Resolution No. 280/1 of 2004 regulating the importation, registration and use of pesticides

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V, - - ~ - - ~ ~1 - - r. \o 1 C I I;;, K - - .I; .i; Annexes ~ ;;..J\...o.:i......il :\ f-1lJ ~ u~ ~ ~I.Jj yl .9-l o-ll.cl l>.J~I :\" ~J ~ 0 ~ ~ ~l )j y13 j ~ '-:-1.ll~\ ~':J : i ~ J ~ ;;.J\j.)1 J;i§ U.<i c-)<:..J.7 .JI :UW.\I j\ ,..,.Jl j\ ,..,.JI ~':J : i ~ J ~ EPA List 1 JI ~ ;;j ?.- , ,,JI ~'} :0 ~J ~ ;;j.F.--~\ w~i.a...l\3 Aj~\ EPA List 2 .J\ ;.il\ ~ : 1 ~ J ~ ~'11 4it114 Annex # 1: Pesticide Registration Form in Lebanon Annex # 2: Pesticide Re-registra tion Form in Lebanon Annex # 3: List of Maximum Levels of Tolerated Impurities for Active Ingredients Issued by the Ministry Annex # 4: EPA List 1: Inerts of Toxicological Concern Annex# 5: EPA List 2: Potentially Toxic Inerts/High priority for Testing Ar.mex # 6: The regulation m English version ==== b~ ~ (,J1 4..i.:Jj\ t,..U, ~ J ul...dl ~ J)L;. i.::..i\.J~':11 . ~~\ c--i .. ).:i L}.Q ul~ :~l~-U o..>WI J ' ::, I I) I II ~ ilil~\ ~ ~L:,.. ;;jl.g. ,,:;i ~ 9--A-:1 JI ,, .. ; • ,,':J\3 j,.r.W u1 ~ ,J~':113 ~~ o~ U.<i J~ ':JI ~ 4.li~ li .J ,..... ~ 4.bj.u,-aJI 4..,:.l,J\ ol.Jl.:i':J\ . )I ;;jt.g .:Ll\ ;iJi)W I y.::-. ~ .ho:.i.::....i....9 , .JA )I I ~ l....::ii.e I , . • • -~ 11 · ~ ':JI .;.. · "~\L ~ ~->"' UA - c ~. 4.J ~ 4.e-l..Jj!I rk. ..);J~ 4.i91 , ,,J1 ~ ~~ ,~I.Jjll ~j':J\ ~ .~l >jll ;;~I ✓.~ WI.he. : "-'..u..>'-'-'.JI S.1 WI ~. 9.)'11 ~ ~1 >ly.11 I~ j\y, cjµ:,.:; u~ ~ o.J• ;.,..., ., jJ 31 4,.·, .. ,a J1 ~1 ijll : a.:ut....i.JI o.1L0-U ..J \ y.ll I~ ~ y--:::,.i ~ ;; b 1.JA c4 o~WI w~\3 wb~\ ~ ~ )..J~ Jl.--.. ~ YW;!I ~ ~ y\..9) ,./'1 3 \ t,j I~ I ~ 4..c 1 ij11 y.. j-9 u-<> .) ji .4..l~\ : ;u..,li.11 i>.1WI I~ ~J va.J~ ~ ~ ~ • .Jly.11 :~u.JI oJWI ~....9 ·r.Y:? Lr" &...J ilyll \~ ~ .~ )\ o.l.l~y {)fa .J~ ~ y •• £/ o,,/1 o t) w~ 4.c. \ )jll y j-9 t1.b.0'-'=-~ ======= i~JJ.:ic.Li Annex 1 0l;J iJ ✓1Jj ~Ip ,J.:,:,-r c,J4:;...,I acl;jJl o;ljj :L..:1;}' ~,'c!,11 a...t-1.>.o Pesticide Registration Form in Lebanon I.General Information Name and address of manufacturer ot' active ingredient: Name and address of Pesticide formulator, Name and address of importer: Commercial Name, Specify Use Category (Insecticide, Fungicide, Herbicide, Plant growth regulator, ... ) 1-1. Status of application: A- ImtlOrtcd Pesticides I.The a.i is imported for the first time for use in Lcb,mon 2. New Trade name for a pesticide for which the a.i is used in Lcbm1011 B- Pesticides Locally Formulated I.The a.i is imported mu! the formulation is done in Lebanon 2. The a.i is produced in Lebanon C- Ex.pe1;111ental Use Permit □ □ □ □ □ :~~!.'.·\-\ ~ J.J'--A 4>1 Jj '-!J~; - i <!P-'>JF--'~~;~ r-' .r ui.;l ,J .L..c..... .iw ;,1,, ,#' 2. Active Ingredients 2-1. Active Ingredient Specifications Common namc(.s), Percent Active Ingredient(s): Code number: CAS No.: Chemical name: EmJ)irical Formula: Structural Formula: Chemical Class: Molecular Weight (M.Wt.): 2-2. Tcclmicill Grade Active lngrcdicnt(s) (TGAI) Min cc11ificd Limits of A.J.(s) (g/kg): 2-3. Phvsical and chcmic;1! prope11ics of the active ingredient Color: Physical State: Odor: <i.<:IJjJI o;lj:) 4,.s:.IJ -11 o,,..ir a,~~ :~\ = •'J.J,]J iJJ .. ;tlJ.JJl~1'3) " :.;~11"""''}1 0 :.j~l~pl .. :~I ~ pl .. :;.,;'-='-,5'.]1.W\..J1 " ~\ ;iJ\...iJJ(~l ,11) 0.1\\.1, Y-Y :~/?l j, iJl...ih(~l}l)o~J.:.l.l "yJ.11 W1 r. Melting 1>oint & Boiling point: Decomposition 1>0int: Corrosion prope1iics, Density: Solubility in water and organic soln:nts: ai:.,J ;i, &/39 a.....1;.i.JI o,;.H l,~ Partition coefficient between water and non-miscible :.h.l,,; U ,i,.41.ifi Ji, ~~J.l.l.'J ~1.1.1 .:t:!;; p:.:J1 J.-1.<- • solvent: pH (acidity/alkalinity): Flash point : Explosivity: 3. Data on Formulated Product 3-1. Tvpe of Fornmlation (WP, EC, ... ): 3-2. Phvsical nnd Chemical pro1lertics of fonnulaled product ~1'-,?jtj.\-'r :( ... ,p 7" ~ ,J.l,U J-;ti J)"'-') ..;=.:-l.14.f j ;i ½,!, .., ,- 4½r-ih ~li...o1}1 {-JJ,; • Present the physical propc11ics according to the t:ypc and formulation of the pesticide Color: :u ;lll Physical state: Odor: pH: Flammability: Explosivity: Viscosity: Conosivity: Density: Wettability: Suspensibility: Percent Persistent Foam: Wet sieve test: Dry sieve test: Emulsion stability: Flash point: 3-3. Toxicity Class According to WHO classiticat1011: 3.t:IJjJI o;fj1 ~1; ;11 03,w a., t!~ ;...,.;1)1 4-)1 ~)~ .'!"-r' ,WHOJ1J.,:...oi..,.......,,. • 4. Data on Toxicity Studies 4-1. Fate of Pesticide in animals 4--2. Acute Toxicity Oral LOSO for rats: Dermal LOSO for rats: LCSO for nits: Possibility of eye and skin irritation: 4-3. Sub-chronic toxicitv 90-day feeding studies: 90-day inhalation studies: 90-day dermal studies: 4-4. Chronic toxicitv Long tenn toxicity: Oncogenicity (Carcinogenicity): Tcratogenicity: Reproduction (2gcncnitiom): 4-5. Detaved Neurotoxicitv +6. Mutagenicitv ~IJj/1 "Jlj, ~IJj/1 os,'JI ~.,1.).o ::......:,1.11 . ;,-), if ; .,.Jl :..L1...ll .,, di .-. }.-1 • • • ;i.,,,j1uJl ~1 .r-1 :t.. ,, ~. ;,;Jt ;'.-;,'l'I Ji,l-.;,-" .:i:Ji • ~}1~1 f-t : ,,':fl.);#1:c.......!I • 4-7. Acceptable daily intake {ADD 5. Environmental Fate 5-1. Fate of pesticide in Water Surface and Underground wat!!r Biodegradation: Hydrolysis: Photolysis: Evaporation: 5-2. Fate of pesticide in Soil Accumulation: Degradation: Leaching: 6. Ecotoxicology 6-1. Effect of pesticide on non-target organisms Bee toxicity: Toxicity to soil microorganisms: 6-4. Effect of ncsticidc on natural cnenuc.s ;i..,1;}' .;;i;, ~1.,;/1 .;,;.i, :i.. ,..<M ~\,1.1 iJ ~,y.l1 J;:-A' • ,-o :..,iy,IJ~l,l,11 J..:l;}f o;fjj a....c l;jlf P!i.411 a., ..t'..1.,o 6-5. Effect of pesticide on Emihwonn J" J~' o~ J~ Js, ~,1.t.11 ~\:; .1"-'\ 6-6. Effect of pesticide on Birds J.,J,11 Js- ~,JJ.11 Ab . 1-, 7. Biological Properties J..9~1 ul.9'./1 tY J A.?--y ~\ u~ly.1 . V and Target Pests 7-1 Purpose and rate of use j~")I ..., ...,; J ..::.,'1~ I --V Cro1ls that may be sprayed by the j)esticide: ¥. -~11., J.........,, c.>"'-11 , 1.,.,\Jci O Targeted Pests & Rate of Use: Maximum Residue limits (MRL): Prc-ha.-vest interval {PHI): Re-entry pedod: 4'!1Jj!1 oJlj.9 :;. .. dJ~f 0.9,,,Jf a.. ,...,,. 7-2 Mode of action on Pest .i'/1 ~ .11..t.!1 .,r:lb ~fa r -v (Systemic, Contact, Stomach ... ) ( ... o..w1 J;J, y, ,.. .'.>'-\4 ,.;Jlf':J 8. Phytotoxicity ...:.,\.:-JI~ ~I .A 9. Compatibility ~).1 ~~. ~ 10. Safety handling 0-4~1 J~":/1., , 11. Storage and Disposal of ;iJ:. Juvl ~Jj'J\ ~ly, rY ~\ Jyb J ~jidi.,, Empty Pesticide Containers Storage period: Ways of Disposal of cmJlty containers: 12. Container Type of Container(Material used): Packing (Volume or weight): 13. Attachments (Refer back to Decree) 13-1 General Info1mation :L:1;}1 ~;1j9 a..: rJ ;,, os;,r 3., ,.,...., ~I l.,o" )I (:':"l}l,;,, iJwJ1 o>Wl ~1 ,:;f-.,,.,. J <i>UJ (-.JJ,; • Present Certificate about the manufacturer of active ingredient from the official authorities ..,J.bl1 r-.JJ,; = i.:... .:r ¼'?')I.., iJ.o J.i:i 'J ..,.....,....U ISO 9001:2000 scope formulation Ji o,1J1 r-JJJJ • Present Ce11ificate ofISO 9001 :2000 scope formulation for the fo1·mulator dated not later thall one year upon a1>plication 13-2 Certificates of Use and Registration fot' Pesticides ~1J)i ;;,,.J,'>IJ J,,:,....J1 J~1 .:..,1,1p t- 1 T' .~I -'-4 q iJwJ1 o>WJ . .:;~I .,..-:-11 J,,:<.-J J J~I .;.>I>~ (-Jj; • Present Ce11iticatcs of Use and Registration for the connnercial product of the active ingredient in country of origin . .!.UJ ~ ....,,,.:J.1 ~1).1 J.,i i)" o""""'1.I JJ..UI .;,' J;> ..:.,'}:,,.] .i.JwJ1 o>Wl J....,.. ,LJ ~ ..;.,1;~ (-J.l;:iJ;.IJ:.I iJwll -'lr,lJ • . .:i1.u,h For new active ingredients: Present Certificates of use & Registration for the active ingredient from the official authorities of 3 of the apJ>roved countries. 13-3 Authorization Letter from the Drnducc1· to the Agent 13-4 Technical Grndc Active Ingredients (TGAI) ,...;1.,.:.J1 ;,,...; J iJ....U1 (JI.fl) .,u.1 i JW .., i ~ ,S ,.:...11 ~ i J.ffl TGA1 Ji Jel>', ·~~ ,:r ........i (-.,, ;; o Submit a copy of a standard analysis certificate of the TGAI that indicates the degree of purity of active ingredient(s) and the IH~rccntagc of impurities. 13-5 Data on Formulated Product Present a standard composition certificate ~l ,j,11 & ,lj g 4-a:IJ ;JI os ,ill :Uy..1.o l.?JL,:,di .r=-J.1 ,:r ,.:;,1., ,.i.... o-\T' ~~ I ~ .;i •;4-!- r-..1.il rj 'J.P JJ,1 ..:,1,iJJ.1J :aw..11 ;1 ,l.1 ,j' .;i ; r. J Jl,,- cj Ji EPA Listi Ji rj -~ y.-}1 ~,;1 ,:r .;i ; f'; J r.!.s> if C:I~ J' -~i!J (-.JjJ e .1.,. ;i ; .,...i ~~ J 11>-4..li ~ EPA List 2 Ji Present a ce1iificate stating that the formulated product does not contain any of the com11ounds listed in EPA List l. In case the product contains any of the additives or solvents specified in the EPA List 2, its concentration should be mentioned. 13-6 Storage Stability y; .s/:.ilJ ,s ,.aJ u.l.,,,.) •J';·•· ,Y.;; ~ ..:,\.p ydll ~ {-.u; e Present data for the accelerated storage test on highest nod lowest temperatures 13-7 Methods of Analysis Present Methods of analysis used for the Formulated Product Active ingredient Residues J,,1,-=ll 1.J j:, V- I I" :.:,- fl ..i.....:..-11 ,/1.,4J1 ~I J f (-JJ, f$J~l~I 0 ..ii....J1 ,;\l.1 • 13-8 Pesticides imported for trials y 1 1.:c:d-l a; .,,, l, d.!J~~, /\-, r ~J.k.l •IJ.UI ~ ~,r,j i;)I ~I y ;l>;,.,JI ~9 J!.}J {-.u; • Submit a report of the results of local trials conducted on the new Pesticide. 13-9 Label J,Alll '\-1 T' 'i.,:..:\1 ~ J ~I ~I er' :i,;....J {-..J.i:; • Submit a copy of the label specimen used in the coWttry of origin .:it.:,J ,J .. ,, J <.$Pl ,.;-a.U.1 t,Jr-' er'..,; ; {-.ti; o Submjt a copy of the label intended f01· use in Lebanon 13-10 Tcctuuciil Data File 14. Declaration ~l;j,ll o;1jj ~1))11 ;;, 411 a.. ..,..u ,YJJ ,riJ)i oiJJ.li ,:t i.,."5' i$j "-11 ~i) ,~lll:!J ~,J..1 tp ,l1 '-:---" h...,>,...PJ ii!~L.p ,/' 4Jl..:..,'J! o,l. rj i~;l ,ll QI., .,WI ii!\S' 0½ C.r"j J,j .)' ~ J-P ;, 4A j'iU I .:.ill,1.,:,>-'JI J .:,'Jl,.o;...'JI u pJ ui J, .r' , W o JP .i.l, .;,I., .,w, t' J!l.b.,r 1$ )~, J\M:..,W )i y J\::,:.ll vj J.l,!1 J! ):.,,h) uW;'I A.!w; JWl' O~h.- .:,i,. ,lu i;i ,:f- ;i) JJJ1 r~I! 4A fa 65'" .,.:Ji uj .u,.b., . .s' ..!.11 I hereby declare t/lat tlte i,iformation furnished in tltis form is true and correct according to the today state of the urt. I guarantee that any consignment of the product entering the country whether for experimeutal or commercial use will conform with the requirements stated herewith, providing that the uses and precautionary measures recommended by the company are followed. 11ie company is committ.ed to inform the country of new ji11di11gs, wlticlz are of relevance to human or environmental safety. Company Stam1>: Name: Address: Website: E-Mail: Date: Signature: rrJJJ=d.ri Annex 2 .:i~ .j ir'-'J ~,j.:i ~ ii.:il.::;f ii ,w:.., Pesticide Re-registration Form in Lebanon a.:l;jll o ,fj.9 ;\.l:IJ,.i/1 o.s,.,!/1 a...)/...1.0 Name and address of manufacturer of active :aJwJ! o~l.JI ~! 0r~~ ~1 o ingredient: Nmne and address offornmlator: Name and address of importer: Pesticide Registration Number: Commercial Nrune: Use Categoiy (Insecticide, Fungicide ... ): Other needed infonnation: Company Stamp: Date: Signature: Fungicides # Chemical Type Impurities 1 Anilazine Tech Water: Max 3g/Kg Anilazine WP Water: Max 20g/Kg 2 Benomyl Tech Water: Max 3g/Kg 2,3-diaminophenazine: 0.5 mg/Kg 2-amino-3-hvdroxvohenazine: 0.5 ma/Kg Benomyl WG 2,3-diaminophenazine: 0.5 mg/Kg 2-amlno-3-hydroxvnhenazlne: 0.5 ma/Ka Benomyl WP 2,3-diaminophenazine: 0.5 mg/Kg 2-amino-3-hydroxvohenazine: 0.5 ma/Ka 3 Bitertanol Disp. Cone. Water: Max 5!'.,/kg Bitertano1 Tech Water: Max 5g/kg Material insoluble in acetone: Max 5g/ko 4 Captan Dust P Perchlormethvlmercaptan: 1 % of Caotan content Captan Tech Perchlormethylmercaptan: 1 Og/kg Loss on drvinQ: 150/ka Captan WP Perchlormethylmercaptan: 1% of Captan content 5 Carbendazim Tech Phen az ine-2 ,3-diam ine: O. 003g/kg 3-aminoohenazin-2-ol: 0.00050/ka Carbendazim Water Disp.Gra Phenazine-2,3-diamine: 0.003g/kg 3-aminoohenazln-2-ol: 0.0005a/ka Carbendazim WP P henazl ne-2,3-d iam ine: 0. 0 03g/kg 3-aininophenazin-2-ol: O.OOOSa/ka 6 Chlorothalonil Tech Hexachlorobenzene: Max 0.3g/kg Material insoluble in xvlene: Max 3.Sa/ka Chlorothalonil WP Hexachlorobenzene: Max 0.03% of the chlorothalonil content 7 Copper Carbonate basic Tech Cu soluble in water: 20X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) Lead:Max O.SX mg/kg (X=Cu content g/kg) Cadmium:Max 0.1X ma/ko (X::::Cu content o/kal ;\,,;IJjJ1 iiJlj;1 a .. .c1J.~1 ".9Je!I a.i.,,<Ml rrJ;r Annex 3 o )jyl J.i ,;r o~I a.I~\ ~1 ,.JJ ~\~\ W";J List of Maximum Levels of Tolerated Impurities for Active Ingredients Issued by the Ministry Fungicides Herbicides Insecticides Acaricides Insecticides-Acaricides Insecticides-Acaricides-Fungicides-Herbicides Insecticides-Fungicides Fungicides-Acaricides Plant Growth Regulators Fungicides # Chemical Type Impurities 1 Anilazine Tech Water: Max 3g/Kg Anilazine WP Water: Max 20g/Kg 2 Benomyl Tech Water: Max 3g/Kg 2,3-diaminophenazine: 0.5 mg/Kg 2-amino-3-hvdroxvchenazine: 0.5 ma/Ka Benomyl WG 2,3-diaminophenazine: 0.5 mg/Kg 2-amino-3-hvdroxyphenazine: 0.5 mq/Kq Benomyl WP 2,3-diaminophenazine: 0.5 mg/Kg 2-amino-3-hydroxyphenazine: 0.5 mq/Kci 3 Bitertanol Disp. Cone. Water: Max 5a/kg Bitertanol Tech Water: Max 5g/kg Material insoluble in acetone: Max 5q/kq 4 Captan Dust P Perchlormethvlmercaptan: 1% of Caotan content Captan Tech Perchlormethylmercaptan: 1 Og/kg Loss on drvina: 15a/ka Captan WP Perchlormethylmercaptan: 1% of Captan content 5 Carbendazim Tech Phenazine-2,3-diamine: 0.003g/kg 3-aminophenazin-2-ol: 0.0005q/ka Carbendazim Water Disp.Gra Phenazine-2,3-diamine: 0.003g/kg 3-aminoohenazin-2-ol: 0.0005a/kQ Carbendazim WP Phenazine-2,3-diamine: 0. □03g/kg 3-aminophenazin-2-ot 0.0005g/kQ 6 Chlorothalonil Tech Hexachlorobenzene: Max 0.3g/kg Material insoluble in xvlene: Max 3.5a/ka Chlorothalonil WP Hexachlorobenzene: Max 0.03% of the chlorothalonil content 7 Copper Carbonate basic Tech Cu soluble in water: 20X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) Lead:Max O.SX mg/kg {X=Cu content g/kg) Cadmium:Max 0.1 X mo/kq (X=Cu content a/kq) Fungicides # Chemical Type Impurities 8 Capper oxide Dust P Metalic Copper:Max 50X mg/kg (X=Cu content g/kg} Cupric copper: Max 120X mg/kg (X=Cu content g/kg) Cu soluble in water:Max 25X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) Lead:Max 0.5X mg/kg (X=Cu content g/kg) Canmfum·Max 0.1 X mn/kn <X=Cu content a/ka) Capper oxide Tech Metalic Copper:Max 50X mg/kg (X-Cu content g/kg) Cupric copper: Max 100X mg/kg (X=Cu content g/kg) Cu soluble in water:Max 25X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) 'Lead:Max 0.5X mg/kg (X=Cu content g/kg) Cadmium:Max 0.1X mg/kg (X=Cu content g/kg) '• --- -- "-ccum --Ir,·•--· ••~ 1!';n/kn Copper oxide WP Metalic Copper:Max 50X mg/kg (X=Cu content g/kg} Cupric copper: Max 120X mg/kg (X=Cu content gfkg) Cu soluble in water:Max 25X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) Lead:Max O.SX mg/kg (X=Cu content g/kg) Cadmium:Max 0.1 X mct/kn IX-Cu content a/ka\ 9 Copper oxychlaride Dust P Cu soluble in water:Max 1 OX mg/kg (X=Cu content g/kg) Arsenic:Max 0.1 X mg/kg (X=Cu content g/kg} Lead:Max 0.5X mg/kg (X=Cu content g/kg) Cadmium:Max 0.1X ma/kn (X-Cu content a/kal Copper oxychlaride Tech Cu soluble. in water:Max 10X mg/kg (X=Cu content g/kg) Arsenic:Max 0.1 X mg/kg (X=Cu content g/kg) Lead:Max O.SX ing/kg (X=Cu content g/kg) Cadmium:Max 0.1 X mg/kg (X=Cu content g/kg) Loss on d~inn: Max 20n/kn Capper oxychloride WP Cu soluble in water:Max 10X mg/Kg (X=Cu content gfkg) Arsenic:Max 0.1 X mg/kg (X::cu content g/kg) Lead:Max 0.5X mg/kg (X=Cu content g/kg) Cadmium:Max 0.1 X mn/kn lX-Cu content a/ka\ 10 Copper Sulfate Tech Arsenic:Max 0.1X mg/kg (X=Cu content g/kg) Lead:Max 0.5X mg/kg (X=Cu content g/kg) Cadmium:Max 0.1 X mn/ka (X-Cu content a/ka\ 11 Dichlofluanid Tech Materials insoluble in Acetone: Max 25g/kg 12 Dodine Tech Water: Max 1 Og/ka Fungicides # Chemical Type Impurities 13 Fantin Acetate Tech Inorganic Tin: 5g/kg Loss on Vacuum drvlna; Max 10Q/ka Fentin Acetate WP Loss on Vacuum drying: Max 30g/kg 14 Fentin Acetate+Maneb WP Inorganic Tin: 0.5% of fentin acetate content Loss on Vacuum drving: Max 20q/ko 5 Fentin hydroxide Tech Inorganic Tin: 5g/kg Loss on Vacuum drying: Max 1 OQ/kQ Fentin hydroxide WP Loss on Vacuum drving: Max 300/kg 15 Fantin hydroxide+Maneb WP Inorganic Tin: 0.5% of fentin hydroxide content Loss on Vacuum drvirsci: Max 20q/ka 17 Flusilazole EC Material Insoluble in acetone: Max: 1q/KQ Flusilazole Emulsion in Water Material insoluble in acetone: Max: 1a/Ka Flusilazole Tech Material insoluble in acetone: Max: 1 a/Ka Flusilazole Water Disp.Gra Material insoluble in acetone: Max: 1g/Kg 18 Folpet Dust P Water:Max 50q/ko Folpet Tech Water: Max 200/kq Folpet WP Water:Max 500/kg 19 Fosethyl-Al Tech Loss on drying: Max 10g/Kg lnoraanic ohosohate: MaY 10,::.'!<::; c,xuressed as Al-ohosohite Fosethyl-AI WP Water: Max 1 Sg/Kg lnoraanlc phosohate: Max 1 % as Al phosohite 20 lprodione Tech Loss on dryin!"l: Max 10g/Kq lprodione WP Water: Max 200/KQ 21 Mancozeb Diso. Powder Water: Max 2% Mancozeb Dust P Water: Max 2% Mancozeb Tech Water: Max 1 % :22 Maneb Disp. Powder Water:Max 1.5% Zn: 0.5% Maneb Dust P Water:Max 2% Maneb Tech Water:Max 1.5% Zn: 0.5% 23 Metalaxyl EC 2,6-dimethylaniline: Max 0.1 % of Metalaxvt content Metalaxyl G 2,6-dlmethv[ani!ine: Max 0,1% of Metalaxvl content MetalaXYI Solution for Seed trtm. 2,6-dimethvlaniline: Max 0.1 % of Metalaxvl content Metalaxvl Teel"> 2,6-dimethvlaniline: Max 1o/KQ Metalaxvl Water Dlso Powder 2,B-dimethylaniline: Max 0.1% of Metalaxvl content Metalaxyl WP 2,6--dimethylanlline: Max 0.1 % of Metalaxvl content Fungicides # Chemical Type Impurities 24 Propineb Disp. Powders Arsenic: 30% of propineb declared Water: 2.5% Propineb Dust Arsenic: 20ug/g Water: 2% Propineb Tech Arsenic: 25ug/g Water: 2.5% 25 Sulfur Aciueous Dispersions Arsenic:Max 5X -uq/o (X;;;% S\ Sulfur DisP. Powder Arsenic:Max 5X -uo/o IX"'% S) Sulfur Dust P Arsenic:Max 5X -UQ/Q (X=% S\ 26 Thiophanate-methyl Aqueous Suspension 2,3-diaminophenazine Max: 0.0005g/Kg of the thiophanate--methyl content 2--amina-3-hydraxyphenazine Max: O.OOOSg/Kg of the thiophanate-methyl content Thiophanate-methyl EC 2,3-diaminophenazine Max: O.OOSg/Kg 2-amino-3-hvdroxvphenazine Max: O.OOSa/Ka Thiophanate-methyl Tech 2,3-diaminophenazine Max: 0.0005g/Kg of the thiophanate-methyl content 2-amino-3-hydroxyphenazine Max: 0. OOOSg/Kg of the thiophanate-methyl content Thiophanate-methyJ WP 2,3-diaminophenazine Max: 0.00059/Kg of the thlophanate--methyl content 2-amino-3-hydroxyphenazine Max: 0.0005g/Kg of the thiophanate-methyl content 27 Thiram Oisp.Powder Water:Max 2% Thiram Dust P Water: Max 2% Thiram Powders for seed trt. Water: Max 2% Thiram Tech Water solubles: O. 7% Water:Max 1.5% Oil: 0% Thiram Water Disp. Gra Watl:!r: Max 25a/Kg 28 Tolvlfluanld Tech Material insoluble in acetone: Max: 25a/Ka Tolylfluanid WP Water: Max 1 Sa/KQ Fungicides # Chemical Type Impurities 29 Triadernefon Dust P 4-Chlorophenol: Max 0.5% of the triadlmefon content Water: Max 2Da/Ka Triademefon EC 4-Chlorophenol: Max 0.5% of the triadimefon content Water: Max 5a/Ka Triademefon Granules 4-Chloroohenol: Max 0.5% of the triadimefon content Triadernefon Tech 4-Chlorophenol; Max 0.5% Water: Max 1 Og/Kg Material insoluble in acetone: Max Sa/Ka Triademefon Tech Concent 4-Chlorophenol: Max 0.5% of the triadimefon content Water: Max 15g/Kg Material insoloble in acetone: 600/Ko Triademefon Water Disp. Gra 4-Chlorophenol: Max 0.5% of the triadimefon content Water: Max 30a/Ka Triademefon WP 4-Chlorophenol: Max 0.5% of the triadirnefon content Water: Max 20a/Ka 30 Triadirnenol Disp.conc 4-Chlorophenol: Max 0.5% of the triadimenol content Water: Max 3a/Ka Triadimenol Dust P 4-Chlorophenol: Max 0.5% of the triadimenof content Water: Max 200/Ka Triadimenol Granules 4-Chlorophenol: Max 0.5% of the triadimenol content Triadimenol Oil miscible Liq 4-Chlorophenol: Max 0.5% of the triadimenol content Water: Max 3a/Ko Triadimenol Tech 4-Chlorophenol: Max 5g/Kg Water: Max 5g/Kg Material insoluble in acetone:Max Sa/Ka Triadimenol Water Disp.Gra 4-Chlorophenol: Max 0.5% of the triadimenof content Water: Max 25a/Ka Triadimenol WP 4-Chlorophenol: Max 0.5% of the triadimenol content 31 Vincfozoline Dust P Water: Max 50a/Ka Vinctozoline Tech Water: 20a/Ka Vinclozoline Water Disp.Gra Water: Max40Q/Ka Vinclozoline WP Water: Max 40g/Kg Fungicides # Chemical Type Impurities 32 Zineb Disp. Powder Arsenic:Max 25Dmg/kg Water:Max 1.5% Mn: 0.5% Zineb Dust P Arsenic:Max 2.5X + 20mg/kg (X=%Zineb declared) Water:Max 2% Zineb Tech Arsenic:Max 250mg/kg Water:Max 1.5% Mn: 0.5% 33 Ziram Disp.Powder Arsenic:Max 2.5X mg/kg (X;:;::%Ziram declared) Water:Max 2% Ziram Dust P Arsenic:Max 2.5X + 20mg/kg (X=%Ziram declared) Water:Max 2% Ziram Tech Arsenic:Max 250mg/kg Water:Max 1.5% Ziram Water Disp.Gra Arsenic: Max 0.25:xX + 20mg/kg, where Xis the Ziram conten~ (g/kg) Water: Max 25a/Ka Herbicides # Chemical Type Impurities 1 2,4-0 Tech Free Phenols: Max 3g/kg calculated as 2,4-dichlorophenol Water: Max 1 Sg/kg Sulphated ash: Max 5 g/kg Triethanolamine insolubles: a triethanolamine solution of the material shall leave not more than1 g/kg residue on a 1 0Sum test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 2 2,4-D Dichlorprop salt Aqueous solution Free phenols: Max(0.5X+1.5Y)% expressed as 2,4 dichlorophenol where X and Y are the 'of the 2,4-D and dichlorprop contents. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 a/ka shall remain on a 1 S0um test sieve. 3 2.4-D Sodium salt Aqueous solution Free phenols: Max Sg/kg expressed as 2.4 dichlorophenol of the 2.4-D content. Water insolubles: The product shall pass through a 250um 'test sieve and not more than 1 g/kg shall remain on a 150 um test sieve. 2,4-D Sodium salt Ester EC Free phenols: Max Sg/kg calculated as 2,4-dichlorophenol of the 2,4-D content. Material insoluble in oil: The product shall give a clear, or opalescent, homogeneous solution which shall leave not more than 1 g/1 residue on a 150 um test sieve, and the sieved solution shall contain not more than a trace of sediment. Water: Max Sg/kg 2,4-D Sodium salt Tech Free phenols: Max 5g/kg expressed as 2,4 dichlorophenol of the 2,4-D content. Water: Max 90g/kg Water insoluble: Max 1a/ko 2,4-D Sodium salt Tech Esters Free phenols: Max Sg/kg calculated as 2,4-dichlorophenol of the 2,4~0 content. Free acidity: Max 30g/kg expressed as 2,4-D of the extractable acid content. Suspended solids: Max 1g/kg Water Content: Max 1 Og/kg, Visible water shall be absent Herbicides # Chemical Type Impurities 2,4-D Sodium salt Water soluble powders Free phenols: Max 5g/kg expressed as 2,4 dichlorophenol of the 2,4-D content. Water insolubles: When the product is dissolved in standard water C, any insoluble material shall pass completely through a 250 um test sieve, not more than 1 g/kg shall remain on a 150 um test sieve. and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 4 2,4-D+Mecoprop salt Aqueous solution Free phenols: Max(0.5X+1.5Y)% expressed as 4-chloro 2-methyl-phenol, where X and Y are the of the 2,4-D and Mecoprop contents. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 a/ka shall remain on a 1 S0um test sieve. 5 2,4-DB Tech Free phenols: Max 20g/kg, expressed as 2,4-dichlorophenol of the 2,4 DB content. Sulphated ash: Max 1 0g/kg Triethanolamine insolubles: A triethanolamine solution of the material shall leave riot more than 1 g/kg of residue on a 105um test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 6 2.4-DB Potassium salt Aqueous solution Free phenols: Max15g/kg expressed as 2,4 dichlorophenol of the 2,4 DB content. Water insoll!bles: The product shall pass through a 250um test sieve and not more than 1 g/kg shall remain on a 1 S0um test sieve. 2,4-DB Potassium salt Tech Free phenols: Max15g/kg expressed as 2,4 dichlorophenol of the 2,4 DB content. Water: Ma·x 15g/kg Water insolubles: An aqueous solution of the material shall pass completely through a 250um test sieve, not more than 1 g/kg shall remain on a 150um test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. Herbicides # Chemical Type Impurities 2,4-DB Potassium salt Tech esters Free phenols: Max 1 Sg/kg calculated as 2,4 dichlorophenol of the 2,4 DB content. Free acidity: Max 30g/kg expressed as 2,4-DB of the extractable acid content. Suspended solids: Max 1g/kg Water content: Visible water shall be absent. 7 2,4-DB+MCPA Salt Aqueous Solution Free phenols: Max (1.5X+0.5Y)% expressed as 2,4-dichlorophenol where X and Y are the 2,4 DB and MCPA content. Water insolubles: The product shall pass through a 250um test sieve and not more than 1a/ka shall remain on a 150um test sfeve. 8 Alachlor EC Water: Max 2g/kg Alachlor Tech Acetone insolubles:Max 0.2 g/kg 'Water:Max 3 g/kg '2-Chloro-2',6'-di C2H5 acetanilide:Max 30 g/kg 2'-sec-butyl-2-chloro-6'-ethyl-N-(methoxymethyl)acetanilide: Max 19g/kg 9 Ametryn Tech NaCl: 2% 10 Amitro[e Tech Loss on drying: Max 2% Water: Max 20g/kg Water Insoluble: 5o/kg Amitrole Water Soluble Powders Water: Max 20g/kg 11 Atrazine Tech NaCl: 2% 12 Bentazone Salt Aaueous Solution Water insoluble: 1 a/ka Senta zone Tech Triethanolamine insoluble: Max residue left on a 1 OSum test sieve:1 g/kg. The sieved solution should be clear Water: 10 q/kq Bentazone Tech Cone Water insoluble: 1 Q/kg Bentazone WP Water: 20 g/kg 13 Bifenox Aqueous SC 2,4-Dichlorophenol: Max 3 g/kg 2,4-Dichloroanisole: Max 6 g/kg Loss on Drying: Max 10 a/ka Bifenox Tech 2,4-Dichlorophenol: Max 3 g/kg 2,4-Dichloroanisole: Max 6 g/kg Loss on Drvino: Max 10 o/ko Herbicides # Chemical Type Impurities 14 Bromacil Tech Water: Max 1 o o/ko Bromacil Water Disp. Granulate Water: Max 15 g/kg Bromacil WP Water: Max 20 g/kg 15 Bromoxynil Tech Ory material: Max 1 Sg/kg Wet Material: Max 1 OOg/kg Sulfated ash: Max Sq/kq 16 Bromoxynil heptanoate EC Water: Max 2g/l Bromoxynil heptanoate Tech Free acidity: Max 1 O ml in 1 N sulfuric acid % Water: Max 1g/kg Sulfated ash: Max Sg/kg Material insoluble in xvlene: Max 1a/ka 17 Bromoxynil octanoate EC Water: Max 2g/l Bromoxynif octanoate Tech Free acidity: Max 1 O ml in 1 N sulfuric acid % Water: Max 1 g/kg Sulfated ash: Max Sg/kg Material insoluble in xvlene: Max 1a/ka 18 Butachlor EC Water: 2 g/kg Butachlor Tech Acetone insolubles: 0.2 g/kg 'Water: 3 g/kg 2-Cl-2',6' di C2H5 acetanilide: 20 g/kg Dibutoxymethane: 13 g/kg Butyl chtoroacetate: 10 g/kg 'N-butoxv CH3-2'-sec-butvl-2 Cl-6'-athvlacetanilide: 14 a/ka 19 Carbetamide Tech Water and Volatile impurities: Max 1 Og/kg Acetone insolubles: Max So/kq 20 Chloridazon Tech 4-Amino-5-chloro-isomer: Max 60g/kg Water: Max 20q/ka Chloridazon Tech Cone Water: Max SOg/kq Chloridazon Water Diso.Gran Water: Max 50g/kg Chloridazon WP Water: Max 50g/kg 21 Chlorotoluron Tech 3-(3-chloro-4-tolyl)-1-methylurea: Max 8g/kg 3-(4-tolyl)-1, 1-dimethylurea: Max 8a/ka 22 Chlorpropham Tech Material insoluble in perchloroethylene: Max 0.5% Loss on Vaccum drying at 20C: Max 1.5% Chloroaniline: Max 250uo/o Herbicides # Chemical Type Impurities 23 Chlorsulfuron Tech Water: Max Sg/kg Material insoluble in acetone: Max 10a/kq Chlorsulfuron Water Disp.Gran Water: Max 1 0g/kq 24 Chlorthiamid Oisp. Powders Acidity or-Alkalinity: Max Acidity:2% calculated as H2S04 Max Alkalinitv: 1 % calculated as NaOH Chlorthiamid Tech Water content: Max 0.5% 25 Cyanazine Suspension Cone. 2-2-methyl propionitrile*: Max 2% of the cyanazine content Simazine: Max 1 % of the cvanazine content Cyanazine Tech 2-2-methyl propionitrile*: Max 20g/kg Simazine: Max 1 0g/kg 'Inorganic chloride*: Max Sg/kg Loss 011 drylng at 70C to constant weight~: Max 1 Sg/kg Water: Max Sg/kg Chloroform insolubles": Max 20a/ka Cyanazine WP 2-2-methyl propionitrile": Max 2% of the cyanazine content Simazine: Max 1 % of the cvanazine content 26 Oalapon-Sodium Tech Loss on drying: Max 3% 'Water insoluble material: Max 0.5% Coarse material insoluble in water: Not less than 99.8% of the product shall oass throuQh a 150um test sieve. Dalapon-Sodium Water soluble Powder Material insoluble in water: An aqueous solution of the product shall leave not more than 0.25% on a 150um test sieve. The sieved solution shall be clear or opalescent and shall not contain more than a trace of sediment. PH of 10% aqueous solution: Min: 4.5 Max: 7 Water: Max 1 % 27 Desmetryn Tech 1socuum cnionae content: Max L'ro Water: Max 2% 28 Dicamba Aqueous Solution PH of solution: Min:6 - Max:8 Dicamba Tech Material insoluble in Alkali: Max: 2ml/1 00g Material insoluble in Toluene: Max: 2ml/100g Loss on vaccum dryin~: Max:3% Herbicides # Chemical Type Impurities 29 Dichlorprop Tech Free phenols: Max 1 Sg/kg, expressed as 2,4-dichlorophenol of the dichlorprop content Sulphated ash: Max 10g/kg Triethanolamine insolubles: A triethanolamine solution of the material shall leave not more than 1 g/kg of residue on a 105um test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. Dichlorprop Tech Esters Free phenols: Max 15g/kg, calculated as 2,4-dichlorophenol of the dichlorprop content. Free acidity: Max 30g/kg expressed as dichlorprop, of the extractable acid content. Suspended solids:Max 1g/kg Water content: Visible water shall be absent. 30 Dichlorprop Aqueous solution Free phenols: Max 15g/kg, expressed as 2,4-dichlorophenol of the Potassium salt dichlorprop content. Water insolubles: The product shall pass through a 250um test sieve, and not more than 1Q/kQ shall remain on a 1 SOum test sieve Dichlorprop Tech Potassium salt Free phenols: Max 1 Sg/kg, expressed as 2,4-dichlorophenol of the dichlorprop content. Water: 1 Sg/kg Water insolubles: An aqueous solution of the material shall pass completely through a 250um test sieve, not more than 1g/kg shall remain on a 1 SOum test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 31 Dichlorprop+MCPA EC Free phenols: Max (1.5X+1Y)% expressed as 2,4-dichlorophenol where X Mixed Ester and Y are the dichlorprop and MCPA contents. Material insoluble in oil: The product shall give a reasonably clear, homogeneous solution which shall leave not more than 1g/l of residue on a 1 SOum test sieve, and the sieved solution shall contain not more than a trace of sediment. Water:Max Sg/ka Herbicides # Chemical Type Impurities 32 Oichlorprop+MCPA Aqueous Solution Free phenols: Max (1.5X+1Y)% expressed as 2,4-dichlorophenol where X Salt and Y are the dichlorprop and MCPA contents. Water insolubles: The product shall pass through a 250um test sieve, and not more than 1 Q/kQ shall remain on a 1 S0um test sieve. C ;chiorprop+Mecoprop Aqueous Solution Free phenols: Max 1.5% expressed as 2,4-dichlorophenol of the total Salt dichlorprop and mecoprop contents. Water insolubles: The product shall pass through a 250um test sieve, and not more than 1 a/ka shall remain on a 1 S0urn test sieve. 33 Diflufenican Tech Water: Max 1 OOg/kg 34 Diquat-dibromide Aqueous Solution Free 2,2'-Bipyridyl: Max 0.25% of the diquat content Diquat-dibromide Tech Cone. Ethylene dibromide: Max 1 0mg/kg Free 2 2'-Biovridvl: Max 0.2% bv weiaht of the diauat dibromide content 35 Diquat-Paraquat Aqueous Solution Free 2,2'-Bipyridyl: Max 0.25% of the diquat content Free 4,4'-Bipvridvl: Max 0.25% of the paraquat content 36 Diuron Disp. Powders Free amine salts:Max 0.4%of the diuron content, calculated as dimethylamine hydrochloride Water: Max 2.5% Diuron Tech Free amine salts:Max 0.4%calculated as dimethylamine hydrochloride Water: Max 1% Diuron Water Disp. Granules Free amine salts:Max 0.4%of the diuron content, calculated as dimethylamine hydrochloride Water: 15 o/ka 37 Fenoprop Tech Free phenols: Max 1 Sg/kg expressed as 2,4,5-Trichlorophenol of the Fenoprop content. Sulphated ash: Max 10g/kg Triethylanolamine insolubles: A triethanolamine solution of the material shall leave not more than 1 g/kg residue on a 1 0Sum test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 2,3, 7 ,8-Tetrachlorodibenzo-p~dioxin: Max0.01 ug/g of the Fenoprop content. Herbicides # Chemical Type Impurities 38 Fenoprop-Salt Aqueous Solution Free phenols: Max 1 Sg/kg expressed as 2.4,5-Trichlorophenol of the Fenoprop content. Water insolubles: The product shall pass through a 250um test sieve, and not more than 1 g/kg shall remain on a 150um test sieve. 2,3, 7 ,8-Tetrachlorodibenzo-p-dioxin:Max0.01 ug/g of the Fenoprop conlent. Fenoprop-Salt Tech Free phenols: Max 15g/kg expressed as 2,4,5-Trichlorophenol of the Fenoprop content. Water:Max 15g/kg Water insolubles: An aqueous solution of the material shall pass completely tl1rough a 250um test sieve, not more than 1 g/kg shall remain on a 150um test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 2,3, 7 ,8-Tetrachlorodibenzo-p-dioxin:Max0.0 1 ug/g of the Feno prop content declared. 39 renoprop+Mecoprop Aqueous Solution Free phenols: Max 1.5% expressed as 2,4,5-Trichlorophenol of the total Salt Fenoprop and Mecoprop contents. Water insolubles: The product shall pass through a 250um test sieve, and not more than 1 g/kg shall remain on a 150um test sieve. 2,3, 7,8-Tetrach!orodibenzo-p-dioxin:Max0.01 ug/g of the Fenoprop content. 40 Fluchloralin EC Water: Max 2Q/kg Fluchloralin Tech Water: Max Sg/kg 41 Glyphosate Soluble Concentrate Insolubles in Water: 100 mg/kg 1,4-Dioxane: 1 ma/ka Glyphosate Tech Insolubles in 1 M NaOH: 0.2 g/kg N-methvl alvohosate: 28 a/k.a Herbicides # Chemical Type Impurities 42 Hexazinone Granules Carbamic acid ethyl ester: Max 0.005% of hexazinone declared Water: Max 20Q/kq Hexazinone SC Carbamic acid ethyl ester: Max 0.005% of hexazinone declared Hexazinone Tech Carbamic acid ethyl ester: Max S0mg/kg Water: Max 1 0q/kq Hexazinone Water Disp.Gran Carbamic acid ethyl ester: Max 0.005% of hexazinone declared Water: Max 1 0o/kg Hexazinone Water Soluble Powders Carbamic acid ethyl ester: Max 0.005% of hexazinone declared Water: Max 1 Oo/ko 43 loxynil Tech Dry material: Max 1 Sg/kg Wet Material; The water content shall be declared (Max 1 00g/kg). Sulfated ash: Max Sq/ka 44 loxynil octanoate EC Water: Max 2g/! loxynil octanoate Tech Free acidity: Max 10 ml in iN sulfuric acid% (equivalent to 37.ig/kg expressed as ioxynil, RMM=370.9) Water: Max 1 g/kg Sulfated ash: Max Sg/kg Material insoluble in xvlene: Max 1a/ka 45 lsoproturon Tech Loss on drying: Max 2g/kg Jsoproturon isomers: Ortho isomer= N, N-dimethyl-N'-[2-(1-methylethyl)phenyl]urea: Max 1 0g/kg Meta isomer= N,N-dimethyl-N'-[3-(1-methylethyl)phenyl]urea:Max 20g/kg Svmetrical Urea: N N'Bis-f3-(i-methylethvl)ohenvllurea: Max 10a/ka lsoproturon WP Water: Max 25g/kg 46 Unuron Disp. Powders Free amine salts:Max 0.4% of the Linuron content, calculated as dimethylamine hydrochloride. Water: Max 2.5% Linuron Tech Free amine salts:Max 0.4% calculated as dimethylamine hydrochloride Water: Max 1 % Linuron Water Disp. Granules Free amine salts: Max 0.4% of the linuron content calculated as d1methylamine hydrochloride Water: Max 15 r.i/ko Herbicides # Chemical Type Impurities 47 MCPA Tech Water: Max 1 Sg/kg Free phenols: Max 1 Og/kg, expressed as 4-chloro-2 methyl-phenol of the MCPA content. Sulphated ash: Max 1 Og/kg Triethanolamine insolubles: A triethanolamine solution of the material shall leave not more than 1 g/kg residue on a 1 OS um test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 48 MCPA Esters EC Free phenols: Max 1 Og/kg, calculated as 4-chloro-2 methyl-phenol of the MCPA acid equivalent content. Oil insoluble material: The product shall give a clear, or opalescent, homogen eous solution which shall leave not more than 1g/kg residue on a 1 SOum test sieve, and the sieved solution shall contain not more than a trace of sediment. Water: Max 5q/kq MCPA Esters Tech Free phenols: Max 10g/kg, calculated as 4-chloro-2 methyl-phenol of the MCPA content. Free acidity: Max 30g/kg expressed as MCPA calculated from the total ester sample. Suspended solids: Max 1g/kg Water: Max 1 Oo/kq 49. MCPA Salt Aqueous Solution Free phenols: Max 10g/kg, expressed as 4-chloro-2 methyl-phenol of the MCPA acid equivalent content. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 q/kQ shall remain on a 1 SOum test sieve. MCPA Salt Tech Free phenols: Max 1 Og/kg, expressed as 4-chloro-2 methyl-phenol of the MCPA content. Water: Max 15g/kg Water: insolubles: An aqueous solution of lhe material shall pass completely through a 250um test sieve, not more than 1 g/kg shall remain on a 150um test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. Herbicides # Chemical Type Impurities MCPA Salt WP Free phenols: Max 1 Og/kg, calculated as 4-chloro-2 methyl-phenol of the MCPA content. Water insolubles:When the product is dissolved in CIPAC standard water C,any insoluble material shall pass completely through a 250um test sieve, not more than 1g/kg shall remain on a 150um test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 50 MCPA+MCPB salt Aqueous solution Free phenols: Max (1 OX+30Y)g/kg, expressed as 4-chloro 2-methyl phenol, where X and Y are the MCPA and MCPB contents. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 a/ka shall remain on a 150 um test sieve. 51 MCPB Tech Free phenols: Max 30g/kg, expressed as 4-chloro 2-methylphenol of the MCPB content. Sulphated ash: Max 10g/kg Triethanolamine insolubles: A triethanolamine solution of the material shall leave not more than 1 g/kg residue on a 105um test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 52 MCPB Potassium salt Aqueous solution Free phenols: Max 30g/kg, expressed as 4-chloro 2-methylphenol of the MCPB content. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 Q/kg shall remain on a 150 um test sieve. MCPB Potassium salt Tech Free phenols: Max 30g/kg, expressed as 4-chloro 2-methylphenol of the MCPB content. Water: Max 15g/kg Water insolubles: An aqueous solution of the material shall pass completely through a 250um test sieve, not more than 1g/kg shall remain on a 150um test sieve, and the sieved solution shall be clear or coalescent and shall contain not more than a trace of sediment. Herbicides # Chemical Type Impurities 53 Mecoprop Tech Free phenols: Max 15g/kg, expressed as 4-chloro 2-methylphenol of the Mecoprop content. Sulphated ash: Max 1 Og/kg Triethanolamine insolubles: A triethanolamine solution of the material shall leave not more than 1 g/kg residue on a 1 OSum test sieve and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 54 Mecoprop Metal salt Aqueous solution Free phenols: Max 15g/kg, expressed as 4-chloro 2-methylphenol of the Mecoprop content. Water insolubles: The product shall pass through a 250um test sieve and not more than 1 g/kg shall remain on a 150um test sieve. Mecoprop Metal salt Tech Free phenols: Max 1 Sg/kg, expressed as 4-chloro 2-methylphenol of the Mecoprop content. Water: Max 15g/kg Water insolubles: An aqueous solution of the material shall pass completely through a 250um test sieve, not more than 1 g/kg shall remain on a 1 SOum test sieve, and the sieved solution shall be clear or opalescent and shall contain not more than a trace of sediment. 55 Metamitron Tech Water: 5 g/kg Metamitron Tech Concentrate Water: 15g/kg Material insoluble in acetone: Max 150 g/kg Metamitron Water Disp. Granules Water:20g/kg 56 Metolachlor EC 6-ethyl-o-toluidine: Max 0. 1 % of the metolachlor content Metolachlor Granules 6-ethyl-o-toluidine: Max 0.1 % of the metolachlor content Metolachlor Tech 6-ethyl-o-toluidine: Max 1 g/kg 6-ethyl-N-(2 methoxy-1-methylethyl)-o-toluidine: Max 1g/kg 2-Chloro-6'-ethvlacet-o-toluidine: Max 15q/kq 57 Metribuzin Tech Water: 1 Og/kg Material insoluble in acetone: Max 1 O a/ka Metribuzin Tech Concentrate Water: 15g/kg Material insoluble in acetone: Max 150 g/kg Metribuzln Water Disp. Granules Water:20g/kg Metribuzin WP Water:25g/kg Herbicides # Chemical Type Impurities 58 M~tsulfuron Methyl Tech Water: Max 3g/kg Material insoluble in acetone: Max 10o/kq Metsulfuron Methyl Water Disp.Gran Water: Max 15g/kg 59 Monuron Disp. Powders Free amine salts: Max 0.4% of the Monuron content calculated as dimethylamine hydrochloride Water:. Max 1 % Monuron Tech Free amine salts: Max 0.4% calculated as dimethylamine hydrochloride Water: Max 1 % 60 Paraquat-salt Aqueous solution Free 4,4'-Bipyridyl: Max 0.25% of the .Paraquat content Pa raq uat-sa It Tech Cone. Free 4,4'-Bipyridyl: Max 0.2% by weight of the paraquat dichloride content 61 Prometryn Tech NaCl: 2% 62 Propachlor Tech . Acetone insolubles: Max 0.5 g/kg Water: Max 3 g/kg 2-Chloroacetanilide: Max 18 g/kg N,N~di-isopropylaniline: Max 20 g/kg 2 2-dichloro-N-isooroovlacetanilide: Max 12 o/ka 63 Propanil EC Acidity or Alkalinity: Max Acidity:0.1 % calculated as H2SO4 'Max Alkalinity: 0.3% calculated as NaOH Water: Max 1 % Propanil Tech Acidity: Max 0.3% calculated as H2SO4 Water: Max 0.3% 64 Propazine Tech NaCl: 2% 65 Propham Tech Non volatile impurities: Max 0.5% Loss on Vaccum drying at 20C: Max 2% Aniline: Max 1 % Herbicides # Chemical Type Impurities 66 Sodium Chlorate Aqueous Solution Water insoluble material: All the product shall pass through a 250um test sieve and not less than 99.9% shall pass throuQh a 150 um test sieve. Sodium Chlorate Tech Total material insoluble in water: Max 0.5%, Coarse material insoluble in water: Max 0.05% Sodium Chlorate Water Soluble Powders Total material insoluble in water: Max 0.5% Coarse material insoluble in water: Max 0.05% Sodium Chlorate Water SolublePowders containing 25% Organic material: Max 0.5% Sodium chloride Coarse material insoluble in water: Max 0.05% 67 Sulfometuron methyl Tech Water: Max 3g/kg Insolubles in n-rnethylpvrrolidone: Max 1 Og/kg Sulfometuron methyl Water Disp.Gran Water: Max 15g/kg 68 Terbutryn Tech NaCl: 2% 69 Trifluralin EC N-nitroso-di-n-propylamine: Max 1xX mg/kg, where Xis the trifluralin content Water: Max 2.Sg/kg Trifluralin Tech N-nitroso-di-n-propylamine: Max 1 mg/kg * Method available from the plant protection officer, FAO Plant Production and Protection division. · Insecticides # Chemical Type Impurities 1 Acephate Tech Methamidophos: Max Sg/kg O,O,S-trimethyl phosphorothioate: Max 1g/kg Acetamide: Max 1g/kg Water: Max 2g/kg Acephate Water soluble Powders 11V1et11am1t1opnos: l\7Tax u.ti"/o or me acepnate comem O,O,S-trimethyl phosphorothioate: Max 0.1 % of the acephate content Ace1amide: Max 0.1 % of the acephate content Water: Max 20g/kg Material insoluble in water: Max 220 g/kg 2 Aluminium phosphide Pellets or Tablets Arsenic: Max 0.04g/kg corresponding to Max 0.1g As/kg in phosphorus used for production of metal phosphide. Aluminium phosphide Powder Arsenic: Max 0.04g/kg corresponding to Max u.1g AS/kg m pnosphorus used for production of metal phosphide. 3 Bioresmethrin+ EC Water: Max Sg/kg Piperonvl butoxide Bioresmethrin+ Solutions Water: Max Sg/kg Piperonyl butoxide 4 Bromophos Disp. Powders Acidity or Alkalinity: Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Bromophos Dusts Acidity or Alkalinity: Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Bromophos EC Acidity or Alkalinity: Max Acidity: 0 .3% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Bromophos Solutions Acidity or Alkalinity: 'Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.5% Bromophos Tech Acidity: Max 0.3% calculated as H2SO4 Water: Max 0.2% Material insoluble in Acetone: Max 0.2% lnsecticides # Chemical Type Impurities 5 Camphechlor EC Acidity: Max 0.15% calculated as HCI Water: Max 0 .15% Camphechlor Tech Acidity: Max 0.1% calculated as HCl Camphechlor Tech Solutions Water: Max 0.5% 6 Carbary! DP 2-Naphthol: 0.05% of carbaryl content 2-Naphthyl methylcarbamate: 0.05% of carbaryl content Carbary! Tech 2-Naphthol: 0.5g/kg of carbaryl content 2-Naphthyl methylcarbamate: 0.5g/kg of carbaryl content Loss of vaccum on drying: 1 0g/l<g Carbary! WP 2-Naphthol: o.u:,% of carbaryI content 2-Naphthyl methylcarbamate: 0.05% of carbaryl content 7 Carbosulfan EC Carbofuran: 2% Water: 2g/kg Carbosulfan Gran Carbofuran: 2% Carbosulfan Tech Carbofuran: 20g/kg Water; 2o/kg Carbosulfan UltraLow Volume Uq Carbofuran: 2% Water: 2g/kg 8 Chlorovriohos EC Water: Max 2g/kg Chlorpyriphos Tech water: Max 1 g/kg Acetone insolubles: Max Sg/kg 9 Cyflulhrin EC Water: Max 3g/kg Cyfluthrin Tech Water: Max 'lg/kg Cvfluthrin UltraLow Volume Lio Water: Max 2g/kg Cyfluthrin WP Water: Max 35g/kg 10 Cypermethrin EC Water: 2g/kg Cvoermethrin Tech Water: 1g/kg Cvoermethrin Tech Cone Water: 1 g/kg Cypermethrin Ullralow Volume Liq water: 2g/k.g 11 D-trans Allethrin+ EC Water: Max 0.5% Piperonvl butoxide D-trans Allethrin+ Solutions Water: Max 0.5% Piperonyl butoxide Insecticides # Chemical Type Impurities 12 Deltamethrin DP Deltamethrin R isomer: Max 2% of the deltamethrin content Deltamethrin EC Deltamethrin R isomer: Max 1 % of the deltamethrin content Water: Max 5g/kg Deltamethrin Tech Deltamethrin R isomer: Max 10g/kg Acid chloride corresponding to deltamethrin:Max 2g/kg Acid anhvdride corresoonding to deltamethrin:Max 1 Og/kg Deltamethrin Ultralow Volume Liq Deltamethrin R isomer: Max 1 % of the de1tamethrin content Water: Max Sg/kg Deltamethrin WP D eltamethrin R isomer: Max 2% of the deltamethrin content 13 Fenitrothion DP S-methyl fentrothion: 2.5% of the fenitrothion content Fenitrothion EC S-ethyl fentrothion: 2% of the fenitrothion content Water: 2g/kg Fenitrothion Solutions S-ethyl fentrothion: 2% of the fenitrothion content Water: 2g/kg Fenitrothion Tech S-ethyl fentrothion: 20g/kg Water: 1g/kg Fenitrothion Ullralow Volume Liq S-ethyl fentrothion: 2% of the fenitrothion content Water: 2g/kg Fenitrothion WP S-methyl fentrothion: 2.5% of the fenitrothion content 14 Fenthion Disp. Powders Acidity: Max 0.3% as H2S04 Alkalinitv: Max 0.2% as NaOH Fenthion Dust Acidity: Max 0.1% as H2S04 Alkalinitv: Max 0.2% as NaOH Fenthion EC Water: Max 2g/kg Fenthion Solutions Water: Max 1.5 g/kg Fenthion Tech water: Max 2g/kg Material insoluble in acetone: Max Sg/kg 15 Fioronil Tech Water: For the wet m·aterial 60-90 g/kg Fipronil Ultra Low Volume liq Water: Max: 2g/l 16 lsofenphos EC Water: 5g/kg lsofenohos Tech Water: 2g/kg Insecticides # Chemical Type Impurities 17 Lindane Aqueous Suso. cone. Alpha-SCH: Max 0.5% of the gamma-HCH content Lindane DP Alpha-HCH: Max 0.5% of the gamma-HCH content Lindane EC Alpha-HCH: Max 0.5% of the gamma-HCH content Water: Max 1 .5g/kg Lindane Soiutions Alpha-HCH: Max 0.5% of the gamma-HCH content Water: Max 0.Sg/kg Lindane Solutions for seed trt. Water: Max 0.5% Lindane Tech Alpha-HCH: Max 0.5% of the gamma-HCH content Material insoluble in acetone: Max 1g/kg Loss on vaccum drying: Max 1g/kg Lindane WP Alpha-HCH: Max 0.5% of the gamma-HCH content 18 Magnesium Phosphide Pellets or Tablets Arsenic: Max 0.04g/kg corresponding to Max 0.1g As/kg in phosphorus used for production of metal phosphide. Magnesium J='.hosphide Powder Arsenic: Max o.04g/KQ corresponding to Max 0.1g As/Kg m phosphorus used for production of metal phosphide. 19 Methiocarb G Water: 150g/kg Methiocarb Tech Water: 2g/kg Methiocarb Tech Cone Water: 20g/kg Material insoluble in acetone: 180g/kg Methiocarb WP Water: 25g/kg 20 Methoprotryn Tech NaCl: 2% · 21 Methoxychlor Disp. Powders Acidity or Alkalinity: Max Acidity: 0.2% calculated as H2SO4 Max Alkalinitv: 0.2% calculated as NaOH M ethoxych lo r EC Acidity. or Alkalinity: Max Acidity: 0.05% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.2% Methoxychlor Tech Material insoluble iil acetone: Max 1 % Acidity: Max 0.3% calculated as H2SO4 Chloral hydrate: Max 0.025% Loss on Vaccum drvina: Max 1 % Insecticides # Chemical Type Impurities 22 Oxydemeton-methyl EC Acidity:Max 1.4% of the oxydemeton-methyl content.calculated as H2SO4 Water: Max 0.6% Oxydemeton-methyl Tech Solutions Ac1c11ty or AJKallntty: Max Acidity: 0.7% calculated as H2SO4 'Max Alkalinity: 0.01 % calculated as NaOH Acetone insolubles: Max 0.3% Water: Max 0.8% 23 Parathion-methyl DP $-methyl parathion: Max 2% of parathion-methyl content Parathion: Max 0.25% of parathion-methyl content Parathion-methyl EC S-methyl parathion: Max 1.3% of parathion-methyl content Parathion: Max 0.25% of parathion-methyl content Water: Max 3g/kg Parathion-methyl Solutions S-methyl parathion: Max 1.3% of parathion-methyl content Parathion: Max 0.25% of parathion-methyl content Water: Max 3g/ka Parathion-methyl Tech S-methyl parathion: Max 1.3% of the parathion-methyl content Parathion: Max 2.5g/kg Acetone insolubles: Max 5g/kg Water: Max 3g/kg Parathion-methyl Tech Cone Solution S-methyl parathion: Max 1 .3% of the parathion-methyl content Parathion: Max 2.5g/kg Water: Max 3g/k.g Acetone insoluble: Max 5g/kg Parathion-methyl WP s-metnyT parathion: Max 1.5% of parath1on-methy1 content Parathion: Max 0.25% of parathion-methyl content 24 Permethrin EC Water: 3g/kg Permethrln Tech Water: 1 g/kg 25 Propoxur DP Water: Max 20g/kg Propoxur EC Water: Max Sg/kg Propoxur Tech Water: Max 2g/kg Material insolubles in acetone: Max 1g/kg Propoxur WP Water: Max 20g/kg 26 Pyrethrum Extract Dusts Water: Max 1 % Pyrethrum Extract Tech(Extract) Water: l\ilax 0.5% Material insoluble in Dichlarodifluoromethane: Max 1.5% Insecticides # Chemical Type Impurities 27 Thiodicarb AqueousSusp.con~ Manufacturing impurities: Methomyl: Max 0.5% of the thiodicarb content Thiodicarb Tech Manufacturing impurities: Methomyl: Max 5g/kg 1 hiodicarb Water Dip. Gran Manufacturing impurities: Methomyl: Max 0.5% of the thiodicarb content Water: Max 15g/kg Thiodicarb WP IManuractunng 1mpunt1es: Methomyl: Max 0.5'% of the thiodicarb conten! Water: Max 20g/kg 28 Trichlorfon Soluble Cone. Water: Max 7g/kg Trichlorfon Tech Water: Max 3g/kg Acetone insolubles: Max Sg/kg Trichlorfon Water Soluble Powders Water: Max 1 Sg/kg Water insolubles: The content of solid matter insoluble in water shall be declared (g/kg) and when determined, the content obtained shall not differ from that declared by more than +/- 15% Trichlorfon WP Water: Max 1 0g/kg # Chemical Type Impurities 1 Dicofol EC DDT & DDT related impurities:Max 0.1 % of active isomers. Water: Max 5 g/kg Dicofol Tech DDT & DDT related impurities: Max 1 g/kg of active isomers. Water: Max 0.5 g/kg Dicofoi WP DDT & DDT related impurities:Max 0.1 % of active isomers. 2 F-enbutatin oxide Tech Bis[hydroxy bis(2-methyl-2-phenylpropyl)tin}oxide: Max 20g/kg 3 Propargite Tech Acetone mso!ul:)les: Max 1g11<g Water: Max 2g/kg lnsecti-Accaricides # Chemical Type Impurities 1 Azinphos-ethvl EC Water-: 2g/kg Azinphos-ethyl Tech Acetone insolubles: 5 g/Kg \Nater: 2g/kg 2 Azinphos-m ethyl EC Water: 2g/kg Azinphos-methyl 1 ech Acetone msolubles: o 911<9 Water: 2g/kg 3 Chlorienvinphos Disp. Powders Acidity or Alkalinity: Max Acidity: 0.5% calculated as H2SO4 Max Alkalinity: 0.5% calculated as NaOH Chlorfenvinphos EC Acidity or Alkalinity: Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.5% Chlorfenvinphos Tech Acidity: Max 0.5%, calculated as H 2 SO 4 Water: Max 0.3% 4 Demeton EC Acidity or Alkalinity: Max Acidity: 0.4% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.3% Demeton Tech Ac1d1ty or Alkalinity: Max Acidity: 0.8% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.2% 5 Derneto n-S-Methyl EC Acidity or Alkalinity: Max Acidity: 0.35% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.2% Demeton-S-Methyl Tech Acidity or Alkalinity: Max Acidity: 0.35% calculated as H2SO4 Max Alkalinity: 0.05% calculated as NaOH Water: Max 0.25% I nsecti-Accaricides # Chemical Type Impurities 6 Diazinon EC O,S-TEPP: Max 0.22 x xmg/kg, where xis the diazinon content S,S-TEPP: Max 2.8 x xmg/kg, where x is the diazinon content Water: Max 2g/kg Diazinon Solution O,S-TEPP: Max 0.22 x xmg/kg, where xis the diazinon content S,S-TEPP: Max 2.8 x xmg/kg, where xis the diazinon content Water: Max 2g/kg Diazinon Tech U,5-1 E::PP: Max U,;.::'.Q/KQ S,S-TEPP: Max 2.Sg/kg Water: Max 0.69/kg Acetone insolubles: Max 1 .Sg/kg 7 Dichlorvos EC Water: Max 1g/kg Dichlorvos SC Water: Max 0.8g/kg Dichlorvos Tech -Chloral: Max 591kg Water: Max 0.Sg/kg 8 Dimethoate DP Water: Max 2g/kg Dimethoate EC Water: Max 2g/kg Dimethoate Soluble Cone. Water: Max 2g/kg Dimethoate Tech Omethoate: Max Sg/kg Mineral acidity: Max 1 0g/kg calculated as H2SO4 Acetone insoluble: Max Sg/kg Water: Max 2g/kg Dimethoate WP Water: Max 2g/kg 9 Disulfoton Tech water: Max 3g/kg Xylene insolubles: Max 1 g/kg I nsecti-Acca ricides # Chemical Type Impurities 10 Endosulfan DP Water: Max 20g/ko Endosulfan EC Water: Max 0.Sg/kg Endosulfan Solutions Water: Max Sg/kg Endosulfan Tech Endosulfan ether: 1091Kg Endosulfan alcohol: 20g/kg Endosulfan sulfate: 2g/kg Loss on drying: 1 0g/kg Material insoluble in acetone: 1 Og/kg Endosulfan WP Water: Max 20g/kg 11 Ethion EC Acidity:Max 3g/kg as H 2 SO4 Water: Max 2g/kg Ethion Tech Acidity: Max 3g/kg as H2SO4 Acetone insolubles: Max Sg/kg Water: Max 2□/ka 12 Fenvalerate EC Water: Max 2g/kg Fenvalerate Tech Water: Max 2g/kg 13 Malathion EC Iron: Max 1.5% of the malathion content Water: Max 2g/kg Malathion Solution Iron: Max 1.5% of the malathion content Water: Max 2a/kg Malathion Tech Iron: Max 10mg/kg Water: Max 1 g/kg Acetone insoluble: Max Sg/kQ Malathion WP lsomalathion: Max 1.8% of the malathion content 14 Mecarbam EC 1:c1:hyl-N-me1:nyl-1\l-~n1oroace1:y1caroama1:e:1v1ax L. • .e::-✓oOT the mecarbam content Ethyl-N-methyl Carbamate: Max 2% of the mecarbam content 3-methyl oxazolid-2,4-dione:Max 1 .1 % of the mecarbam content O,O,S-Triethylphosphorothiolothionate:Max 1.3% of the mecarbam content O,O,O-Triethylphosphorothionate:Max 1.1 % of the mecarbam content Water: Max 2.Sg/kg lnsecti-Accaricides # Chemical Type Impurities Mecarbam Tech c-.:ny1-N-me1:ny1-N-'--n1oroacety1caroamate: Max ..:::-ro or rne mecarbam content Ethyl-N-methyl Carbamate: Max 2% of the mecarbam content 3-methyl oxazoJid-2,4-dione:Max 1% of the mecarbam content. O,O,S-Triethylphosphorothiolothionate:Max 1.2% of the mecarbam content 0,0,0-Triethylphosphorothionate:Max 1% of the mecarbarn content Water: Max 1 .2g/kg Mecarbam WP t:.II 1y1-l\l-r, '"" ll I y1-1'1.1-vl II u, .............. ~y lt..d1 IJdl lldL~.IVld.><. L..L. 7o0i the mecarbam content Ethyl-N-methyl Carbamate: Max 2% of the mecarbam content. 3-methyl oxazolid-2,4-dione:Max 1.1 % of the mecarbam content. 0,0,S-Triethylphosphorothiolothionate:Max 1.3% of the mecarbam content 0,0;0-Triethylphosphorothionate:Max 1.1 % of the mecarbam content Water: Max 1 % 15 Mcthamidophos Solution Water: Max 5g/kg Manufacturing impurities: Jn case of doubt, check according to provisional specification 355/TK/F/P (1992) for methamido□hos technical concentrates. Methamidophos Tech O,o-dimethyl phosphoramidothioate: Max 90g/kg N'-methyl homologues: Max 80g/kg O,o,o-trimethyl phosphorothioate: Max 70g/kg O,o,S-trimethyl phosphorothioate: Max 20g/kg Water: Max 1 a/ka I nsecti-Accaricides # Chemical Type Impurities \llethamidophos Tech Cone O,o-dimethyl phosphoramidothioate: Max 13% of the methamidophos content N-methyl homologues: Max 12% of the methamidophos content O,o,o-trimethyl phosphorothioate: Max 10% or the methamidophos content O,o,S-trimethyl phosphorothioate: Max 3% of the methamidophos content Water- 1\/1<0.v ?n/kn 16 Methiocarb Gran Water: Max 1 S0o/kg Methiocarb Tech Water: Max 2g/kg Methiocarb Tech Cone. Water: Max 20g/kg Material insoluble in acetone: Max 180q/kg Methiocarb WP Water: Max 25g/kg 17 Methomyl Soluble Cone. Water: Max 3g/kg Material insoluble in water: The maximum water insoluble inerts should be declared Methomyl Tech Water: Max 3g/kg Material insoluble in water: Max 2g/kg Methomyl Water Soluble Powder vvater: ax 3g/Kg Material insoluble in water: The maximum water insoluble inerts should be declared 18 Mevinphos EC Water: Max o .2% Mevinphos Tech Water insolubles: Max 0.1 % Xylene insolubles: Max 0.1% Particle matter: On visual inspection, no particle matter shall be oresent. 19 Monocrotophos Soluble Cone. Trimethyl phosphate: Max 0.036xXg/kg where X is the rnonocrotophos content (g/kg). Water: Max 2.5g/kg Monocrotophos Tech l nmethyl phosphate: Max LUQ/Kg Water: Max 2g/kg Water insolubles: Max 0.5 g/kg Acetone insoluble: Max 1g/ko I nsecti-Accari cid es # Chemical Type Impurities Monocrotophos UltraLow Volume Liq Trimethyl phosphate: Max 0.036xXg/kg where Xis the monocrotophos content (g/kg). Water: Max 2.5g/kg 20 Naled EC Water: Max 2g/kg Naled Tech Ac1an:y or All-ca11n1ty: Max Acidity: 1 0g/kg calculated as H2SO4 Max Alkalinity: 2g/kg calculated as NaOH Acetone insolubles: Max Sg/kg Water: Max 2g/kg 21 Petrolium Oil Summer Use(Emulsion Phenols: Max 0.2% w/w Products Petrolium Oil Summer Use(Miscible) Acidity: Not more than 1 00ug of KOH shall be required to Products neutralize 1 g of the oroduct. Petrolium Oil Winter Use on Acidity: Not more than 1 00ug of KOH shall be required to Products Dormant Pits (Miscible) neutralize 1 g of the oroduct. Petrolium Oil Winter Use on Phenols: Max 0.2o/o w/w Products Dormant Pits (Emulsion) 22 Phenthoate Disp. Powders Acidity or Alkalinity: Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.1 %, calculated as Na OH Phenthoate EC Acidity or Alkalinity: Max Acidity: 0.2% calculated as H2SO4 Max Alkalinity: o. 1 % calculated as Na OH Water: Max 0.5% Phenthoate Tech t-'--'U pnenL11oa1:e: 1v1ax u ...,-,o Acidity: Max 0.3% calculated as H2SO4 Water: Max 0.5% Material insoluble in Acetone: Max 0.5% 23 Phosalone EC Water: Max Sg/kg Phosalone I Tech Water and volatile impurities: Max 10g/kg 24 Plrimiphos-methyl EC Water: Max 5g/kg Plrimiphos-methyl Tech Water: Max 2g/kg lnsecti-Accaricides # Chemical Type Impurities 25 Profenofos Tech 4-Bromo-2-chlorophenol: Max 1 % Water: Max 0.2% 26 Thiometon EC Acidity or Alkalinity: Max Acidity: 0.5% calculated as H2SO4 Max Alkalinity: 0.1 % calculated as NaOH Water: Max 0.3% Thiometon EC Acidity or Alkalinity: Max Acidity: 0.3% calculated as H2SO4 Max Alkalinity: 0.1 % calculated as NaOH Water: Max 0.3% Thiometon Tech Acidity or Alkalinity: Max Acidity: 0.5% calculated as H2SO4 Max Alkalinity: 0.1 % calculated as Na OH Material Insoluble in Acetone: Max 0.5% Water: Max 0.3% Thiometon Tech Solutions Material lnsoluNe m Acetone: Max u.::no Insoluble Material in the product: Max 0.5% Mercaptans: Max 0.1% Water: Max 0.3% Acidity or Alkalinity: Max Acidity: 0.5% calculated as H2SO4 Max Alkalinity: 0.1 % calculated as NaOH Thiometon Tech Solutions 1v1atena1 mso1uo1e m ACel:one: 1v1ax u . .:no Water: Max 0.3% Acidity or Alkalinity: Max Acidity: 0.5% calculated as H2SO4 Max Alkalinity: 0.1 % calculated as Na OH lnsecti-Fungicide # Chemical Type Impurities 1 Copper Ammonium carbonate Aqueous Solution Arsenic:Max 0.1 X mg/kg (X=Cu content g/kg) Lead: Max 0.5X mg/kg (X=Cu content g/kg) Cadmium: Max 0.1X mg/kg (X=Cu content g/kg) Material insoluble in water: Max 3g/l 2 Copper Hydroxide SC Arsenic: Max 0.1xX where X is the copper content in g/kg Lead: Max 0.5xX where X is the copper content in g/kg Cadmium: Max 0.1 xX where X is the conner content in a/ka Copper Hydroxide Tech Arsenic: Max 0.1xX where Xis the copper contenting/kg Lead: Max 0.SxX where X is the copper content in g/kg Cadmium: Max 0.1xX where Xis the copper contenting/kg Copper Hydroxide Water Disp.Gra Arsenic: Max 0.1xX where Xis the copper content in g/kg Lead: Max 0.5xX where Xis the copper contenting/kg Cadmium: Max 0.1xX where Xis the copper contenting/kg Copper Hydroxide WP Arsenic: Max 0.1 xX where X is the copper content in g/kg Lead: Max o.SxX where Xis the copper content in g/kg Cadmium: Max O.1xX where Xis the copper contenting/kg # Chemical Type Impurities 1 DNOC Tech Mineral Acidity: Max 0.5% of the dry weight expressed as H 2S04 Water: The average percentage of water in the batch supplied shall be declared. Solubility of Ammonium, Diethanolamine and Sodium salts: When the ammonium, diethanolamine and sodium salts of DNOC are prepared, the resulting solutions in CIPAC. Standard water content shall be clear with not more than 0.1 % of alkali insoluble material. Plant Growth Regulator # Chemical Type Impurities 1 Ethephon Tech Manufacturing impurities: MEPHA mono 2-chloroethyl ester, 2-chloroethyl phosphonic acid: Max 20g/kg 1,2-dichloroethane: Max 0.5g/kg Ethephon Tech Cone Manufacturing impurities: MEPHA: mono 2-chloroethyl ester, 2-chloroethyl phosphonic acid: Max 2% of the ethephon content 1,2-dichloroethane: Max 0.05% of the ethephon content Material insoluble in water: The product shall pass through a 250um test sieve and not more than 1a/ka shall remain on a 150um test sieve. Ethephon Solubl Cone Manufacturing impurities: MEPHA: mono 2-chloroethyl ester, 2-chloroethyl phosphonic acid: Max 2% of the ethephon content 1 2-dichloroethane: Max 0.05% of the etheohon content # Chemical Type Impurities 1 Dinobuton Tech Free Dinoseb and its salts: Max 5g/kg of free phenol from the salts Loss on drying: Max Sg/kg Potassium Chloride: Max 20 g/kg Water: Max 1 o g/kg Dinobuton WP Free Dinoseb and its salts: Max 1 Oo/ko Dinobuton EC Free Dinoseb and its salts: Max 0.5% of the dinobuton content Water: Max Sa/ka f~.JJ.:iJ.o Annex 4 ~1.,jllc.,1J!f a...e1J ;/I §Jr/'"'.-' ...... EPA List 1: Inerts of Toxicological Concern No. Chemical Name l Aniline 2 Asbestos Fiber 3 1,4-Benzenediol 4 Cadmium compounds 5 Carbon tetrachloride 6 Chloroform 7 p-Dichlorobeozene 8 Di-(2-ethylhexyl)adipate 9 1,2-Dichloropropane 10 Di-etbylhexvlphthalate 11 Dimethylformamide 12 Dioxane 13 Epichlorohydrin 14 2-ethoxyetbanol 15 Ethanol ethoxyacetate 16 Ethylene dichloride 17 Ethylene ~lycol monomethyl ether 18 Ethyl acrylate 19 n-Hexane 20 Hydrazine 21 Isophorone 22 Lead Compounds 23 Malachiteereen 24 Methyl n-butyl ketone 25 Methyl chloride 26 Methylene chloride 27 NonyhJhenol 28 Perchloroetbylene 29 Phenol 30 o-Phenvlt>henol 31 Propylene oxide 32 Pyrethrins 33 RhodamiI~e B 34 Sodium dichromate 35 Toluene disocyanate 36 1,1,2-Trichloroethane 37 Tributyl tin oxide 38 Trichloroethylene 39 Tri-orthocresy lphos phate(TOCP) o~.J~ Annex 5 41:l~jlf cJljJ J....:1,))/1 &., • ..i, a., ,, ..... EPA List 2: Potentially Toxic Inerts/ High Priority for Testing No. Chemical Name 1 Butyl benzvl phthalate 2 Dibutvl pbthalate 3 Diethyl phthalate 4 Dimethyl pbthalate 5 Dicotyl phthalate 6 2-Chlorotoluene 7 Cresols 8 o-Cresol 9 p-Cresol 10 m-Cresol 11 Cyclohexanone 12 o-Dichlorobenzene 13 Diethylene e:lycol monobutyl ether 14 Diethylene glycol monoethyl ether 15 Diethylene e:lvcol monomethyl ether 16 Di1>ropylene glycol monomethyl ether. 17 2-ButOJl.'Y-1-ethanol 18 l-Butoxv-2-propanoJ 19 1-Butoxve thoxv-2-provanol 20 1-Methoxy-2-pronanol 21 Propylene elycol monobutyl ether 22 Tripropylene 2Jycol monomethyl ether 23 Mesityl oxide 24 Methyl isobutvl ketone 25 Methyl ethyl ketoxime 26 Monochlorobenzene 27 Nitromethane 28 Toluene 29 Tolyl triazole 30 1,2,3-Benzotriazole 31· ,. 2-·Benzvl-4-cl~~~rophenol 32 CWorocthane No. 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 Chemical Name p-Chloro-m-xylenol . Dichlorophene Ethyl benzene Merca pto benzothiazole Methyl bromide Chlorodifluoromethane Dichloromonofluoromethane 1, 1-Difluoroethane 1-Chloro-1,1-difluoroethane ~1Jj!1 o ,lj~ J...c!),.~I oj ;Jl a, ,-1.., ,, Isopropyl phenols Petroleum hydrocarbons Xylene p-Ni trophenol Butylene oxide Nit.roe thane Acetonitrile 1,1,1-Trichloroethane Triethanolamine Diethanolamine , Butyl methacrylate Methyl methacrylate Xylene ~range aromatic solvents 2,5-Dichloroaniline 3,4-DichJoroaniline 3 ,5-Dichloroaniline 2,4-Dichloroaniline 2,3-Dichloroaniline 2,6-Dichloroaniline Diphenyl ether Trichlorotrifluoroethane Dichlorodifluo rome thane Dichlorotetrafluoroethane 1 rtJJ ~ Annex6 :a,,.1 ,jll<>Jlj , a..:t; ;/1 &., ,;JI :l., y<M All agricultural companies having the License for import of pesticides in Lebanon) have to register their products according to the following needed information and their respective Annexes: 1. General Information • Name and address of manufacturer of active ingredient accompanied with a Certificate from the official authorities. • Name and address of pesticide fonnulator together with certificate of ISO 900 I :2000 scope formulation, dated not later than one year upon application. • Name and address of importer • Corrnnercial name as mentioned on certificates of use and registration in country of origin, this name should be different from the common name and from any other registered name :in Lebanon. Registration with another name is possible on condition that the trade name stated :in certificate of registration :from countly of orig:in will be written together with the new chosen name. i» Specify Use Category (Insecticide, Fungicide, Herbicide, Plant growth regulator, ... ) 1 -1. Status of application: A- Imported Pesticides I. The active ingredient (a.i) is imported for the first time for use in Lebanon 2. New Trade name for a pesticide for which the a.i is used in Lebanon B- Pesticides Locally Formulated l. The a. i is impo1ted and the fonnulation is done in Lebanon 2. The a.i is produced in Lebanon ~: Fill in the Registration fmm in Arabic or English for (A) and (B) (Annexl); this fmm should be filled by the producing or fonnulating Company. C- Re-registration :U: 1)Jl1 c )1j5 ..,, ,~ ;11 s,;ir ~ ,., ., . Five years after the registration. of any agricultural pesticide, a new application for the extension of the registration of the pesticide for 5 more years is required accompanied by the Re-registration Form (Annex 2). D- Experimental Use Permit • Fill in the Registration Fonn (Annex I) with the available inf01mation cited in points 2-12. e The importer must info1m the Ministry about the date and location of the intended trials when a request to import samples is submitted. He should also present a report on the results of local trials conducted on the new pesticide. 1-2. Certificates oft.Jse and Registration for Pesticides • To present Certificates of use and Registration for the commercial product of the active ingredient issued by the official authorities in the country of 01igin. In case the product is not used or registered in the counny of origin, a request must be submitted to the Plant Resource Department at the Ministry of Agriculture explaining the reasons why the product is not used in the country of origin and lists a number of countties where this product is registered or used & submit certificate of registration for one of these countries. Exceptions are for the pesticides fonnulated in Lebanon on condition that they comply with the other rules and regulations. e For the registration of new active ingredients in Lebanon: The company should submit Certificates or declarations of use & Registration for the active ingredient from the official authorities of 3 of the approved countries, Company of origin should be the manufacturer of this active ingredient, as such: Present Ce1tificates of use & Registt·ation for the commercial product of the active ingredient from the official authorities of 3 of the approved countries, and for the same uses specified in point 7 of this decree. TI1e approved countries are: Countties of the European Community, Unit~d States of America, United Kingdom, Switzerland, Canada and Japan. Exempted from this are the pesticides mentioned in the official and most recent publications issued by these countries (Fann Chemicals Handbook, Pesticide Manual, ACT A, Index Phywsanitaire, Japanese Pesticide List, Switzerland Produits pour le traitement des plantes). l.cf;j.Jf &;lj5 a...c ,J ;.rr os}JT . , ~."..<: In case the product is registered in only one or two of the approved countries, the file will be refen-ed for review by the pesticide committee to take the :final decision. 1-3. Authorization Letter from the Producer to the Agent e Letter of Authorization from the producer of Active ingredient to the local fonnulator, pemutting him to use the ai and fo1mulate it. e Letter of Authorization :from the producer of Active ingredient to the fonnulator in country of origin of the formulated pesticide, pennitting him to use the ai and formulate it 2. Active Ingredients 2-1. Active Ingredient specifications c Common Name according to ISO and its synonyms for the active ingreclient(s) in the pesticide fo1mulation. e Percent Active Ingredient(s). & Code number (manufacturer's development code number) (If available) o CAS No. (If available) o Chemical name according to the IUPAC or C.A./. For biological pesticides the genus & species must be cited and if needed the strain. 0 Empirical fonnula o Structural fo1mula (If available) & Chemical Class 0 Molecular Weight (M. W.) 2-2 Teclmical Grade Active lngredient(s) (TGAI) 0 M:in. certified Limits of Active Ingredient(s) (g/Kg). 0 To submit a copy of a standard analysis ce1iificate of the TGAI that indicates the degree of purity of active ingredient(s) and the percentage of impurities. TI1is document must be stamped by the company. The percentage of toxic isomers and impwities should not exceed the percentages determined by the F AO, WHO or EPA or the latest list of maximum levels of tolerated impmities issued by the Minisny (Annex3). 2-3. Physical and Chemical prope1ties of the active ingredient Color, Physical State, Odor, Melting point and boiling point, Decomposition point, Com .. sion prope1iies, Density, Solubility in water and organic solvents, Prutition coefficient between water and an approp1iate non miscible solvent, pH (acidity/alkalinity), Flash point, Explosivity. 3. Data on Formulated Products 3-1. Type offonnulation (WP, EC, ... ) 3-2. FommJation Composition ~l;jJ! o;lj!J :1...,;11 ;.t1 o, ,.u ;i., ,,..¼ e To present a standard compos1t1011 ce1ti:ficate stamped by the manufacturing Company stating the percentage of active ingredient(s) and of other ingredients ( adjuvants, surfactants, ... ) in the commercial product. o To present a certificate stating that the fonnulated product does not contain any of the compounds listed in EPA List 1 (Annex 4). In case the product contains any of the additives or solvents specified in the EPA List 2 (Annex5), its concentration should be mentioned clearly. 3-3. Physical and chemical properties offonnulated product 0 To present the physical properties according to the type and fonnulation of the pesticide: Color, Physical state, Odor, pH, Flammability, Explosivity, Viscosity, C01rnsivity, Density, Wettability, Suspensibility, Percent Persistent foam, Wet sieve test, D1y sieve test, Emulsion stability, Flash point. c Storage Stability: To present data for the accelerated storage tests on highest and lowest temperatures, according to the specifications of F AO and CIPAC, as well as their influence on the chemical and physical properties of the product. 3-4. Methods of Analysis To present Methods of analysis used for the fonnulated product, active ingredient(s) and residues. 3-5. Toxicity class: Oral & Dennal LD50 for rats, cite according to WHO classification. 4. Data on Toxicity Studies 4-1. Fate of pesticide in animals 4-2. Acute Toxicity f) Oral & Dennal LDso for rats. 0 LCso for rats (for some pesticides) 6 Possibility of eye and skin iITitation (except cases where it is known that the pesticide is corrosive). 4-3. Sub-chronic toxicity 90- day feeding studies, 90- day inhalation studies, or 90- day dennal studies. 4-4. Chronic toxicity Long term toxicity: Oncogenicity (Carcinogenicity) Teratogenicity Reproduction (2 generations) 4-5. Delayed N eurotoxicity 4~6. Mutagenicity 4-7. Acceptable daily intake (ADI) 5. Environmental Fate (The available information) 5-l. Fate of pesticide in Water: (Surface and underground water) Biodegradation, Hydrolysis, Photolysis, Ev~poration 5-2. Fate of pesticide in soil: Accumulation, Degradation, Leaching 6. Ecotoxicology (The available information) 6-1. Effect of pesticide on non-target organisms: Bee toxicity/ Toxicity to soil microorganisms 6-2. Effect of pesticide on natural enemies 6-3. Effect of pesticide on Eatthwonn 6-4. Effect of pesticide on Birds J..-:1 , ;.tl o ,1 ;1 ~r;.;Jr o~;.ir a.;:? ..... Note: A Summruy of these toxicological studies (4, 5 and 6) issued by the official institutions that conducted these studies must be submitted. 7. Biological Properties and Target Pests 7-1. Uses and Rec01mnendations Crops that may be sprayed by the pesticide/ Targeted Pests & Rate of Use/ Maximum residue limits ·(MRL) for the pesticide according to registrntion by crop/ Pre-harvest interval (PHI) for the· pesticide according to registration by crop/ Re-entiy period if applicable. 7-2. Mode of action on Pest (Systemic, Contact, Stomach, ... ) 8. Phytotoxicity 9. Compatibility ~!,JI oJlj-' l...c.1J i,11 &., ,;/1 a. .,..i..o Compatibility or incompatibility with other products (pesticides, fextilizers, honnones, ... ). 10. Safety handling e First Aid o Antidote if present and any other recommended treatments in case of poisoning. 11. Storage and Disposal of Empty Pesticide Containers • Storage period o Ways of disposal of empty containers 12. Container Type of container (Material used)/ Packing (Volume or Weight) 13. Label • To submit a copy of the label specimen used in the count:Ly of origin or the countries ci~ed under 1-2 (tt·anslated to Arabic, English, or French). • To submit a copy of the label intended for use in Lebanon. The label should confonn to the specifications set by the Plant Protection Department and must receive the official approval of this deparnnent according to decree# 92/1 dated 20/5/1998. 14. Technical Data File To present the Technical Data File of the pesticide, issued and stamped by the producing company in one of:the three languages (Arabic, English or French). This file should contain the infonnation cited in points 2-12, in case some 1.·equired data are not included iu the file, these should be submitted as attachments to the teclmical file. 15. Discontinuation of Pesticide Reo-istration '"' Pesticide Registration is discontinued in the fo])owirnr cases: • !fit is not imp011ed for 5 years. • lfthe Registration Ce1tificate from the country of origin is not renewed. • If the i11~pc:~fog company does not present an applieatic:! fnr Re registrntion within 5 years from the previous registration. • If the Registration was made upon falsified or incomplete infonnation. <lcl.ij,11 iijlj3 :W:IJ,.i/1 ½fll a., ,.i.., ., o If the importer did not follow the officially approved label or did some changes on the data after its approval by the Plant Protection Department. e If under nonnal conditions it had side effects or recent studies showed its ineffectiveness. 16. Miscellaneous e The status of all previously registered pesticides ( according to the provisions of decision No.29/1 dated 07/02/1995) will be subject to reevaluation. Therefore, importers must submit all missing documents that are required by the present decision within six months of publication of this decision in the official gazette. 0 The plant protection department will approve additions or modifications of any infonnation on the label, only after the presentation of official supporting documents (new certificate of registration, revised technical bulletin or corrected label from the approved countries). • Whenever the ·Minishy of Agriculture receives new infonnation concerning a registered pesticide, the Minisuy reserves the right to reevaluate its registration status. e Any person, company national or foreign, who presents falsified infonnation or docmnents will be liable to prosecution. • All necessary documents mentioned in this decree should be submitted to the Directorate of Plant Resources -Plant Protection Department Plant Phannacy Section. • The study of a Registration file takes nonnally a maximum of 3 months after the completion of the file. But new active ingredients need the approval of the pesticide committee. 0 All submitted documents should be recent that is issued, at most, I 0 months earlier, except for the documents still active during date of submission.