a:66v 'tTJ<; oe: e:na:cpfi µe: ,;o uyp6 ox.ocpa:.c; 6e:v e:Cva:1, µ1,x.p6,;e:po ,;ou op1, Coµfvou. To ne:p1,&~p1,o 2I3.I56 6e:v &a: fxe:1. e:cpa:pµoyfiv cre: 2I3.I57 J:.i:: I. , , 1 ,, J;. , ue:..,.cxµe:Vt.c; a:no e:v1.oxuµe:vT) rc,\a:o,;1,Kll UAT) e:cpout.aoµe:ve:c; µe: ono1..o 6fino,;e:. aAAo ovo-i-T)µa: anaA.01,cpfic; -i-ou x1,v66vou an6 cpop,;Ca, npoe:p E<DHMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPQTO) X 6 µ i v<t ( 6 YI µ.1, o u py o 6 µe: vex) 6 1, exp><.o 6 OT) c; 'tT) c; 1tA T) p~ae:wc;, e:cp,'6aov fxe:t. xa:m6e:1.x-&e:C. 6t.ex 1tpexK"&1,K(jc; auy><.pt.'tt.><.-fjc; 213.157 (EuNe:xCce­ 'U:Ctl.) 60><.1.µ-fjc; ouµcpwvwc; 1tpoc; 'tO 1tEpt.-&CJpt.OV 213.158 6,;1, 0 Xp6 VO«;. xex1'.a:p.wcre:w..c; (1,1,e:'t<X-1t't.wi:1..x6c; xp6voc;) i:ou cpopi:Cou i::ou OT)µt.oupyouµfvou e:vi:6c; 'tT)«; oe:~aµe:v(jc; 61,ap><.06crric; 'tTJ~ 1tATJ­ p~oe:w§ e:.Cvat. t.o:o66va:µoc; µe: ,:ov xp.6vov ,:ov A-a:µj3exv6µe:vov y 1.a µe:.'taAA 1. ><. 1j 6 e:~aµe: v(j exvexA-6y w,v b 1-CX<!f<ioe:w.v • .f ~1.~1211-~~~-~2~i!!-~-.L!~f1l2~) • (l} tuy><.pt, 't.l, K-fj 60.x t. µ'fi TOV xp6 vou X<XAexpwoe:wc; T)AE­ x,:poo,:,a;,:,1, xo6 cpop,:Cou auµcp~ywc; 1tpoc; i:ouc; 6pouc; 6oxt.µ1jc; i:.ou.c; rce:p1,ypacpoµlvouc; <Yt.T)v napcfypexcpo (2) -&a 61.e~cxx-&e:C I e:nC npw,:o,;6nou 6e~cxµe:v1jc; 41,Jt> evt.oxuµfvt'}; 1tAcx<Yt 1.x~c; 6AT)<; . 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Kcf,:w 'tOU 7 5 ·(;·ll)(:- e:><.exi:a;s, 't.T) c; XCJJ+)TJ't 1.­ ><.6'&.T)'to c; µe a:ui:6i1£1, vo6µe:vov (AUTOMOTIVE) xcx6at.­ µov V'tl')l;E:A, µCa: ava:1..oxCa: 'tOU 01t0Cou 61,fpxe:-cex1, 1t O w.ai:.e: T) 1t11J X v6 't.T)lJ., 't Ou cp Op,: C Ou 'tT) c; 0 A l, X ~ c; pol')c;, va: e:C va:L 1te:pC1tou 100 U C/M 3• 213. 158 (13) H fv,:aa"-1 ,:ou 1te:6Cou Et. c; i:ov .xCipov a:i:µ06 'tT)c; 6e:~a:µevl')c; Va µ~,:pd,:a:1, 61,a: xa:,:ex;\;\'fi;\ou µf,:pou ne6Cou auvex.wv evoeC(;e:wv µov,:a:pt.dµEvou µe:·,:ov cf(; 0 vcf 'tOU }ta-8-ei:o V lt(Xl, 't07to-&e:'t.T) µf VO V 'tOUACXX t, O'tO V <J>..::E.:..:."--=-2=25:.... ..:...:::' E=-.a(l),-;...H=M...c..cE~P II~: T-,-H I .~VBEP.NHIEOI·-(TEVXOJ.:,nP.aro) 20 .CM an6 i:ov >tcf{tE1:ov owAi,vcx n~.r)p~d.E~c;;.... 2I:3,~I58 Ilctpo µo C<X- 6ol-t.t. µ~ ~a 6.1. e:,a:x.-&e:t: E:r.C -•o e~ a:µe vf, <; (-:luvc.x·C C& ~ext.) E.K x~;>-~u~o <; 'tTJ ~ .ono~a<; ,;o n;\(i-uo c;,, 1-1,~¾o ~·, ,-k.Q,-l. 6:y,1.0~ El va1, f:=V't--6.£:; ,;.ou 15 ·iol(t, EXCXTQ.' . E)f.f:Cvwv ·nic; e:, e:v1.crxuµfv11c; 1tMW't:t,Xfi.c; uA.;ric; &.e:taµe:vfic;, ,, e1tC 6e:l;,cxµEvf)c; eC: ·e:v1.-axvµfvn,c; 7t/\.CX~vl.X/i<; 6A.T}<; oµo{WV 01,CXO't'..<fae:wv, E:7t~VO€l,-.. ovµfvric; .eaw:r.e;p1,x(f>c; .. µc µe:1;a~J\~>t6 :.X-ent1;iLq>~ii.:>1.p. cru. v6 ef>E•µ~-~o µi:: 't"T) yn. (2.)'01, ncxpcx:>t<f-cw; ~9L 'TT!c; 60¾1.µfic; -&a '.tfi:po6vt,a;1,:;...· c~) H 60>1.1,µ:f\ -&ex. 01,&~<iyaU'C.t. a~ 'KO:AUµµlvov. X,l~OV •'v1t6 ·Gl.>v­ &~Ka~ oxe:'I:.t,x,ic; V'fpaoCcx.c; xtf.i;w; 't"OU 80 '&01..c; .EKCX't'6v~ (ti) To CXU'L:OKt. vo6µc.vo v xcx~ .. cnµov v,;;fi CEA -r;o >:,prrat.µ.ono 1,0~.;.. µe: \lO v e: 1, c; ·n) v, 6ox 1,µ~ v -&~ fx e 1, aywy ~µcS 't.T)'t<X- a·v&ncxu·A'ac; (RE~ CONDUCTIVITY) <TTT) -&e:pµoxpacrCa. µe:,;p~oew.c; µe:,;a:~·15 3 )(.ext,·-~- pS/M. Au,;fj -&a µe:,;pcf'ta:1, ·at -X:l1i;,;cxpo. ◊~ot.x:i::Co.8 C;J![,L) e1, c; 'to ono-Cov T) .VT ' · • ·6 -- e:Cvcx1, µ1,Kp6,;.e:pT) 1'i COT) µe: 2.5 X IO • D2 .Sn.OU Ji -• Eq>a:pµo,Coµf VT) 't<fo1, t; (a:no.a'L:<Xot, j) D::= :,clr>poi;/'µe:-r;.cx,o T1Ae:wcpo6Cwv cre:. µf~pa: ~:· - 01,:&p.xe:1,a .µ£1:p1'ioe:ti.½; oe: 6e:u,;.e:p6;\eni:a. • • H a:ywy,1,,µ.6-i-l'}c; a:vcfn;av>..~c; (REST CONDUCTIVIT~) .µ.e-r;/.ou~ µf.vT) btC &e:1,yµcf-r;.wv -i-ov npot6vr:oc; AT)cp&fv,;wv i;Jot'l\1 &e:.~cxµe:~ Oc:>"Kt.µ~i µe:,;~ 't'l')V n11.~pwc11.v 6e:.v -&a. 6:.1,0:cpfpe:,t.­ or. 6~:ahox1..xfc; &ox1,µfc; enC ni\.aa,;1,xt.5v xa1, µe:,;ai\r-.1,-x.i!)v 6c:l;.<iµe:vdiv Ka-c.& 1tep1,006"te:po-v 't'WV 0~5 Ps/M. ·, .E<i>HMEPII THI KYBEPNHIEQI (TEYXOI nPQTO) : . fT l H ni\ fi pwcn. c; -l,a; • y.C v e:'t'a: 1, µ e: o"ta:-&-E p6 'pu B-µ6 e: V't'6 c; 't'T) c; 213. I 58 x;i.Cµaxoc;· I lw~ 2 i?;'to /\.E:7t't.6V Kett, {ta; e:Cva:1, 0 C6t.oc; 61,a; -i;ri·v 6e:~aµe:vfj'v ~40 e:v1.axuµlvibi ni\a:ITTt. i-t~ 6i\1J.1 xa:1, ft. a 't'l}V .6·e:f:a;µe; VVj «/-x,cf"A.u -f3~ b t, <; 'tO -i;'fi\o c; 'tT) <; 1tA.T)­ pwae:u.>'c;;j·- T) p ofi' 7t p ln E.I, • va ·6 I, a: >tOJt't e: 't(x:t, e:1, c; xp6 VO V 0 onoC O c;' e-C va:1, f3pax6 c;· 9'\JYl-t.P I, v6µe: VO c;· µe: 'tO V xp6 vov xa:­ i\a:pwae:wc;. (RELAZATION TLvIE)··y1,a 'to cpopvCo e:1.c; 'tl)V 6e:­ t;,a;µe:~v e:x xcf11:u~oc;. ( o) H ·nu,l-t. v6 't.T) c; Tou cpo p-i;C ou· 'IQa; #£'t pcf-i;a;1, ft· i.. l-t.o:'t!·"A.11. l)i\O µf-i;po. - cru-ve:xwv ·e:.v6 e:Ce;. e:w.v ( n. X•, 't'thi:ou FI ELD MILL /µoX~u/) e:µ~u,&1, <:ciµevou El, c; 'tO npo'i:6v >ta;t, 't07tO-&e:'tT)­ µf vou 6aov -i;o~ 6uva-i;6v ne:.1,6 }{.OV'ta o'tov awAfiva: n·AT)~ (e:} Ot. awi\fi·ve:c;' -i;po~oQoo:Ca:c; l-t.a;1, o l-t.a-&e:-i;oc; awi\'fiv ni\r,p·w­ {;aw-i;.e:p I, l-1.'t) c; . -. cre:wc; -l}a; cC va:1,/ 61, a:µf-i;pou IO CM ( e:l-t.. ') l-t.a:1,· -&a· l-t.a:'tai\ ri ,. youv. cre: f~o6ov· crwArivoc; ni\T)pwcre:w.c; 'tlJnou 11 T 11 • (au;) Kau>..i\T)Aov µ1,l-t.pocpCi\-i;pov ~{ µe: pu-&µ·1,(;oµfvriv na:pcc~ l-t.a:µn't-fjp1,ov xa-l,1,a-i;ouaa 6uva;-i;ljv 'tT)V pu!o-µ1,a'1 'tT)c; 01,' CXUT~<; 0L£PXOµEVr)c; pofic;, -l}a; e:cpa;pµ61;;e:'ta;I, .6Xt. <fvw 'tWV 5 µf.-i;pwv a:n6 'tT) v f~o&o v -i;ou awi\ ~ vo c; ni\ripwae:wc;. • <t. : • (c;.) H O"t'a-&µT) 'tp-u uypov. 6~v -&a: cp-&c{oe:1, 'tOV nu-&.µfva (l-t.if'tw • • ni6Cou µfpoc;) -i;pu owAfjvoc; ni\T)pwcr~wc; 1j -i;ou µ(rpou/ (t'IELD :; i ivIETER ). ~/ To llELLUMIT 5 e:upf-&11 6,;1, e:Cva:1, xcc-i;.cfi\i\T)i\ov. EQ>HMEPII THI KYBEPNHtEQI (TEYXOI nPOTO) , 1~1~B1E1~-~e~~~~-~~~~e~E~~~-!g~!~~!Q! ~!~!2> (3) H cxpxi.,dj 't'1.µfi 't'TJ<; Evt<fcrEwc; -1tE6CotJ -&ex ECvcxi. TJ x.a,;:aypacpe:Cacx e:1, c;· 'to EVwpC't'cx't'.ov xpovi.x.ov OT)µe:Cov µe-m 2I3;.I58 (l:uvexC Ca­ ta i.) 't'TJ v ncx~o'1 't'TJ c; pofi c; 't".ou xaua~µou ·6"'av µCa AECa xcxµm1AT) e:C:cxd-&Evfiaew;c; (DECAY CURVE) 611µ1.oupyT)-&e:C. 0 xp6'voc; XCXAc:tpc!> ; ' a e:wc; (RELAXAT l.O N TIME) e& t a:µcp6~&P.·£ <; ,; 1, c; 6ox. 1, µ f <; -&ex' & 1, a, . . . • ' . , 't'U1to6~1, w.~ 0 xp6vo <; 1tOU xp.e:1,ao~T)Ke. T) f V't'(XQ'I, c; 1te:6Cou vex e:C:acr{h;vficre.1. (cp-&Cve:1,) <X1to 't'T}v· cxpX,1.Kfi 't'1,µ1j e:1.c; o.37·•n1c; ap t (4) 0- xp6voc; XctAcxpwcre:wc; (RELAXATION TIME) 't'TJ<; '1,,t!P e:v1.oxuµlv~ 1t/\CXQ"tl,}1,'41 '6Al\1 6e:,aµe:v4-f 6EV -&a unep~aCve:1. 't'O V. 't'T) <; Vie x'1AU '3cat, & e:,aµe: vfi c;. 213.159 , 213~'999 . . ECDHMEPlt THI KYBEPNHI:EOI (TEYXOI nPOTO) ITN8EEIE YAAOY "Y.a;Ao~·-E: E6 .. v.&eo1, ~ K<X't.a p&.po~;­ IlupC'il) ~ AC-&o ~ (A t.ol; c:c~· 61.0 nup.t.'tC ou.) (S 1,. 0 2 ) A?~ou.µC va (AL 20 3 ) .,. A oj3 ecn.o ~­ May vr;aC.ct. Bop1.Kov 0C:eC61.ov g),&6~1.0. OC:aC61,o 'tOV 01,l)l'ipou: o, e:C &·1.0 T1, 'ta..vC ou AAX<XA1.x& Ol;eCoi.a. Yer.Ao~ c: E~v-&eoi.,~ Ka'tcf ~dpo~: 6.t. o, e.C o t.o. nvp1, 't.C ou Al\.ouµC va. "Aoj3e0"1'.o ~ Ma'.)' VT) aC a Bo~1.x6v OteC61.ov i.:Col)po~ o,d<'.ho 'tou Na.'tpCou 0l;e.C&1,o 'tou Ka:A.Cou, (ea. o) (MG- 0) (B203) (F) (FE 2o 3 ) . ) (T·1, 0 2 ) ) (Na:.20 ,/- -K~O)) (S 1, o 2 ) (AL203) ( Ca. 0) (MG 0) (B203) (Fe2o3 ) (Iicx2o) (K 20) 14-i - IS.5 " " I6. 5 - rs "· 4·~ 5.5 " 6. 5 - 21 " .. o .2-- o.6 " <. I " ": It: " . < I "' H• 63.0 - 65 . " If· 4 - 4. 5 " ft: 14 - 14.5 " "·· 2.5 -- 3 " " 5 - 6.5 " n o.3·ot• ft 7 - 9 " II o.7 - I " " .ECl>HMEPII THI KYBEPNHIEOI '(TEYXOI.RPQTO)' · ~.:~r£~~!:~-! u,~11. J; 8s) MT)X<X,v1. oµ6c;; ( enc. v6T)oc. ~) 61,a ,;T) v µf'tpT)Ot.--V 'tT) ~ cxv,;1, o-moe:wc;; >tpo6:.. 1tC1t·"t;Q'l'.l;O~ O'EW~ µfou.y; ~<fpou, oqiac.p 1.xou dxpou WEIGHT GUIDANCE :-Kcx-&o&~yrio1..~ Bapov~ SPECIMEN:- &e:Cyµcx. SEC'.rIO N AA' :-•(A 1..a )-i:.oµ~ AA' :ANGL~BAR WELDED TO CHASSIS:!"" rw.v1..urr..(j ~ oKo ~- auyxoA~T)µf:VT) <Yt"o aaaat·· STEEL .. CHASSIS :- aaac1.C an6 xci;>..u Sa. CONCRET'E BASE:-- f3'101, ~ cxno µ1te:--c6v • o:y6~wv TIGHTENING RING (CLAMP):- Lla:,1,i;uAt.o~ aucrq,Cy.!;e:w~ (aqny,1,,;fip) SPECIMEN-PL~.TE:- nAcf.,1,a: ( fAo:.aµ.a:) . 6-e: C yµa:'to ~ , (GASOOU S PHASE) :- ae:p1. WOT) ~ cpadt..~) TEFLON JO I NT :"", t·vwo.1.:£ ~ZFLO N t ; •. '· CO NifECT ING TUBE:-- - au .v& e:,; :t; l-i-0.,£. owX,1 v GLASS CYLINDER:-- u<fi\.1..,vo~ KUA.1, . .vopo·~ L.EVEL. OI!' LIQ1lID :.-t cna-OµT) (e:1rC·1u:.60} uypou • .. , ( HEATING .fuXJJH:·~ -&~;c.T) -&e:pµc1vo.sw£ TKE'LON JOINT. :~ fvwo1, c;; TEFLON SPECIMEN PLATE:- 1c11.awx ( D.aaµa) oc:Lyµaxc·~ (LIQUID PHASE) :- (uyp:fi q>li.01.~J . TIGHTENING RING (CLAMP):- Lla>t'tUAt.0~·0t>crcp.Cy:.!;:Ewc;•focp1.yl1.'tfjp) BOLTS THREADED TO WING NUTS:- BC&£<; ,1,ox11:1,.wµfvs~ OE rc'te:puyw:t:if.nEpL­ ,1,6X~~a ~' t Diagram f Device for measuring impact resistance by means of a spherically-ended falling weight r Wf•i!Jht ~l~~da~--- .--- .. T I I 0 0 ! A . II II ---TBO -Tf d=---~-;-4 -'I II . • if 11 ! :1 · I • I 11 '' I\ lt 1! i-~" °)"-'\'. r•- .· 0 0 0 .M 7 f I 200 -------i ~-+- I < ( ( ( • ( ( •. ( (: (:I Spedmen .. l • .• ·,', '.·' ,:,,, r---~' • --.- - m ] 0 p ·~ t . . ' ' '· ... , ', ' •. ' • ' . • ···:<:~>:~-~s~~:~~~~ : ! •• - ·----1· --.... ' , . -...; ' '· ·, :---. ·.:( . .. I ·- ~- " •• .-- •• \~\:\~~~ ,;::~~':,~~~~~--~~---~<,t~~-~~~~~-~~ .• " .· ' ~---"- ... , \'. ', ', ·.' · .. ·.', 1.,:,'<~, ~-0~"~:-....~ ---\~­<·-.. ·, .', -~<, <·< -.. -... :,., <<·· ··---"-...:,"-:,"" ~,--<- '•,:-, ' ' ' • ' ' "· • ' ·:-., ' • .• ' '· '· '·, • '· 'f '•, '· '·' • •. • ... ,,. ' . ·•." • ' ' ' I I ,. I ll • 0 U'l 25 0 ~ ~ 1- ,- ----M -----.:• I .---- 400 0 U'l Section AA' ·· I en ~ . II 1 = f f so-1 12190 Angle-bar welded to chassis' tteel chassis Concrete base :,,. 'd. 'd (t) • ::i, p., I-'' >< b:i . 1--'-1 (") . r..: z ., m a :c s: m "'O M I :c M ,a;: < a, m "'O 2 :c M m IO M ~ m < X 0 ~ :::J "'O lO 1 0 .·· E<l>HMEPII>':THltKYBEPNHIEOI (TEYXOI nPOT.O) AppendixB.lc .,,, •·'·•···· .,,., .. , ... , .... • Di.a gram 2 . ~ ,. ::, Device to test r~istance to, chemical agents I l'I I I ~II 1 ~ *:, .- -/J1 •. , .• • :.::-iT. 125 -+-------1 190 =-- ------= . .,-- -- ....... ~, I .-=-=---.II ' . ~' +-+-+-- / / 1\ \ / \ // ,, Tightening ring (clamp) Specimen-plate ........ (Gaseous phaN) • . . . . . Teflon joint =-=-~7"'.:-''--t--------· Connecting tube level of liquid Heating sheath Teflon Joint Specimen plate Tightening rln.g (clamp) . Bolts threaded.to wing nuts· (M6 x 200) • Eil>HMEP.II THI KYBEPNHIEDI (TEYXOI nPOTO) I:XHMATIKH LHATA2IE THE U"EKEYHE .6IA l:YTKPITIKON • EAErXON STORAGE TANK.:~ 6E3AMENf-L AilOSHKEY.tEQ.t FLOW ·MET~:- Mf~,po . pofi c;· FLOW:- Pofj PUMP:- A VTkC.<l. 1<lLCRO.:i!"'ILTER :- M 1, rtp.o(p{ AT{).O. '· BY PASS:- .Ilcx.p.a..xaµn,;fip.t.a,.~. SUPPLY PIPBS :- EWA~ve.c;))J,;ppcpoob:ola:c; CHARGE DENSIT.Y METER)'l-. Ml:tp.o nli1•.w,v6xrr1:o.c;. ~opiX.ou FILLING P1'PE :- Ew11.fjv .. ·.1tAYJ:pwqeuJ.c; FIELD MB:!CER.:- Metp.o rt~!-ou TANK UNDER ·TEST.:~ Ll~ct!..LEVfj vn6 &.e:·Y:xov % Diagram 3 SC.Hll1ATIC LAYOlfl' OF' RIG FOR COMPARATIVE TEST STORAGE TANK .o-- FWW METER FIJJW BY PASS l MICROFILTER PUMP SUPPLY PIPES 'x CHARGE DENSITY / Mm'ER p ½ / FILLING PIPE FIELD METER · --- • ··---· TANK UNDER TEST ~ 'd (I) ::s p.. I-'· >< til . I-' 0 ..,... ;r. Iv tv ~· m e ::c S:·-m · .,, M 4 ::c M " -< 01 m .,, 2 ::c M m :0 M =i m < X 0 M :::J .,, :0 4 0 ·~ E<l>HMEPII: THI: KYBEPNHI:EQI: (TEYXOI: nPOTO) ll12~!i!!:!L~.:.f §;~ 0P0I LiIE!I0.NTEZ TA Y.AIKA KAI TH}[ KATAZKEYHN ETA6EPrrn L\EEAMENQN, AYOiVIENQI{ flE3AMENQN, KAI KEL\.Yg}QN (MITOiilTIQN) L\E2AMEN0-C0.NTAINERS (flE3AMEN0-YII060XEQN)., IIP00PI ZO~NqN" AIA. THN METAOOPAN AIAN­ 'fYrMENQN YrP0II0IHMENQN AEPIQN THE KAAZEQE 2 . . . . . 214.000 214• 249 2I4. 250 Kct't:.g;oKOM1 l:wv-t:.a l. arc6 xcfAul3a, aAou µC v 1, o, Kp.cfµa aAouµ 1, vC ou, XctA.K6 ~ Kp.ctµa xa11.><.ou, • 1t. x. ope:CxcxAKO. Ev "[QU't"Ql, c;, ooxe:Ccx, oe:,a.t-1,e.v<U Kai. KEA6-cp11 Ka,;acrKe:uao,µfva cxno xaAx6 ~ xpciµa :XctA>t.06 -&ex w1,J.pf.nwvm1, µ6vov y1,a afp1,a µT) rce:p1.€xov,;a. ex>t.e:,;u,;>.., E.\tl.O v• 1:0 a1,-&uA f v 1, o v µrcop e: C e: v -rou ,:o 1, c; ~a rce:p 1, EX e: 1, oxt. 1te:p.1.ocr6't.e:po an6 0.005 ~ta.. e:Ka't"b CXKE'tUAEVl,OV. ~): M6vov UAl,Ka KO:'t.aAAT)Act. 3'1,a 'tT)V xaµT)Awtfpav -&e:p­ µoKpcx.a!a,.v 11.e.1.:mv;pyCa~ ,;w.v oox.e:Cwv, 6e:~aµe:v<f>v xa1, xe:Aucpwv 'KO:.:I, '"&'.WV e:~ap'tT)~'tW.V Ka1,· 1texpcti1.0AOU-&T)µa,;wv au't"<f>V µrcopouv vex XP-1'.J c11, µorco 1, 11-&06 v. 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